Ergothioneine organic solvent extraction reaction kettle

Abstract

The utility model is suitable for the technical field of reaction kettles, and provides an ergothioneine organic solvent extraction reaction kettle which comprises a support frame, the heat insulation cylinder is fixed on the support frame and is used for heat insulation and heat preservation; the material storage barrel is arranged in the heat insulation barrel and is used for providing an ergothioneine organic solvent extraction space; a heating pipe is sleeved outside the material storage barrel; the oil cylinder is fixed on the support frame, and a connecting plate is mounted on an output rod of the oil cylinder; the bottom plate is arranged on the connecting plate and is used for sealing the heat insulation barrel; the protective cover is fixed on the bottom plate and is used for sealing the material storage barrel; and the stirring mechanism is arranged on the heat insulation barrel and is used for stirring the ergothioneine organic solvent. The ergothioneine organic solvent extraction reaction kettle provided by the scheme is convenient to disassemble and clean, provides a proper reaction environment to accelerate the reaction rate, and improves the extraction efficiency.

Description

TECHNICAL FIELD

[0001] The utility model belongs to the technical field of reaction kettle, especially relates to a ergothioneine organic solvent extraction reaction kettle. BACKGROUND

[0002] Ergothioneine (mercaptohistidine trimethyl inner salt, ergothioneine, EGT) is a compound found in 1909, is found in a kind of fungus Claviceps purpurea initially, pure product is white crystal, water-soluble, (soluble 0.9 mol / L at room temperature), it will not be self-oxidized in physiological pH and strong alkali solution.

[0003] Reaction kettle needs to be used when ergothioneine organic solution is extracted, and the existing reaction kettle has high integrity, so that the inside of the reaction kettle is inconvenient to clean. UTILITY MODEL CONTENT

[0004] The utility model provides a kind of ergothioneine organic solvent extraction reaction kettle, to solve the problem that the existing reaction kettle has high integrity, is inconvenient to clean the inside of the reaction kettle as described in the above background art.

[0005] To solve the above problems, the utility model is realized as follows: a kind of ergothioneine organic solvent extraction reaction kettle, comprising: support frame;Heat-insulating cylinder for heat insulation is fixed on the support frame;Installation is used to provide ergothioneine organic solvent extraction space in the heat-insulating cylinder for the storage cylinder, the storage cylinder is equipped with heating pipe;Oil cylinder is fixed on the support frame, the output rod of the oil cylinder is installed with connecting plate;Bottom plate for closing the heat-insulating cylinder is arranged on the connecting plate and protective cover for closing the storage cylinder is fixed on the bottom plate;Stirring mechanism for stirring ergothioneine organic solvent is arranged on the heat-insulating cylinder.

[0006] Preferably, the stirring mechanism includes a servo motor fixed on the heat-insulating cylinder, an installation plate installed on the output shaft of the servo motor, an adjustable plate detachably installed on the installation plate, and a stirring rod fixed on the adjustable plate for uniform ergothioneine organic solvent temperature.

[0007] Preferably, the bottom of the protective cover is provided with a discharge pipe extending to the outside of the heat-insulating cylinder, a plug cap for closing the discharge pipe is threadedly sleeved on the discharge pipe, anti-slip lines are hung on the outer wall of the plug cap, and a support seat for stabilizing the stirring rod is rotatably installed at the bottom of the stirring rod and extendable into the discharge pipe.

[0008] Preferably, the top of the storage cylinder is provided with a cylinder body, the cylinder body is provided with extension pipes, the number of the extension pipes is not less than three and the extension pipes are respectively used for adding main materials, adding auxiliary materials and outputting steam, and the extension pipes are provided with valves for adjusting opening and closing of the extension pipes.

[0009] Preferably, the outer wall of the heat insulation cylinder is fixed with a heat insulation net for assisting heat insulation to prevent scalding, the bottom of the support frame is detachably provided with a support leg for supporting equipment, and the bottom of the support leg is provided with a support plate for increasing a contact area.

