Low-oxygen high-purity zinc small ingot forming glove box device

By designing a low-oxygen high-purity zinc ingot molding glove box device, the automatic molding of zinc materials is realized in a vacuum environment, and the problems of low automation and long turnover time during the molding, heating and melting of zinc ingots in the prior art are solved, and product quality and work efficiency are improved.

CN120243843APending Publication Date: 2025-07-04DONGFANG ELECTRIC (LESHAN) EBAN HIGH-PURITY MATERIALS CO LTD

Patent Information

Application Number
CN202510519767.3
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-04-24
Publication Date
2025-07-04

AI Technical Summary

Technical Problem

In the prior art, vacuum glove boxes lack the problem of automated forming and long turnover time during the forming and heating and melting of zinc ingots.

Method used

A low-oxygen high-purity zinc ingot molding glove box device is designed, including a box, glove box door, glove mouth, vacuum extraction system, heating device, mold assembly, crucible assembly, transfer mechanism and dumping assembly. The crucible assembly is moved and lifted through the transfer mechanism, and the dumping assembly is used to pour materials into the mold assembly, combining vacuum extraction and inert gas protection to achieve automated molding.

Benefits of technology

It improves the forming quality and working efficiency of zinc ingots, avoids oxidation of zinc materials, reduces turnover time, and enhances the sense of security.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention discloses a low-oxygen high-purity zinc small ingot forming glove box device, which relates to the technical field of oxygen-free glove boxes, and comprises a box body, a glove box door arranged on one side of the box body, a glove opening arranged on one side of the box body, and a vacuum extraction system, the heating device is arranged on one side in the box body, the mold assembly is arranged on the other side in the box body, the crucible assembly is heated through the heating device, the transferring mechanism drives the crucible assembly to move and ascend and descend, the pouring assembly is used for pouring materials in the crucible assembly into the mold assembly, and the pouring assembly is located between the transferring mechanism and the mold assembly. The transfer mechanism, the dumping assembly and the mold assembly are sequentially lowered in height. The device is reasonable in design and ingenious in structural design in the transferring and transferring process, zinc materials are molten in the glove box, the glove box is vacuumized and then filled with inert gas, the zinc materials are prevented from being oxidized in the forming process, in addition, the transferring mechanism drives the crucible assembly to move and ascend and descend, and the dumping assembly assists the crucible assembly in obliquely dumping materials. By arranging the glove box, the product quality and the working efficiency are improved.
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Description

Technical Field

[0001] The present invention relates to the technical field of glove boxes in an anaerobic environment, and more specifically to the technical field of glove box devices for forming low-oxygen high-purity zinc ingots. Background Art

[0002] A vacuum glove box is a laboratory device that fills a high-purity inert gas into the box body and circulates to filter out the active substances therein. It is also called a glove box, an inert gas protection box, a dry box, etc. It mainly removes O2, H2O, and organic gases. It is widely used in ultra-pure environments without water, oxygen, and dust, such as: the forming of low-oxygen high (ultra)-pure materials, lithium-ion batteries and materials, semiconductors, supercapacitors, special lamps, laser welding, brazing, etc. This product is an ideal device for scientific experiments in institutions of higher learning, research units, and enterprise laboratories, and is widely used in departments such as biochemistry, metallurgy, electronics, chemical engineering, geology, minerals, and medicine.

[0003] A glove box is a sealed box body with a transparent panel made of plexiglass in the front, and two gloves are installed on the panel. Operations inside the box can be carried out through the gloves. The prior art has disclosed the following technologies:

[0004] The patent with the publication number CN104908063A and the patent name "A Vacuum Glove Box" discloses the following content: It includes a box body, a box cover, an air extraction chamber, a mobile terminal, and a digital microscope. A tool slot is provided on the inner surface of the box body. The box body is provided with rubber gloves and a lamp box. A bolt tightener is arranged between the rubber gloves and the box body. A hinge device is arranged between the box body and the box cover, and the hinge device is mounted on the lamp box. The air extraction chamber is provided with a gas extraction port and an inert gas replenishment port. A barometer is installed above the air extraction chamber. The mobile terminal is located inside the box body. A titanium alloy hose is installed on the back of the mobile terminal, and a magnet is installed at the end of the titanium alloy hose. The digital microscope is located in the tool slot. The vacuum glove box has the advantages of video recording, taking photos, and microscopic functions.

