Composition, preparation method, formed product and application

Abstract

The invention discloses a composition, a preparation method, a product formed by the composition and application, the composition comprises a sugar alcohol component, a porous medium and an auxiliary component, the sugar alcohol component comprises xylitol and a first component sugar alcohol, the first component sugar alcohol is erythritol and / or isomaltitol, and the auxiliary component comprises xylitol and a second component sugar alcohol. The mass ratio of the xylitol to the first component sugar alcohol is (300-500): (100-300); the mass ratio of the sugar alcohol component to the porous medium is (400-700): (10-70). According to the present invention, the mass ratio of the xylitol to the first component sugar alcohol is set to be 300-500: 100-300, and the porous medium is matched so as to form the stable dispersion system, such that the heated adhesion is reduced, and the hot melt stability is improved.

Description

Technical Field

[0001] The present invention belongs to the technical field of dietary supplements, and particularly relates to a composition, a preparation method, and the resulting product and application. Background Art

[0002] Compared with solid powder products that need to be mixed with liquid, solid powder products that can be eaten directly have the advantages of being easy to carry and easy to eat. They are currently popular among consumers. And because they can be eaten directly, they are more suitable for today's fast-paced consumer experience needs.

[0003] Existing edible solid powders with low sugar alcohol content (e.g., less than or equal to 30%) often suffer from a poor taste experience, including noticeable grittiness, stickiness, and poor dissolution. When these solid beverages or sprinkles are taken, the powder tends to clump together and not dissolve, affecting the ingestion experience.

[0004] In order to avoid the above-mentioned defects, it is usually necessary to increase the sugar alcohol content. However, when the sugar alcohol content is high, due to the small particle size of the sugar alcohol component, products containing more small-particle sugar alcohols are often accompanied by problems of agglomeration and hot melting during production and storage. Existing flash-dissolve products usually contain xylitol and erythritol. In order to avoid the hot-melt agglomeration defect, the xylitol content is usually set lower than the erythritol content. This is because the xylitol molecule has a strong polarity, which makes the flash-dissolve product more soluble, but it is also more likely to cause adhesion and aggregation between particles, and more likely to be bonded by heat, that is, hot-melt instability occurs. However, the methods of increasing the total proportion of sugar alcohol components and reducing the xylitol content ratio in the prior art can only alleviate the agglomeration defect, and cannot completely avoid the hot-melt agglomeration defect.

[0005] Therefore, it is necessary to find new ideas to prepare the composite material. Summary of the Invention

[0006] The object of the present invention is to avoid the shortcomings of the prior art and provide a composition, by setting the mass ratio of xylitol and the first component sugar alcohol to 300-500:100-300, and the mass ratio of the sugar alcohol component to the porous medium to 400-700:10-70, so as to form a stable dispersion system, reduce thermal adhesion, and improve the hot melt stability of the composition.

[0007] In order to achieve the above objectives, this application adopts the following technical solutions: A composition includes a sugar alcohol component, a porous medium, and an auxiliary component. The sugar alcohol component includes xylitol and a first component sugar alcohol, wherein the first component sugar alcohol is erythritol and / or isomalt, and the mass ratio of the xylitol to the first component sugar alcohol is 300-500:100-300; the mass ratio of the sugar alcohol component to the porous medium is 400-700:10-70.

[0008] Furthermore, the porous medium is one or a combination of microcrystalline cellulose, resistant dextrin and maltodextrin.

[0009] Furthermore, the first component sugar alcohol is erythritol.

[0010] Furthermore, the porous medium is microcrystalline cellulose.

[0011] Furthermore, the mass proportion of the sugar alcohol component in the composition is not less than 40 wt %.

[0012] Furthermore, the mesh size of the sugar alcohol component is 60 mesh to 200 mesh.

[0013] Furthermore, the auxiliary components include one or more of silicon dioxide, flavor, fruit powder, acidity regulator, and functional composition.