[0010] Preferably, the storage cylinder and the bottom plate are both provided with extension plates, the two extension plates are both provided with sealing rings for preventing liquid leakage on the side close to each other, and the two sealing rings are in contact.

[0011] Preferably, the heat insulation cylinder is provided with a temperature sensor for monitoring an extraction temperature, a detection probe of the temperature sensor extends into the storage cylinder, and the support seat is provided with rubber elastic blocks for buffering and damping.

[0012] Preferably, the heat insulation cylinder is fixed with a protective plate for isolating a heating environment, the protective plate is connected with the storage cylinder for stabilizing the storage cylinder, and the storage cylinder is made of stainless steel.

[0013] Compared with the related art, the ergothioneine organic solvent extraction reaction kettle has the following beneficial effects:

[0014] Compared with the prior art, the ergothioneine organic solvent extraction reaction kettle provided by the scheme moves related components through an oil cylinder, facilitates opening of the heat insulation cylinder and the storage cylinder, facilitates cleaning, realizes heat insulation and heat preservation of the heat insulation cylinder, provides a suitable temperature environment through the heating pipe, makes the solvent uniformly mixed and the temperature uniformly distributed through the stirring mechanism, accelerates a reaction rate, is detachable and facilitates maintenance, and prevents scalding through the heat insulation net. BRIEF DESCRIPTION OF DRAWINGS

[0015] Figure 1 is a front view of the ergothioneine organic solvent extraction reaction kettle provided by the utility model;

[0016] Figure 2 is a front view of the stirring mechanism in the utility model;

[0017] Figure 3 is a bottom view of the storage cylinder in the utility model;

[0018] Figure 4 is a three-dimensional structure diagram of the storage cylinder in the utility model.

[0019] Reference numerals in the attached drawings: 1. Support frame; 2. Insulation cylinder; 3. Storage cylinder; 4. Oil cylinder; 5. Connecting plate; 6. Base plate; 7. Protective cover; 8. Heating tube; 9. Discharge pipe; 10. Plug cap; 11. Support leg; 12. Protective plate; 13. Insulation mesh; 14. Extension disc; 15. Sealing ring; 16. Cylinder body; 17. Extension pipe; 18. Servo motor; 19. Mounting plate; 20. Adjusting plate; 21. Stirring rod; 22. Support base; 23. Valve. Detailed Implementation

[0020] Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs; the terminology used herein in the specification of the application is for the purpose of describing particular embodiments only and is not intended to limit the application; the terms "comprising" and "having," and any variations thereof, in the specification, claims, and foregoing description of the drawings are intended to cover non-exclusive inclusion. The terms "first," "second," etc., in the specification, claims, or foregoing drawings are used to distinguish different objects, not to describe a particular order; the terms "inner," "outer," "left," and "right" indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of the present invention.

[0021] In this document, the term "embodiment" means that a particular feature, structure, or characteristic described in connection with an embodiment may be included in at least one embodiment of this application. The appearance of this phrase in various places throughout the specification does not necessarily refer to the same embodiment, nor is it a separate or alternative embodiment mutually exclusive with other embodiments. It will be explicitly and implicitly understood by those skilled in the art that the embodiments described herein can be combined with other embodiments.

[0022] This utility model embodiment provides an ergothioneine organic solvent extraction reaction vessel, such as... Figures 1-4 As shown, the ergothioneine organic solvent extraction reactor includes: a support frame 1; a heat insulation cylinder 2 fixed on the support frame 1 for heat insulation; a storage cylinder 3 installed inside the heat insulation cylinder 2 to provide space for ergothioneine organic solvent extraction, the storage cylinder 3 being fitted with a heating pipe 8; a hydraulic cylinder 4 fixed on the support frame 1, the output rod of the hydraulic cylinder 4 being fitted with a connecting plate 5; a bottom plate 6 disposed on the connecting plate 5 for sealing the heat insulation cylinder 2 and a protective cover 7 fixed on the bottom plate 6 for sealing the storage cylinder 3; and a stirring mechanism disposed on the heat insulation cylinder 2 for stirring the ergothioneine organic solvent.

