Continuous reaction type energy-saving acidification kettle
By designing an automatic feeding and discharging system and a stirring mechanism, the continuous reaction acidification reactor has solved the problem of low production efficiency of existing acidification reactors, achieved the continuity and stability of the reaction, improved production efficiency and reduced energy consumption.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- HUBEI HAIRUI PHARMACEUTICAL CO LTD
- Filing Date
- 2025-05-23
- Publication Date
- 2026-04-24
AI Technical Summary
The existing acidification reactor cannot automatically feed and discharge materials after the reactants reach the reaction standard, resulting in discontinuous production and low production efficiency.
A continuous reaction energy-saving acidification kettle was designed, which includes an automatic feeding and discharging system. The material is conveyed by a motor-driven conveying shaft and spiral blades, and the material is mixed by the first and second stirring mechanisms. The heating, air pressure and liquid level are controlled by the transmission mechanism and sensors to achieve automated operation.
The automatic feeding and discharging of the acidification reactor has been achieved, ensuring the continuity and stability of the reaction, improving production efficiency, reducing energy consumption, and ensuring the safe operation of the equipment.
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Figure CN224156874U_ABST
Abstract
Description
Technical Field
[0001] This application relates to the field of acidification reactor technology, and in particular to a continuous reaction energy-saving acidification reactor. Background Technology
[0002] Acidification refers to the process of adding acid to change a system from alkaline or neutral to acidic. It is a very important step in chemical production. Different acids and amounts of acid are selected according to the purpose of acidification. For example, to oxidize potassium iodide in sodium arsenate (Na3AsO4) solution, the solution must be acidified to a strong acid state using strong acid such as sulfuric acid or hydrochloric acid. This is because sodium arsenate only has strong oxidizing properties under strong acid conditions. Acidification is the process of adding hydrogen ions to the solution to lower the pH value, and the added acid will not react with the ions in the original solution.
[0003] A search revealed that patent document CN213348873U discloses a continuous reaction acidification reactor. The technical solution includes an acidification reactor body with an auxiliary mechanism extending outwards. The auxiliary mechanism includes a motor fixedly mounted on the top of the acidification reactor body. A square rod is fixedly connected to the motor via an output shaft. The square rod is positioned on the top of the acidification reactor body and extends into its interior. A sleeve is fitted around the square rod, and auxiliary components are located outside the sleeve. The beneficial effect is that the design of the auxiliary mechanism, along with the sleeve and reciprocating screw, allows for stirring of the material inside the acidification reactor body. Simultaneously, the first stirring rod moves downwards, preventing centrifugal forces from forming within the material and ensuring optimal acidification.
[0004] In practical use, it was found that existing acidification reactors cannot automatically feed and discharge materials after the reactants reach the reaction standard, resulting in discontinuous production and low production efficiency. Therefore, we proposed a continuous reaction energy-saving acidification reactor to solve the above problems. Utility Model Content
[0005] The purpose of this application is to provide a continuous reaction energy-saving acidification kettle, which has the functions of automatic feeding and discharging, continuous reaction, and improved production efficiency.
[0006] The above-mentioned technical objective of this application is achieved through the following technical solution: a continuous reaction energy-saving acidification reactor, comprising an acidification reactor, a conveying cylinder fixedly installed on the top of the acidification reactor, a functional box fixedly installed on the left side of the conveying cylinder and the acidification reactor, a storage tank fixedly installed on the top of the functional box and the conveying cylinder, a common feed pipe between the storage tank and the conveying cylinder, a feed valve installed in the feed pipe, a common discharge pipe between the conveying cylinder and the acidification reactor, a partition fixedly installed on the inner wall of the acidification reactor, and the bottom end of the discharge pipe extending below the partition; a first stirring mechanism and a second stirring mechanism are provided inside the acidification reactor, a feeding mechanism is provided inside the conveying cylinder, a motor can be fixedly installed on the left side of the functional box, a rotating shaft is rotatably installed on the inner wall of the left side of the functional box, the rotating shaft is located below the motor, the right end of the rotating shaft extends above the partition, a discharge pipe is provided at the bottom right side of the acidification reactor, a discharge valve is provided on the discharge pipe, and a heating mechanism is provided between the functional box and the acidification reactor.