[0014] Furthermore, it includes 400-700 parts of sugar alcohol components, 10-70 parts of porous media, 1-6 parts of silicon dioxide, 0.1-50 parts of flavors, 0.1-50 parts of fruit powder, 0.1-50 parts of acidity regulators, and 0.1-50 parts of efficacy compositions.

[0015] Furthermore, the functional composition includes at least one of prebiotics, probiotics, and proteins of animal and plant origin.

[0016] The present application also provides a method for preparing the composition as described above, comprising: The sugar alcohol component, the porous medium and the auxiliary component are crushed, sieved and weighed respectively, and then mixed to obtain a composition.

[0017] The present application also provides a product comprising the composition as described above.

[0018] The present application also provides the use of the above-mentioned composition and / or the above-mentioned product in food and medicine.

[0019] The present invention has the following beneficial effects: The present application abandons the formula of reducing the xylitol content in the prior art, and sets the mass ratio of xylitol to the first component sugar alcohol to 300-500:100-300, and the mass ratio of the sugar alcohol component to the porous medium to 400-700:10-70; that is, the xylitol content is higher than the sugar alcohol content of the first component, and at the same time, the porous medium with a lower density is used to form a stable dispersion system of the sugar alcohol component under a specific component and the porous medium; at the same time, when the xylitol content is high, the strong molecular polarity of xylitol is used to help the dispersion system have better solubility, and the addition of the porous medium helps to reduce the hydrogen bonding between xylitol and the first component sugar alcohol and water, reduce the probability of thermal adhesion, improve the hot melt stability of the composition, and avoid the problem of hot melt agglomeration of the composition during the preparation process. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] Figure 1 Schematic diagram of the sample that does not agglomerate in the thermal sensitivity test; Figure 2 Schematic diagram of the sample with false agglomeration in the thermal sensitivity test; Figure 3 Schematic diagram of samples that clumped or melted during the heat sensitivity test. DETAILED DESCRIPTION

[0021] The preferred embodiments of the present invention will be described in more detail below with reference to specific examples. Although preferred embodiments of the present invention are shown in the specific embodiments, it should be understood that the present invention can be implemented in various forms and should not be limited by the embodiments set forth herein. On the contrary, these embodiments are provided to make the present invention more thorough and complete and to fully convey the scope of the present invention to those skilled in the art.

[0022] The present application provides a composition comprising a sugar alcohol component, a porous medium and an auxiliary component, wherein the sugar alcohol component comprises xylitol and a first component sugar alcohol, wherein the first component sugar alcohol is erythritol and / or isomalt, and the mass ratio of the xylitol to the first component sugar alcohol is 300-500:100-300; the mass ratio of the sugar alcohol component to the porous medium is 400-700:10-70.

[0023] Preferably, the mass ratio of the xylitol to the first component sugar alcohol is 350-450:150-250.

[0024] The porous medium is specifically one or a combination of microcrystalline cellulose, resistant dextrin and maltodextrin.

[0025] The mass ratio of the sugar alcohol component to the porous medium is 600:10-70, for example, the mass ratio of the sugar alcohol component to the porous medium is 600:10, 600:20, 600:30, 600:40, 600:50, 600:60 or 600:70.

[0026] Preferably, the porous medium is microcrystalline cellulose. The mass ratio of the sugar alcohol component to the microcrystalline cellulose is 600:10-70, for example, the mass ratio of the sugar alcohol component to the microcrystalline cellulose is 600:10, 600:20, 600:30, 600:40, 600:50, 600:60 or 600:70.

[0027] The sugar alcohol of the first component is preferably erythritol, and the mass ratio of xylitol to erythritol is 300-500:100-300; preferably, the mass ratio of xylitol to erythritol is 350-450:150-250.

[0028] The mass proportion of the sugar alcohol component in the composition is not less than 40wt%, for example, not less than 40wt%, 45wt%, 50wt%, 55wt%, 60wt%, 65wt%, 70wt%, 75wt%, 80wt%, 85wt%, 90wt% or 95wt%.

[0029] The mesh size of the sugar alcohol component is 60-200 mesh, for example, 60-120 mesh, 60-100 mesh, 80-200 mesh, 100-200 mesh.

