GM806 gas chromatograph system and operation method
Through the design of the GM806 gas chromatograph system, the use of automated injection and high-efficiency capillary columns combined with optimized temperature control has achieved efficient separation and high-sensitivity detection of complex samples, solving the problems of poor separation effect and high detection limit of domestic gas chromatographs, and improving the practicality and stability of domestic instruments.
Patent Information
- Application Number
- CN202510866493.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-06-26
- Publication Date
- 2025-10-03
AI Technical Summary
Existing domestic gas chromatographs have problems such as poor separation effect and high detection limit when analyzing complex samples, which reduces their practicality and stability, and the field of high-precision analysis relies on imported equipment.
A GM806 gas chromatograph system was designed, including an injection module, a separation module, a detection module, and an analysis module. It used an automated injection device, multiple detectors, and a high-efficiency capillary column, combined with an optimized temperature control program, to achieve precise injection, component separation, and high-sensitivity detection.
It improves the separation efficiency and detection comprehensiveness of complex samples, enhances the adaptability and stability of the instrument, solves problems such as poor separation effect and high detection limit, and improves the performance of domestic gas chromatographs.
Smart Images

Figure CN120741692A_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of gas chromatographs, and in particular to a GM806 gas chromatograph system and an operating method. Background Art
[0002] Currently, gas chromatographs are precision instruments widely used in chemical analysis, environmental monitoring, food safety, and other fields. While existing domestically produced gas chromatographs can generally meet analytical needs, there is still room for improvement in terms of analysis speed, detection sensitivity, and ease of operation. Existing gas chromatographs often face problems such as poor separation and high detection limits when analyzing complex samples, reducing their practicality, stability, and instrument adaptability. Applications in the field of high-precision analysis mostly rely on imports, so it is necessary to develop a domestically produced gas chromatograph with superior performance to address these issues. Summary of the Invention
[0003] In response to the problems shown above, the present invention provides a GM806 gas chromatograph system and operation method to solve the problems mentioned in the background technology that the existing gas chromatographs often face when analyzing complex samples, such as poor separation effect and high detection limit, which reduces the practicality, stability and adaptability of the instrument.
[0004] A GM806 gas chromatograph system, the system comprising:
[0005] The sampling module is used to collect target samples through an automated sampling device and select a separation column for precise sampling;
[0006] A separation module, used for separating components of a target sample through a separation column;
[0007] The detection module is used to detect the separated sample components, obtain the detection data, and calibrate and verify the detection data;
[0008] The analysis module is used to analyze the test data after calibration and verification, and generate an analysis report for the target sample based on the analysis results.
[0009] Preferably, the injection module comprises:
[0010] A first determination submodule is used to determine the sample form of the target sample and the analytical properties of the target sample, and determine the sample collection condition requirements and sample collection volume requirements based on the sample form and the analytical properties of the sample;
[0011] The collection submodule is used to collect target samples through an automatic sampling device based on the sample collection condition requirements and sample collection volume requirements;
[0012] The injection submodule is used to determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
[0013] Preferably, the separation module includes:
[0014] The configuration submodule is used to determine the solubility parameters of the target sample and configure the mobile phase carrier of the target separation column according to the solubility parameters;
[0015] A loading submodule, used for loading the stationary phase carrier of the target separation column;
[0016] An optimization submodule is used to determine the high temperature tolerance of the target separation column, determine the temperature rise threshold range based on the high temperature tolerance, obtain the separation efficiency requirement for the target sample, select a target temperature value from the temperature rise threshold range based on the separation efficiency requirement, and optimize the current temperature rise parameters based on the target temperature value;
[0017] The separation submodule is used to heat the target sample with the optimized heating parameters to assist the mobile phase carrier in washing the target sample for component separation, and obtain the component distribution of multiple components of the target sample between the mobile phase and the stationary phase.