[0005] The patent with the publication number CN109093654B and the patent name "A fully transparent vacuum glove box" discloses the following content: It includes a box body, a first vacuum valve, a first pressure gauge, a transition chamber, a second vacuum valve, a second pressure gauge, a box door, a workbench, gloves, a sealing connector, and an auxiliary lighting device. The first vacuum valve is inserted into the inner side of the through hole on the left side of the top of the box body, and the connection part is sealed with sealant. The first pressure gauge is inserted into the inner side of the through hole on the right side of the top of the box body, and the connection part is sealed with sealant. To solve the problem that the gloves need to be disassembled and replaced, and the sealing performance at the connection part is poor, a sealing connector is provided. By installing a sealing sleeve, the gap between the gloves and the box body at the connection part is reduced. At the same time, the outer ring cooperates with the inner ring and is embedded in the inner and outer sides of the sealing sleeve, reducing the gap when the sealing sleeve is installed, greatly enhancing the sealing performance, and thus achieving the effect of enhancing the sealing performance at the connection part between the gloves and the box body.

[0006] The above-mentioned patent vacuum glove box solves the problems of the sealing and vacuum pumping of the glove box, but does not involve the problems of the forming and heating melting of small zinc ingots, how to achieve automated forming, and how to save the turnover time. How to solve the above situation has become a technical problem to be solved by those skilled in the art. Summary of the Invention

[0007] The purpose of the present invention is: To solve the above-mentioned technical problems, the present invention provides a glove box device for forming low-oxygen high-purity zinc small ingots.

[0008] The present invention specifically adopts the following technical solutions to achieve the above purpose:

[0009] The present invention provides a glove box device for forming low-oxygen high-purity zinc small ingots, which includes a box body, a glove box door arranged on one side of the box body, a glove port arranged on one side of the box body, and a vacuum extraction system. It also includes a heating device arranged on one side inside the box body, a mold assembly arranged on the other side inside the box body, a crucible assembly heated by the heating device, a transfer mechanism for driving the crucible assembly to move and lift, and a pouring assembly for pouring the material in the crucible assembly into the mold assembly. The pouring assembly is located between the transfer mechanism and the mold assembly, and the heights of the transfer mechanism, the pouring assembly, and the mold assembly decrease in sequence.

[0010] In one embodiment, the transfer mechanism includes a gantry fixing frame, a longitudinal rod that moves horizontally and transversely along the gantry fixing frame, a lifting mechanism that moves along the length direction of the longitudinal rod, and a movable connector arranged at the bottom of the lifting mechanism. The movable connector is connected to the crucible assembly, and the crucible assembly can rotate in the vertical direction around the movable connector.

[0011] In one embodiment, the lifting mechanism includes a gantry motor and an electric lifting rod arranged at the output end of the gantry motor, and the movable connector is arranged at the bottom of the electric lifting rod.

[0012] In one embodiment, the movable connecting piece includes a "U"-shaped mounting plate with an opening facing downward, a bearing disposed at the opening of the "U"-shaped mounting plate, the axis line of the bearing is longitudinally arranged, a connecting shaft is fixed on the inner ring of the bearing, both ends of the connecting shaft are fixedly connected to the opening of the "U"-shaped mounting plate, and the crucible assembly is fixed on the outer ring of the bearing through a connecting frame.

[0013] In one embodiment, the crucible assembly includes an outer graphite crucible and a quartz crucible sleeved inside the graphite crucible.

[0014] In one embodiment, the heating device includes a heating coil disposed inside the box body, an intermediate frequency furnace disposed outside the box body, and a power adjustment knob disposed on the intermediate frequency furnace. The heating coil is vertically arranged, both ends of the heating coil are respectively connected to the intermediate frequency furnace, and the inner diameter of the heating coil is larger than the outer diameter of the graphite crucible.

