Gas-liquid separation device in methanol-to-hydrogen equipment
By designing a gas-liquid separation device in a methanol-to-hydrogen equipment and utilizing induced draft, cooling, and multi-stage dewatering technologies, the problem of low gas-liquid separation efficiency was solved, achieving a highly efficient gas-liquid separation effect, reducing reaction liquid waste, and increasing the hydrogen processing reaction volume.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- HEBEI HAITE WEIYE PETROCHEM
- Filing Date
- 2025-05-15
- Publication Date
- 2026-05-12
AI Technical Summary
In existing methanol-to-hydrogen equipment, the gas-liquid separation efficiency is low, resulting in waste of reaction liquid and affecting the amount of hydrogen processed.
Design a gas-liquid separation device, including a gas-liquid separation tank, an induction air chamber, a cold water tank, a conical water collection hood with a V-shaped water collection ring, and a heat exchange chamber. Combined with induction air, drainage, and refrigeration mechanisms, it achieves efficient gas-liquid separation through multi-stage drainage and heat exchange.
It significantly improves gas-liquid separation efficiency, reduces reaction liquid waste, and increases the amount of hydrogen processing reaction.
Smart Images

Figure CN224221062U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of methanol-to-hydrogen technology, specifically to a gas-liquid separation device in a methanol-to-hydrogen equipment. Background Technology
[0002] Against the backdrop of the global push for carbon neutrality, methanol-to-hydrogen technology is of great significance. In the current process of hydrogen production using methanol, some methanol evaporates and moves out during the reaction, and then moves into the reaction vessel along with the gas produced after the reaction. During this process, it is not possible to separate the gas mixture into liquid and gas in a timely and rapid manner, which leads to a large amount of the reaction liquid being removed and wasted, thus affecting the amount of hydrogen produced.
[0003] A search revealed that patent CN220531005U discloses a gas-liquid separation device in a methanol-to-hydrogen equipment. This device utilizes the structural functions of a corrugated water-collecting plate and a refrigeration unit to circulate cooling liquid within a cooling pipe. Simultaneously, cooling gas is generated outside the cooling pipe. Combined with the rotation of a fan blade, the cooling gas accumulated on the outer wall of the cooling pipe is transported to the surface of the corrugated water-collecting plate, significantly reducing its surface temperature. This cools the gas-liquid mixture in contact with the plate, causing the vaporized liquid inside to liquefy and collect again, facilitating gas-liquid separation and preventing waste of methanol liquid during hydrogen production. Although the corrugated water-collecting plate has a good water-collecting effect, its effectiveness still needs improvement, thus limiting the gas-liquid separation efficiency. Therefore, this paper proposes a gas-liquid separation device in a methanol-to-hydrogen equipment with even better water-collecting performance, further enhancing gas-liquid separation efficiency. Utility Model Content
[0004] (a) Technical problems to be solved
[0005] To address the shortcomings of existing technologies, this invention provides a gas-liquid separation device in a methanol-to-hydrogen equipment, which has a better water-gathering effect and further improves gas-liquid separation efficiency.
[0006] (II) Technical Solution
[0007] To achieve the above objectives, this utility model provides the following technical solution: a gas-liquid separation device in a methanol-to-hydrogen equipment, comprising a gas-liquid separation tank, wherein the interior of the gas-liquid separation tank is arranged from bottom to top as follows: an induction chamber, a cold water tank, a conical water-collecting hood with multiple continuous V-shaped water-collecting rings, and a heat exchange chamber. The top of the conical water-collecting hood is sealed and fixedly connected through the top of the gas-liquid separation tank and connected to a gas guide tank with a conveying pipe. The bottom of the gas-liquid separation tank is fixedly connected to an air inlet pipe that communicates with the induction chamber. Multiple heat exchange pipes are vertically fixedly connected through the cold water tank. The device also includes a drainage mechanism. An induction mechanism for inducing air upwards is provided in the induction chamber.
[0008] Preferably, the heat exchange chamber is fixedly connected to the cold water tank via a connecting water pipe, and the cold water tank, the connecting water pipe, and the heat exchange chamber are filled with heat exchange cold water. It also includes a refrigeration mechanism connected to the heat exchange chamber and the cold water tank. The refrigeration mechanism includes a water pump and a cooler fixedly installed on the top of the gas-liquid separator. The input end of the water pump is fixedly connected to the cold water tank via a water pumping pipe, and the output end of the water pump is connected to the input end of the cooler. The output end of the cooler is fixedly connected to the top of the gas-liquid separator and connected to the heat exchange chamber.