[0018] Preferably, the detection module includes:
[0019] The second determination submodule is used to determine the separation target for the target sample, select the detector type according to the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirement for each sample component according to the concentration parameters;
[0020] A third determination submodule is configured to determine the detection sensitivity requirement of the detector corresponding to each sample component according to the detection accuracy requirement for each sample component;
[0021] The detection submodule is used to set the detection parameters of the target type detector based on the detection sensitivity requirements, and detect each sample component through the set target type detector;
[0022] The analysis and calibration submodule is used to obtain the detection data of each sample component based on the detection results, perform mass spectrometry verification and quantitative analysis on each sample component, and calibrate and check the detection data based on the analysis results.
[0023] Preferably, the analysis module includes:
[0024] An analysis submodule is used to determine the ratio parameters of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameters;
[0025] The fourth determination submodule is used to determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample requirements based on the qualified conclusion of the labeled amount;
[0026] The first generation submodule is used to screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components;
[0027] The second generation submodule is used to generate an analysis optimization report for the target sample according to the optimization suggestion and upload it to the server terminal.
[0028] A method for operating a GM806 gas chromatograph comprises the following steps:
[0029] Collect target samples through an automated sampling device and select a separation column for precise injection;
[0030] Separate the target sample into components using a separation column;
[0031] Detect the separated sample components, obtain the test data, and calibrate and check the test data;
[0032] Analyze the test data after calibration and generate an analysis report for the target sample based on the analysis results.
[0033] Preferably, the method of collecting the target sample by an automated sampling device and selecting a separation column for accurate sampling includes:
[0034] Determine the sample form and analytical properties of the target sample, and determine the sample collection conditions and sample collection volume requirements based on the sample form and analytical properties of the sample;
[0035] Based on the sample collection condition requirements and sample collection volume requirements, target samples are collected through an automated sampling device;
[0036] Determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
[0037] Preferably, the component separation of the target sample by a separation column comprises:
[0038] Determine the solubility parameters of the target sample and configure the mobile phase carrier of the target separation column according to the solubility parameters;
[0039] A stationary phase carrier loaded into a target separation column;
[0040] Determine the high temperature tolerance of the target separation column, determine the temperature rise threshold range based on the high temperature tolerance, obtain the separation efficiency requirement for the target sample, select a target temperature value from the temperature rise threshold range based on the separation efficiency requirement, and optimize the current heating parameters based on the target temperature value;
[0041] The optimized heating parameters are used to heat the sample to assist the mobile phase carrier in flushing the target sample for component separation, and the component distribution of the multiple components of the target sample between the mobile phase and the stationary phase is obtained.
[0042] Preferably, the detecting of the separated sample components, obtaining the detection data, and calibrating and checking the detection data include:
[0043] Determine the separation target for the target sample, select the detector type based on the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirements for each sample component based on the concentration parameters;
[0044] Determine the detection sensitivity requirements of the detector corresponding to each sample component based on the detection accuracy requirements for each sample component;
[0045] Setting detection parameters for the target type detector based on the detection sensitivity requirements, and detecting each sample component through the set target type detector;
[0046] The detection data of each sample component is obtained based on the detection results, mass spectrometry verification and quantitative analysis are performed on each sample component, and the detection data is calibrated and checked based on the analysis results.
[0047] Preferably, the analysis of the calibration-verified test data and the generation of an analysis report of the target sample based on the analysis results include:
[0048] Determine the ratio parameter of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameter;
[0049] Determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample regulations based on the qualified conclusion of the labeled amount;
[0050] Screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components;
[0051] Generate an analysis and optimization report for the target sample based on the optimization suggestions and upload it to the server terminal.
[0052] Other features and advantages of the present invention will be described in the following description, and in part will become apparent from the description, or will be understood by practicing the present invention. The purpose and other advantages of the present invention can be realized and obtained by the structures particularly pointed out in the written description and the accompanying drawings.
[0053] The technical solution of the present invention is further described in detail below through the accompanying drawings and embodiments. BRIEF DESCRIPTION OF THE DRAWINGS
[0054] The accompanying drawings are used to provide further understanding of the present invention and constitute a part of the specification. They are used to explain the present invention together with the embodiments of the present invention and do not constitute a limitation of the present invention.
