A powder preparation device of titanium diboride for lithium battery preparation
By using a ball screw nut pair driven by a servo motor and a contact assembly with the reactor wall, the problems of low mixing efficiency and adhesion in the preparation of titanium diboride powder were solved, achieving efficient mixing and increased yield, while reducing energy consumption and preparation costs.
Patent Information
- Application Number
- CN202310840954.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2023-07-10
- Publication Date
- 2025-11-18
- Estimated Expiration
- 2043-07-10
AI Technical Summary
In the existing technology for preparing titanium diboride powder, titanium dioxide tends to adhere to the surface of the reaction vessel, resulting in low mixing efficiency, which affects the yield and purity, and the stirring method is time-consuming.
The apparatus includes a preparation container, a servo motor, a ball screw and nut assembly, a vessel wall contact assembly, and a dispersion assembly. The servo motor drives the ball screw and nut assembly to move the vessel wall contact assembly and the dispersion assembly, thereby achieving vessel wall cleaning and material dispersion. Combined with a vibration assembly, the mixing is accelerated.
This improved the mixing efficiency of titanium dioxide and boron, reduced the material adhering to the reactor wall, increased yield and product quality, and reduced energy consumption and preparation costs.
Smart Images

Figure CN116850926B_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the field of titanium diboride powder preparation technology, specifically to a titanium diboride powder preparation apparatus for lithium battery manufacturing. Background Technology
[0002] In existing technologies, titanium diboride is often prepared by the borothermal method. Using titanium dioxide and elemental boron as raw materials under high temperature and vacuum catalysis, titanium diboride powder can be prepared at a high temperature and vacuum environment not exceeding 1100 degrees Celsius. This is a common preparation method for titanium diboride powder required for lithium battery manufacturing.
[0003] Since the preparation of titanium diboride via the borothermal method is mostly carried out in a reactor, and the purity of the selected titanium dioxide powder is required to be higher than 99%, titanium diboride tends to adhere to the reactor wall during the preparation process. In fact, this part of the titanium dioxide raw material does not participate in the preparation of titanium diboride, which has a certain impact on the yield of titanium diboride. Furthermore, the existing raw material mixing methods mainly use rod-shaped or fan-shaped stirring to mix the materials. During stirring, different materials need to be turned over as a whole or on the surface, which requires a lot of time. This type of stirring method cannot achieve rapid mixing between titanium dioxide and elemental boron, and the mixing process is inefficient. Therefore, we propose a powder preparation device for titanium diboride for lithium battery manufacturing. Summary of the Invention
[0004] The purpose of this invention is to provide a powder preparation apparatus for titanium diboride for lithium battery manufacturing, so as to solve the problems mentioned in the background art.
[0005] To achieve the above objectives, the present invention provides the following technical solution: a powder preparation device for titanium diboride used in lithium battery manufacturing, comprising a preparation container, a controller, a gas pressure gauge and a servo motor, wherein the output end of the servo motor passes through the preparation container and is fixedly connected to a ball screw and nut assembly, a container wall contact component is provided on the outside of the ball screw and nut assembly, and a dispersion component is provided at the end of the ball screw and nut assembly away from the servo motor, wherein the ball screw and nut assembly comprises a screw and ball nuts;
[0006] The dispersion assembly includes a stirring and dispersion seat, a first dispersion blade, a second dispersion blade, and a vibration assembly. The stirring and dispersion seat is fixedly connected to the end of the lead screw away from the connector, and the first dispersion blade and the second dispersion blade are both fixedly connected to the outside of the stirring and dispersion seat.
[0007] Preferably, the vessel wall contact assembly includes a movable sleeve, a fixed sleeve, and a contact brush. One end of the movable sleeve is movably connected to the fixed sleeve via a spring, and the other end is movably connected to the contact brush. The side of the contact brush away from the movable sleeve is movably connected to the inner wall of the preparation container. An infrared receiver is fixedly connected inside the fixed sleeve. An infrared transmitter and a wireless transmission module are fixedly connected inside the contact brush. Both the infrared receiver and the wireless transmission module are electrically connected to the infrared transmitter. The wireless transmission module is electrically connected to the controller. The gas pressure gauge is movably connected to the preparation container.