[0015] In one embodiment, the pouring assembly includes a pourer positioner, a pourer rotating rod for driving the pourer positioner to rotate, and a rotation guiding assembly for increasing the rotation stability of the pourer positioner.

[0016] In one embodiment, the pourer rotating rod is horizontally and longitudinally arranged inside the box body, the pourer rotating rod is driven by a pourer motor, the pourer positioner is in a barrel shape, the outer diameter of the graphite crucible is smaller than the inner diameter of the pourer positioner, and a rotation positioning hole allowing the pourer rotating rod to pass through is provided at the top of the outer wall of the pourer positioner.

[0017] In one embodiment, the rotation guiding assembly includes two arc-shaped guiding tracks respectively arranged on the front and rear inner side walls of the box body. The two arc-shaped guiding tracks on the same side are concentrically arranged, and their centers are both located on the axis line of the pourer rotating rod. The two arc-shaped guiding tracks on the front and rear inner side walls of the box body are correspondingly positioned to form two groups of arc-shaped track assemblies;

[0018] The rotation guiding assembly further includes two horizontally and longitudinally arranged limiting rods, and both ends of each limiting rod are respectively in sliding fit with a corresponding group of arc-shaped track assemblies;

[0019] Limiting holes allowing the corresponding limiting rods to pass through are respectively provided on the left and right sides at the bottom of the outer wall of the pourer positioner.

[0020] Specifically, the setting of the two limiting rods and the two groups of arc-shaped track assemblies increases the stability of the pourer positioner.

[0021] In one embodiment, the mold assembly includes a heating table at the bottom and a mold located on the heating table, and an inclination adjuster is provided between the heating table and the mold;

[0022] An isolated power introduction hole is provided at the top of the box body;

[0023] The vacuum extraction system includes an intake valve and an exhaust valve that communicate with the interior of the box.

[0024] Working principle:

[0025] Open the intake valve and exhaust valve of the glove box, introduce inert gas through the intake valve, and discharge air through the exhaust valve; feed materials from the right glove port into the quartz crucible embedded in the graphite crucible placed in the heating coil. Rotate the power adjustment knob of the intermediate frequency furnace to adjust to an appropriate power to heat and melt the zinc material until it becomes liquid. After that, through the action of the overhead crane motor, lift the electric lifting rod to raise the crucible until the lower bottom surface is higher than the upper surface of the heating line of the intermediate frequency furnace. Then, the overhead crane motor drives the graphite crucible to move left, right, forward, and backward to a suitable position through the load-bearing hook. After the overhead crane motor lowers the electric lifting rod and completely places the graphite crucible in the tilter locator, after positioning by extending and retracting the tilter motor, rotate the tilter motor. The connection between the graphite crucible and the electric lifting rod rotates through the bearing, and the limit rod slides along the arc-shaped guide rail and slowly tilts to a set appropriate position to complete a pouring operation. The tilter motor rotates reversely to reset, and then perform the positioning operation again, pouring materials into each mold groove in turn. After the pouring is completed, place the graphite crucible back into the heating coil through the action of the overhead crane motor. After the zinc liquid on the mold solidifies, use tweezers to remove it, and then complete one forming operation.

[0026] The beneficial effects of the present invention are as follows:

[0027] 1. The present invention is reasonably designed, and the structure design in the transfer and transportation process is ingenious. The zinc material is melted in the glove box, and the glove box is filled with inert gas, which avoids the zinc material from being oxidized by contacting with air during the forming process. In addition, the transfer mechanism drives the crucible assembly to move and lift, and the tilting assembly pours the materials in the crucible assembly into the mold assembly. After the glove box door is opened, multiple zinc materials can be placed into the glove box at one time. After the zinc material is formed in the mold once, it is demolded through the glove port and placed on one side inside the glove box. After repeating the above process multiple times, open the glove box door once to take out multiple formed zinc materials. Therefore, the setting of this glove box improves the product quality, increases the work efficiency and sense of security.