[0007] A further configuration of this application is as follows: the first stirring mechanism includes a first stirring shaft and a stirring rod. The first stirring shaft is rotatably mounted on the inner wall of the top of the acidification reactor. The bottom end of the first stirring shaft extends to below the partition plate. The first stirring shaft is located on the left side of the feed pipe. A stirring rod is provided on the first stirring shaft. The stirring rod is located below the partition plate. A gear mechanism is provided between the first stirring shaft and the rotating shaft.
[0008] By adopting the above technical solution, and by setting up a first stirring mechanism, the first stirring shaft can drive the stirring rod to rotate, thereby stirring the incoming material through the stirring rod. This allows the material to begin mixing fully the moment it enters the reaction zone, promoting the rapid progress of the reaction.
[0009] A further configuration of this application is as follows: the second stirring mechanism includes a second stirring shaft and a blade, the same second stirring shaft is rotatably mounted on the left inner wall of the functional box and the right inner wall of the acidification kettle, the second stirring shaft is located between the partition and the discharge pipe, the blade is provided on the second stirring shaft, the blade is located inside the acidification kettle, and a second transmission mechanism is provided between the second stirring shaft and the rotating shaft.
[0010] By adopting the above technical solution and by setting a second stirring mechanism, the second stirring shaft can drive the blades to rotate, which can realize the stirring of the material in the lower part of the acidification kettle by the blades, and can ensure that the material in the entire reaction area is fully mixed, thereby improving the uniformity and efficiency of the reaction.
[0011] A further configuration of this application is as follows: the feeding mechanism includes a conveying shaft and a spiral blade, the conveying shaft is fixedly installed on the motor output shaft, the right end of the conveying shaft is rotatably connected to the inner wall of the right side of the conveying cylinder, the spiral blade is provided on the conveying shaft, the spiral blade is located inside the conveying cylinder, and a first transmission mechanism is provided between the conveying shaft and the rotating shaft.
[0012] By adopting the above technical solution, and by setting up...
[0013] A further feature of this application is that the gear mechanism includes two bevel gears, and bevel gears are fixedly sleeved on both the first stirring shaft and the right end of the rotating shaft. Both bevel gears are located above the partition plate and mesh with each other.
[0014] By adopting the above technical solution and by setting a gear mechanism, the rotating shaft can drive the first stirring shaft to rotate synchronously.
[0015] A further configuration of this application is as follows: the first transmission mechanism includes two first transmission wheels and a first transmission belt. The first transmission wheels are fixedly sleeved on both the conveying shaft and the rotating shaft. The first transmission wheels are located inside the functional box, and the same first transmission belt is sleeved on both first transmission wheels.
[0016] By adopting the above technical solution and by setting up a first transmission mechanism, the conveying shaft can drive the rotating shaft to rotate synchronously.
[0017] A further configuration of this application is: the second transmission mechanism includes two second transmission wheels and a second transmission belt, with the second transmission wheels fixedly sleeved on both the second stirring shaft and the rotating shaft, the second transmission wheels being located to the left of the first transmission wheel, and the same second transmission belt being sleeved on both second transmission wheels.
[0018] By adopting the above technical solution and by setting a second transmission mechanism, the rotating shaft can drive the second stirring shaft to rotate synchronously.
[0019] A further configuration of this application is as follows: the heating mechanism includes a controller, a heating plate and a temperature sensor. The controller is located on the front side of the functional box, the heating plate is located on the right side of the acidification kettle, and the temperature sensor is located at the bottom of the partition. The temperature sensor is located on the left side of the first stirring shaft, and the temperature sensor, the heating plate and the controller are electrically connected.
[0020] By adopting the above technical solution and setting up a heating mechanism, the temperature sensor can monitor the temperature inside the acidification kettle in real time and feed the temperature data back to the controller. The controller can accurately adjust the working state of the heating plate according to the preset temperature range. When the temperature is close to the upper limit, the heating power is reduced, and when it is close to the lower limit, the heating power is increased. This can avoid the overheating or cooling phenomenon that may occur in traditional heating methods, thereby achieving the goal of energy saving.