[0008] Preferably, the movable sleeve has a first accommodating cavity for accommodating the spring, and the fixed sleeve has a second accommodating cavity for accommodating the movable sleeve and the spring. Both accommodating cavities have bolt holes on one side, and each bolt hole is screwed with a retaining bolt. One end of the retaining bolt passes through the bolt hole and engages with the spring.
[0009] Preferably, the contact brush has a slot for accommodating an infrared transmitter and a wireless transmission module, a card plate is expanded to one side of the slot, and tempered glass is fixedly connected inside the card plate.
[0010] Preferably, one end of the lead screw is fixedly connected to the output end of the servo motor via a connector, the other end of the lead screw is fixedly connected to the dispersion component, and the ball nut is disposed on the outside of the lead screw and movably connected to the lead screw.
[0011] Preferably, the oscillation assembly includes a first mesh plate, a second mesh plate, and a sleeve. The middle part of the sleeve is rotatably connected to the corresponding lead screw. The second mesh plate is provided with a plurality of insert rods. A first trapezoidal platform and a second trapezoidal platform are respectively provided on the two ends of the sleeve. The highest and lowest points of the first and second trapezoidal platforms are the same height and the same shape. A limit plate is provided on the outer wall of the sleeve. The limit plates are respectively provided on the outer walls of the two ends of the sleeve. A partition is provided in the middle of the sleeve. The diameter of the partition is the same as the diameter of the limit plates on both sides. Inner plates are respectively provided on the sleeve on both sides of the partition. The diameter of the inner plates is larger than the diameter of the partition. Connecting rods are provided on the side edges of the inner plates on both sides of the partition. A top plate is provided, the top plate having the same diameter as the corresponding inner plate. A through-hole is opened in the middle of the top plate on each side, and a lead screw is rotatably connected in the through-hole. A rotating port is opened in the middle of the sleeve corresponding to the lead screw, and the lead screw is inserted into the corresponding rotating port. A first return spring and a second return spring are respectively sleeved on the sleeve between the limiting plate and the inner plate on each side of the sleeve. The first return spring and the second return spring are respectively located between the corresponding inner plate and the limiting plate. An inner rod is provided on each side of the top plate, the inner rod facing the corresponding first trapezoidal platform and the second trapezoidal platform. A ball head is provided on the output end of each side of the inner rod, and each ball head is slidably connected to the edge of the corresponding first trapezoidal platform and the second trapezoidal platform. The first mesh plate is set on the outer connecting rod of the corresponding first trapezoidal platform, and the second mesh plate is set on the outer connecting rod of the second trapezoidal platform.
[0012] Preferably, the preparation container includes a vessel body, a vessel lid movably connected to the vessel body, and a base disposed at the bottom of the vessel body. A vacuum port and a discharge port are fixedly connected to the outside of the vessel body, and the servo motor is fixedly connected to the vessel lid.
[0013] Preferably, a support frame is fixedly connected to the outside of the vessel body, the gas pressure gauge is movably connected to the support frame, and the output end of the gas pressure gauge passes through the vessel body and communicates with the interior of the vessel body.
[0014] Preferably, the vessel wall contact components are arranged in a circular array with the center line of the lead screw as the baseline, and are evenly distributed on the outside of the ball nut. There are a total of six sets of vessel wall contact components, and the included angle between any two adjacent vessel wall contact components is always 60°.
[0015] Preferably, a lifting lug is fixedly connected to one side of both the vessel body and the vessel lid, and the lifting lugs are evenly distributed on the outer side of the vessel body and the vessel lid. A screw head hole is opened inside the contact brush, and a screw head is fixedly connected to the end of the movable sleeve away from the fixed sleeve. The screw head is adapted to the screw head hole.