[0023] In the embodiment, the connecting plate 5, the bottom plate 6 and the protective cover 7 are moved by the oil cylinder 4, so that the heat insulation cylinder 2 and the storage cylinder 3 can be conveniently opened, the inside of the reaction kettle is cleaned, the problem that the existing reaction kettle is not convenient to clean due to high integrity is solved, the heat insulation cylinder 2 plays a heat insulation and heat preservation role, the heating pipe 8 arranged on the storage cylinder 3 can provide a suitable temperature environment for ergot alkaloid organic solvent extraction, which is beneficial to the extraction reaction, the stirring mechanism can stir the ergot alkaloid organic solvent, so that the solvent is uniformly mixed, the extraction reaction rate is accelerated, and the extraction efficiency is improved.

[0024] In the further preferable embodiment of the utility model, the stirring mechanism comprises a servo motor 18 fixed on the heat insulation cylinder 2, a mounting plate 19 installed on the output shaft of the servo motor 18, an adjusting plate 20 detachably installed on the mounting plate 19 and a stirring rod 21 fixed on the adjusting plate 20 and used for uniformly mixing the ergot alkaloid organic solvent.

[0025] In the embodiment, the stirring rod 21 in the stirring mechanism can stir the ergot alkaloid organic solvent, so that the solvent is uniformly mixed, the extraction reaction rate is accelerated, and the extraction efficiency is improved; the stirring rod 21 can uniformly mix the ergot alkaloid organic solvent, so that the local temperature is not too high or too low, the extraction reaction is not affected, the stability and efficiency of the extraction reaction are further ensured; the adjusting plate 20 is detachably installed on the mounting plate 19, when the stirring mechanism is faulty or the stirring rod 21 needs to be replaced, the adjusting plate 20 can be conveniently detached from the mounting plate 19 for maintenance or replacement, so that the maintenance cost and difficulty are reduced; the servo motor 18 (Siemens 1FT7 servo motor) is used as a power source to drive the stirring rod 21 to rotate.

[0026] In the further preferable embodiment of the utility model, the bottom of the protective cover 7 is provided with a discharge pipe 9 extending out of the heat insulation cylinder 2, a plug 10 for closing the discharge pipe 9 is threadedly sleeved on the discharge pipe 9, anti-skid lines are hung on the outer wall of the plug 10, and a support seat 22 for stabilizing the stirring rod 21 is rotatably installed at the bottom of the stirring rod 21 and can extend into the discharge pipe 9.

[0027] In the embodiment, the discharge pipe 9 is arranged to facilitate the discharge of the ergot alkaloid organic solvent after the extraction reaction is completed, the plug 10 is threadedly sleeved on the discharge pipe 9, so that the discharge pipe 9 can be effectively closed to prevent the solvent from leaking during the reaction, the anti-skid lines on the outer wall of the plug 10 facilitate the rotation of the plug 10 by the operator to perform the discharge operation, the support seat 22 rotatably installed at the bottom of the stirring rod 21 can extend into the discharge pipe 9, so that the stirring rod 21 is stably supported during the stirring process, the shaking of the stirring rod 21 is reduced, and the stability and reliability of the stirring are improved.

[0028] In a further preferred embodiment of the present invention, the top of the storage cylinder 3 is provided with a cylinder body 16, and the cylinder body 16 is provided with an extension pipe 17. The number of extension pipes 17 is not less than three and they are respectively used for adding main material, adding auxiliary material and outputting steam. The extension pipe 17 is provided with a valve 23 for adjusting the opening and closing of the extension pipe 17.

