Purification device for methylindole

Abstract

The utility model relates to the technical field of methylindole purification, and discloses a methylindole purification device which comprises a base, the left side of the top end of the base is fixedly connected with an extraction kettle, the right side of the extraction kettle is fixedly connected with a distillation kettle, and the right side of the distillation kettle is fixedly connected with a liquid collection tank. A methylindole crude product is placed in an extraction kettle, a high-density organic solution and the methylindole crude product are dissolved firstly, then a low-density organic solution which is not dissolved with methylindole is added, full stirring is conducted, after standing and layering are conducted, an infusion pump is started, the infusion pump pumps an organic solvent containing methylindole in the lower layer into a distillation kettle, a control base starts a heating pipe, and the methylindole crude product is obtained. The heating seat heats the distillation kettle, different heating temperatures are adjusted, the outer side of the third communicating pipe is sleeved with the condensation pipe, and methylindole enters the liquid collecting tank through the third communicating pipe in a gas form when reaching the boiling point, so that methylindole is purified.

Description

Technical Field

[0001] This utility model relates to the field of methylindole purification technology, specifically to a methylindole purification device. Background Technology

[0002] Methylindole is a class of organic compounds containing an indole ring and a methyl group attached to a nitrogen or carbon atom. These compounds have wide applications in organic synthesis, medicinal chemistry, and materials science.

[0003] The purification apparatus for methylindole is used to separate and purify methylindole. The purification of methylindole is relatively complicated, requiring staff to constantly change instruments and perform steps such as shaking and heating the instruments. The operation is inconvenient and has certain limitations, which can easily lead to waste of materials.

[0004] Now, a purification apparatus for methylindole is proposed to solve the above problems. Utility Model Content

[0005] The purpose of this invention is to provide a purification device for methylindole, so as to solve the problems that the purification methods mentioned in the background art are cumbersome and inconvenient, and have certain limitations.

[0006] To achieve the above objectives, this utility model provides the following technical solution: a purification device for methylindole, comprising a base, an extraction vessel fixedly connected to the left side of the top of the base, an inlet at the top of the extraction vessel, a first outlet pipe at the bottom right side of the extraction vessel, a distillation vessel fixedly connected to the right side of the extraction vessel, a first inlet pipe at the left side of the distillation vessel, a pump fixedly connected between the extraction vessel and the inlet, a first connecting pipe fixedly connected between the first outlet pipe and the pump, a second connecting pipe fixedly connected between the first inlet pipe and the pump, a heating seat fixedly connected to the right side of the top of the base, a heating tube installed inside the heating seat, a gas collecting plate fixedly connected to the top of the distillation vessel, a liquid collecting tank fixedly connected to the right side of the distillation vessel, a third connecting pipe fixedly connected between the top of the distillation vessel and the top of the liquid collecting tank, a condenser sleeved on the outside of the third connecting pipe, a control seat fixedly connected to the middle of the base, and a control button fixedly connected to the front end of the base.

[0007] As a further technical solution of this utility model, the feed inlet, extraction vessel, and first liquid outlet pipe are internally connected, and the distillation vessel, third connecting pipe, and liquid collection tank are internally connected.

[0008] As a further technical solution of this utility model, the liquid pump is electrically connected to the control base, and the control button is electrically connected to the control base.

[0009] As a further technical solution of this utility model, the heating tube is electrically connected to the control base, and the top of the heating base is tightly fitted to the top of the base.

[0010] As a further technical solution of this utility model, a limiting seat is fixedly connected to the left side of the bottom of the base, a servo motor is installed at the top of the limiting seat, a rotating seat is movably connected to the top of the servo motor, a first magnet is fixedly connected inside the rotating seat, a movable block is movably connected to the bottom of the extraction vessel, and a second magnet is fixedly connected inside the movable block.

[0011] As a further technical solution of this utility model, the servo motor is electrically connected to the control base, the first magnet and the second magnet attract each other, and the output end of the servo motor is connected to the rotating base.

[0012] As a further technical solution of this utility model, the top of the extraction vessel is fixedly connected to a mounting base, the top of the mounting base is fixedly connected to two sets of solvent tanks, the bottom of the two sets of solvent tanks is provided with a second liquid outlet pipe, the inside of the second liquid outlet pipe is fixedly connected to a flow meter, and two sets of second liquid inlet pipes are provided on both sides of the top of the extraction vessel, the top of the two sets of second liquid inlet pipes is fixedly connected to a solenoid valve.

[0013] As a further technical solution of this utility model, the two sets of flow meters are electrically connected to the control base, and the two sets of solenoid valves are electrically connected to the control base.