[0055] Figure 1 A schematic structural diagram of a GM806 gas chromatograph system provided by the present invention;
[0056] Figure 2 This is a structural schematic diagram of a separation module in a GM806 gas chromatograph system provided by the present invention;
[0057] Figure 3 A workflow diagram of the GM806 gas chromatograph operating method provided by the present invention;
[0058] Figure 4 This is another workflow diagram of the GM806 gas chromatograph operating method provided by the present invention. DETAILED DESCRIPTION
[0059] Exemplary embodiments will be described in detail herein, with examples illustrated in the accompanying drawings. In the following description, when referring to the drawings, identical numerals in different figures represent identical or similar elements, unless otherwise indicated. The embodiments described in the following exemplary embodiments are not intended to represent all possible embodiments consistent with the present disclosure. Rather, they are merely examples of apparatus and methods consistent with certain aspects of the present disclosure, as detailed in the appended claims.
[0060] At present, gas chromatograph is a precision instrument widely used in the fields of chemical analysis, environmental monitoring, food safety, etc. Although the gas chromatograph in the existing domestic technology can basically meet the analysis needs, there is still room for improvement in terms of analysis speed, detection sensitivity and ease of operation. When analyzing complex samples, existing gas chromatographs often face problems such as poor separation effect and high detection limit, which reduces the practicality, stability and adaptability of the instrument. However, applications in the field of high-precision analysis mostly rely on imports. Therefore, it is necessary to develop a domestically produced gas chromatograph with better performance to solve these problems. In order to solve the above problems, this embodiment discloses a GM806 gas chromatograph system.
[0061] A GM806 gas chromatograph system, such as Figure 1 As shown, the system includes:
[0062] The sampling module 101 is used to collect the target sample through an automated sampling device and select a separation column for accurate sampling;
[0063] The separation module 102 is used to separate the components of the target sample through a separation column;
[0064] The detection module 103 is used to detect the separated sample components, obtain detection data, and calibrate and verify the detection data;
[0065] The analysis module 104 is used to analyze the calibrated and verified test data and generate an analysis report of the target sample based on the analysis results.
[0066] In this embodiment, the GM806 gas chromatograph can be equipped with a variety of detectors such as FID hydrogen flame ionization detector, TCD thermal conductivity detector, PDHID and DID helium photoionization detector;
[0067] In this embodiment, a high-efficiency capillary column is used as the separation column, and an optimized temperature control program is combined to achieve component separation;
[0068] In this embodiment, the separated sample components are detected by various detectors, and high-precision detection is achieved by setting the sensitivity of the detectors for components with different concentrations.
[0069] The working principle of the above technical solution is: first, the target sample is collected through the injection module through the automatic injection device and the separation column is selected for precise injection; secondly, the separation module is used to separate the components of the target sample through the separation column; then, the separated sample components are detected based on the detection module, the detection data is obtained, and the detection data is calibrated and checked; finally, the analysis module is used to analyze the calibrated and checked detection data, and an analysis report of the target sample is generated according to the analysis results.
[0070] The beneficial effects of the above technical solution are: by using a high-efficiency capillary column and combining it with an optimized temperature control program, efficient separation of complex samples can be achieved, thereby improving separation efficiency and separation effect. At the same time, by setting the sensitivity of the detector to achieve low-concentration component detection, comprehensive and reliable detection of all components of the target sample can be achieved, thereby improving detection efficiency and comprehensiveness as well as practicality and stability. It solves the problems mentioned in the prior art that existing gas chromatographs often face when analyzing complex samples, such as poor separation effect and high detection limit, which reduces the practicality, stability and instrument adaptability.
[0071] In one embodiment, the injection module comprises:
[0072] A first determination submodule is used to determine the sample form of the target sample and the analytical properties of the target sample, and determine the sample collection condition requirements and sample collection volume requirements based on the sample form and the analytical properties of the sample;
[0073] The collection submodule is used to collect target samples through an automatic sampling device based on the sample collection condition requirements and sample collection volume requirements;
[0074] The injection submodule is used to determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
[0075] The beneficial effects of the above technical solution are: by adopting an automated sampling device, sampling can be performed quickly and accurately, human operation errors are reduced, and the degree of automation is improved. Furthermore, by selecting a target separation column, a precise and reliable separation column can be selected according to the chemical properties of the target sample to separate the components, thereby improving the adaptability of the separation column.