[0021] A further feature of this application is that a pressure sensor is provided at the bottom of the partition, the pressure sensor is located between the feed pipe and the first stirring shaft, and the pressure sensor, the discharge valve and the controller are electrically connected.
[0022] By adopting the above technical solution and installing a pressure sensor, the pressure changes inside the acidification reactor can be detected in real time. When the pressure reaches the set threshold, it indicates that the reaction of the reactants has reached the standard. At this time, the controller immediately controls the discharge valve to open for discharge and closes the feed valve at the same time. This can prevent more material from entering and further increasing the pressure, ensuring the safe operation of the equipment and avoiding dangers caused by excessive pressure.
[0023] A further feature of this application is that a liquid level sensor is provided on the inner wall of the left side of the acidification reactor. The liquid level sensor is located between the partition and the second stirring shaft. The liquid level sensor, the feed valve, and the controller are electrically connected.
[0024] By adopting the above technical solution and installing a liquid level sensor, the liquid level in the acidification reactor can be monitored in real time. When the liquid level is low, it indicates that the amount of material in the reactor is insufficient. The controller will close the discharge valve and start the feed valve, so that new material can enter the acidification reactor in a timely manner, maintain the continuous reaction, and achieve the purpose of ensuring the continuity and stability of production.
[0025] The beneficial effects of this application are:
[0026] (1) Through the cooperation of motor, conveying shaft and spiral blade, the spiral blade can be driven by motor to rotate, and the material falling from the feed pipe through the spiral blade can be continuously and stably conveyed to the feed pipe, so as to achieve the purpose of feeding material to acidification kettle.
[0027] (2) Through the cooperation of the first transmission wheel, the first transmission belt, the rotating shaft, the bevel gear, the first stirring shaft and the stirring rod, the conveying shaft can drive the stirring rod to rotate, and the stirring rod can stir the incoming material, so that the material can start to mix fully the moment it enters the reaction area, thus promoting the rapid progress of the reaction. Through the cooperation of the second transmission wheel, the second transmission belt, the second stirring shaft and the blade, the rotating shaft can drive the blade to rotate synchronously, and the blade can stir the material in the lower part of the acidification kettle, thus ensuring that the material in the entire reaction area can be fully mixed, thereby improving the uniformity and efficiency of the reaction.
[0028] (3) Through the cooperation of the controller, air pressure sensor, liquid level sensor, feed valve and discharge valve, when the air pressure reaches the set threshold, it indicates that the reaction of the reactants has reached the standard. At this time, the controller immediately controls the discharge valve to open for discharge and closes the feed valve at the same time. This can prevent more material from entering and further increasing the air pressure, ensuring the safe operation of the equipment and avoiding the danger caused by excessive air pressure. When the liquid level is low, it indicates that the amount of material in the reactor is insufficient. The controller will close the discharge valve and start the feed valve, which can allow new material to enter the acidification reactor in time, maintain the continuous reaction, and achieve the purpose of ensuring the continuity and stability of production. Attached Figure Description
[0029] To more clearly illustrate the technical solutions in the embodiments of this application, the accompanying drawings used in the description of the embodiments will be briefly introduced below. Obviously, the accompanying drawings described below are only some embodiments of this application. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort.
[0030] Figure 1 This is a three-dimensional structural schematic diagram of a continuous reaction energy-saving acidification reactor according to this application;
[0031] Figure 2 This is a schematic diagram of the internal structure of the acidification vessel and conveying cylinder of a continuous reaction energy-saving acidification vessel according to this application;
[0032] Figure 3 This is a schematic diagram of the internal structure of the functional box and conveying cylinder of a continuous reaction energy-saving acidification reactor according to this application;
[0033] Figure 4 This is a schematic diagram of structure A of a continuous reaction energy-saving acidification reactor according to this application.
