Zirconia-based all-ceramic false tooth and preparation method thereof

By using calcium magnesium silicon ceramic powder in the core-shell structure of zirconia-based dentures to co-sinter with zirconia-based dentures, the problems of poor permeability of zirconia ceramic dentures and insufficient strength of porcelain powder are solved, achieving high strength and With improved aesthetics, it is suitable as a dental restorative material.

CN114368966AActive Publication Date: 2022-04-19ZHEJIANG DANSDEN BIOMATERIALS CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
ZHEJIANG DANSDEN BIOMATERIALS CO LTD
Filing Date
2021-03-26
Publication Date
2022-04-19

AI Technical Summary

Technical Problem

Existing zirconia ceramic dentures have poor permeability after sintering and are dull under natural light. The strength of the porcelain powder is insufficient, making it difficult to meet the needs of aesthetics and mechanical properties.

Method used

Zirconia-based all-ceramic dentures with core-shell structure are added by adding ZrO2, Y2O3, Al2O3, Fe2O3, Er2O3, MnO2 to the core layer of the zirconia-based denture, and using CaCO3, SiO2, MgO, Fe2O3, Er2O3 and MnO2 synthesize calcium magnesium silicon ceramic powder to form calcium magnesium silicon ceramic slurry and sinter it together with zirconia-based dentures. The high bending strength and biocompatibility of calcium magnesium silicon ceramic are used to improve the overall mechanical properties, and through Fe2O3, Er2O3 and MnO2 adjust the color.

Benefits of technology

It achieves the high strength and good jade texture of zirconia-based dentures, enhances the aesthetics, and forms a perfect combination through the melting, penetration and coating of calcium-magnesium-silicon ceramics, improving the overall mechanical properties and biocompatibility of zirconia-based dentures. .

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Abstract

The invention relates to a zirconia-based all-ceramic false tooth and a preparation method thereof. A core layer of the zirconia-based all-ceramic false tooth is prepared from the following components in parts by mass: 90 to 94 parts of ZrO2, 5 to 9 parts of Y2O3, 0.1 to 0.5 part of Al2O3, 0.01 to 0.5 part of Fe2O3, 0.01 to 0.5 part of Er2O3 and 0 to 0.2 part of MnO2, and a shell layer of the zirconia-based all-ceramic false tooth is prepared from the following components in parts by mass: 24.5 to 49.5 parts of CaCO3, 45 to 50 parts of SiO2, 0 to 25 parts of MgO, 0.01 to 0.5 part of Fe2O3, 0.01 to 0.5 part of Er2O3 and 0 to 0.2 part of MnO2. The preparation process comprises the following steps: performing dry pressing and isostatic pressing on raw materials of the core layer, presintering, and carving to obtain a zirconia-based false tooth biscuit; meanwhile, calcining raw materials of a shell layer, then adding deionized water, a dispersing agent and an adhesive, and carrying out ball milling and mixing to obtain calcium-magnesium-silicon-based ceramic slurry; and coating the calcium-magnesium-silicon-based ceramic slurry on the surface of the zirconium oxide-based false tooth biscuit, and sintering to obtain the zirconium oxide-based all-ceramic false tooth provided by the invention. The zirconia-based all-ceramic false tooth has good jade texture and is closer to the natural color of natural teeth.
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Citation Information

Patent Citations

  • CN100370963C

  • CN102302799A

  • CN102357260A

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  • CN103641472A

Cited By

  • CN114790116A

  • CN114790116B

  • CN115745599A

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  • CN115894016A