[0076] In this embodiment, determining the sample form of the target sample and the analytical properties of the target sample, and determining the sample collection condition requirements and sample collection volume requirements based on the sample form and the analytical properties of the sample include:
[0077] Determine the object attributes of the target sample, determine the object feature sequence of the target sample based on the object attributes, and determine the formal feature vector of the target sample based on the object feature sequence;
[0078] Determine the sample form of the target sample according to the form feature vector, and obtain sample data of the target sample;
[0079] Discretize the sample data to determine multiple attribute entropies, obtain the analysis mechanism of each attribute entropy and the analysis purpose for the target sample, and perform fitness matching between the analysis mechanism and the analysis purpose;
[0080] According to the matching results, the target attribute entropy with the largest fitness is selected as the analysis attribute for the target sample;
[0081] Determine a sample collection service type based on the sample form and analysis attributes of the sample, and obtain multiple conditional attributes corresponding to the sample collection service type;
[0082] Determine the scene space requirements and scene environment requirements of each condition attribute, and determine the sample collection definition requirements of each condition attribute based on the scene space requirements and scene environment requirements;
[0083] Integrate the sample collection definition requirements of each condition attribute to determine the sample collection condition requirements for the target sample;
[0084] Determining a plurality of analysis objects and a target indicator for each analysis object based on analysis attributes of the target sample;
[0085] Determine the task bias factor based on the target indicators of each analysis object, and determine the analysis volume requirement for each analysis object based on the task bias factor;
[0086] The analytical volume requirements for each analytical object are integrated to determine the sample collection volume requirements for the target sample.
[0087] In this embodiment, the object attributes are expressed as the expression attributes of the target sample's belonging object, such as gas attributes, solid attributes, and liquid attributes;
[0088] In this embodiment, the condition attributes are represented by specific parameters and characteristic attributes of the acquisition conditions executed when acquiring the target sample;
[0089] In this embodiment, the task bias factor is expressed as a volume bias factor for the target sample collection task when analyzing each analysis object.
[0090] The beneficial effects of the above technical solution are: by deeply analyzing the analysis task of the target sample to determine multiple analysis objects and the weight of the analysis sampling task for each analysis object, the complete volume collection of the target sample can be achieved while maximizing the satisfaction of the analysis task, thereby improving stability and reliability. Furthermore, by determining multiple collection condition attributes for the target sample and then determining the sample collection condition requirements, the stable collection of the target sample can be guaranteed, further improving stability and work efficiency.
[0091] In one embodiment, Figure 2 As shown, the separation module 102 includes:
[0092] Configuration submodule 1021, for determining the solubility parameters of the target sample and configuring the mobile phase carrier of the target separation column according to the solubility parameters;
[0093] The loading submodule 1022 is used to load the stationary phase carrier of the target separation column;
[0094] An optimization submodule 1023 is configured to determine the high temperature tolerance of the target separation column, determine a temperature increase threshold range based on the high temperature tolerance, obtain a separation efficiency requirement for the target sample, select a target temperature value within the temperature increase threshold range based on the separation efficiency requirement, and optimize the current temperature increase parameters based on the target temperature value;
[0095] The separation submodule 1024 is used to heat the target sample using the optimized heating parameters to assist the mobile phase carrier in washing the target sample to separate the components, and obtain the distribution of multiple components of the target sample between the mobile phase and the stationary phase.
[0096] The beneficial effects of the above technical solution are: by automatically optimizing the heating parameters, it is possible to ensure the separation effect of the various components of the target sample under temperature catalysis while also effectively protecting the separation column from overheating, thereby increasing the product life, reducing costs, and further improving practicality.
