Device for improving hydrometallurgy oil phase recovery rate

Abstract

The utility model relates to the technical field of hydrometallurgy two-phase production, in particular to a device for improving the hydrometallurgy oil phase recovery rate, and aims to solve the problems of oil-water two-phase entrainment and large oil phase loss in the existing hydrometallurgy. The device is mainly characterized in that a flow baffle is mounted on the inner wall of a two-phase solution storage tank to promote oil-water separation and oil phase aggregation; an oil phase overflow groove is formed in the inner wall of the storage tank, floating oil is collected, and an oil phase is recovered; the pipeline is additionally arranged at the liquid inlet and is directly communicated with the bottom of the tank, so that the oil-water separation time is favorably prolonged, turbulent flow of a solution in the tank body is reduced, the oil-water separation efficiency is improved, after the oil-water two-phase solution passes through the equipment, the oil-phase recycling is ensured, the oil-phase recovery rate is effectively improved, the cost is reduced, oil and water are effectively separated, and oil content entrainment in a water phase is reduced; the quality of a product solution is improved, further separation of oil and water is promoted, energy consumption is not additionally increased, the production process is not changed, fixed number of workers and working procedures are not increased, manufacturing is easy, and the oil phase recovery rate is increased.

Description

TECHNICAL FIELD

[0001] The utility model relates to a two-phase production technology field of hydrometallurgy, specifically relates to a device for improving oil phase recovery rate of hydmetallurgy. BACKGROUND

[0002] Two-phase mixing reaction is an important component in hydrometallurgical production, and is often applied to solution purification and separation such as extraction process. Extraction is a process of mixing and separating organic phase oil phase and ionic solution water phase, so as to purify the impurity content in ionic solution and obtain water solution meeting the requirements. In order to promote the speed of ionic separation, the two-phase mixing process is very intense, which leads to the difficulty of subsequent two-phase separation. According to the form of oil phase in water phase, it is generally divided into dispersed oil, suspended oil, emulsified oil and dissolved oil. In order to separate the two phases, a special two-phase separation process is often added in production to remove most of the oil, but it is difficult to separate completely, and the water solution still contains a certain amount of oil. Therefore, in order to further reduce the entrained oil in the water solution, a component can be added in the existing storage tank to realize the separation of oil and water and the recovery of oil phase again. SUMMARY

[0003] The utility model provides a device for improving oil phase recovery rate of hydrometallurgy to solve the problems in the above background.

[0004] In order to achieve the above purpose, the utility model adopts the following technical scheme:

[0005] The utility model discloses a device for improving oil phase recovery rate of hydrometallurgy, which comprises a two-phase solution storage tank, a two-phase solution inlet is arranged at the top of the two-phase solution storage tank, a water phase outlet is arranged at the bottom of the two-phase solution storage tank, an oil phase overflow tank is fixedly arranged at the upper side wall of the inner side of the two-phase solution storage tank, an oil phase discharge port is connected to the outer wall of the two-phase solution storage tank opposite to the oil phase overflow tank, and a flow baffle is obliquely and detachably arranged at the lower side wall of the inner side of the two-phase solution storage tank.

[0006] Further, the oil phase overflow tank comprises a bottom plate fixedly connected to the upper side wall of the inner side of the two-phase solution storage tank, and an oil phase overflow weir is vertically arranged at the end of the bottom plate away from the inner side wall of the two-phase solution storage tank.

[0007] Further, the flow baffle is provided with a flow baffle middle plate on one side of the axis line in the two-phase solution storage tank, a connecting frame is fixedly arranged on the other side of the flow baffle, and the flow baffle is connected to the two-phase solution storage tank through the connecting frame.

[0008] Further, a straight pipe is connected to one end of the two-phase solution inlet extending into the two-phase solution storage tank, and an overflow port is further arranged on the outer side of the top of the two-phase solution storage tank.

[0009] The utility model has the following beneficial effects:

[0010] This utility model provides a device for improving the oil phase recovery rate in hydrometallurgical processes. It mainly involves installing baffles on the inner wall of a two-phase solution storage tank to facilitate oil-water separation and oil phase aggregation; installing an oil phase overflow tank on the inner wall of the tank to collect floating oil and recover the oil phase; and adding a pipe directly connecting the inlet to the bottom of the tank to increase oil-water separation time while reducing turbulence within the tank, thus improving oil-water separation efficiency. After the oil-water two-phase solution passes through this equipment, it achieves several benefits: first, it increases the oil phase recovery rate, allowing for oil phase recycling and reducing costs; second, it effectively separates oil and water, reducing oil entrainment in the aqueous phase and improving the quality of the product solution; third, this equipment does not increase energy consumption, production processes, labor, or staffing, making it easy to implement and operate; and fourth, this equipment demonstrates significant, rapid, and highly effective oil phase recovery. Attached Figure Description

[0011] Figure 1 This is a schematic diagram of the overall structure of this utility model.

[0012] Figure 2 This is a top view of the overflow channel of this utility model, showing a cross-section AA.

[0013] Figure 3 This is a top view of the BB cross-section of the integrated baffle of this utility model.

[0014] Figure 4 This is a top view of the middle plate of the baffle of this utility model.

