A hexachloroethane reaction kettle convenient to clean
By installing a water distribution plate and bearing sleeve on the lower surface of the hexachloroethane reactor lid, the problem of poor stability of the cleaning pipeline in the prior art is solved, realizing convenient and efficient reactor cleaning and improving the stability of the reactor.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- NANTONG DONGGANG DRAINAGE CO LTD
- Filing Date
- 2025-07-10
- Publication Date
- 2026-05-29
AI Technical Summary
The existing cleaning pipeline of the hexachloroethane reactor needs to be fixed to the inner wall of the reactor by fasteners, which results in poor stability and short service life. In addition, screw holes need to be made in the inner wall of the reactor, which increases the processing difficulty.
A water distribution plate is installed on the lower surface of the vessel lid. The water distribution plate has an annular groove and side and bottom water outlet holes, which are connected by bolts. It is used to rinse the inner wall of the vessel and the stirring paddle. A bearing sleeve is installed at the center of the water distribution plate to improve the stability of the stirring shaft.
It improves the ease of cleaning and cleaning effect, enhances the stability of the vessel body, reduces the difficulty of processing the vessel body, and eliminates the need to drill holes in the inner wall of the vessel body.
Smart Images
Figure CN224293274U_ABST
Abstract
Description
Technical Field
[0001] This utility model relates to the field of reaction vessel technology, specifically to a hexachloroethane reaction vessel that is easy to clean. Background Technology
[0002] After dehydration, tetrachloroethane is reacted at 90-100℃. When the reaction solution changes from turbid to clear and crystals appear, chlorination is stopped. The temperature is then raised to 120℃ to remove residual chlorine. After discharge, the material undergoes hot water washing, neutralization, centrifugal filtration, and finally drying and pulverizing to obtain the final product.
[0003] Tetrachloroethane and chlorine typically react in a vacuum reactor. After the reaction is complete and the material is discharged, the inside of the reactor usually needs to be cleaned. Currently, most methods involve manual rinsing through the cleaning port. Some methods use cleaning pipelines installed inside the reactor. However, existing cleaning pipelines require fixing to the inner wall of the reactor using fasteners. To install these fasteners, screw holes need to be drilled in the inner wall of the reactor. Furthermore, the pipelines have poor stability and a short service life. Therefore, an improved technology is urgently needed to solve this problem in the existing technology. Utility Model Content
[0004] The purpose of this invention is to provide a hexachloroethane reactor that is easy to clean, so as to solve the problems mentioned in the background art.
[0005] To achieve the above objectives, this utility model provides the following technical solution: a hexachloroethane reactor that is easy to clean, comprising a reactor body, a reactor cover, and a water distribution plate;
[0006] The upper surface of the vessel body is provided with a vessel lid, and a motor is provided at the center of the upper surface of the vessel lid via a motor base. The output shaft of the motor is connected to the top of the stirring shaft via a coupling. A stirring paddle is provided at the lower end of the stirring shaft. The stirring paddle is rotatably disposed inside the vessel body. A discharge port is provided at the bottom of the vessel body. The vessel body is wrapped with a jacket.
[0007] The water distribution plate is bolted to the lower surface of the vessel lid. An annular groove is formed on the upper surface of the water distribution plate. Several side water outlets are formed on the side wall of the water distribution plate. Several bottom water outlets are formed on the water distribution plate located in the annular groove along the axial direction. A water inlet is provided on the upper surface of the vessel lid. The water inlet is connected to the annular groove of the water distribution plate. A central hole is formed at the center of the water distribution plate. A bearing sleeve is provided at the central hole of the water distribution plate. The stirring shaft passes through the bearing sleeve and cooperates with the bearing sleeve. A sleeve is provided on the water distribution plate located in the annular groove along the axial direction. A feed inlet is also provided through the vessel lid. The feed inlet passes through the sleeve.
[0008] Preferably, the present invention provides a hexachloroethane reactor that is easy to clean, wherein a chlorine gas inlet is provided at the lower part of the side wall of the reactor body, the chlorine gas inlet is inserted through the jacket and communicates with the interior of the reactor body, and a chlorine gas outlet is provided at the upper part of the side wall of the reactor body.
[0009] Preferably, the present invention provides a hexachloroethane reactor that is easy to clean, wherein the side wall of the reactor body is provided with a thermometer port and a pressure gauge port.
[0010] Preferably, the present invention provides a hexachloroethane reactor that is easy to clean, wherein the lower part of the jacket is provided with a heat exchange medium inlet, the upper part of the jacket is provided with a heat exchange medium outlet, and a number of support seats are provided around the jacket.
[0011] Compared with the prior art, the beneficial effects of this utility model are:
[0012] (1) A water distribution plate is provided on the lower surface of the vessel lid. The water distribution plate has an annular groove. The water distribution plate washes the inner wall of the vessel and the stirring paddle through the side water outlet and the bottom water outlet, which greatly improves the convenience and cleaning effect. In addition, it is connected to the vessel lid by bolts, which is more stable than the pipe. There is no need to make holes in the inner wall of the vessel, which reduces the processing difficulty of the reaction vessel.