[0029] In this embodiment, the multiple extension tubes 17 are used for adding main materials, adding auxiliary materials, and outputting steam, respectively, making the addition of materials and the output of steam more convenient and orderly. The opening and closing of each extension tube 17 can be flexibly controlled according to actual production needs, which improves production efficiency and operational flexibility. The valve 23 can precisely adjust the opening and closing of the extension tubes 17, making it easy to control the amount of materials added and the amount of steam output, ensuring the stability of the reaction process and product quality.

[0030] In a further preferred embodiment of the present invention, a heat insulation net 13 for assisting heat insulation to prevent burns is fixed on the outer wall of the heat insulation cylinder 2, and a support leg 11 for supporting the equipment is detachably installed at the bottom of the support frame 1, and a support plate for increasing the contact surface is installed at the bottom of the support leg 11.

[0031] In this embodiment, the support leg 11 is detachably installed at the bottom of the support frame 1, which facilitates the transportation and installation of the equipment. When the equipment needs to be moved or the installation position changed, the support leg 11 can be easily disassembled. The support plate installed at the bottom of the support leg 11 increases the contact area between the equipment and the ground, improves the stability of the equipment, and prevents the equipment from shaking during use, which could affect production safety and product quality.

[0032] In a further preferred embodiment of the present invention, an extension disc 14 is installed on both the storage cylinder 3 and the bottom plate 6, and a sealing ring 15 for preventing leakage is installed on the side of the two extension discs 14 that are close to each other, and the two sealing rings 15 are in contact with each other.

[0033] In this embodiment, the extension plate 14 and the sealing ring 15 are arranged so that when the bottom plate 6 closes the heat insulation cylinder 2, the two sealing rings 15 are in close contact to form a reliable sealing structure, which effectively prevents material leakage in the storage cylinder 3, ensures the safety and environmental protection of the production process, and also reduces material waste and lowers production costs.

[0034] In a further preferred embodiment of the present invention, a temperature sensor for monitoring the extraction temperature is installed on the heat insulation cylinder 2, the detection probe of the temperature sensor extends into the storage cylinder 3, and a rubber elastic block for buffering and shock absorption is provided in the support base 22.

[0035] In the embodiment, the detection probe of the temperature sensor (PT100) extends into the storage cylinder 3, which can monitor the extraction temperature in real time and accurately, and the operator can adjust the power of the heating pipe 8 in time according to the temperature data, so that the extraction reaction is carried out under the optimal temperature condition, the product quality and the extraction efficiency are improved, the rubber elastic blocks play a buffering and damping role in the stirring process of the stirring rod 21, the vibration and impact force generated when the stirring rod 21 rotates are reduced, the equipment noise is reduced, the service life of the equipment is prolonged, and the stability and uniformity of stirring are also improved.

[0036] In the further preferred embodiment of the utility model, the heat insulation cylinder 2 is fixed with a protective plate 12 for isolating the heating environment, the protective plate 12 is connected with the storage cylinder 3 for stabilizing the storage cylinder 3, and the storage cylinder 3 is made of stainless steel.

[0037] In the embodiment, the protective plate 12 is connected with the storage cylinder 3, which provides additional support for the storage cylinder 3 and enhances the stability of the storage cylinder 3, so that the storage cylinder 3 is prevented from shaking or moving during stirring or heating, and the smooth progress of the reaction process is ensured, the storage cylinder 3 is made of stainless steel, has good corrosion resistance and high temperature resistance, can adapt to the corrosion of various chemicals and high temperature environment in the extraction process, prolongs the service life of the storage cylinder 3, and also ensures the quality of the extraction product.

[0038] In summary, compared with the related art, the device moves the related components by the oil cylinder 4, facilitates opening the heat insulation cylinder 2 and the storage cylinder 3, facilitates cleaning, the heat insulation cylinder 2 realizes heat insulation, the heating pipe 8 provides a suitable temperature environment, the stirring mechanism makes the solvent mix uniformly and the temperature uniform, accelerates the reaction rate, is detachable and facilitates maintenance, and the heat insulation net 13 prevents scalding.