[0016] Compared with the prior art, the beneficial effects of the present invention are:
[0017] 1. This invention utilizes a vibrating assembly with a sleeve mounted on a lead screw. The sleeve rotates with the lead screw. The sleeve has a partition and a limiting plate. Inner plates are positioned between the partition and the limiting plates on both sides of the sleeve, allowing the inner plates to slide on the sleeve. A first return spring and a second return spring are positioned between each inner plate and its corresponding limiting plate. The return springs push the inner plates towards the partition positions. Each inner plate is connected to a top plate via a connecting rod. The top plate has a ball head, and a first trapezoidal platform is positioned on the sleeve corresponding to the ball head. The second trapezoidal platform, when rotated, can push the top plates on both sides to move vertically, thereby driving the first and second mesh plates to move vertically. When the first and second mesh plates are close together, the insertion rods can be inserted; when they are far apart, the rotation of the sleeve can cause the first and second mesh plates to vibrate, thus making the titanium dioxide and boron on the first and second mesh plates more loose. Through the above settings, titanium dioxide and boron can be mixed more easily and the mixing between titanium dioxide and boron can be accelerated.
[0018] 2. In this invention, the spring can buffer the contact brush during the movement of the fixed sleeve and the movable sleeve, and reduce the contact impact force between the contact brush and the vessel body caused by material agglomeration on the side wall of the vessel body. This provides a certain degree of protection for both the contact brush and the vessel body. Furthermore, if the spring is damaged due to excessive buffering, it can be quickly replaced by disassembling the retaining bolt and the bolt hole. The operation is simple and the spring replacement is quick and convenient. Attached Figure Description
[0019] Figure 1 This is a schematic diagram of the overall structure of the present invention;
[0020] Figure 2 This is a schematic diagram of the internal structure of the container prepared according to the present invention;
[0021] Figure 3 This is a schematic diagram of the structure of the vessel wall contact assembly of the present invention;
[0022] Figure 4 This is a cross-sectional view of the movable sleeve and the fixed sleeve of the present invention;
[0023] Figure 5 This is a schematic diagram of the contact brush structure of the present invention;
[0024] Figure 6 This is a schematic diagram of the discharge port structure of the present invention;
[0025] Figure 7 A top view of the internal structure of the container was prepared for this invention;
[0026] Figure 8This is a schematic diagram of the structure of the oscillation component of the present invention;
[0027] Figure 9 This is a partially enlarged structural diagram of the oscillation component of the present invention.
[0028] In the diagram: 1. Preparation container; 11. Kettle body; 12. Kettle lid; 13. Vacuum port; 14. Discharge port; 15. Support frame; 16. Lifting lug; 17. Base; 2. Controller; 3. Gas pressure gauge; 4. Servo motor; 41. Connector; 5. Ball screw and nut pair; 51. Screw; 52. Ball nut; 6. Kettle wall contact assembly; 7. Dispersion assembly; 71. Stirring and dispersing seat; 72. Dispersion blade one; 73. Dispersion blade two; 74. Vibration assembly; 741. First mesh plate; 742. Second mesh plate; 7421. Insert rod; 743. Connecting rod; 7431. Through port; 7432. Top plate; 744. Sleeve; 744 1. Limiting plate; 7442. First trapezoidal platform; 7443. Second trapezoidal platform; 7444. Rotating port; 745. First return spring; 746. Second return spring; 747. Inner rod; 7471. Ball head; 748. Partition plate; 749. Inner plate; 8. Movable sleeve; 81. First accommodating cavity; 82. Screw head; 9. Fixed sleeve; 91. Second accommodating cavity; 10. Contact brush; 101. Screw head hole; 102. Slot; 103. Card plate; 104. Tempered glass; 110. Spring; 120. Snap ring bolt; 130. Bolt hole; 140. Infrared receiver; 150. Infrared transmitter; 160. Wireless transmission module. Detailed Implementation
[0029] The technical solutions of the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present invention, and not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of the present invention.
[0030] Please see Figure 1-9This invention provides a technical solution: a powder preparation device for titanium diboride used in lithium battery manufacturing, comprising a preparation container 1, a controller 2, a gas pressure gauge 3, and a servo motor 4. The output end of the servo motor 4 passes through the preparation container 1 and is fixedly connected to a ball screw nut assembly 5. A container wall contact assembly 6 is provided outside the ball screw nut assembly 5. A dispersion assembly 7 is provided at the end of the ball screw nut assembly 5 away from the servo motor 4. The container wall contact assembly 6 includes a movable sleeve 8, a fixed sleeve 9, and a contact brush 10. One end of the movable sleeve 8 is connected by a spring 11. One end of the sleeve is movably connected to the fixed sleeve 9, and the other end is movably connected to the contact brush 10. The side of the contact brush 10 away from the movable sleeve 8 is movably connected to the inner wall of the preparation container 1. An infrared receiver 140 is fixedly connected inside the fixed sleeve 9. An infrared transmitter 150 and a wireless transmission module 160 are fixedly connected inside the contact brush 10. The infrared receiver 140 and the wireless transmission module 160 are both electrically connected to the infrared transmitter 150. The wireless transmission module 160 is electrically connected to the controller 2. The gas pressure gauge 3 is movably connected to the preparation container 1.