[0009] Preferably, the drainage mechanism includes a drainage main pipe fixedly connected to drainage branch pipe one and drainage branch pipe two. A drainage valve is installed at the bottom of the drainage main pipe. Drainage branch pipe one is connected to the top of the cold water tank on the gas-liquid separator. Drainage branch pipe two is connected to the bottom of the induction chamber on the gas-liquid separator. A connecting air pipe is also fixedly connected to the drainage main pipe, located above drainage branch pipe one and fixedly connected to the gas-liquid separator.
[0010] Preferably, the cold water tank has drainage grooves located directly below the multiple V-shaped water collection rings, and a connecting groove is provided between the multiple drainage grooves and the first drainage branch pipe on the cold water tank. The multiple heat exchange pipes and the multiple drainage grooves are arranged in a cross pattern.
[0011] Preferably, the bottom of the gas-liquid separator has a certain slope towards the two sides of the drain branch pipe.
[0012] Preferably, the air-inducing mechanism includes a fan blade disposed in the air-inducing chamber and rotatably connected to the bottom of the gas-liquid separator, and a drive motor for driving the fan blade to rotate is also fixedly installed at the bottom of the gas-liquid separator.
[0013] (III) Beneficial Effects
[0014] Compared with the prior art, this utility model provides a gas-liquid separation device in a methanol-to-hydrogen equipment, which has the following beneficial effects:
[0015] The gas-liquid separation device in this methanol-to-hydrogen equipment facilitates gas entry from the bottom via an inlet pipe, an induced draft chamber, a cold water tank, and a conical water-collecting hood with multiple continuous V-shaped water-collecting rings. Gas passes through the cold water tank for initial water removal, and then through the conical water-collecting hood with multiple continuous V-shaped water-collecting rings, the upward-flowing air is concentrated and converged. During this convergence process, the water is further removed as completely as possible through the multiple V-shaped water-collecting rings, resulting in better water removal than using inclined corrugated water-collecting plates, thus further improving gas-liquid separation efficiency. An induction mechanism guides the gas entering the induced draft chamber upwards, and the separated gas enters a gas guide tank and is then transported to the next operating stage via a delivery pipe. A drainage mechanism facilitates the discharge of the drained water. This gas-liquid separation device in the methanol-to-hydrogen equipment exhibits superior water collection, further enhancing gas-liquid separation efficiency. Attached Figure Description
[0016] Figure 1 This is a schematic diagram showing a partial cross-section of the present invention.
[0017] Figure 2 This is a schematic diagram of the overall structure of this utility model;
[0018] Figure 3 This is a structural schematic diagram of the present invention from other perspectives, showing a partial cross-section of the whole;
[0019] Figure 4 This is a structural schematic diagram of the present invention from another perspective, showing a partial cross-section of the whole;
[0020] Figure 5 This is a structural schematic diagram of the present invention from other perspectives;
[0021] Figure 6 This is a structural schematic diagram of the present invention from another perspective;
[0022] Figure 7 This is a structural schematic diagram of the present invention from a partial cross-sectional view or individual perspective.
[0023] The attached diagram is labeled as follows: 1. Gas-liquid separator; 2. Cold water tank; 3. Conical water collection hood; 4. V-shaped water collection ring; 5. Air guide tank; 6. Air inlet pipe; 7. Heat exchange pipe; 8. Drainage trough; 9. Drainage branch pipe one; 10. Drainage main pipe; 11. Connecting air pipe; 12. Drainage branch pipe two; 13. Drain valve; 14. Fan blade; 15. Drive motor; 16. Connecting water pipe; 17. Water pump; 18. Refrigerator; 19. Pumping pipe. Detailed Implementation
[0024] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.