[0014] Compared with the prior art, the beneficial effects of this utility model are: the methylindole purification device not only realizes the purification of methylindole, but also realizes the stirring of the liquid in the extraction vessel so that it can be dissolved more fully, and also realizes the accurate control of organic solvents.

[0015] (1) By setting up an extraction vessel, a feed inlet, a first liquid outlet pipe, a distillation vessel, a first liquid inlet pipe, a liquid pump, a first connecting pipe, a second connecting pipe, a heating base, a heating pipe, a gas collecting plate, a third connecting pipe, a condenser pipe, and a liquid collecting tank, when in use, the crude methylindole is placed in the extraction vessel, the crude methylindole is first dissolved in a high-density organic solution, and then a low-density organic solution that is insoluble in methylindole is added. After stirring thoroughly and waiting for the layers to separate, the liquid pump is started, and the liquid pump draws the lower layer of organic solvent containing methylindole into the distillation vessel. The heating pipe is started by the control base, and the heating base heats the distillation vessel. By adjusting different heating temperatures, a condenser pipe is connected to the outside of the third connecting pipe. When the methylindole reaches its boiling point, it enters the liquid collecting tank in the form of gas through the third connecting pipe, thereby achieving the purification of methylindole.

[0016] (2) By setting up a limited seat, servo motor, rotating seat, first magnet, movable block and second magnet, when using crude methylindole and organic solution, if manual shaking is used, it is relatively laborious. When stirring with stirring blades, it is easy to cause the liquid to stick to the stirring blades. By starting the servo motor, the servo motor drives the rotating seat. The first magnet is fixedly connected inside the rotating seat. The movable block is movably connected to the bottom of the extraction vessel. The second magnet is fixedly connected inside the movable block. The first magnet and the second magnet attract each other. The first magnet drives the second magnet to rotate, thereby realizing the stirring of the liquid in the extraction vessel.

[0017] (3) By setting up a mounting base, solvent tank, second outlet pipe, flow meter, second inlet pipe, solenoid valve and control button, when in use, two different organic solutions are respectively placed in different solvent tanks. By starting the flow meter through the control base, the amount of organic solution can be effectively controlled. When the specified value is reached, the solenoid valve is started to close it, thereby achieving accurate control of organic solvent and improving the accuracy of reaction. Attached Figure Description

[0018] Figure 1 This is a front view cross-sectional structural diagram of the present invention;

[0019] Figure 2 For the present utility model Figure 1 Enlarged cross-sectional view of a portion of point A in the middle section;

[0020] Figure 3 For the present utility model Figure 1 Enlarged cross-sectional view of section B in the middle section;

[0021] Figure 4 For the present utility model Figure 1 Enlarged cross-sectional view of section C.

[0022] In the diagram: 1. Base; 2. Extraction vessel; 3. Feed inlet; 4. First outlet pipe; 5. Distillation vessel; 6. First inlet pipe; 7. Pump; 8. First connecting pipe; 9. Second connecting pipe; 10. Heating seat; 11. Heating tube; 12. Gas collecting plate; 13. Third connecting pipe; 14. Condenser; 15. Liquid collecting tank; 16. Control seat; 17. Limit seat; 18. Servo motor; 19. Rotating seat; 20. First magnet; 21. Movable block; 22. Second magnet; 23. Mounting seat; 24. Solvent tank; 25. Second outlet pipe; 26. Flow meter; 27. Second inlet pipe; 28. Solenoid valve; 29. ​​Control button. Detailed Implementation

[0023] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0024] Example: Please refer to Figure 1-4 A purification apparatus for methylindole includes a base 1, an extraction vessel 2 fixedly connected to the left side of the top of the base 1, an inlet 3 at the top of the extraction vessel 2, a first outlet pipe 4 at the bottom right side of the extraction vessel 2, a distillation vessel 5 fixedly connected to the right side of the extraction vessel 2, a first inlet pipe 6 at the left side of the distillation vessel 5, a pump 7 fixedly connected between the extraction vessel 2 and the inlet 3, a first connecting pipe 8 fixedly connected between the first outlet pipe 4 and the pump 7, and a connection between the first inlet pipe 6 and the pump 7. There is a second connecting pipe 9. A heating seat 10 is fixedly connected to the right side of the top of the base 1. A heating pipe 11 is installed inside the heating seat 10. A gas collecting plate 12 is fixedly connected to the top of the distillation vessel 5. A liquid collecting tank 15 is fixedly connected to the right side of the distillation vessel 5. A third connecting pipe 13 is fixedly connected to the top of the distillation vessel 5 and the top of the liquid collecting tank 15. A condenser pipe 14 is sleeved on the outside of the third connecting pipe 13. A control seat 16 is fixedly connected to the middle of the base 1. A control button 29 is fixedly connected to the front end of the base 1.

