A high-efficiency antistatic ATO dispersion preparation device

Abstract

This utility model relates to the field of ATO dispersion preparation, and more particularly to a high-efficiency antistatic ATO dispersion preparation device, comprising a box, a collection tank, a filter screen, and a base plate. The base plate is located inside the box, and a filter screen is fixed to the upper part of the base plate. The rear half of the filter screen has an upwardly curved design. Both the base plate and the filter screen have through holes on their surfaces. A lead screw is rotatably mounted on one side of the inner wall of the box, and the lead screw is threadedly connected to the filter screen and the base plate. A linear motor is fixed to the upper end of the box, and a groove is provided on one side of the linear motor. A push plate is located inside the box, and a collection tank is fixed to one side of the linear motor. A nozzle is provided at the lower end of the collection tank, penetrating the upper surface of the box. This device utilizes a drip irrigation method to ensure complete reaction and can quickly separate precipitates, solving the problem that existing dispersion preparation devices lack efficient and complete reaction and rapid separation functions.

Description

Technical Field

[0001] This utility model relates to the field of ATO dispersion preparation, and in particular to a high-efficiency antistatic ATO dispersion preparation device. Background Technology

[0002] The preparation of ATO involves a co-precipitation process, which requires pH control. Ammonia (NH3·H2O) or NaOH solution is used as the precipitant and added slowly (e.g., 1-2 mL / min) using a peristaltic pump or dropping funnel. This avoids localized over-alkaliness that could lead to asynchronous precipitation of Sn and Sb. Rapid addition would cause Sn(OH)4 and Sb(OH)3 to precipitate in steps, disrupting the uniformity of doping.

[0003] A search revealed patent publication number CN209985393U, which discloses a device for preparing nano-metal oxide dispersions. The device includes a sealed reaction tower, a crucible for holding the reaction liquid, a microwave heater, a tail gas exhaust mechanism, a powder transport pipe, a sand mill, and a reaction vessel. The sealed reaction tower houses the microwave heater, with the crucible positioned above it. The tail gas exhaust mechanism is connected to the sealed reaction tower, which is connected to the sand mill via the powder transport pipe. The sand mill is connected to the reaction vessel. This invention is energy-saving and environmentally friendly; the entire production process, from powder generation to dispersion output, is sealed, preventing impurities from entering; it employs a composite dispersion method, efficiently preparing nano-metal oxide dispersions with narrow particle size distribution and good repeatability, enabling continuous production and significantly improving production efficiency.

[0004] While existing technologies can achieve certain dispersion preparation effects, they suffer from drawbacks: the lack of efficient and complete reaction and rapid separation functions in existing dispersion preparation devices leads to slow dispersion preparation, incomplete reaction, impurities, and a series of other problems. In view of this, we propose a high-efficiency antistatic ATO dispersion preparation device that solves the above problems. Utility Model Content

[0005] The purpose of this invention is to address the problems existing in the background technology by proposing a highly efficient antistatic ATO dispersion preparation device.

[0006] The technical solution of this utility model is as follows: A high-efficiency antistatic ATO dispersion preparation device, comprising a box, a collection tank, a filter screen, and a bottom plate. The bottom plate is provided inside the box, and a filter screen is fixed at the upper end of the bottom plate. The rear half of the filter screen is designed to be curved upwards. Both the bottom plate and the filter screen have through holes on their surfaces. A lead screw is rotatably installed on one side of the inner wall of the box. The lead screw is threadedly connected to the filter screen and the bottom plate. A linear motor is fixed at the upper end of the box, and a groove is provided on one side of the linear motor. A push plate is provided inside the box, and a collection tank is fixed on one side of the linear motor. A nozzle is provided at the lower end of the collection tank, penetrating the upper surface of the box.