[0031] The servo motor 4 drives the ball screw nut assembly 5 to rotate. On one hand, the screw 51 drives the ball nut 52 to move along the axial direction of the screw 51. On the other hand, the rotation of the screw 51 drives the dispersion component 7 to rotate. During the forward and reverse motion of the output end of the servo motor 4, the ball nut 52 drives the vessel wall contact component 6 to move along the axial direction of the screw 51. This causes the contact brush 10 inside the vessel wall contact component 6 to sweep off the material adhering to the inside of the vessel 11 after contacting the inner wall of the vessel 11. The material settles to the bottom of the vessel 11 under the action of gravity. When the screw 51 rotates axially, the dispersion component 7 rotates to achieve the dispersion and stirring of the material at the bottom of the vessel 11. The stirring of the material by the rotation of the dispersion component 7 can improve the material preparation rate. Moreover, the purpose of sweeping the vessel wall and dispersing the material by the dispersion component 7 can be completed with only one servo motor 4. This allows the purpose of improving the material preparation rate and reducing material loss to be achieved simultaneously in an energy-saving environment, effectively achieving the goal of reducing costs and improving output and product quality.
[0032] Preferably, the movable sleeve 8 has a first accommodating cavity 81 for accommodating the spring 110, and the fixed sleeve 9 has a second accommodating cavity 91 for accommodating the movable sleeve 8 and the spring 110. Each of the first accommodating cavity 81 and the second accommodating cavity 91 has a bolt hole 130 on one side. Each of the two bolt holes 130 is screwed with a retaining bolt 120, and one end of the retaining bolt 120 passing through the bolt hole 130 is engaged with the spring 110.
[0033] After screwing the retaining bolt 120 into the bolt hole 130, the end of the retaining bolt 120 inserted into the bolt hole 130 is inserted into the segment of the spring 110 and the spring 110 is locked in place. As the spring 110 moves between the fixed sleeve 9 and the movable sleeve 8, it can buffer the contact brush 10 and reduce the contact impact force between the contact brush 10 and the vessel body 11 caused by material agglomeration on the side wall of the vessel body 11. This provides a certain degree of protection for both the contact brush 10 and the vessel body 11. Furthermore, if the spring 110 is damaged due to excessive buffering, it can be quickly replaced by disassembling the retaining bolt 120 from the bolt hole 130. The operation is simple and the replacement of the spring 110 is quick and convenient.
[0034] Preferably, the contact brush 10 has a slot 102 inside for accommodating the infrared transmitter 150 and the wireless transmission module 160. A retaining plate 103 is expanded to one side of the slot 102. A tempered glass 104 is fixedly connected inside the retaining plate 103. An infrared receiver 140 is fixedly connected inside the retaining sleeve 9. The infrared transmitter 150 and the wireless transmission module 160 are fixedly connected inside the contact brush 10. Both the infrared receiver 140 and the wireless transmission module 160 are electrically connected to the infrared transmitter 150. The wireless transmission module 160 is electrically connected to the controller 2. The gas pressure gauge 3 is movably connected to the preparation container 1.
[0035] Since both the infrared receiver 140 and the wireless transmission module 160 are electrically connected to the infrared transmitter 150, and the wireless transmission module 160 is electrically connected to the controller 2, during the contact brush 10's contact with the vessel body 11, the infrared transmitter 150 emits an infrared signal in a straight line, which is received by the infrared receiver 140. If the movable sleeve 8 and the fixed sleeve 9 are relatively offset, this offset can easily cause the contact brush 10 to not adhere to the side wall of the vessel body 11, affecting the cleaning efficiency of the contact brush 10 on the vessel body 11. If the infrared signal emitted by the infrared transmitter 150 cannot be received by the infrared receiver 140, the wireless transmission module 160 will transmit the situation where the infrared transmitter 150 does not map the signal with the infrared receiver 140 to the controller 2, reminding personnel to perform maintenance.