[0039] In the several embodiments provided in the present application, it should be understood that the disclosed device can be implemented in other ways.

[0040] The above embodiments are only used to illustrate the technical solutions of the utility model, and not to limit the protection scope of the utility model. Obviously, the described embodiments are only some of the embodiments of the utility model, not all the embodiments. Based on these embodiments, all other embodiments obtained by those skilled in the art without creative labor fall within the scope of protection of the utility model. Although the utility model has been described in detail with reference to the above embodiments, those skilled in the art can still combine, add or delete the features in the embodiments of the utility model according to the circumstances without creative labor, so as to obtain different other technical solutions which do not deviate from the concept of the utility model, and these technical solutions also belong to the scope of protection of the utility model.

Claims

1. An ergothioneine organic solvent extraction reaction vessel, characterized by, It includes: Support frame; Fixed on the support frame for heat insulation heat insulation cylinder; Installed in the heat insulation cylinder for providing ergothioneine organic solvent extraction space of storage cylinder, the storage cylinder is equipped with heating pipe; Fixed on the support frame of the oil cylinder, the output rod of the oil cylinder is installed with connecting plate; Set on the connecting plate for closing the bottom plate of the heat insulation cylinder and fixed on the bottom plate for closing the protective cover of the storage cylinder; Set on the heat insulation cylinder for stirring ergothioneine organic solvent stirring mechanism.

2. The ergothioneine organic solvent extraction reactor of claim 1, wherein, The stirring mechanism includes a servo motor fixed on the heat insulation cylinder, an installation plate installed on the output shaft of the servo motor, a regulating plate detachably installed on the installation plate, and a stirring rod fixed on the regulating plate for uniform ergothioneine organic solvent temperature.

3. The ergothioneine organic solvent extraction reactor as described in claim 2, characterized in that, The bottom of the protective cover is provided with a discharge pipe extending to the outside of the heat insulation cylinder, the discharge pipe is threadedly sleeved with a plug cap for closing the discharge pipe, the outer wall of the plug cap is hung with anti-skid lines, and the bottom of the stirring rod is rotatably installed with a support seat which can extend into the discharge pipe for stabilizing the stirring rod.

4. The ergothioneine organic solvent extraction reactor as described in claim 1, characterized in that, The top of the storage cylinder is provided with a cylinder body, the cylinder body is provided with an extension pipe, the number of the extension pipe is not less than three and is respectively used for adding main material, adding auxiliary material and outputting steam, and the extension pipe is provided with a valve for adjusting the opening and closing of the extension pipe.

5. The ergothioneine organic solvent extraction reactor of claim 1, wherein, The outer wall of the heat insulation cylinder is fixed with a heat insulation net for assisting heat insulation to prevent scalding, the bottom of the support frame is detachably installed with a support leg for supporting equipment, and the bottom of the support leg is installed with a support plate for increasing the contact area.

6. The ergothioneine organic solvent extraction reactor as described in claim 1, characterized in that, The storage cylinder and the bottom plate are both installed with an extension disc, the side of the two extension discs close to each other is installed with a sealing ring for preventing liquid leakage, and the two sealing rings are in contact.

7. The ergothioneine organic solvent extraction reactor as described in claim 3, characterized in that, The heat insulation cylinder is installed with a temperature sensor for monitoring the extraction temperature, the detection probe of the temperature sensor extends into the storage cylinder, and the support seat is provided with a rubber elastic block for buffering and damping.

8. The ergothioneine organic solvent extraction reactor as described in claim 1, characterized in that, The heat insulation cylinder is fixed with a protective plate for isolating the heating environment, the protective plate is connected with the storage cylinder for stabilizing the storage cylinder, and the storage cylinder is made of stainless steel.

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