Efficient distillation and separation device for side-chain alcohol synthesis

Abstract

The utility model discloses an efficient distillation and separation device for side chain alcohol synthesis, which relates to the technical field of distillation and separation devices and comprises a device table, an electric heating round seat is integrally formed at the upper end of the device table, a seat leaning plate is arranged on one side of the electric heating round seat, and the seat leaning plate and the device table are of an integral structure. An electric push rod is fixedly arranged on the outer wall of one side of the seat leaning plate through a screw; the distillation retort is mounted in the electric heating round seat, a top sealing cover is arranged right above the distillation retort, a vacuum suction pump is arranged at the rear end of the electric heating round seat, and a suction pipe of the vacuum suction pump is communicated with the interior of the distillation retort; the condensation tank is arranged on one side of the distillation tank, and the problem that the side-chain alcohol synthesis effect is affected due to the fact that the existing distillation device lacks protection on thermosensitive substances in the using process and the thermosensitive substances needed by side-chain alcohol synthesis can be decomposed by the distillation device for side-chain alcohol synthesis is solved.

Description

A high-efficiency distillation and separation apparatus for the synthesis of side-chain alcohols Technical Field

[0001] This utility model relates to the field of distillation and separation equipment technology, specifically to a high-efficiency distillation and separation equipment for the synthesis of side-chain alcohols. Background Technology

[0002] Side-chain alcohol synthesis refers to the process of attaching specific side-chain groups to alcohol molecules through chemical reactions to generate new compounds or materials. Side-chain alcohols play an important role in organic synthesis and are often used in fields such as drug synthesis and materials science. The synthesis of side-chain alcohols requires separation and processing using distillation equipment.

[0003] For example, the announcement number CN219897088U (named "A Subdivision Distillation Apparatus for the Preparation of Synthetic Leaf Alcohol") includes a support base, a heating base, a distillation kettle, a feed pipe, a steam guiding pipe, a condenser, and a condenser. The heating base is connected to the upper left side of the support base, and the distillation kettle is connected to the top of the heating base. The feed pipe is connected to the upper left side of the distillation kettle, and the steam guiding pipe is connected to the top of the distillation kettle. The condenser is connected to the upper right side of the steam guiding pipe, and the condenser is connected to the lower part of the condenser. The feed pipe is connected to an external conveying device, which transports the raw material to the distillation kettle. The heating base then heats the raw material, and the generated steam enters the condenser through the steam guiding pipe. Under the action of the condenser, the steam condenses into liquid in the condenser and is discharged. The output shaft of the servo motor rotates, which drives the rotating disk to rotate. The rotating disk rotates, which in turn drives the collection bottle to rotate, so that the collection bottle is located below the outlet of the condenser. The collection bottle can be automatically replaced according to the different liquids formed by condensation, improving the convenience of operation.

[0004] The aforementioned distillation apparatus lacks protection against heat-sensitive substances during use, which can lead to the decomposition of these substances required for the synthesis of side-chain alcohols, thus affecting the synthesis efficiency. Therefore, we provide a highly efficient distillation and separation apparatus for the synthesis of side-chain alcohols. Summary of the Invention

[0005] The purpose of this invention is to provide a highly efficient distillation and separation device for the synthesis of side-chain alcohols, in order to solve the problem mentioned in the background art that the existing distillation devices lack protection for heat-sensitive substances during use, which leads to the decomposition of the heat-sensitive substances required for the synthesis of side-chain alcohols, thus affecting the synthesis effect of side-chain alcohols.

[0006] To achieve the above objectives, the present invention provides the following technical solution: a high-efficiency distillation and separation device for the synthesis of side-chain alcohols, including a device platform, an electric heating round seat integrally formed on the upper end of the device platform, a backing plate on one side of the electric heating round seat, the backing plate and the device platform being an integral structure, and an electric push rod fixedly mounted on the outer wall of one side of the backing plate by screws.

[0007] Also includes:

[0008] A distillation vessel is installed inside the heating element, and a top cover is provided on the top of the distillation vessel. A vacuum pump is provided at the rear end of the heating element, and the pumping pipe of the vacuum pump is connected to the interior of the distillation vessel.

[0009] A condenser is located on one side of the distillation tank, and a sleeve pipe and a drain pipe are respectively connected to the upper and lower ends of the condenser. A guide pipe is connected to the top of the top cover, and the guide pipe is movably connected to the sleeve pipe.

[0010] The receiving cylinder is set on the support plate on the outer wall of one side of the device platform. One end of the drain pipe is connected to the receiving cylinder. The condenser is equipped with six diversion pipes inside, and the two ends of the six diversion pipes are connected to the sleeve pipe and the drain pipe, respectively.

[0011] Preferably, two on / off valves are connected to one side of the outer wall of the condenser, and one end of the two on / off valves is respectively connected to a water injection pipe and a drain pipe.

[0012] Preferably, a sealing plug is fixed to the lower end of the top cover by adhesive, and the top cover is connected to the top of the distillation jar by the sealing plug.