[0036] Furthermore, the movable connection between the card slot 102 and the card plate 103 facilitates the maintenance of the infrared transmitter 150 and the wireless transmission module 160, and also ensures that floating materials do not enter the infrared transmitter 150 and the wireless transmission module 160.
[0037] Preferably, the ball screw nut assembly 5 includes a screw 51 and a ball nut 52. One end of the screw 51 is fixedly connected to the output end of the servo motor 4 via a connector 41, and the other end of the screw 51 is fixedly connected to the dispersion assembly 7. The ball nut 52 is disposed on the outside of the screw 51 and is movably connected to the screw 51.
[0038] Preferably, the dispersion component 7 includes a stirring and dispersion seat 71, a first dispersion blade 72, a second dispersion blade 73, and a vibration component 74. The stirring and dispersion seat 71 is fixedly connected to the end of the lead screw 51 away from the connector 41, and the first dispersion blade 72 and the second dispersion blade 73 are both fixedly connected to the outside of the stirring and dispersion seat 71.
[0039] During the rotation of the ball screw nut assembly 5, the ball nut 52 can move along the axial direction of the screw 51 and drive the vessel wall contact assembly 6 to move along the axial direction of the screw 51. During this process, the contact brush 10 inside the vessel wall contact assembly 6 is movably connected to the inner wall of the vessel 11 and cleans the vessel 11. At the same time, the rotation of the screw 51 drives the stirring and dispersing seat 71 to rotate. After the stirring and dispersing seat 71 rotates, it drives the first dispersing blade 72 and the second dispersing blade 73 to rotate to disperse and stir the material at the bottom of the vessel 11, thereby increasing the material preparation speed.
[0040] The oscillation assembly 74 includes a first mesh plate 741, a second mesh plate 742, and a sleeve 744. The middle part of the sleeve 744 is rotatably connected to the rod body of the corresponding lead screw 51. The second mesh plate 742 is provided with a plurality of insert rods 7421. A first trapezoidal platform 7442 and a second trapezoidal platform 7443 are respectively provided on both ends of the sleeve 744. The highest points of the first trapezoidal platform 7442 and the second trapezoidal platform 7443 are at the same height, and the lowest points of the first trapezoidal platform 7442 and the second trapezoidal platform 7443 are at the same height. The shapes of the first trapezoidal platform 7442 and the second trapezoidal platform 7443 are... Similar in shape, the sleeve 744 has a limiting plate 7441 on its outer wall, with the limiting plates 7441 respectively disposed on the outer walls of both ends of the sleeve 744. A partition 748 is disposed in the middle of the sleeve 744, the diameter of which is the same as the diameter of the limiting plates 7441 on both sides. Inner plates 749 are respectively disposed on the sleeve 744 on both sides of the partition 748, the diameter of which is larger than the diameter of the partition 748. Connecting rods 743 are disposed on the side edges of the inner plates 749 on both sides of the partition 748, and top plates 7432 are disposed on the outer ends of the connecting rods 743. The top plate 7432 and the corresponding inner plate 749 have the same diameter. Each side of the top plate 7432 has a through-hole 7431 in the middle. A lead screw 51 is rotatably connected to the through-hole 7431. A rotating opening 744 is provided in the middle of the sleeve 744 corresponding to the lead screw 51. The lead screw 51 is inserted into the corresponding rotating opening 7444. A first return spring 745 and a second return spring 746 are respectively sleeved on the sleeve 744 between the limiting plate 7441 and the inner plate 749 on each side of the sleeve 744. The first return spring 745 and the second return spring 746 are located on the corresponding inner plate. Between 749 and the limiting plate 7441, an inner rod 747 is provided on each side of the top plate 7432. The inner rod 747 faces the corresponding first trapezoidal platform 7442 and second trapezoidal platform 7443. A ball head 7471 is provided on the output end of each inner rod 747. Each ball head 7471 is slidably connected to the edge of the corresponding first trapezoidal platform 7442 and second trapezoidal platform 7443. The first mesh plate 741 is provided on the outer connecting rod 743 of the corresponding first trapezoidal platform 7442, and the second mesh plate 742 is provided on the outer connecting rod 743 of the second trapezoidal platform 7443.