[0030] The mesh size range refers to the mass percentage meeting the mesh size range calculated according to the manual screening method in the second method of 0982 of the fourth volume of the Chinese Pharmacopoeia, which is not less than 80%, such as 80%, 85%, 90%, 95% or 99%.

[0031] The auxiliary components in this application include silicon dioxide, essence, fruit powder, acidity regulator, and functional composition.

[0032] The flavor is at least one selected from sweet orange flavor, lemon flavor, passion fruit flavor, pineapple flavor, peach flavor, apple flavor, grape flavor, and strawberry flavor.

[0033] The fruit powder is at least one selected from the group consisting of sweet orange fruit powder, lemon fruit powder, passion fruit powder, pineapple fruit powder, peach fruit powder, apple fruit powder, grape fruit powder, and strawberry fruit powder.

[0034] The acidity regulator includes at least one of citric acid, sodium citrate, lactic acid, tartaric acid, and malic acid.

[0035] The efficacy composition includes at least one of prebiotics, probiotics, and animal and plant-derived proteins. The probiotics include lactic acid bacteria and / or Streptococcus thermophilus; the prebiotics include at least one of fructooligosaccharides, isomaltooligosaccharides, galacto-oligosaccharides, xylo-oligosaccharides, and inulin. The animal and plant-derived proteins include at least one of whey protein powder, yeast protein, collagen peptides, soy protein, pea protein, and oat protein.

[0036] Specifically, the composition of the present application includes 400-700 parts of sugar alcohol component, 10-70 parts of porous medium; 1-6 parts of silicon dioxide, 0.1-50 parts of flavor, 0.1-50 parts of fruit powder, 0.1-50 parts of acidity regulator, and 0.1-50 parts of efficacy composition.

[0037] The present application also provides a method for preparing the composition, comprising: The sugar alcohol component, the porous medium and the auxiliary component are crushed, sieved and weighed respectively; After uniformly mixing the sugar alcohol component, the porous medium and the auxiliary components, a composition is obtained.

[0038] The present application also provides a product comprising the composition. Preferably, the product is a powder, tablet, capsule or soft candy.

[0039] The present application abandons the formula of reducing the xylitol content in the prior art, and sets the mass ratio of xylitol to the first component sugar alcohol to 300-500:100-300, that is, the xylitol content is higher than the first component sugar alcohol content. At the same time, a porous structure is adopted, and the sugar alcohol component with a specific component content and the porous medium form a stable dispersion system; in this dispersion system, due to the high xylitol content, the strong molecular polarity of xylitol helps the dispersion system to have better solubility (that is, it has a flash dissolution effect); at the same time, the porous medium in the dispersion system helps to reduce the hydrogen bonding between xylitol and the first component sugar alcohol and water, reduce the probability of thermal bonding, improve the hot melt stability of the composition, and avoid the problem of hot melt agglomeration of the composition during the preparation process.

[0040] Example 1 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0041] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0042] Example 2 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of isomalt, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0043] This embodiment provides a method for preparing a composition, comprising: Xylitol, isomalt, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, isomalt, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0044] Example 3 This embodiment provides a composition comprising 300 parts of xylitol, 300 parts of erythritol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0045] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0046] Example 4 This embodiment provides a composition comprising 500 parts of xylitol, 100 parts of erythritol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0047] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0048] Example 5 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 10 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0049] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0050] Example 6 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 30 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0051] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0052] Example 7 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 70 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0053] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0054] Example 8 This embodiment provides a composition comprising 267 parts of xylitol, 133 parts of erythritol, 60 parts of microcrystalline cellulose, 6 parts of silicon dioxide, 10 parts of sweet orange powder, 10 parts of composite bacterial powder, 20 parts of whey protein powder, 10 parts of sweet orange powder flavor, and 10 parts of citric acid. The mesh size of the sugar alcohol component is 60-200 mesh.