[0013] Preferably, support rods are welded to both outer walls of the condenser, and both support rods are welded to the device platform.

[0014] Preferably, a connecting rod is welded to the top of the electric push rod piston rod, and one end of the connecting rod is welded to the top cover.

[0015] Preferably, a switch is provided on one side of the electric heating base, and a power supply box is provided on the front end of the device platform. The output and input ends of the switch are electrically connected to the power supply box and the electric heating plate inside the electric heating base respectively via power lines.

[0016] Preferably, an air extraction valve is provided at the air inlet end of the vacuum pump extraction pipe, and the air inlet and outlet ends of the air extraction valve are respectively connected to the distillation tank and the vacuum pump extraction pipe.

[0017] Compared with the prior art, the beneficial effects of this utility model are:

[0018] This invention uses a vacuum pump to extract the internal gas of the distillation tank, reducing the internal pressure. Then, pressing a switch powers the power supply to the heating element, which in turn heats the tank for distillation. During distillation, the substances required for synthesis are heated in a low-pressure environment, allowing for distillation and separation without reaching the boiling point of the liquid. This overcomes the problem of existing distillation devices lacking protection for heat-sensitive substances, which can lead to the decomposition of these substances in the synthesis of side-chain alcohols, thus affecting the synthesis efficiency. Attached Figure Description

[0019] Figure 1 is a front view of the structure of the high-efficiency distillation and separation device for side-chain alcohol synthesis of this utility model;

[0020] Figure 2 is a rear view of the structure of the high-efficiency distillation and separation device for side-chain alcohol synthesis of this utility model;

[0021] Figure 3 is a top view of the structure of the high-efficiency distillation and separation device for side-chain alcohol synthesis of this utility model;

[0022] Figure 4 is an enlarged schematic diagram of part A of this utility model;

[0023] In the diagram: 1. Apparatus platform; 2. Support plate; 3. Electric push rod; 4. Power supply box; 5. Switch; 6. Heating round seat; 7. Feeding cylinder; 8. Distillation tank; 9. Top cover; 10. Sealing plug; 11. Connecting rod; 12. Socket pipe; 13. Guide pipe; 14. Condenser; 15. Support rod; 16. Drain pipe; 17. Vacuum pump; 18. Water injection pipe; 19. Drain pipe; 20. Vacuum valve; 21. Diverter pipe; 22. Opening and closing valve. Detailed Implementation

[0024] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present utility model. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments.

[0025] Please refer to Figures 1-4. One embodiment of this utility model is provided: a high-efficiency distillation and separation device for side-chain alcohol synthesis, including a device platform 1. An electric heating round seat 6 is integrally formed on the upper end of the device platform 1. A backrest plate 2 is provided on one side of the electric heating round seat 6. The backrest plate 2 and the device platform 1 are integrally formed. An electric push rod 3 is fixed on the outer wall of one side of the backrest plate 2 by screws.

[0026] Also includes:

[0027] Distillation tank 8 is installed inside the electric heating base 6, and a top cover 9 is provided on the top of the distillation tank 8. A vacuum pump 17 is provided at the rear end of the electric heating base 6, and the suction pipe of the vacuum pump 17 is connected to the inside of the distillation tank 8.

[0028] The condenser 14 is located on one side of the distillation tank 8, and the upper and lower ends of the condenser 14 are respectively connected to the sleeve pipe 12 and the drain pipe 16. The top of the top cover 9 is connected to the guide pipe 13, and the guide pipe 13 is movably connected to the sleeve pipe 12.

[0029] The receiving cylinder 7 is set on the support plate on the outer wall of one side of the device platform 1. One end of the drain pipe 16 is connected to the receiving cylinder 7. The condenser 14 is equipped with six diversion pipes 21. The two ends of the six diversion pipes 21 are connected to the sleeve pipe 12 and the drain pipe 16 respectively.

[0030] In use, the substances required for the synthesis of side-chain alcohols are poured into the interior of the distillation tank 8 for distillation. The top cover 9 is pressed down by the electric push rod 3, sealing the top of the distillation tank 8. Then, the evacuation valve 20 is opened, and the gas inside the distillation tank 8 is extracted by the vacuum pump 17, reducing the pressure inside the distillation tank 8. Then, the switch 5 is pressed, which powers the electric heating element 6 from the power supply box 4. The electric heating element 6 heats the distillation tank 8 for distillation. During the distillation process, the substances required for synthesis are heated in a low-pressure environment, so that the distillation separation of the substances required for synthesis can be achieved without heating to the boiling point of the liquid. This avoids the decomposition of the heat-sensitive substances required for the synthesis of side-chain alcohols due to excessive heating temperature. The distilled liquid vapor enters the interior of the condenser 14 through the guide pipe 13 and the sleeve pipe 12. The interior of the condenser 14 is pre-filled with condensate. After the hot vapor is split by the split pipe 21, it is cooled into liquid by the pre-filled condensate and finally flows into the receiving cylinder 7 through the drain pipe 16 for collection, thereby achieving the purpose of separating the liquid from the mixed liquid.