[0041] Furthermore, a sleeve 744 is provided on the lead screw, which can rotate with the lead screw 51. The sleeve 744 is provided with a partition 748 and a limiting plate 7441. Inner plates 749 are respectively provided between the partitions 748 and the limiting plates 7441 on both sides of the sleeve 744, allowing the inner plates 749 to slide on the sleeve 744. A first return spring 745 and a second return spring 746 are respectively provided between each inner plate 749 and the corresponding limiting plate 7441. The return springs can push the inner plate 749 towards the partition 748. Each inner plate 749 is connected to a top plate 7432 via a connecting rod 743. The top plate 7432 is provided with a ball head 7471, and the ball head 7471 corresponds to a sleeve... The cylinder 744 is provided with a first trapezoidal platform 7442 and a second trapezoidal platform 7443. When the trapezoidal platforms rotate, they can push the top plates 7432 on both sides to move vertically, thereby driving the first mesh plate 741 and the second mesh plate 742 to move vertically. When the first mesh plate 741 and the second mesh plate 742 are close together, the insertion rod 7421 can be inserted. When they are far apart, the first mesh plate 741 and the second mesh plate 742 can vibrate as the sleeve 744 rotates, so that the titanium dioxide and boron on the first mesh plate 741 and the second mesh plate 742 can be more loose. Through the above arrangement, the titanium dioxide and boron can be mixed more easily and the mixing between titanium dioxide and boron can be accelerated.
[0042] To elaborate further, the first screen plate 741 has several holes, and a second screen plate 742 is provided below the first screen plate 741. The holes on the first screen plate 741 and the second screen plate 742 are not opposite each other. The second screen plate 742 is provided with a rod 7421, which can extend and retract within the holes of the first screen plate 741, so that the raw material will not be blocked in the hole.
[0043] At the same time, the contact brush 10 is movably connected to the inner wall of the vessel 11 and cleans the vessel 11. The material adhering to the inner wall of the vessel 11 can be swept to the bottom of the vessel 11 by the contact brush 10, thereby reducing the amount of material adhering to the inner wall of the vessel 11 that is not being prepared, improving the material preparation rate and the yield of finished products, and improving the purity of the material preparation. Furthermore, when the servo motor 4 drives the ball screw nut pair 5 and the dispersion component 7 to rotate simultaneously, it can effectively reduce energy consumption and reduce the cost of material preparation.
[0044] Preferably, the preparation container 1 includes a vessel body 11, a vessel cover 12 movably connected to the vessel body 11, and a base 17 disposed at the bottom of the vessel body 11. A vacuum port 13 and a discharge port 14 are fixedly connected to the outside of the vessel body 11, and the servo motor 4 is fixedly connected to the vessel cover 12.
[0045] The vacuum port 13 can be connected to a vacuum tube. Before material preparation, the vacuum port 13 is connected to the vacuum tube, and the vacuum pump is used to evacuate the inside of the vessel 11 through the vacuum port 13, so that the reaction can proceed smoothly and the material can be prepared smoothly.
[0046] Preferably, a support frame 15 is fixedly connected to the outside of the vessel body 11, the gas pressure gauge 3 is movably connected to the support frame 15, and the output end of the gas pressure gauge 3 passes through the vessel body 11 and communicates with the interior of the vessel body 11.
[0047] The gas pressure gauge 3 can perform gas pressure leak detection tests on the vacuuming operation inside the vessel 11 to avoid the situation where the vessel 11 is not in a vacuum environment before material preparation or the vessel 11 is not sealed during the material preparation process, which may lead to poor preparation.
[0048] Preferably, a lifting lug 16 is fixedly connected to one side of both the vessel body 11 and the vessel lid 12, and the lifting lug 16 is evenly distributed on the outer side of the vessel body 11 and the vessel lid 12.
[0049] The preparation container 1 can be transported by using a crane or other transportation equipment after being connected to the hook and the lifting lug 16. The preparation container 1 is convenient and quick to transport.