[0025] Example:
[0026] Please see Figure 1-7 A gas-liquid separation device in a methanol-to-hydrogen equipment includes a gas-liquid separation tank 1. The interior of the gas-liquid separation tank 1 is arranged from bottom to top as follows: an induction chamber, a cold water tank 2, a conical water-collecting hood 3 with multiple continuous V-shaped water-collecting rings 4, and a heat exchange chamber. The top of the conical water-collecting hood 3 is sealed and fixedly connected through the top of the gas-liquid separation tank 1 and connected to a gas guide tank 5 with a delivery pipe. The bottom of the gas-liquid separation tank 1 is fixedly connected to an air inlet pipe 6 that communicates with the induction chamber. Multiple heat exchange pipes 7 are vertically fixedly connected through the cold water tank 2. The device also includes a drainage mechanism. An induction mechanism for inducing air upwards is provided in the induction chamber.
[0027] Specifically, the heat exchange chamber is fixedly connected to the cold water tank 2 via a connecting water pipe 16. The cold water tank 2, the connecting water pipe 16, and the heat exchange chamber are filled with heat exchange cold water. The system also includes a refrigeration mechanism connected to the heat exchange chamber and the cold water tank 2. The refrigeration mechanism includes a water pump 17 and a cooler 18 fixedly installed on the top of the gas-liquid separator 1. The input end of the water pump 17 is fixedly connected to the cold water tank 2 via a pumping pipe 19. The output end of the water pump 17 is connected to the input end of the cooler 18. The output end of the cooler 18 is fixedly connected to the top of the gas-liquid separator 1 and to the heat exchange chamber. When the water pump 17 and the cooler 18 are turned on, the heat exchange cold water in the cold water tank 2 is drawn out through the water pumping pipe 19 and sent into the cooler 18 for further cooling. Then, after passing through the heat exchange chamber, it is sent back to the cold water tank 2 through the connecting water pipe 16. It continues to exchange heat with the gas passing through the heat exchange pipes 7 through multiple heat exchange pipes 7, forming preliminary water drainage. The drained water falls into the bottom of the induced draft chamber. Due to the setting of the refrigeration mechanism, the heat exchange cold water in the heat exchange chamber exchanges heat with the conical water collection shroud 3, so that the conical water collection shroud 3 maintains a certain water drainage efficiency.
[0028] Specifically, the drainage mechanism includes a main drainage pipe 10 that is fixedly connected to a first drainage branch pipe 9 and a second drainage branch pipe 12. A drain valve 13 is installed at the bottom of the main drainage pipe 10. The first drainage branch pipe 9 is connected to the top of the cold water tank 2 on the gas-liquid separator 1, and the second drainage branch pipe 12 is connected to the bottom of the induction chamber on the gas-liquid separator 1. A connecting air pipe 11 is also fixedly connected to the main drainage pipe 10, located above the first drainage branch pipe 9 and fixedly connected to the gas-liquid separator 1. The first drainage branch pipe 9 facilitates the drainage of the induced water into the main drainage pipe 10. The connecting air pipe 11 maintains the internal air pressure balance. The second drainage branch pipe 12 facilitates the drainage of the water that has drained through the heat exchange tube 7 into the induction chamber. Then, the drain valve 13 is opened to facilitate the drainage of the drained water.
[0029] Specifically, each of the cold water tank 2 has a drain trough 8 located directly below the multiple V-shaped water collecting rings 4. Each of the multiple drain troughs 8 and the drain branch pipe 9 is connected by a connecting groove on the cold water tank 2. The multiple heat exchange pipes 7 and the multiple drain troughs 8 are arranged in a cross pattern. The multiple drain troughs 8 facilitate the collection of water drained from the V-shaped water collecting rings 4 and allow it to flow to the drain branch pipe 9 through the connecting groove. This allows the water drained from the multiple V-shaped water collecting rings 4 to be concentrated and transported to the drain branch pipe 9.
[0030] Specifically, the bottom of the gas-liquid separator 1 has a certain slope towards the drain branch pipe 2 12, which facilitates the transport of the drained water to the drain branch pipe 2 12.
[0031] Specifically, the air-inducing mechanism includes a blower blade 14 disposed in the air-inducing chamber and rotatably connected to the bottom of the gas-liquid separator 1. A drive motor 15 for driving the blower blade 14 to rotate is also fixedly installed at the bottom of the gas-liquid separator 1. Starting the drive motor 15 facilitates the rotation of the blower blade 14, thereby inducing the air entering the air-inducing chamber to rise.