[0097] In this embodiment, the target temperature value is selected from the temperature rise threshold range according to the separation efficiency requirement, including:
[0098] Determining the flow rate parameters of the mobile phase carrier according to the separation efficiency requirement, and determining the instantaneous flow gain value of the mobile phase carrier at each temperature value within the temperature rise threshold range;
[0099] The stability of the mobile phase carrier at each temperature value is determined according to the carrier gas instantaneous flow gain value and the flow rate parameters of the mobile phase carrier;
[0100] Determine the relative stability of the mobile phase at each temperature value
[0101] In one embodiment, the detection module includes:
[0102] The second determination submodule is used to determine the separation target for the target sample, select the detector type according to the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirement for each sample component according to the concentration parameters;
[0103] A third determination submodule is configured to determine the detection sensitivity requirement of the detector corresponding to each sample component according to the detection accuracy requirement for each sample component;
[0104] The detection submodule is used to set the detection parameters of the target type detector based on the detection sensitivity requirements, and detect each sample component through the set target type detector;
[0105] The analysis and calibration submodule is used to obtain the detection data of each sample component based on the detection results, perform mass spectrometry verification and quantitative analysis on each sample component, and calibrate and check the detection data based on the analysis results.
[0106] The beneficial effects of the above technical solution are: by configuring a high-sensitivity detector, it is possible to detect sample components at extremely low concentrations, ensuring comprehensive separation and detection of all components of the target sample without omission, thereby improving reliability and stability.
[0107] In one embodiment, the analysis module includes:
[0108] An analysis submodule is used to determine the ratio parameters of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameters;
[0109] The fourth determination submodule is used to determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample requirements based on the qualified conclusion of the labeled amount;
[0110] The first generation submodule is used to screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components;
[0111] The second generation submodule is used to generate an analysis optimization report for the target sample according to the optimization suggestion and upload it to the server terminal.
[0112] The beneficial effect of the above technical solution is: by determining the qualified results of the labeled amount of each sample component to conduct sample suitability assessment, the qualified components and unqualified components of the target sample can be comprehensively determined, and then effective optimization measures can be generated for the unqualified components, thereby ensuring the subsequent optimization qualification of the target sample.
[0113] In one embodiment, this embodiment also discloses a method for operating a GM806 gas chromatograph, such as Figure 3 As shown, the following steps are included:
[0114] Step S301: Collect target samples through an automated sampling device and select a separation column for precise sampling;
[0115] Step S302, separating the target sample into components using a separation column;
[0116] Step S303: Detect the separated sample components, obtain detection data, and calibrate and check the detection data;
[0117] Step S304: Analyze the calibrated and verified test data, and generate an analysis report for the target sample based on the analysis results.
[0118] The working principle and beneficial effects of the above technical solution have been explained in the system embodiment and will not be repeated here.
[0119] In one embodiment, the step of collecting a target sample by an automated sampling device and selecting a separation column for precise sampling comprises:
[0120] Determine the sample form and analytical properties of the target sample, and determine the sample collection conditions and sample collection volume requirements based on the sample form and analytical properties of the sample;
[0121] Based on the sample collection condition requirements and sample collection volume requirements, target samples are collected through an automated sampling device;
[0122] Determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
[0123] In one embodiment, separating the components of the target sample by using a separation column comprises:
[0124] Determine the solubility parameters of the target sample and configure the mobile phase carrier of the target separation column according to the solubility parameters;
[0125] A stationary phase carrier loaded into a target separation column;
[0126] Determine the high temperature tolerance of the target separation column, determine the temperature rise threshold range based on the high temperature tolerance, obtain the separation efficiency requirement for the target sample, select a target temperature value from the temperature rise threshold range based on the separation efficiency requirement, and optimize the current heating parameters based on the target temperature value;
[0127] The optimized heating parameters are used to heat the sample to assist the mobile phase carrier in flushing the target sample for component separation, and the component distribution of the multiple components of the target sample between the mobile phase and the stationary phase is obtained.
[0128] In one embodiment, Figure 4 As shown, the detection of the separated sample components, obtaining the detection data, and calibrating and checking the detection data include:
[0129] Step S401: Determine the separation target for the target sample, select the detector type according to the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirement for each sample component based on the concentration parameters;
[0130] Step S402: determining the detection sensitivity requirement of the detector corresponding to each sample component according to the detection accuracy requirement for each sample component;
[0131] Step S403: setting detection parameters for the target type detector based on the detection sensitivity requirement, and detecting each sample component through the set target type detector;
[0132] Step S404: Acquire detection data of each sample component according to the detection results, perform mass spectrometry verification and quantitative analysis on each sample component, and calibrate and check the detection data according to the analysis results.