[0028] 2. A quartz crucible and an intermediate frequency furnace heating coil are provided inside the glove box. By rotating the power adjustment knob of the intermediate frequency furnace to adjust to an appropriate power to heat and melt the zinc material in the quartz crucible, the heating temperature and heating time can be controlled.

[0029] 3. After positioning by extending and retracting the tilter motor, rotate the tilter motor. The connection between the graphite crucible and the electric lifting rod rotates through the bearing, and the limit rod slides along the arc-shaped guide rail and slowly tilts to a set appropriate position. The setting of this structure increases the stability of the pouring process. Description of the drawings

[0030] To more clearly illustrate the technical solutions of the embodiments of the present invention, the following will briefly introduce the drawings required for the embodiments. It should be understood that the following drawings only show some embodiments of the present invention, and therefore should not be regarded as limiting the scope. For those of ordinary skill in the art, without creative efforts, other related drawings can also be obtained based on these drawings.

[0031] Figure 1 is a schematic structural diagram of a glove box device for forming low-oxygen high-purity zinc ingots of the present invention;

[0032] Figure 2 is a schematic structural diagram of the dumping assembly;

[0033] Figure 3 is a schematic structural diagram of the transfer mechanism;

[0034] Figure 4 is Figure 3 a partial structural diagram of

[0035] Figure 5 is Figure 4 a partial enlarged view of

[0036] Figure 6 is Figure 1 a rendering of

[0037] Reference numerals: 1, glove box door; 2, box body; 3, isolated power lead hole; 4, overhead crane fixing frame; 5, tilter rotating rod; 6, tilter motor; 7, load-bearing hook; 8, overhead crane motor; 9, electric lifting rod; 10, exhaust valve; 11, bearing; 12, quartz crucible; 13, graphite crucible; 14, heating coil; 15, intermediate frequency furnace; 16, intake valve; 17, limit rod; 18, dumper positioner; 19, arc guide track; 20, inclination adjuster; 21, mold; 22, heating table; 23, glove port; 24, power adjustment knob; 25, overhead crane transverse movement motor; 26, overhead crane longitudinal movement motor. Detailed Embodiments

[0038] To make the technical problems, technical solutions and technical effects of the present invention clearer, the following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the drawings in the embodiments of the present invention. Obviously, the described embodiments are some, but not all, of the embodiments of the present invention. Usually, the components of the embodiments of the present invention described and shown in the drawings here can be arranged and designed in various different configurations.

[0039] Accordingly, the following detailed description of the embodiments of the present invention provided in the accompanying drawings is not intended to limit the scope of the claimed invention, but merely represents selected embodiments of the present invention. All other embodiments obtained by those of ordinary skill in the art based on the embodiments of the present invention without creative efforts fall within the scope of protection of the present invention.

[0040] It should be noted that like reference numerals and letters denote like items in the following drawings. Therefore, once an item is defined in one drawing, it does not need to be further defined and explained in subsequent drawings. In addition, the terms "first", "second", etc. are only used for descriptive distinction and cannot be construed as indicating or implying relative importance.

[0041] In the description of the embodiments of the present invention, it should be noted that the orientation or positional relationship indicated by terms such as "inner", "outer", "upper", etc. is based on the orientation or positional relationship shown in the drawings, or the orientation or positional relationship in which the inventive product is habitually placed during use. It is only for the convenience of describing the present invention and simplifying the description, and does not indicate or imply that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be construed as a limitation of the present invention.

[0042] Embodiment 1

[0043] As Figures 1 to 6 shown, this embodiment provides a glove box device for forming low-oxygen high-purity zinc ingots, which includes a box body 2, a glove box door 1 provided on one side of the box body 2, a glove port 23 provided on one side of the box body 2, and a vacuum extraction system. It further includes a heating device provided on one side inside the box body 2, a mold assembly provided on the other side inside the box body 2, a crucible assembly heated by the heating device, a transfer mechanism for driving the movement and lifting of the crucible assembly, and a pouring assembly for pouring the material in the crucible assembly into the mold assembly. The pouring assembly is located between the transfer mechanism and the mold assembly, and the heights of the transfer mechanism, the pouring assembly, and the mold assembly decrease in sequence.