[0055] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0056] Example 9 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 60 parts of microcrystalline cellulose, 6 parts of silicon dioxide, 10 parts of sweet orange powder, 10 parts of composite bacterial powder, 20 parts of whey protein powder, 10 parts of sweet orange powder flavor, and 10 parts of citric acid. The mesh size of the sugar alcohol component is 60-100 mesh.

[0057] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0058] Example 10 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, and 50 parts of composite bacterial powder, wherein the composite bacterial powder is a mixture of lactic acid bacteria and Streptococcus thermophilus. The mesh size of the sugar alcohol component is 60-200 mesh.

[0059] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose, silicon dioxide and composite bacterial powder are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and composite bacterial powder were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0060] Example 11 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, and 50 parts of oligofructose. The mesh size of the sugar alcohol component is 60-200 mesh.

[0061] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose, silicon dioxide and oligofructose were crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and oligofructose were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0062] Example 12 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, and 50 parts of strawberry powder. The mesh size of the sugar alcohol component is 60-200 mesh.

[0063] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and strawberry powder respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and strawberry powder were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0064] Example 13 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, and 50 parts of citric acid. The mesh size of the sugar alcohol component is 60-200 mesh.

[0065] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose, dioxide, and silicon citrate were crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and citric acid were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0066] Example 14 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, and 50 parts of whey protein powder. The mesh size of the sugar alcohol component is 60-200 mesh.

[0067] This embodiment provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and whey protein powder were crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, and whey protein powder were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0068] Example 15 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of resistant dextrin, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0069] This comparative example provides a method for preparing a composition, comprising: Xylitol, erythritol, resistant dextrin and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, resistant dextrin, and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0070] Example 16 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of maltodextrin, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0071] This comparative example provides a method for preparing a composition, comprising: Grinding and sieving xylitol, erythritol, maltodextrin and silicon dioxide respectively; Xylitol, erythritol, maltodextrin and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0072] Example 17 This embodiment provides a composition comprising 400 parts xylitol, 200 parts erythritol, 50 parts microcrystalline cellulose, 6 parts silicon dioxide, 10 parts sweet orange powder, 5 parts composite bacterial powder, 10 parts whey protein powder, 2 parts sweet orange powder essence, and 5 parts citric acid. The mesh size of the sugar alcohol component is 80-200 mesh.

[0073] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0074] Example 18 This embodiment provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 50 parts of microcrystalline cellulose, 6 parts of silicon dioxide, 10 parts of sweet orange powder, 5 parts of composite bacterial powder, 10 parts of whey protein powder, 2 parts of sweet orange powder flavor, and 5 parts of citric acid. The mesh size of the sugar alcohol component is 100-200 mesh.

[0075] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0076] Comparative Example 1 This comparative example provides a composition comprising 400 parts of xylitol, 200 parts of maltitol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0077] This comparative example provides a method for preparing a composition, comprising: Grinding and sieving xylitol, maltitol, microcrystalline cellulose and silicon dioxide respectively; Xylitol, maltitol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0078] Comparative Example 2 This comparative example provides a composition comprising 400 parts of xylitol, 200 parts of sorbitol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0079] This comparative example provides a method for preparing a composition, comprising: Xylitol, sorbitol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, sorbitol, microcrystalline cellulose, and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0080] Comparative Example 3 This comparative example provides a composition comprising 400 parts of xylitol, 200 parts of lactitol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0081] This comparative example provides a method for preparing a composition, comprising: Xylitol, lactitol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, lactitol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0082] Comparative Example 4 This comparative example provides a composition comprising 200 parts of xylitol, 400 parts of erythritol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0083] This comparative example provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0084] Comparative Example 5 This comparative example provides a composition comprising 550 parts of xylitol, 50 parts of erythritol, 50 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0085] This comparative example provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0086] Comparative Example 6 This comparative example provides a composition comprising 400 parts of xylitol, 200 parts of isomalt, 5 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0087] This comparative example provides a method for preparing a composition, comprising: Xylitol, isomalt, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, isomalt, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0088] Comparative Example 7 This comparative example provides a composition comprising 400 parts of xylitol, 200 parts of erythritol, 80 parts of microcrystalline cellulose, and 6 parts of silicon dioxide. The mesh size of the sugar alcohol component is 60-200 mesh.