[0013] (2) A bearing sleeve is provided at the center of the water distribution plate, which improves the stability of the stirring shaft and the stirring paddle, thereby improving the stability of the reactor during operation. Attached Figure Description
[0014] Figure 1 This is a schematic diagram of the structure of this utility model;
[0015] Figure 2 This is a schematic diagram of the cross-sectional structure of the water distribution plate;
[0016] Figure 3 This is a top view of the water distribution plate structure.
[0017] In the diagram: 1. Vessel body; 2. Vessel cover; 3. Motor; 4. Stirring shaft; 5. Stirring paddle; 6. Discharge port; 7. Jacket; 8. Water distribution plate; 9. Annular groove; 10. Side water outlet; 11. Bottom water outlet; 12. Water inlet; 13. Bearing sleeve; 14. Sleeve; 15. Feed inlet; 16. Chlorine gas inlet; 17. Chlorine gas outlet; 18. Thermometer port; 19. Pressure gauge port; 20. Heat exchange medium inlet; 21. Heat exchange medium outlet; 22. Support base. Detailed Implementation
[0018] The technical solution of this utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of this utility model, and not all embodiments. Based on the embodiments of this utility model, all other embodiments obtained by those skilled in the art without creative effort are within the protection scope of this utility model.
[0019] It should be noted that in the description of this utility model, the terms "inner", "outer", "upper", "lower", "both sides", "one end", "the other end", "left", "right", etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this utility model.
[0020] Please see Figure 1-3 This utility model provides a technical solution: a hexachloroethane reactor that is easy to clean, including a reactor body 1, a reactor cover 2, and a water distribution plate 8;
[0021] A lid 2 is provided on the upper surface of the vessel body 1. A motor 3 is mounted on the center of the upper surface of the lid 2 via a motor mount. The output shaft of the motor 3 is connected to the top of a stirring shaft 4 via a coupling. A stirring paddle 5 is provided at the lower end of the stirring shaft 4 and is rotatably mounted inside the vessel body 1. A discharge port 6 is provided at the bottom of the vessel body 1. A jacket 7 is provided around the vessel body 1. A heat exchange medium inlet 20 is provided at the lower part of the jacket 7, and a heat exchange medium outlet 21 is provided at the upper part of the jacket 7. Several support seats 22 are also provided around the jacket 7. The heat exchange medium (such as hot gas or hot oil) enters the jacket 7 through the heat exchange medium inlet 20 and the heat exchange medium outlet 21, thereby achieving... The heating inside the reactor body 1 is achieved by supporting and fixing the reactor body through the support base 22. A chlorine gas inlet 16 is provided at the lower part of the side wall of the reactor body 1. The chlorine gas inlet 16 passes through the jacket 7 and is connected to the inside of the reactor body 1. A chlorine gas outlet 17 is provided at the upper part of the side wall of the reactor body 1. Chlorine gas enters the reactor body 1 through the chlorine gas inlet 16 to react with tetrachloroethylene, thereby generating hexachloroethane crystals and solution. The residual chlorine is discharged through the chlorine gas outlet 17. A thermometer port 18 and a pressure gauge port 19 are provided on the side wall of the reactor body 1 to install a thermometer and a pressure gauge respectively, thereby realizing the monitoring of the temperature and pressure inside the reactor body 1.
[0022] The water distribution plate 8 is bolted to the lower surface of the vessel cover 2. The upper surface of the water distribution plate 8 has an annular groove 9. The side wall of the water distribution plate 8 has several side water outlet holes 10. The water distribution plate 8 is located at the annular groove 9 and has several bottom water outlet holes 11 along the axial direction. The upper surface of the vessel cover 2 is provided with a water inlet 12, which is connected to the annular groove 9 of the water distribution plate 8. A central hole is provided at the center of the water distribution plate 8. A bearing sleeve 13 is provided at the central hole of the water distribution plate 8. The stirring shaft 4 passes through the bearing sleeve 13 and cooperates with the bearing sleeve 13. The water distribution plate 8 is located in the annular groove 9 and has a sleeve 14 along the axial direction. The vessel cover 2 is also provided with a feed inlet 15, which passes through the sleeve 14.