[0007] In use, the base liquid and reaction liquid for ATO dispersion preparation are introduced into the tank and collection tank respectively. The base liquid is continuously stirred under the drive of a rotating motor, and the reaction liquid is dripped from the nozzle at the bottom of the collection tank using a flow valve. After the reaction liquid comes into contact with the base liquid, a precipitate is formed. At regular intervals, a servo motor drives a lead screw to move the bottom plate and filter screen upwards. When the filter screen moves to the bottom of the push plate, a linear motor drives the push plate to push the precipitate out of the outlet for collection, and then proceeds to the next processing step. This device has the function of efficient and complete reaction and separation of precipitate, and can accurately control the specific gravity of reactants by drip irrigation to achieve precise preparation of dispersion.

[0008] Preferably, a bracket is fixed to the lower end of the housing, a base is fixed to the lower end of the bracket, a control panel is fixed to one side of the outer wall of the housing, and a discharge port is provided on one side of the outer wall of the housing. The bracket and the base provide rigid support to ensure the accuracy of the screw lifting and the push plate movement.

[0009] Preferably, a feed pipe is provided on one side of the lower end of the tank, and a discharge pipe is provided on one side of the feed pipe. The feed pipe enables continuous replenishment of the bottom liquid and the reaction liquid, and the discharge pipe, in conjunction with the push plate, quickly discharges the precipitate, reducing manual intervention and improving process efficiency.

[0010] Preferably, the linear motor has an output end on one side and a connecting frame is fixed on one side of the output end. A push plate is fixed at the lower end of the connecting frame. One side of the push plate is designed with an arc shape. The arc edge of the push plate fits the curved surface of the filter screen to ensure that the sediment is completely pushed out and reduce material loss.

[0011] Preferably, a servo motor is provided at the upper end of the housing, the output shaft of the servo motor is fixedly connected to the lower end of the lead screw, and a limiting rod is provided at the four corners inside the housing, the limiting rod being inserted into the bottom plate and the filter screen.

[0012] Preferably, a monitor is embedded in the outer wall of one side of the housing, and a flow valve is provided at the lower end of the nozzle. The monitor displays the acceleration of the reaction droplets and the precipitation state in real time, and the flow valve dynamically adjusts the flow rate according to the feedback to ensure that the stoichiometric ratio of the reaction liquid to the base liquid is accurate and controllable.

[0013] Preferably, a stirring rack is provided at the lower end of the box body, and a rotating motor is fixed at the lower end of the box body. The output shaft of the rotating motor is fixedly connected to the rotation center of the lower end of the stirring rack.

[0014] Compared with existing technologies, the advantages of this utility model are:

[0015] I. This utility model achieves dropwise addition of the reaction solution to the base liquid through the cooperation of the nozzle and the flow valve, simulating the slow dropwise addition operation in the laboratory, avoiding asynchronous precipitation caused by local over-alkaliness, ensuring uniform co-precipitation of Sn and Sb, and meeting the requirements for fine pH control in the co-precipitation method.

[0016] Second, based on the first beneficial effect, the screw drives the lifting and lowering of the filter screen and the bottom plate, combined with the pusher plate to push out the precipitate, realizing continuous operation of reaction and separation, reducing the residence time of particles in the reaction system and inhibiting agglomeration; the through holes of the bottom plate and the filter screen, combined with the stirring rack, promote the uniform flow of the reaction liquid, avoid the accumulation of precipitate, and improve the mass transfer efficiency.

[0017] Of course, any product implementing this utility model does not necessarily need to achieve all of the advantages described above at the same time. Attached Figure Description

[0018] Figure 1 This is a three-dimensional schematic diagram of the present invention;

[0019] Figure 2 This is a rear view schematic diagram of the present invention;

[0020] Figure 3 This is a partial cross-sectional view of the present invention;

[0021] Figure 4 This is a top view of the present invention;

[0022] Figure 5 This is a side view of the present invention;

[0023] Figure 6 For the present utility model Figure 3 Enlarged schematic diagram of structure A in the middle.

[0024] Figure label:

[0025] 1. Housing; 2. Linear motor; 3. Collection tank; 4. Servo motor; 5. Groove; 6. Lead screw; 7. Push plate; 8. Filter screen; 9. Discharge port; 10. Control panel; 11. Base; 12. Bracket; 13. Monitor; 14. Connecting frame; 15. Feed pipe; 16. Discharge pipe; 17. Rotary motor; 18. Stirring rack; 19. Base plate; 20. Limiting rod; 21. Flow valve; 22. Nozzle. Detailed Implementation

[0026] To make the above-mentioned objectives, features and advantages of this utility model more apparent and understandable, the specific embodiments of this utility model will be described in detail below with reference to the accompanying drawings.