[0089] This comparative example provides a method for preparing a composition, comprising: Xylitol, erythritol, microcrystalline cellulose and silicon dioxide are crushed and sieved respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0090] Comparative Example 8 This comparative example provides a composition comprising 133 parts of xylitol, 67 parts of erythritol, 60 parts of microcrystalline cellulose, 6 parts of silicon dioxide, 100 parts of sweet orange powder, 50 parts of composite bacterial powder, 100 parts of whey protein powder, 10 parts of sweet orange powder flavor, and 10 parts of citric acid. The mesh size of the sugar alcohol component is 60-200 mesh.

[0091] This comparative example provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose and silicon dioxide were weighed according to the above mass fractions, and the weighed components were uniformly mixed to obtain a composition.

[0092] Comparative Example 9 This embodiment provides a composition comprising 400 parts xylitol, 200 parts erythritol, 50 parts microcrystalline cellulose, 6 parts silicon dioxide, 10 parts sweet orange powder, 5 parts composite bacterial powder, 10 parts whey protein powder, 2 parts sweet orange powder flavor, and 5 parts citric acid. The mesh size of the sugar alcohol component is 20-60 mesh.

[0093] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0094] Comparative Example 10 This embodiment provides a composition comprising 400 parts xylitol, 200 parts erythritol, 50 parts microcrystalline cellulose, 6 parts silicon dioxide, 10 parts sweet orange powder, 5 parts composite bacterial powder, 10 parts whey protein powder, 2 parts sweet orange powder flavor, and 5 parts citric acid. The mesh size of the sugar alcohol component is 200-250 mesh.

[0095] This embodiment provides a method for preparing a composition, comprising: Grind and sieve xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid respectively; Xylitol, erythritol, microcrystalline cellulose, silicon dioxide, sweet orange powder, compound bacterial powder, whey protein powder, sweet orange powder essence, and citric acid were weighed according to the above mass fractions, and the weighed components were evenly mixed to obtain a composition.

[0096] The following test methods of this application are specifically: Method for determining the mesh number of sugar alcohols: The manual sieving method in the second method of 0982 of the General Chapter of Part IV of the Chinese Pharmacopoeia was adopted. Specifically, an appropriate amount of sample was weighed and passed through a 60-mesh sieve and a 200-mesh sieve respectively to obtain the weight of the 60-200 mesh sieve and calculate its proportion.

[0097] Solubility test method: Take 2g of sample, pour it into a clean and dry flat-bottomed glass dish (about 7cm in diameter), spread it flat, add 10ml of warm water at 30℃~40℃, shake the glass dish lightly clockwise 3 times, observe the time, and evaluate the flash solubility effect according to the evaluation criteria in Table 1 when all the particles are immersed in water within the specified time.

[0098] Table 1 Solubility test standards

[0099] Thermal sensitivity test method: Take 2g of sample, place it in an aluminum composite bag and seal it. Place it in a hot air drying oven at 55℃±5℃ (the temperature at the time of preparation) for 3 hours, then take it out and cool it to room temperature. Open the bag to confirm the sensory properties and characterize the sample's instability index. The lower the instability index, the more stable the sample. In the following test process, no caking is represented by -. The sample is shown in the figure below. Figure 1 As shown; false agglomeration is indicated by +, and the sample diagram is as shown Figure 2 As shown; agglomeration or heat melting is indicated by ++, and the sample diagram is as follows Figure 3 shown.

[0100] Experimental Example 1-Screening of sugar alcohol types The samples in Example 1, Example 2, Comparative Example 1, Comparative Example 2 and Comparative Example 3 were respectively subjected to thermal sensitivity test and solubility test in the above manner. The test results are shown in Table 2.