[0015] The meanings of the reference numerals in the attached figures are as follows:

[0016] 1. Two-phase solution storage tank; 2. Oil phase overflow tank; 2-1. Oil phase overflow weir; 2-2. Bottom plate; 3. Oil phase outlet; 4. Baffle plate; 4-1. Baffle plate intermediate plate; 4-2. Connecting frame; 5. Aqueous phase outlet; 6. Two-phase solution inlet; 7. Overflow port; 8. Straight pipe. Detailed Implementation

[0017] The present invention will be further described below with reference to the accompanying drawings and specific embodiments.

[0018] like Figures 1-4 As shown, an apparatus for improving the oil phase recovery rate in hydrometallurgical processes includes a two-phase solution storage tank 1. A two-phase solution inlet 6 is provided at the top of the two-phase solution storage tank 1, and a water phase outlet 5 is provided at the bottom of the two-phase solution storage tank 1. An oil phase overflow trough 2 is fixedly provided on the upper inner side wall of the two-phase solution storage tank 1. An oil phase outlet 3 is connected to the outer wall of the two-phase solution storage tank 1 directly opposite the oil phase overflow trough 2. A baffle plate 4 is detachably and inclinedly provided on the lower inner side wall of the two-phase solution storage tank 1.

[0019] The oil phase overflow tank 2 comprises a bottom plate 2-2 fixedly connected with the upper side wall of the two-phase solution tank 1, and an oil phase overflow weir 2-1 vertically arranged at the end of the bottom plate 2-2 away from the inner side wall of the two-phase solution tank 1.

[0020] The baffle 4 is provided with a baffle middle plate 4-1 on one side of the axis of the two-phase solution tank 1, and a connecting frame 4-2 is fixedly arranged on the other side of the baffle 4, and the baffle 4 is connected with the two-phase solution tank 1 through the connecting frame 4-2.

[0021] The two-phase solution inlet 6 is connected with a straight pipe 8 at one end extending into the two-phase solution tank 1, and the top outer side of the two-phase solution tank 1 is further provided with an overflow port 7.

[0022] In the specific use, the components are installed well according to the drawings, and then the oil-water two-phase filling and separation process is carried out, which comprises a two-phase solution tank 1, an oil phase overflow tank 2 arranged on the inner wall of the upper part of the two-phase solution tank 1, the oil phase overflow tank comprising an oil phase overflow weir 2-1 and a bottom plate 2-2, the oil phase overflow tank 2 being provided with an oil phase discharge port 3, a baffle 4 arranged in the middle of the two-phase solution tank 1, the baffle middle plate 4-1 being required to be installed at an angle of 25°-45° with the tank wall of the two-phase solution tank 1, a hole being arranged at the connecting position of the baffle 4 and the two-phase solution tank 1 and a connecting frame 4-2 being arranged, a water phase outlet 5 arranged at the bottom of the two-phase solution tank 1, a two-phase solution inlet 6 arranged at the top of the two-phase solution tank 1, a straight pipe 8 arranged in the tank body, and an overflow port 7 arranged at the upper part of the tank body. After the oil-water two-phase solution passes through the equipment, the baffle 4 helps the oil-water separation and the oil phase aggregation, the oil phase overflow tank 2 collects the floating oil and recycles the oil phase, the straight pipe 8 directly passes through the tank bottom, which helps to increase the oil-water separation time, reduces the turbulence of the solution in the tank body, improves the oil-water separation efficiency, improves the oil phase recovery rate, realizes the recycling of the oil phase, reduces the cost, effectively separates the oil and water, reduces the oil entrainment in the water phase, improves the quality of the product solution, does not increase the energy consumption, production process, labor amount and labor quota, is convenient to implement and operate, has obvious oil phase recycling effect, fast effect and high effect, and therefore, the device has good practicability.

Claims

1. An apparatus for improving the recovery of hydrometallurgical oil phase, comprising a two-phase solution tank (1), characterized in that: The top of the two-phase solution tank (1) is provided with a two-phase solution inlet (6), the bottom of the two-phase solution tank (1) is provided with an aqueous phase outlet (5), the inner side of the two-phase solution tank (1) is fixedly provided with an oil phase overflow groove (2) on the upper side wall, the oil phase overflow groove (2) is connected with an oil phase discharge port (3) opposite to the outer wall of the two-phase solution tank (1), and the inner side of the two-phase solution tank (1) is obliquely and detachably provided with a flow baffle (4) on the lower side wall.

2. The apparatus for improving the recovery of an oil phase in hydrometallurgy according to claim 1, characterized in that: The oil phase overflow groove (2) comprises a bottom plate (2-2) fixedly connected with the inner side upper side wall of the two-phase solution tank (1), and an oil phase overflow weir (2-1) is vertically arranged at the end of the bottom plate (2-2) away from the inner side wall of the two-phase solution tank (1).

3. The apparatus for improving the recovery of an oil phase in hydrometallurgy according to claim 1, characterized in that: The flow baffle (4) is provided with a flow baffle middle plate (4-1) on one side of the central axis of the two-phase solution tank (1), the other side of the flow baffle (4) is fixedly provided with a connecting frame (4-2), and the flow baffle (4) is connected with the two-phase solution tank (1) through the connecting frame (4-2).

4. The apparatus for improving the recovery of an oil phase in hydrometallurgy according to claim 1, characterized in that: The straight pipe (8) is connected with the end of the two-phase solution inlet (6) extending into the two-phase solution tank (1), and the top outer side of the two-phase solution tank (1) is further provided with an overflow port (7).

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