[0034] In the diagram: 1. Acidification kettle; 2. Conveying cylinder; 3. Functional box; 4. Storage tank; 401. Feed pipe; 201. Discharge pipe; 5. Baffle plate; 6. Controller; 7. Discharge pipe; 8. Heating plate; 101. First stirring shaft; 102. Stirring rod; 103. Second stirring shaft; 104. Paddle; 202. Conveying shaft; 203. Spiral blade; 301. Motor; 302. Rotating shaft; 303. Bevel gear; 304. First transmission wheel; 305. First transmission belt; 306. Second transmission wheel; 307. Second transmission belt; 601. Pressure sensor; 602. Liquid level sensor. Detailed Implementation
[0035] The technical solution of this application will be clearly and completely described below with reference to specific embodiments. Obviously, the described embodiments are only a part of the embodiments of this application, and not all of them. All other embodiments obtained by those skilled in the art based on the embodiments of this application without creative effort are within the scope of protection of this application.
[0036] See Figures 1-4 This application provides a continuous reaction energy-saving acidification reactor, including an acidification reactor 1. A conveying cylinder 2 is fixedly installed on the top of the acidification reactor 1. A functional box 3 is fixedly installed on the left side of the conveying cylinder 2 and the acidification reactor 1. A storage tank 4 is fixedly installed on the top of the functional box 3 and the conveying cylinder 2. A feed pipe 401 is provided between the storage tank 4 and the conveying cylinder 2. A feed valve is provided inside the feed pipe 401. A discharge pipe 201 is provided between the conveying cylinder 2 and the acidification reactor 1. A baffle 5 is fixedly installed on the inner wall of the acidification reactor 1. The bottom end of the feed pipe 201 extends to below the partition 5; the acidification tank 1 is equipped with a first stirring mechanism and a second stirring mechanism, the conveying cylinder 2 is equipped with a feeding mechanism, the left side of the function box 3 can be fixedly installed with a motor 301, the inner wall of the left side of the function box 3 is rotatably installed with a rotating shaft 302, the rotating shaft 302 is located below the motor 301, the right end of the rotating shaft 302 extends to above the partition 5, the bottom right side of the acidification tank 1 is equipped with a discharge pipe 7, the discharge pipe 7 is equipped with a discharge valve, and a heating mechanism is provided between the function box 3 and the acidification tank 1.
[0037] Specifically, the first stirring mechanism includes a first stirring shaft 101 and a stirring rod 102. The first stirring shaft 101 is rotatably mounted on the inner wall of the top of the acidification reactor 1. The bottom end of the first stirring shaft 101 extends to the bottom of the partition 5. The first stirring shaft 101 is located to the left of the feed pipe 201. The stirring rod 102 is provided on the first stirring shaft 101. The stirring rod 102 is located below the partition 5. A gear mechanism is provided between the first stirring shaft 101 and the rotating shaft 302.
[0038] Specifically, the second stirring mechanism includes a second stirring shaft 103 and a paddle 104. The same second stirring shaft 103 is rotatably mounted on the inner left side of the functional box 3 and the inner right side of the acidification vessel 1. The second stirring shaft 103 is located between the partition plate 5 and the discharge pipe 7. The paddle 104 is provided on the second stirring shaft 103 and is located inside the acidification vessel 1. A second transmission mechanism is provided between the second stirring shaft 103 and the rotating shaft 302.
[0039] Specifically, the feeding mechanism includes a conveying shaft 202 and a spiral blade 203. The conveying shaft 202 is fixedly installed on the output shaft of the motor 301. The right end of the conveying shaft 202 is rotatably connected to the inner wall of the right side of the conveying cylinder 2. The spiral blade 203 is provided on the conveying shaft 202 and is located inside the conveying cylinder 2. A first transmission mechanism is provided between the conveying shaft 202 and the rotating shaft 302.
[0040] Specifically, the gear mechanism includes two bevel gears 303. Both the first stirring shaft 101 and the right end of the rotating shaft 302 are fixedly fitted with bevel gears 303. Both bevel gears 303 are located above the partition plate 5 and mesh with each other.
[0041] Specifically, the first transmission mechanism includes two first transmission wheels 304 and a first transmission belt 305. The first transmission wheels 304 are fixedly sleeved on both the conveying shaft 202 and the rotating shaft 302. The first transmission wheels 304 are located inside the functional box 3, and the same first transmission belt 305 is sleeved on the two first transmission wheels 304.
[0042] Specifically, the second transmission mechanism includes two second transmission wheels 306 and a second transmission belt 307. The second transmission wheels 306 are fixedly sleeved on both the second stirring shaft 103 and the rotating shaft 302. The second transmission wheels 306 are located to the left of the first transmission wheel 304, and the same second transmission belt 307 is sleeved on both second transmission wheels 306.