[0050] Preferably, the vessel wall contact components 6 are arranged in a circular array with the center line of the lead screw 51 as the baseline, and are evenly distributed on the outside of the ball nut 52. There are a total of six sets of vessel wall contact components 6, and the included angle between any two adjacent vessel wall contact components 6 is always 60°.
[0051] The vessel wall contact component 6 is set as a regular hexagon, so that the contact brush 10 inside the vessel wall contact component 6 can contact the inner wall of the vessel body 11 to the maximum extent, thereby achieving the most efficient scraping effect of the material on the inner wall of the vessel body 11, and further improving the material preparation quantity and the purity of the material preparation.
[0052] Preferably, the contact brush 10 has a screw head hole 101 inside, and the movable sleeve 8 is fixedly connected to a screw head 82 at the end away from the fixed sleeve 9, and the screw head 82 is adapted to the screw head hole 101.
[0053] The contact brush 10 can be removed from the movable sleeve 8 by screwing the screw head 82 into the screw head hole 101, which facilitates the maintenance of the contact brush 10 and the infrared transmitter 150 and wireless transmission module 160 inside the contact brush 10.
[0054] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.
[0055] Although embodiments of the invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the invention, the scope of which is defined by the appended claims and their equivalents.
Claims
1. A powder preparation apparatus for titanium diboride used in lithium battery manufacturing, comprising a preparation container (1), a controller (2), a gas pressure gauge (3), and a servo motor (4), characterized in that: The output end of the servo motor (4) passes through the preparation container (1) and is fixedly connected to a ball screw nut pair (5). A container wall contact component (6) is provided on the outside of the ball screw nut pair (5). A dispersion component (7) is provided at the end of the ball screw nut pair (5) away from the servo motor (4). The ball screw nut pair (5) includes a screw (51) and a ball nut (52). The dispersion assembly (7) includes a stirring dispersion seat (71), a first dispersion blade (72), a second dispersion blade (73), and a vibration assembly (74). The stirring dispersion seat (71) is fixedly connected to the end of the lead screw (51) away from the connector (41). The first dispersion blade (72) and the second dispersion blade (73) are both fixedly connected to the outside of the stirring dispersion seat (71). The vessel wall contact assembly (6) includes a movable sleeve (8), a fixed sleeve (9), and a contact brush (10). One end of the movable sleeve (8) is movably connected to the fixed sleeve (9) via a spring (110), and the other end is movably connected to the contact brush (10). The side of the contact brush (10) away from the movable sleeve (8) is movably connected to the inner wall of the preparation container (1). An infrared receiver (140) is fixedly connected inside the fixed sleeve (9). An infrared transmitter (150) and a wireless transmission module (160) are fixedly connected inside the contact brush (10). The infrared receiver (140) and the wireless transmission module (160) are both electrically connected to the infrared transmitter (150). The wireless transmission module (160) is electrically connected to the controller (2). The gas pressure gauge (3) is movably connected to the preparation container (1). The oscillation assembly (74) includes a first mesh plate (741), a second mesh plate (742), and a sleeve (744). The middle part of the sleeve (744) is rotatably connected to the rod of the corresponding lead screw (51). The second mesh plate (742) is provided with a plurality of insert rods (7421). A first trapezoidal platform (7442) and a second trapezoidal platform (7443) are respectively provided on both ends of the sleeve (744). The highest points of the first trapezoidal platform (7442) and the second trapezoidal platform (7443) are at the same height, and the lowest points of the first trapezoidal platform (7442) and the second trapezoidal platform (7443) are at the same height. The shapes of the first trapezoidal platform (7442) and the second trapezoidal platform (7443) are... Similarly, a limiting plate (7441) is provided on the outer wall of the sleeve (744), and the limiting plate (7441) is respectively provided on the outer wall of the two ends of the sleeve (744). A partition plate (748) is provided in the middle of the sleeve (744), and the diameter of the partition plate (748) is the same as the diameter of the limiting plates (7441) on both sides. An inner plate (749) is provided on the sleeve (744) on both sides of the partition plate (748), and the diameter of the inner plate (749) is larger than the diameter of the partition plate (748). A connecting rod (743) is provided on the side edge of