[0027] Many specific details are set forth in the following description in order to provide a full understanding of the present invention. However, the present invention may also be implemented in other ways different from those described herein. Those skilled in the art can make similar extensions without departing from the spirit of the present invention. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0028] Secondly, this utility model is described in detail with reference to the schematic diagrams. When describing the embodiments of this utility model, for ease of explanation, the cross-sectional views illustrating the device structure may be partially enlarged, not adhering to the usual scale. Furthermore, the schematic diagrams are merely examples and should not limit the scope of protection of this utility model. In addition, actual manufacturing should include the three-dimensional spatial dimensions of length, width, and depth.

[0029] To make the objectives, technical solutions, and advantages of this utility model clearer, the embodiments of this utility model will be described in further detail below with reference to the accompanying drawings.

[0030] Example 1

[0031] Please see Figures 1-6 As shown, this embodiment is a high-efficiency antistatic ATO dispersion preparation device, including a box 1, a collection tank 3, a filter screen 8 and a bottom plate 19. The bottom plate 19 is provided inside the box 1, and the filter screen 8 is fixed at the upper end of the bottom plate 19. The rear half of the filter screen 8 is designed to be curved upward. Both the bottom plate 19 and the filter screen 8 have through holes on their surfaces. A lead screw 6 is rotatably installed on one side of the inner wall of the box 1. The lead screw 6 is threadedly connected to the filter screen 8 and the bottom plate 19. A linear motor 2 is fixed at the upper end of the box 1. A groove 5 is provided on one side of the linear motor 2. A push plate 7 is provided inside the box 1. The collection tank 3 is fixed on one side of the linear motor 2. A nozzle 22 is provided at the lower end of the collection tank 3 through the upper surface of the box 1.

[0032] When using this device, the base liquid and reaction liquid used in the preparation of ATO dispersion can be introduced into the tank 1 and the collection tank 3, respectively. The base liquid is continuously stirred under the drive of the rotating motor 17. The flow valve 21 controls the nozzle 22 at the lower end of the collection tank 3 to drip the reaction liquid, so that the reaction liquid reacts with the base liquid to form a precipitate. At regular intervals, the servo motor 4 drives the lead screw 6 to move the bottom plate 19 and the filter screen 8 upward. When the filter screen 8 moves to the lower end of the push plate 7, the linear motor 2 drives the push plate 7 to push the precipitate out of the outlet 9 for collection, and then proceed to the next processing step. This device has the function of efficient and complete reaction separation of precipitate. It can use drip irrigation to accurately control the specific gravity of the reactants and achieve precise preparation of the dispersion.

[0033] Example 2

[0034] Please see Figures 1-6 As shown, this embodiment, based on embodiment 1, further includes: a bracket 12 fixed to the lower end of the box 1, a base 11 fixed to the lower end of the bracket 12, a control panel 10 fixed to one side of the outer wall of the box 1, and a discharge port 9 provided on one side of the outer wall of the box 1. The bracket 12 and the base 11 provide rigid support to ensure the accuracy of the lifting of the screw 6 and the movement of the push plate 7, and to avoid secondary agglomeration of particles caused by vibration. The control panel 10 integrates pH monitoring, temperature adjustment and motor speed parameters to realize digital management of reaction conditions.

[0035] A feed pipe 15 is provided on one side of the lower end of the tank 1, and a discharge pipe 16 is provided on one side of the feed pipe 15. The feed pipe 15 enables continuous replenishment of the bottom liquid and the reaction liquid, and the discharge pipe 16, together with the push plate 7, quickly discharges the precipitate, reducing manual intervention and improving process efficiency.

[0036] The linear motor 2 has an output end on one side and a connecting frame 14 is fixed on the output end. A push plate 7 is fixed at the lower end of the connecting frame 14. One side of the push plate 7 is designed with an arc shape. The arc edge of the push plate 7 fits the curved surface of the filter screen 8 to ensure that the sediment is completely pushed out and reduce material loss.