[0101] Table 2 Test results during the screening of sugar alcohol types

[0102] It can be seen that only the dispersion system formed by xylitol, erythritol and microcrystalline cellulose has good solubility and heat sensitivity at the same time, indicating that only under the dispersion system of specific components can the hot melt stability of the composition be improved and the problem of hot melt agglomeration of the composition during the preparation process be avoided.

[0103] Experimental Example 2-Screening of Sugar Alcohol Ratio The samples in Example 1, Example 3, Example 4, Comparative Example 4 and Comparative Example 5 were respectively subjected to heat sensitivity test and solubility test in the above manner. The test results are shown in Table 3.

[0104] Table 3 Test results during the screening of sugar alcohol types

[0105] It can be seen that only when the ratio of xylitol to erythritol is maintained at 300-500:100-300, the dispersed system formed has both good solubility and heat sensitivity. This shows that a dispersed system with a specific weight ratio can improve the hot melt stability of the composition and avoid the problem of hot melt agglomeration of the composition during the preparation process.

[0106] Experimental Example 3-Screening of microcrystalline cellulose ratio The samples in Example 5, Example 6, Example 7, Comparative Example 6 and Comparative Example 7 were respectively subjected to thermal sensitivity test and solubility test in the above manner. The test results are shown in Table 4.

[0107] Table 4 Test results during screening of microcrystalline cellulose ratio

[0108] It can be seen that only when the ratio of the sugar alcohol component to the microcrystalline cellulose is maintained at 600:10-70, the resulting dispersion system has both good solubility and heat sensitivity. This indicates that only a dispersion system with a specific weight ratio can improve the hot melt stability of the composition and avoid the problem of hot melt agglomeration of the composition during the preparation process.

[0109] Experimental Example 4-Screening other porous media ratios The samples in Example 1, Example 15 and Example 16 were subjected to heat sensitivity test and solubility test respectively in the above manner. The test results are shown in Table 5.

[0110] Table 5 Test results during screening of other porous media ratios

[0111] It can be seen that the dispersion system formed by the sugar alcohol component and microcrystalline cellulose has both good solubility and heat sensitivity. When the porous medium is resistant dextrin or maltodextrin, the dispersion system has better solubility and slight pseudo-agglomeration. During the application of the composition, the slight pseudo-agglomeration meets the quality standards and is not significantly different from the non-agglomeration effect in terms of sensory experience. This shows that resistant dextrin, maltodextrin, and microcrystalline cellulose can all form stable dispersion systems with the sugar alcohol component.

[0112] Experimental Example 5-Screening of sugar alcohol component ratio The samples in Example 8, Comparative Example 8 of Example 9 and Comparative Example 9 were subjected to heat sensitivity test and solubility test respectively in the above manner. The test results are shown in Table 6.

[0113] Table 6 Test results during screening of sugar alcohol component ratios

[0114] It can be seen that the proportion of the sugar alcohol component in the formula in Example 8 is 76wt%, and the proportion of the sugar alcohol component in the formula in Example 9 is 55wt%. The proportion of the sugar alcohol component in the formula in Comparative Example 8 is 37wt%, and the proportion of the sugar alcohol component in the formula in Comparative Example 9 is 38wt%. Only when the proportion of the sugar alcohol component in the formula is maintained at more than 40wt% can the dispersion have both good solubility and heat sensitivity. When the proportion of the sugar alcohol component is too low, the heat sensitivity of the dispersion system is relatively stable, but the solubility is poor. This shows that a dispersion system with a specific weight fraction can improve the hot melt stability of the composition and avoid the problem of hot melt agglomeration of the composition during the preparation process.

[0115] Experimental Example 6-Addition of auxiliary components and efficacy compositions The samples in Example 10, Example 11, Example 12, Example 13, and Example 14 were respectively subjected to thermal sensitivity test and solubility test in the above manner. The test results are shown in Table 7.

[0116] Table 7 Test results of auxiliary components and functional composition addition process

[0117] It can be seen that when the mass ratio of xylitol to erythritol and the mass ratio of the sugar alcohol component to microcrystalline cellulose are met, the addition of probiotics, prebiotics, fruit powder, acidity regulator and animal and plant-derived protein to the composition can ensure that the composition has good solubility and heat sensitivity. In actual application, corresponding auxiliary components and functional compositions can be added according to actual needs.