the inner plate (749) on both sides of the partition plate (748), and a top plate (7432) is provided on the outer end of the connecting rod (743). The top plate (7432) and the corresponding inner plate (749) have the same diameter. Each side of the top plate (7432) has a through-hole (7431) in the middle. A lead screw (51) is rotatably connected in the through-hole (7431). The sleeve (744) corresponding to the lead screw (51) has a rotating port (7444) in the middle. The lead screw (51) is inserted into the corresponding rotating port (7444). A first return spring (745) and a second return spring (746) are respectively sleeved on the sleeve (744) between the limiting plate (7441) on each side of the sleeve (744) and the inner plate (749). The first return spring (745) and the second return spring (746) are respectively located on the corresponding inner plate. Between (749) and the limiting plate (7441), an inner rod (747) is provided on each side of the top plate (7432), the inner rod (747) faces the corresponding first trapezoidal platform (7442) and second trapezoidal platform (7443), a ball head (7471) is provided on the output end of each side of the inner rod (747), each ball head (7471) is slidably connected to the edge of the corresponding first trapezoidal platform (7442) and second trapezoidal platform (7443), the first mesh plate (741) is provided on the outer connecting rod (743) of the corresponding first trapezoidal platform (7442), and the second mesh plate (742) is provided on the outer connecting rod (743) of the second trapezoidal platform (7443); The vessel wall contact assembly (6) is arranged in a ring array with the center line of the lead screw (51) as the baseline, and is evenly distributed on the outside of the ball nut (52). There are a total of six sets of the vessel wall contact assembly (6), and the included angle between any two adjacent vessel wall contact assemblies (6) is always 60°.
2. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 1, characterized in that: The movable sleeve (8) has a first accommodating cavity (81) for accommodating the spring (110) inside. The fixed sleeve (9) has a second accommodating cavity (91) for accommodating the movable sleeve (8) and the spring (110) inside. Both the first accommodating cavity (81) and the second accommodating cavity (91) have bolt holes (130) on one side. Both bolt holes (130) are screwed together with snap ring bolts (120). One end of the snap ring bolt (120) passes through the bolt hole (130) and engages with the spring (110).
3. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 2, characterized in that: The contact brush (10) has a slot (102) inside for accommodating an infrared transmitter (150) and a wireless transmission module (160). A card plate (103) is expanded to one side of the slot (102), and a tempered glass (104) is fixedly connected inside the card plate (103).
4. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 3, characterized in that: One end of the lead screw (51) is fixedly connected to the output end of the servo motor (4) via a connector (41), and the other end of the lead screw (51) is fixedly connected to the dispersion component (7). The ball nut (52) is located on the outside of the lead screw (51) and is movably connected to the lead screw (51).
5. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 4, characterized in that: The preparation container (1) includes a vessel body (11), a vessel cover (12) movably connected to the vessel body (11), and a base (17) set at the bottom of the vessel body (11). A vacuum port (13) and a discharge port (14) are fixedly connected to the outside of the vessel body (11). The servo motor (4) is fixedly connected to the vessel cover (12).
6. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 5, characterized in that: A support frame (15) is fixedly connected to the outside of the vessel body (11). The gas pressure gauge (3) is movably connected to the support frame (15). The output end of the gas pressure gauge (3) passes through the vessel body (11) and communicates with the interior of the vessel body (11).
7. The apparatus for preparing titanium diboride powder for lithium battery fabrication according to claim 6, characterized in that: The vessel body (11) and the vessel lid (12) are both fixedly connected to one side of the lifting lugs (16). The lifting lugs (16) are evenly distributed on the outside of the vessel body (11) and the vessel lid (12). The contact brush (10) has a screw head hole (101) inside. The movable sleeve (8) is fixedly connected to a screw head (82) at the end away from the fixed sleeve (9). The screw head (82) is adapted to the screw head hole (101).
Citation Information
Patent Citations
1, 4-cyclohexanedicarboxylic acid preparation device
CN116688871A
Mixing and stirring device for lithium battery materials
CN210021926U
Reaction kettle with automatic cleaning function
CN214320122U
Lithium battery slurry preparation device
CN217313021U