[0031] Please refer to Figure 4. Two on / off valves 22 are connected to one side of the outer wall of the condenser 14. One end of each valve 22 is connected to a water inlet pipe 18 and a drain pipe 19, respectively. The two valves 22 control the opening and closing of the water inlet pipe 18 and the drain pipe 19. Please refer to Figure 1. A sealing plug 10 is fixed to the lower end of the top cover 9 with adhesive. The top cover 9 is connected to the top of the distillation tank 8 by the sealing plug 10. The sealing plug 10, fixed to the lower end of the top cover 9 with adhesive, facilitates the sealing connection between the top cover 9 and the distillation tank 8. Please refer to Figure 1. Support rods 15 are welded to both sides of the outer wall of the condenser 14. Both support rods 15 are welded to the device platform 1. The support rods 15 on both sides of the outer wall of the condenser 14 support and connect the condenser 14 and the device platform 1. Please refer to Figure 1. Electric push A connecting rod 11 is welded to the top of the piston rod of rod 3. One end of the connecting rod 11 is welded to the top cover 9. The connecting rod 11 welded to the top of the piston rod of electric push rod 3 facilitates the linkage of electric push rod 3 with top cover 9. Please refer to the figure. A switch 5 is provided on one side of the electric heating round seat 6. A power supply box 4 is provided on the front surface of the device platform 1. The output and input ends of the switch 5 are electrically connected to the power supply box 4 and the electric heating plate inside the electric heating round seat 6 respectively through power lines. The switch 5 provided on one side of the electric heating round seat 6 controls the start and stop of power supply to the electric heating round seat 6. Please refer to Figure 2. A suction valve 20 is provided at the air inlet end of the suction pipe of vacuum pump 17. The air inlet and outlet ends of suction valve 20 are connected to distillation tank 8 and suction pipe of vacuum pump 17 respectively. The suction valve 20 provided at the air inlet end of the suction pipe of vacuum pump 17 controls the opening and closing of the suction pipe of vacuum pump 17.

[0032] It will be apparent to those skilled in the art that this invention is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or essential characteristics of this invention. Therefore, the embodiments should be considered illustrative and non-limiting in all respects, and the scope of this invention is defined by the appended claims rather than the foregoing description. Thus, it is intended that all variations falling within the meaning and scope of equivalents of the claims be included within this invention. No reference numerals in the claims should be construed as limiting the scope of the claims.

Claims

1. A high-efficiency distillation and separation apparatus for the synthesis of side-chain alcohols, comprising a platform (1), an electrically heated circular seat (6) integrally formed on the upper end of the platform (1), a backrest plate (2) provided on one side of the electrically heated circular seat (6), the backrest plate (2) and the platform (1) being an integral structure, and an electric push rod (3) fixedly provided on the outer wall of one side of the backrest plate (2) by screws; characterized in that: Also includes: A distillation tank (8) is installed inside the electric heating base (6), and a top cover (9) is provided on the top of the distillation tank (8). A vacuum pump (17) is provided at the rear end of the electric heating base (6), and the suction pipe of the vacuum pump (17) is connected to the interior of the distillation tank (8). A condenser (14) is located on one side of the distillation tank (8), and a sleeve pipe (12) and a drain pipe are respectively connected to the upper and lower ends of the condenser (14). (16) The top of the top cover (9) is connected to the guide pipe (13), and the guide pipe (13) is connected to the sleeve pipe (12) in a movable manner; the receiving cylinder (7) is set on the support plate on the outer wall of one side of the device platform (1), one end of the drain pipe (16) is connected to the receiving cylinder (7), and the condenser (14) is provided with six diversion pipes (21) inside, and the two ends of the six diversion pipes (21) are connected to the sleeve pipe (12) and the drain pipe (16) respectively.

2. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: Two on / off valves (22) are connected to one side of the outer wall of the condenser (14), and one end of the two on / off valves (22) is connected to a water injection pipe (18) and a drain pipe (19).

3. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: The lower end of the top cover (9) is fixed with a sealing plug (10) by adhesive, and the top cover (9) is connected to the top of the distillation tank (8) by the sealing plug (10).

4. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: Support rods (15) are welded to both outer walls of the condenser (14), and both support rods (15) are welded to the device platform (1).

5. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: A connecting rod (11) is welded to the top of the piston rod of the electric push rod (3), and one end of the connecting rod (11) is welded to the top cover (9).

6. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: A switch (5) is provided on one side of the electric heating round seat (6), and a power supply box (4) is provided on the front surface of the device platform (1). The output and input ends of the switch (5) are electrically connected to the power supply box (4) and the electric heating plate inside the electric heating round seat (6) respectively through power lines.

7. The high-efficiency distillation and separation apparatus for side-chain alcohol synthesis according to claim 1, characterized in that: The vacuum pump (17) has an air inlet valve (20) at the air inlet end of its air inlet pipe. The air inlet and outlet ends of the air inlet valve (20) are respectively connected to the distillation tank (8) and the vacuum pump (17) air inlet pipe.

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