[0044] Embodiment 2

[0045] As Figures 1 to 6 shown, this embodiment provides a glove box device for forming low-oxygen high-purity zinc ingots, which includes a box body 2, a glove box door 1 provided on one side of the box body 2, a glove port 23 provided on one side of the box body 2, and a vacuum extraction system. It further includes a heating device provided on one side inside the box body 2, a mold assembly provided on the other side inside the box body 2, a crucible assembly heated by the heating device, a transfer mechanism for driving the movement and lifting of the crucible assembly, and a pouring assembly for pouring the material in the crucible assembly into the mold assembly. The pouring assembly is located between the transfer mechanism and the mold assembly, and the heights of the transfer mechanism, the pouring assembly, and the mold assembly decrease in sequence.

[0046] The transfer mechanism includes a gantry fixing frame 4, a longitudinal rod that moves horizontally and transversely along the gantry fixing frame 4, a lifting mechanism that moves along the length direction of the longitudinal rod, and a movable connecting piece provided at the bottom of the lifting mechanism. The movable connecting piece is connected to the crucible assembly, and the crucible assembly can rotate in the vertical direction around the movable connecting piece.

[0047] Specifically, the longitudinal rod moves horizontally and transversely along the gantry fixing frame 4 through a gantry transverse movement motor 25; the lifting mechanism moves along the length direction of the longitudinal rod through a gantry longitudinal movement motor 26.

[0048] The lifting mechanism includes a gantry motor 8 and an electric lifting rod 9 provided at the output end of the gantry motor 8, and the movable connecting piece is provided at the bottom of the electric lifting rod 9.

[0049] The movable connecting piece includes a "U"-shaped mounting plate with an opening facing downwards, and a bearing 11 provided at the opening of the "U"-shaped mounting plate. The axis line of the bearing 11 is set longitudinally. A connecting shaft is fixed on the inner ring of the bearing 11, and both ends of the connecting shaft are fixedly connected to the opening of the "U"-shaped mounting plate. The crucible assembly is fixed on the outer ring of the bearing 11 through a connecting frame.

[0050] Embodiment 3

[0051] This embodiment is further optimized on the basis of Embodiment 2. Specifically:

[0052] The crucible assembly includes an external graphite crucible 13 and a quartz crucible 12 sleeved inside the graphite crucible 13.

[0053] The heating device includes a heating coil 14 provided inside the box body 2, an intermediate frequency furnace 15 provided outside the box body 2, and a power adjustment knob 24 provided on the intermediate frequency furnace 15. The heating coil 14 is vertically arranged, and both ends of the heating coil 14 are respectively connected to the intermediate frequency furnace 15. The inner diameter of the heating coil 14 is larger than the outer diameter of the graphite crucible 13.

[0054] Embodiment 4

[0055] This embodiment is further optimized on the basis of Embodiment 2. Specifically:

[0056] The tilting assembly includes a dumper positioner 18, a dumper rotating rod 5 that drives the dumper positioner 18 to rotate, and a rotation guiding assembly that increases the rotation stability of the dumper positioner 18.

[0057] The dumper rotating rod 5 is horizontally and longitudinally arranged inside the box body 2. The dumper rotating rod 5 is driven by a dumper motor 6. The dumper positioner 18 is in a barrel shape. The outer diameter of the graphite crucible 13 is smaller than the inner diameter of the dumper positioner 18. A rotation positioning hole allowing the dumper rotating rod 5 to pass through is provided at the top of the outer wall of the dumper positioner 18.