[0025] The feed inlet 3, extraction vessel 2, and first liquid outlet pipe 4 are internally connected; the distillation vessel 5, third connecting pipe 13, and collection tank 15 are internally connected; the liquid pump 7 is electrically connected to the control base 16; the control button 29 is electrically connected to the control base 16; the heating tube 11 is electrically connected to the control base 16; and the top of the heating base 10 is tightly fitted to the top of the base 1.

[0026] Specifically, such as Figure 1 and Figure 2 As shown, in use, crude methylindole is placed in extraction vessel 2. First, a high-density organic solution is added to dissolve the crude methylindole, and then a low-density organic solution that is insoluble in methylindole is added. After thorough stirring and allowing the layers to settle and separate, the pump 7 is started. The pump 7 draws the lower layer of organic solvent containing methylindole into distillation vessel 5. The control seat 16 starts the heating tube 11, and the heating seat 10 heats the distillation vessel 5. By adjusting different heating temperatures, a condenser 14 is connected to the outside of the third connecting pipe 13. When methylindole reaches its boiling point, it enters the collection tank 15 in gaseous form through the third connecting pipe 13, thereby achieving the purification of methylindole. The pump 7 and the control seat 16 are electrically connected. This technology is existing technology and will not be described in detail.

[0027] A limiting seat 17 is fixedly connected to the left side of the bottom inside the base 1. A servo motor 18 is installed on the top of the limiting seat 17. A rotating seat 19 is movably connected to the top of the servo motor 18. A first magnet 20 is fixedly connected inside the rotating seat 19. A movable block 21 is movably connected to the bottom inside the extraction vessel 2. A second magnet 22 is fixedly connected inside the movable block 21. The servo motor 18 is electrically connected to the control seat 16. The first magnet 20 and the second magnet 22 attract each other. The output end of the servo motor 18 is connected to the rotating seat 19.

[0028] Specifically, such as Figure 1 and Figure 3 As shown, when mixing crude methylindole with an organic solution, manual shaking is laborious. Stirring with a stirring blade can easily cause the liquid to stick to the blade. By activating the servo motor 18, the servo motor 18 drives the rotating seat 19. A first magnet 20 is fixedly connected inside the rotating seat 19, and a movable block 21 is movably connected to the bottom of the extraction vessel 2. A second magnet 22 is fixedly connected inside the movable block 21. The first magnet 20 and the second magnet 22 attract each other, causing the first magnet 20 to drive the second magnet 22 to rotate, thereby achieving stirring of the liquid inside the extraction vessel 2. The servo motor 18 is electrically connected to the control seat 16. This technology is existing and will not be described further.

[0029] An installation base 23 is fixedly connected to the top of the extraction vessel 2. Two sets of solvent tanks 24 are fixedly connected to the top of the installation base 23. A second liquid outlet pipe 25 is opened at the bottom of the two sets of solvent tanks 24. A flow meter 26 is fixedly connected inside the second liquid outlet pipe 25. Two sets of second liquid inlet pipes 27 are opened on both sides of the top of the extraction vessel 2. A solenoid valve 28 is fixedly connected to the top of the two sets of second liquid inlet pipes 27. The two sets of flow meters 26 are electrically connected to the control base 16. The two sets of solenoid valves 28 are electrically connected to the control base 16.

[0030] Specifically, such as Figure 1 and Figure 4 As shown, in use, two different organic solutions are placed in different solvent tanks 24. The flow meter 26 is activated by the control seat 16 to effectively control the amount of organic solution. When the specified value is reached, the solenoid valve 28 is activated to close it, thereby achieving accurate control of the organic solvent and improving the accuracy of the reaction. The flow meter 26 and the control seat 16 are electrically connected, and the solenoid valve 28 and the control seat 16 are also electrically connected. This technology is existing technology and will not be described in detail.

[0031] Working Principle: In use, this invention first places crude methylindole in extraction vessel 2. A high-density organic solution is then added to dissolve the crude methylindole, followed by the addition of a low-density organic solution that is insoluble in methylindole. The mixture is thoroughly stirred until it settles and separates into layers. Then, pump 7 is activated, drawing the lower layer of organic solvent containing methylindole into distillation vessel 5. Control unit 16 activates heating tube 11, and heating unit 10 heats distillation vessel 5. By adjusting different heating temperatures, a condenser 14 is connected to the outside of the third connecting pipe 13. When methylindole reaches its boiling point, it enters the collection tank 15 as a gas through the third connecting pipe 13, thus purifying the methylindole. Secondly, manually shaking the crude methylindole with the organic solution is laborious; therefore, a more efficient method is used… When the stirring blades are stirring, the liquid can easily stick to them. By starting the servo motor 18, the servo motor 18 drives the rotating seat 19. The rotating seat 19 is fixedly connected to the first magnet 20, and the bottom of the extraction vessel 2 is movably connected to the movable block 21. The movable block 21 is fixedly connected to the second magnet 22. The first magnet 20 and the second magnet 22 attract each other, and the first magnet 20 drives the second magnet 22 to rotate, thereby stirring the liquid in the extraction vessel 2. At the same time, during use, the two different organic solutions are respectively placed in different solvent tanks 24. By starting the flow meter 26 through the control seat 16, the amount of organic solution can be effectively controlled. When the specified value is reached, the solenoid valve 28 is activated to close it, thereby achieving accurate control of the organic solvent and improving the accuracy of the reaction.