[0023] Installation method and operating principle: First, insert the bearing sleeve 13 into the center plate of the water distribution plate 8 and fasten it to the water distribution plate 8 with bolts. Then, connect the water distribution plate 8 to the lower surface of the vessel cover 2 with bolts, and insert the sleeve 14 into the water inlet 12. Install the motor 3 on the upper surface of the motor base, pass the stirring shaft 4 with the stirring paddle 5 through the bearing sleeve 13 and connect it to the output shaft of the motor 3 through the coupling. Next, lift the vessel cover 2, place the stirring paddle 5 into the vessel body 1, and install the vessel cover 2 on the upper surface of the vessel body 1 with bolts to complete the installation. During operation, tetrachloroethylene enters the reactor body 1 through the feed inlet 15. The motor 3 is started, and it drives the stirring paddle 5 to rotate via the stirring shaft 4. At the same time, chlorine gas enters the reactor body 1 through the chlorine gas inlet 16 (connected to an external pipeline) and reacts with the tetrachloroethylene. Hot gas or hot oil enters the jacket 7 through the heat exchange medium inlet 20 and exchanges heat with the interior of the reactor body 1. At an environment of 90–120°C, the reaction liquid changes from turbid to clear and crystals appear. Chlorine flow is stopped, and excess chlorine gas is discharged through the chlorine gas outlet 17, producing hexachloroethane. After being discharged through the discharge outlet 6, it undergoes washing, neutralization, centrifugal filtration, and other processes to obtain dried hexachloroethane. For the next use, external water enters the annular groove 9 of the water distribution plate 8 through the water inlet 12. The water flows from the side outlet 10 of the water distribution plate 8 towards the side wall and then through the bottom outlet 11 towards the stirring paddle 5, thus completing the rinsing of the interior of the reactor body 1. This utility model has a reasonable structure. A water distribution plate 8 is provided on the lower surface of the vessel cover 2. The water distribution plate 8 has an annular groove 9. The water distribution plate 8 washes the inner wall of the vessel body 1 and the stirring paddle 5 through the side water outlet 10 and the bottom water outlet 11, which greatly improves the convenience and cleaning effect. In addition, it is connected to the vessel cover 2 by bolts, which is more stable than pipes. There is no need to make holes in the inner wall of the vessel, reducing the processing difficulty of the reaction vessel. At the same time, a bearing sleeve 13 is provided at the center of the water distribution plate 8, which improves the stability of the stirring shaft 4 and the stirring paddle 5, thereby improving the stability of the reaction vessel during operation.
[0024] Any aspects of this utility model not described in detail are well-known technologies to those skilled in the art.
[0025] Finally, it should be noted that the above specific embodiments are only used to illustrate the technical solution of this utility model and are not intended to limit it. Although this utility model has been described in detail with reference to the embodiments, those skilled in the art should understand that modifications and equivalent substitutions can be made to the technical solution of this utility model without departing from the spirit and scope of the technical solution of this utility model, and all such modifications and substitutions should be covered within the scope of the claims of this utility model.
Claims
1. A hexachloroethane reactor that is easy to clean, characterized in that: Includes the vessel body (1), the vessel lid (2), and the water distribution plate (8); The upper surface of the vessel body (1) is provided with a vessel cover (2). A motor (3) is provided at the center of the upper surface of the vessel cover (2) via a motor base. The output shaft of the motor (3) is connected to the top of the stirring shaft (4) via a coupling. A stirring paddle (5) is provided at the lower end of the stirring shaft (4). The stirring paddle (5) is rotatably located inside the vessel body (1). A discharge port (6) is provided at the bottom of the vessel body (1). A jacket (7) is wrapped around the outside of the vessel body (1). The water distribution plate (8) is bolted to the lower surface of the kettle cover (2). The upper surface of the water distribution plate (8) is provided with an annular groove (9). The side wall of the water distribution plate (8) is provided with several side water outlet holes (10). The water distribution plate (8) is located at the annular groove (9) and is provided with several bottom water outlet holes (11) along the axial direction. The upper surface of the kettle cover (2) is provided with a water inlet (12). The water inlet (12) is connected to the annular groove (9) of the water distribution plate (8). The center of the water distribution plate (8) is provided with a central hole. The center hole of the water distribution plate (8) is provided with a bearing sleeve (13). The stirring shaft (4) passes through the bearing sleeve (13) and cooperates with the bearing sleeve (13). The water distribution plate (8) is located in the annular groove (9) and is provided with a sleeve (14) along the axial direction. The kettle cover (2) is also provided with a feed inlet (15). The feed inlet (15) passes through the sleeve (14).
2. The hexachloroethane reactor that is easy to clean according to claim 1, characterized in that: A chlorine gas inlet (16) is provided on the lower part of the side wall of the vessel body (1). The chlorine gas inlet (16) passes through the jacket (7) and communicates with the interior of the vessel body (1). A chlorine gas outlet (17) is provided on the upper part of the side wall of the vessel body (1).
3. The hexachloroethane reactor that is easy to clean according to claim 1, characterized in that: The side wall of the vessel body (1) is provided with a thermometer port (18) and a pressure gauge port (19).
4. The hexachloroethane reactor that is easy to clean according to claim 1, characterized in that: The jacket (7) is provided with a heat exchange medium inlet (20) at the lower part and a heat exchange medium outlet (21) at the upper part. Several support seats (22) are also provided around the jacket (7).