[0058] The rotation guiding assembly includes two arc-shaped guiding tracks 19 respectively arranged on the front and rear inner side walls of the box body 2. The two arc-shaped guiding tracks 19 on the same side are concentrically arranged, and the centers of both are located on the axis of the tilter rotating rod 5. The two arc-shaped guiding tracks 19 on the front and rear inner side walls of the box body 2 are correspondingly positioned to form two groups of arc-shaped track assemblies;

[0059] The rotation guiding assembly further includes two horizontally and longitudinally arranged limiting rods 17. Both ends of each limiting rod 17 are slidably matched with a corresponding group of arc-shaped track assemblies;

[0060] On the left and right sides at the bottom of the outer wall of the dumper positioner 18, limiting holes are respectively arranged to allow the corresponding limiting rods 17 to pass through.

[0061] Specifically, the setting of the two limiting rods 17 and the two groups of arc-shaped track assemblies increases the stability of the dumper positioner 18.

[0062] In an embodiment, the mold assembly includes a heating table 22 at the bottom and a mold 21 located on the heating table 22. An inclination adjuster 20 is arranged between the heating table 22 and the mold 21;

[0063] An isolated power supply lead-in hole 3 is arranged at the top of the box body 2;

[0064] The vacuum extraction system includes an intake valve 16 and an exhaust valve 10 that communicate with the inside of the box body 2.

[0065] Working principle:

[0066] After opening the exhaust valve 10 of the glove box and closing the intake valve 16 for low vacuum pumping, open the intake valve 16, introduce inert gas through the intake valve 16, and the exhaust valve 10 discharges air; Feed materials from the right glove port 23 into the quartz crucible 12 embedded in the graphite crucible 13 placed in the heating coil 14 of the intermediate frequency furnace 15. Rotate the power adjustment knob 24 of the intermediate frequency furnace 15 to adjust to an appropriate power to heat and melt the zinc material until it becomes liquid. Then, through the action of the overhead crane motor 8, lift the electric lifting rod 9 to lift the crucible until the lower bottom surface is higher than the upper surface of the heating line of the intermediate frequency furnace 15. Then, the overhead crane motor 8 drives the graphite crucible 13 to move to a suitable position in the front, rear, left, and right directions through the load-bearing hook 7. After the overhead crane motor 8 lowers the electric lifting rod 9 and completely places the graphite crucible 13 into the dumper positioner 18, after positioning by telescoping the dumper motor 6, rotate the dumper motor 6. The connection between the graphite crucible 13 and the electric lifting rod 9 rotates through the bearing 11, and the limiting rod 17 slides along the arc-shaped guiding track 19 and slowly tilts to a set appropriate position to complete a pouring operation. The dumper motor 6 rotates reversely to reset, and then performs a positioning operation again, pouring materials into each mold 21 groove in turn. After pouring is completed, through the action of the overhead crane motor 8, place the graphite crucible 13 back into the heating coil 14 of the intermediate frequency furnace 15. After the zinc liquid on the mold 21 solidifies, use tweezers to remove it, and then a forming operation is completed.

Claims

1. A glove box device for forming low-oxygen high-purity zinc ingots, comprising a box body (2), a glove box door (1) arranged on one side of the box body (2), a glove port (23) arranged on one side of the box body (2), and a vacuum extraction system, characterized in that, It further includes a heating device arranged on one side inside the box body (2), a mold (21) assembly arranged on the other side inside the box body (2), a crucible assembly heated by the heating device, a transfer mechanism for driving the movement and lifting of the crucible assembly, and a pouring assembly for pouring the material in the crucible assembly into the mold (21) assembly. The pouring assembly is located between the transfer mechanism and the mold (21) assembly, and the heights of the transfer mechanism, the pouring assembly, and the mold (21) assembly decrease in sequence.

2. The low-oxygen high-purity zinc ingot forming glove box device according to claim 1, characterized in that, The transfer mechanism includes a gantry fixing frame (4), a longitudinal rod that horizontally and laterally moves along the gantry fixing frame (4), a lifting mechanism that moves along the length direction of the longitudinal rod, and a movable connecting piece arranged at the bottom of the lifting mechanism. The movable connecting piece is connected to the crucible assembly, and the crucible assembly can rotate in the vertical direction around the movable connecting piece.