[0037] A servo motor 4 is provided at the upper end of the housing 1. The output shaft of the servo motor 4 is fixedly connected to the lower end of the lead screw 6. Limiting rods 20 are provided at the four corners inside the housing 1. The limiting rods 20 are inserted into the bottom plate 19 and the filter screen 8. The servo motor 4 constrains the movement trajectory of the filter screen 8 through the limiting rods 20 to ensure that the lifting process is stable and to avoid uneven distribution of sediment caused by the tilting of the filter screen 8.

[0038] A monitor 13 is embedded in the outer wall of one side of the housing 1, and a flow valve 21 is provided at the lower end of the nozzle 22. The monitor 13 displays the acceleration of the reaction liquid droplets and the precipitation status in real time, and the flow valve 21 dynamically adjusts the flow rate according to the feedback to ensure that the stoichiometric ratio of the reaction liquid to the base liquid is accurate and controllable.

[0039] A stirring rack 18 is provided at the lower end of the interior of the housing 1. A rotating motor 17 is fixed at the lower end of the housing 1. The output shaft of the rotating motor 17 is fixedly connected to the rotation center of the lower end of the stirring rack 18. The stirring rack 18 generates turbulence under the drive of the rotating motor 17, forcing the reaction liquid and precipitant to fully contact each other, avoiding particle coarsening caused by excessively high local concentrations. Finally, it should be noted that the above description is only a preferred embodiment of this utility model and is not intended to limit this utility model. Although this utility model has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments or make equivalent substitutions for some of the technical features. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of this utility model should be included within the protection scope of this utility model.

Claims

1. A high-efficiency antistatic ATO dispersion preparation device, comprising a housing (1), a collection tank (3), a filter screen (8), and a bottom plate (19), characterized in that: The box (1) is provided with a bottom plate (19) inside. A filter screen (8) is fixed at the upper end of the bottom plate (19). The rear half of the filter screen (8) is designed to be curved upward. Both the bottom plate (19) and the filter screen (8) have through holes on their surfaces. A lead screw (6) is rotatably installed on one side of the inner wall of the box (1). The lead screw (6) is threadedly connected to the filter screen (8) and the bottom plate (19). A linear motor (2) is fixed at the upper end of the box (1). A groove (5) is provided on one side of the linear motor (2). A push plate (7) is provided inside the box (1). A collection groove (3) is fixed on one side of the linear motor (2). A nozzle (22) is provided at the lower end of the collection groove (3) through the upper surface of the box (1).

2. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 1, characterized in that: The lower end of the box (1) is fixed with a bracket (12), the lower end of the bracket (12) is fixed with a base (11), a control panel (10) is fixed on one side of the outer wall of the box (1), and a discharge port (9) is provided on one side of the outer wall of the box (1).

3. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 2, characterized in that: The lower end of the box (1) is provided with a feed pipe (15) and the feed pipe (15) is provided with a discharge pipe (16) on one side.

4. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 1, characterized in that: The linear motor (2) has an output end on one side and a connecting frame (14) is fixed on one side of the output end. A push plate (7) is fixed at the lower end of the connecting frame (14). One side of the push plate (7) is designed in an arc shape.

5. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 1, characterized in that: The upper end of the housing (1) is provided with a servo motor (4), the output shaft of the servo motor (4) is fixedly connected to the lower end of the lead screw (6), and the four corners inside the housing (1) are provided with limiting rods (20), which are inserted into the bottom plate (19) and the filter screen (8).

6. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 1, characterized in that: A monitor (13) is embedded in the outer wall of one side of the housing (1), and a flow valve (21) is provided at the lower end of the nozzle (22).

7. The apparatus for preparing a high-efficiency antistatic ATO dispersion according to claim 1, characterized in that: The lower end of the box (1) is provided with a stirring rack (18), and a rotating motor (17) is fixed at the lower end of the box (1). The output shaft of the rotating motor (17) is fixedly connected to the rotation center of the lower end of the stirring rack (18).

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