[0118] Experimental Example 7-Screening of sugar alcohol component ratio The samples in Example 9, Example 17, Example 18, Comparative Example 9 and Comparative Example 10 were respectively subjected to thermal sensitivity test and solubility test in the above manner. The test results are shown in Table 8.

[0119] Table 6 Test results during screening of sugar alcohol component ratios

[0120] It can be seen that only when the mesh size of the sugar alcohol component is maintained between 60 and 200 mesh does the dispersion have good solubility and heat sensitivity. When the mesh size of the sugar alcohol component is less than 60 mesh or greater than 200 mesh, the dispersion system's solubility deteriorates. This indicates that only when the mesh size of the sugar alcohol component is within a specific range can the dispersion system improve the hot melt stability of the composition and avoid the problem of hot melt agglomeration during the preparation process.

[0121] In summary, the present application abandons the formula of reducing the xylitol content in the prior art, and sets the mass ratio of xylitol to the first component sugar alcohol to 300-500:100-300, that is, the xylitol content is higher than the first component sugar alcohol content. At the same time, a porous medium with a higher density is used to make the sugar alcohol component under a specific component and the porous medium form a stable dispersion system; at the same time, when the xylitol content is high, the strong molecular polarity of xylitol is used to help the dispersion system have better solubility. The addition of the porous medium helps to reduce the hydrogen bonding effect between xylitol and the first component sugar alcohol and water, reduce the probability of thermal bonding, improve the hot melt stability of the composition, and avoid the problem of hot melt agglomeration of the composition during the preparation process.

[0122] It is understandable that the above embodiments only express the preferred implementation modes of the present invention, and the description thereof is relatively specific and detailed, but it cannot be understood as limiting the patent scope of the present invention. It should be pointed out that for ordinary technicians in this field, without departing from the concept of the present invention, the above technical features can be freely combined, and several deformations and improvements can be made, all of which fall within the scope of protection of the present invention. Therefore, all equivalent changes and modifications made to the scope of the claims of the present invention should fall within the scope of coverage of the claims of the present invention.

Claims

1. A composition, characterized in that The invention comprises a sugar alcohol component, a porous medium and an auxiliary component, wherein the porous medium is microcrystalline cellulose, the sugar alcohol component comprises xylitol and a first component sugar alcohol, the first component sugar alcohol is erythritol and / or isomalt, the mass ratio of the xylitol to the first component sugar alcohol is 300-500:100-300; and the mass ratio of the sugar alcohol component to the porous medium is 400-700:10-70.

2. A composition according to claim 1, characterized in that The first component sugar alcohol is erythritol.

3. A composition according to claim 1, characterized in that The mass proportion of the sugar alcohol component in the composition is not less than 40wt%; the mesh size of the sugar alcohol component is 60-200 mesh.

4. A composition according to claim 1, characterized in that The auxiliary components include one or more of silicon dioxide, essence, fruit powder, acidity regulator, and efficacy composition.

5. A composition according to claim 4, characterized in that The invention comprises 400-700 parts of sugar alcohol components, 10-70 parts of porous media, 1-6 parts of silicon dioxide, 0.1-50 parts of flavors, 0.1-50 parts of fruit powder, 0.1-50 parts of acidity regulators and 0.1-50 parts of functional compositions.

6. A composition according to claim 4, characterized in that The efficacy composition comprises at least one of prebiotics, probiotics, and proteins of animal and plant origin.

7. A method for preparing the composition according to any one of claims 1 to 6, characterized in that: include: The sugar alcohol component, the porous medium and the auxiliary component are crushed, sieved and weighed respectively, and then mixed to obtain a composition.

8. A product, characterized in that A composition comprising any one of claims 1 to 6.

9. An application of a product, characterized in that, Use of the product as claimed in claim 8 in food and medicine.

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