[0032] It should be noted that the terms "one embodiment," "embodiment," "exemplary embodiment," "some embodiments," etc., mentioned in the specification indicate that the described embodiment may include a specific feature, structure, or characteristic, but not every embodiment necessarily includes that specific feature, structure, or characteristic. Furthermore, such phrases do not necessarily refer to the same embodiment. Moreover, when a specific feature, structure, or characteristic is described in connection with an embodiment, implementing such a feature, structure, or characteristic in conjunction with other embodiments, whether explicitly described or not, is within the knowledge scope of those skilled in the art.
[0033] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of this application, and are not intended to limit them. Although this application has been described in detail with reference to the foregoing embodiments, those skilled in the art should understand that modifications can still be made to the technical solutions described in the foregoing embodiments, or equivalent substitutions can be made to some or all of the technical features therein. Such modifications or substitutions do not cause the essence of the corresponding technical solutions to deviate from the scope of the technical solutions of the embodiments of this application.
Claims
1. A gas-liquid separation device in a methanol-to-hydrogen equipment, characterized in that: The system includes a gas-liquid separator (1), the interior of which, from bottom to top, is configured as an induction chamber, a cold water tank (2), a conical water-collecting hood (3) with multiple continuous V-shaped water-collecting rings (4), and a heat exchange chamber. The top of the conical water-collecting hood (3) is sealed and fixedly connected through the top of the gas-liquid separator (1) and connected to a gas guide tank (5) with a delivery pipe. The bottom of the gas-liquid separator (1) is fixedly connected to an air inlet pipe (6) that communicates with the induction chamber. Multiple heat exchange pipes (7) are vertically fixedly connected through the cold water tank (2). The system also includes a drainage mechanism. The induction chamber is equipped with an induction mechanism that induces air upwards.
2. The gas-liquid separation device in the methanol-to-hydrogen equipment according to claim 1, characterized in that: The heat exchange chamber is fixedly connected to the cold water tank (2) via a connecting water pipe (16), and the cold water tank (2), the connecting water pipe (16) and the heat exchange chamber are filled with heat exchange cold water. It also includes a refrigeration mechanism connected to the heat exchange chamber and the cold water tank (2). The refrigeration mechanism includes a water pump (17) and a cooler (18) fixedly installed on the top of the gas-liquid separator (1). The input end of the water pump (17) is fixedly connected to the cold water tank (2) via a water pumping pipe (19), and the output end of the water pump (17) is connected to the input end of the cooler (18). The output end of the cooler (18) is fixedly connected to the top of the gas-liquid separator (1) and connected to the heat exchange chamber.
3. The gas-liquid separation device in the methanol-to-hydrogen equipment according to claim 2, characterized in that: The drainage mechanism includes a drainage main pipe (10) that is fixedly connected to drainage branch pipe one (9) and drainage branch pipe two (12). A drainage valve (13) is installed at the bottom of the drainage main pipe (10). Drainage branch pipe one (9) is connected to the top of the cold water tank (2) on the gas-liquid separator (1). Drainage branch pipe two (12) is connected to the bottom of the induction chamber on the gas-liquid separator (1). A connecting air pipe (11) is also fixedly connected to the drainage main pipe (10) above drainage branch pipe one (9) and fixedly connected to the gas-liquid separator (1).
4. The gas-liquid separation device in the methanol-to-hydrogen equipment according to claim 3, characterized in that: The cold water tank (2) has drainage grooves (8) located directly below the multiple V-shaped water collection rings (4). The multiple drainage grooves (8) and the drainage branch pipe (9) are connected by a groove on the cold water tank (2). The multiple heat exchange pipes (7) and the multiple drainage grooves (8) are arranged in a cross pattern.
5. The gas-liquid separation device in the methanol-to-hydrogen equipment according to claim 4, characterized in that: The bottom of the gas-liquid separator (1) has a certain slope towards the drain branch pipe (12).
6. The gas-liquid separation device in the methanol-to-hydrogen equipment according to claim 5, characterized in that: The air-inducing mechanism includes a blower blade (14) disposed in the air-inducing chamber and rotatably connected to the bottom of the gas-liquid separator (1). The bottom of the gas-liquid separator (1) is also fixedly equipped with a drive motor (15) for driving the blower blade (14) to rotate.