[0043] Specifically, the heating mechanism includes a controller 6, a heating plate 8, and a temperature sensor. The controller 6 is located on the front side of the functional box 3, the heating plate 8 is located on the right side of the acidification vessel 1, and the temperature sensor is located at the bottom of the partition 5. The temperature sensor is located on the left side of the first stirring shaft 101, and the temperature sensor, the heating plate 8, and the controller 6 are electrically connected.
[0044] Specifically, a pressure sensor 601 is installed at the bottom of the partition 5. The pressure sensor 601 is located between the feed pipe 201 and the first stirring shaft 101. The pressure sensor 601, the discharge valve and the controller 6 are electrically connected.
[0045] Specifically, a liquid level sensor 602 is installed on the inner wall of the left side of the acidification reactor 1. The liquid level sensor 602 is located between the partition 5 and the second stirring shaft 103. The liquid level sensor 602, the feed valve and the controller 6 are electrically connected.
[0046] In this application, during operation, the motor 301 is first started, and its output shaft drives the conveyor shaft 202 to rotate, which in turn drives the spiral blades 203 to rotate, continuously and stably conveying the material falling from the feed pipe 401 to the feed pipe 201, thus achieving the purpose of feeding material into the acidification reactor 1. At the same time, the conveyor shaft 202 drives the rotating shaft 302 to rotate through the first transmission wheel 304 and the first transmission belt 305, enabling one power source to drive multiple components, reducing the use of additional power equipment and lowering energy consumption. After the rotating shaft 302 rotates, on the one hand, it drives the first stirring shaft 101 to rotate through the two bevel gears 303, which stirs the incoming material through the stirring rod 102, ensuring that the material is fully mixed the moment it enters the reaction zone, promoting the rapid progress of the reaction. On the other hand, it drives the second stirring shaft 103 and the blades 104 through the second transmission wheel 306 and the second transmission belt 307 to stir the material in the lower part of the acidification reactor 1, ensuring that the material in the entire reaction zone is fully mixed, improving the uniformity and efficiency of the reaction.
[0047] The temperature sensor monitors the temperature inside the acidification reactor 1 in real time and feeds the temperature data back to the controller 6. The controller 6 precisely adjusts the working state of the heating plate 8 according to the preset temperature range. When the temperature approaches the upper limit, the heating power is reduced, and when it approaches the lower limit, the heating power is increased. This avoids overheating or overcooling that may occur in traditional heating methods, thus achieving energy saving. The pressure sensor 601 can sense the pressure change inside the acidification reactor in real time. When the pressure reaches the set threshold, it indicates that the reaction has reached the standard. At this time, the controller 6 immediately controls the discharge valve to open for discharge and closes the feed valve at the same time. This prevents more material from entering and further increasing the pressure, ensuring the safe operation of the equipment and avoiding dangers caused by excessive pressure. The liquid level sensor 602 monitors the liquid level inside the acidification reactor 1 in real time. When the liquid level is low, it indicates that the amount of material in the reactor is insufficient. The controller 6 will close the discharge valve and open the feed valve, allowing new material to enter the acidification reactor in a timely manner, maintaining the continuous reaction, and ensuring the continuity and stability of production.
Claims
1. A continuous reaction type energy-saving acidification reactor, characterized in that, The system includes an acidification reactor (1), a conveying cylinder (2) fixedly installed on the top of the acidification reactor (1), a functional box (3) fixedly installed on the left side of the conveying cylinder (2) and the acidification reactor (1), a storage box (4) fixedly installed on the top of the functional box (3) and the conveying cylinder (2), a feeding pipe (401) provided between the storage box (4) and the conveying cylinder (2), a feeding valve provided inside the feeding pipe (401), a discharge pipe (201) provided between the conveying cylinder (2) and the acidification reactor (1), a partition (5) fixedly installed on the inner wall of the acidification reactor (1), and the bottom end of the discharge pipe (201) extending to below the partition (5). The acidification reactor (1) is equipped with a first stirring mechanism and a second stirring mechanism. The conveying cylinder (2) is equipped with a feeding mechanism. A motor (301) can be fixedly installed on the left side of the functional box (3). A rotating shaft (302) is rotatably installed on the inner wall of the left side of the functional box (3). The rotating shaft (302) is located below the motor (301). The right end of the rotating shaft (302) extends to the top of the partition plate (5). A discharge pipe (7) is provided at the bottom right side of the acidification reactor (1). A discharge valve is provided on the discharge pipe (7). A heating mechanism is provided between the functional box (3) and the acidification reactor (1).