3. The low-oxygen high-purity zinc ingot forming glove box device according to claim 2, characterized in that, The lifting mechanism includes a gantry motor (8) and an electric lifting rod (9) arranged at the output end of the gantry motor (8). The movable connecting piece is arranged at the bottom of the electric lifting rod (9).

4. A glove box device for forming low-oxygen high-purity zinc ingots according to claim 3, characterized in that, The movable connecting piece includes a "U"-shaped mounting plate with an opening downward, and a bearing (11) arranged at the opening of the "U"-shaped mounting plate. The axis line of the bearing (11) is arranged longitudinally. A connecting shaft is fixed on the inner ring of the bearing (11), and both ends of the connecting shaft are fixedly connected to the opening of the "U"-shaped mounting plate. The crucible assembly is fixed on the outer ring of the bearing (11) through a connecting frame.

5. The low-oxygen high-purity zinc ingot forming glove box device according to claim 1, characterized in that, The crucible assembly includes an external graphite crucible (13) and a quartz crucible (12) sleeved inside the graphite crucible (13).

6. The low-oxygen high-purity zinc ingot forming glove box device according to claim 5, characterized in that, The heating device includes a heating coil (14) arranged inside the box body (2), an intermediate frequency furnace (15) arranged outside the box body (2), and a power adjustment knob (24) arranged on the intermediate frequency furnace (15). The heating coil (14) is arranged vertically, both ends of the heating coil (14) are respectively connected to the intermediate frequency furnace (15), and the inner diameter of the heating coil (14) is larger than the outer diameter of the graphite crucible (13).

7. The low-oxygen high-purity zinc ingot forming glove box device according to claim 6, characterized in that, The pouring assembly includes a pourer positioner (18), a pourer rotating rod (5) for driving the rotation of the pourer positioner (18), and a rotation guiding assembly for increasing the rotation stability of the pourer positioner (18).

8. A glove box device for forming low-oxygen high-purity zinc ingots according to claim 7, characterized in that, The pourer rotating rod (5) is horizontally and longitudinally arranged inside the box body (2). The pourer rotating rod (5) is driven by a pourer motor (6). The pourer positioner (18) is in a barrel shape. The outer diameter of the graphite crucible (13) is smaller than the inner diameter of the pourer positioner (18). A rotation positioning hole allowing the pourer rotating rod (5) to pass through is arranged at the top of the outer wall of the pourer positioner (18).

9. The low-oxygen high-purity zinc ingot forming glove box device according to claim 8, characterized in that, The rotation guiding assembly includes two arc-shaped guiding tracks (19) respectively arranged on the front and rear inner side walls of the box body (2). The two arc-shaped guiding tracks (19) on the same side are concentrically arranged, and the centers of both are located on the axis of the tilter rotating rod (5). The two arc-shaped guiding tracks (19) on the front and rear inner side walls of the box body (2) are in corresponding positions, forming two groups of arc-shaped track assemblies; The rotation guiding assembly further includes two horizontally and longitudinally arranged limiting rods (17), and both ends of each limiting rod (17) are slidably matched with a corresponding group of the arc-shaped track assemblies; On the left and right sides at the bottom of the outer wall of the dumper positioner (18), limiting holes allowing the corresponding limiting rods (17) to pass through are respectively arranged.

10. A glove box device for forming low-oxygen high-purity zinc ingots according to claim 9, characterized in that, The mold (21) assembly includes a heating table (22) at the bottom and a mold (21) located on the heating table (22). An inclination adjuster (20) is arranged between the heating table (22) and the mold (21); an isolated power lead hole (3) is arranged at the top of the box body (2); the vacuum extraction system includes an intake valve (16) and an exhaust valve (10) communicated with the inside of the box body (2).

Citation Information

Patent Citations

  • Vacuum glove box

    CN104908063A

  • A fully transparent vacuum glove box

    CN109093654B

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  • Preparation device and preparation method based on Cu-Pb-Sn composite metal processing

    CN120538302A

  • Preparation device and preparation method based on Cu-Pb-Sn composite metal processing

    CN120538302B