[0032] It will be apparent to those skilled in the art that this invention is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or essential characteristics of this invention. Therefore, the embodiments should be considered illustrative and non-limiting in all respects, and the scope of this invention is defined by the appended claims rather than the foregoing description. Thus, it is intended that all variations falling within the meaning and scope of equivalents of the claims be included within this invention. No reference numerals in the claims should be construed as limiting the scope of the claims.

Claims

1. A purification device for methylindole comprising a base (1), characterized in that: The left side of the top end of the base (1) is fixedly connected with an extraction kettle (2), the top end of the extraction kettle (2) is provided with a feeding port (3), the bottom end of the right side of the extraction kettle (2) is provided with a first liquid outlet pipe (4), the right side of the extraction kettle (2) is fixedly connected with a distillation kettle (5), the left side of the distillation kettle (5) is provided with a first liquid inlet pipe (6), the extraction kettle (2) and the feeding port (3) are fixedly connected with a liquid pump (7), the first liquid outlet pipe (4) and the liquid pump (7) are fixedly connected with a first communication pipe (8), the first liquid inlet pipe (6) and the liquid pump (7) are fixedly connected with a second communication pipe (9), the right side of the inside of the top end of the base (1) is fixedly connected with a heating seat (10), the inside of the heating seat (10) is provided with a heating pipe (11), the inside of the top end of the distillation kettle (5) is fixedly connected with a gas collecting disc (12), the right side of the distillation kettle (5) is fixedly connected with a liquid collecting tank (15), the top end of the distillation kettle (5) and the top end of the liquid collecting tank (15) are fixedly connected with a third communication pipe (13), the outside of the third communication pipe (13) is sleeved with a condenser pipe (14), the middle of the inside of the base (1) is fixedly connected with a control seat (16), and the front end of the base (1) is fixedly connected with a control button (29).

2. A purification apparatus for methylindole according to claim 1, characterized in that: The feeding port (3), the extraction kettle (2) and the first liquid outlet pipe (4) are connected, and the distillation kettle (5), the third communication pipe (13) and the liquid collecting tank (15) are connected.

3. A purification apparatus for methylindole according to claim 1, characterized in that: The liquid pump (7) and the control seat (16) are electrically connected, and the control button (29) and the control seat (16) are electrically connected.

4. A purification apparatus for methylindole according to claim 1, characterized by: The heating pipe (11) and the control seat (16) are electrically connected, and the top end of the heating seat (10) is closely combined with the top end of the inside of the base (1).

5. A purification apparatus for methylindole according to claim 1, characterized by: The left side of the bottom end of the inside of the base (1) is fixedly connected with a limiting seat (17), the top end of the limiting seat (17) is provided with a servo motor (18), the top end of the servo motor (18) is movably connected with a rotating seat (19), the inside of the rotating seat (19) is fixedly connected with a first magnet (20), the bottom end of the inside of the extraction kettle (2) is movably connected with a movable block (21), and the inside of the movable block (21) is fixedly connected with a second magnet (22).

6. A purification apparatus for methylindole according to claim 5, characterized in that: The servo motor (18) and the control seat (16) are electrically connected, the first magnet (20) and the second magnet (22) are attracted to each other, and the output end of the servo motor (18) is connected with the rotating seat (19).

7. A purification apparatus for methylindole according to claim 1, characterized by: The top end of the extraction kettle (2) is fixedly connected with a mounting seat (23), the top end of the mounting seat (23) is fixedly connected with two groups of solvent tanks (24), the bottom end of the two groups of solvent tanks (24) is provided with a second liquid outlet pipe (25), the inside of the second liquid outlet pipe (25) is fixedly connected with a flowmeter (26), and the top end of the extraction kettle (2) is provided with two groups of second liquid inlet pipes (27), the top end of the two groups of second liquid inlet pipes (27) is fixedly connected with an electromagnetic valve (28).

8. A purification apparatus for methylindole according to claim 7, characterized in that: Two groups of said flow meters (26) are electrically connected with the control base (16), and two groups of said electromagnetic valves (28) are electrically connected with the control base (16).

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