2. The continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: The first stirring mechanism includes a first stirring shaft (101) and a stirring rod (102). The first stirring shaft (101) is rotatably mounted on the inner wall of the top of the acidification reactor (1). The bottom end of the first stirring shaft (101) extends to below the partition plate (5). The first stirring shaft (101) is located on the left side of the feed pipe (201). A stirring rod (102) is provided on the first stirring shaft (101). The stirring rod (102) is located below the partition plate (5). A gear mechanism is provided between the first stirring shaft (101) and the rotating shaft (302).
3. The continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: The second stirring mechanism includes a second stirring shaft (103) and a blade (104). The same second stirring shaft (103) is rotatably installed on the left inner wall of the functional box (3) and the right inner wall of the acidification kettle (1). The second stirring shaft (103) is located between the partition plate (5) and the discharge pipe (7). A blade (104) is provided on the second stirring shaft (103). The blade (104) is located inside the acidification kettle (1). A second transmission mechanism is provided between the second stirring shaft (103) and the rotating shaft (302).
4. The continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: The feeding mechanism includes a conveying shaft (202) and a spiral blade (203). The conveying shaft (202) is fixedly installed on the output shaft of the motor (301). The right end of the conveying shaft (202) is rotatably connected to the inner wall of the right side of the conveying cylinder (2). The spiral blade (203) is provided on the conveying shaft (202). The spiral blade (203) is located inside the conveying cylinder (2). A first transmission mechanism is provided between the conveying shaft (202) and the rotating shaft (302).
5. A continuous reaction energy-saving acidification reactor according to claim 2, characterized in that: The gear mechanism includes two bevel gears (303). The first stirring shaft (101) and the right end of the rotating shaft (302) are both fixedly fitted with bevel gears (303). The two bevel gears (303) are located above the partition plate (5) and mesh with each other.
6. The continuous reaction energy-saving acidification reactor according to claim 4, characterized in that: The first transmission mechanism includes two first transmission wheels (304) and a first transmission belt (305). The first transmission wheels (304) are fixedly sleeved on both the conveying shaft (202) and the rotating shaft (302). The first transmission wheels (304) are located inside the functional box (3). The same first transmission belt (305) is sleeved on the two first transmission wheels (304).
7. The continuous reaction energy-saving acidification reactor according to claim 3, characterized in that: The second transmission mechanism includes two second transmission wheels (306) and a second transmission belt (307). The second transmission wheels (306) are fixedly sleeved on both the second stirring shaft (103) and the rotating shaft (302). The second transmission wheels (306) are located to the left of the first transmission wheel (304), and the same second transmission belt (307) is sleeved on both second transmission wheels (306).
8. The continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: The heating mechanism includes a controller (6), a heating plate (8) and a temperature sensor. The controller (6) is located on the front side of the functional box (3), the heating plate (8) is located on the right side of the acidification kettle (1), and the temperature sensor is located at the bottom of the partition (5). The temperature sensor is located on the left side of the first stirring shaft (101). The temperature sensor, the heating plate (8) and the controller (6) are electrically connected.
9. The continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: A pressure sensor (601) is provided at the bottom of the partition (5). The pressure sensor (601) is located between the feed pipe (201) and the first stirring shaft (101). The pressure sensor (601), the discharge valve and the controller (6) are electrically connected.
10. A continuous reaction energy-saving acidification reactor according to claim 1, characterized in that: A liquid level sensor (602) is provided on the inner wall of the left side of the acidification reactor (1). The liquid level sensor (602) is located between the partition plate (5) and the second stirring shaft (103). The liquid level sensor (602), the feed valve and the controller (6) are electrically connected.
Citation Information
Patent Citations
Acidification kettle for continuous reaction
CN213348873U