[0133] In one embodiment, analyzing the calibration-verified test data and generating an analysis report of the target sample based on the analysis results includes:
[0134] Determine the ratio parameter of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameter;
[0135] Determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample regulations based on the qualified conclusion of the labeled amount;
[0136] Screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components;
[0137] Generate an analysis and optimization report for the target sample based on the optimization suggestions and upload it to the server terminal.
[0138] Those skilled in the art should understand that the first and second in the present invention simply refer to different application stages.
[0139] Other embodiments of the present disclosure will readily occur to those skilled in the art after considering the specification and practicing the disclosure herein. This application is intended to cover any variations, uses, or adaptations of the present disclosure that follow from the general principles of the present disclosure and include common knowledge or customary techniques in the art not disclosed herein. The description and examples are to be considered as exemplary only, with the true scope and spirit of the present disclosure being indicated by the following claims.
[0140] It should be understood that the present disclosure is not limited to the exact structures that have been described above and shown in the drawings, and that various modifications and changes can be made without departing from the scope thereof. The scope of the present disclosure is limited only by the appended claims.
Claims
1. A GM806 gas chromatograph system, characterized in that: The system includes: The sampling module is used to collect target samples through an automated sampling device and select a separation column for precise sampling; A separation module, used for separating components of a target sample through a separation column; The detection module is used to detect the separated sample components, obtain the detection data, and calibrate and verify the detection data; The analysis module is used to analyze the test data after calibration and verification, and generate an analysis report for the target sample based on the analysis results.
2. The GM806 gas chromatograph system according to claim 1, characterized in that: The injection module comprises: A first determination submodule is used to determine the sample form of the target sample and the analytical properties of the target sample, and determine the sample collection condition requirements and sample collection volume requirements based on the sample form and the analytical properties of the sample; The collection submodule is used to collect target samples through an automatic sampling device based on the sample collection condition requirements and sample collection volume requirements; The injection submodule is used to determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
3. The GM806 gas chromatograph system according to claim 1, characterized in that: The separation module comprises: The configuration submodule is used to determine the solubility parameters of the target sample and configure the mobile phase carrier of the target separation column according to the solubility parameters; A loading submodule, used for loading the stationary phase carrier of the target separation column; An optimization submodule is used to determine the high temperature tolerance of the target separation column, determine the temperature rise threshold range based on the high temperature tolerance, obtain the separation efficiency requirement for the target sample, select a target temperature value from the temperature rise threshold range based on the separation efficiency requirement, and optimize the current temperature rise parameters based on the target temperature value; The separation submodule is used to heat the target sample with the optimized heating parameters to assist the mobile phase carrier in washing the target sample for component separation, and obtain the component distribution of multiple components of the target sample between the mobile phase and the stationary phase.
4. The GM806 gas chromatograph system according to claim 1, characterized in that: The detection module includes: The second determination submodule is used to determine the separation target for the target sample, select the detector type according to the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirement for each sample component according to the concentration parameters; A third determination submodule is configured to determine the detection sensitivity requirement of the detector corresponding to each sample component according to the detection accuracy requirement for each sample component; The detection submodule is used to set the detection parameters of the target type detector based on the detection sensitivity requirements, and detect each sample component through the set target type detector; The analysis and calibration submodule is used to obtain the detection data of each sample component based on the detection results, perform mass spectrometry verification and quantitative analysis on each sample component, and calibrate and check the detection data based on the analysis results.
5. The GM806 gas chromatograph system according to claim 1, characterized in that: The analysis module includes: An analysis submodule is used to determine the ratio parameters of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameters; The fourth determination submodule is used to determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample requirements based on the qualified conclusion of the labeled amount; The first generation submodule is used to screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components; The second generation submodule is used to generate an analysis optimization report for the target sample according to the optimization suggestion and upload it to the server terminal.
6. A GM806 gas chromatograph operating method, characterized in that: The following steps are involved: Collect target samples through an automated sampling device and select a separation column for precise injection; Separate the target sample into components using a separation column; Detect the separated sample components, obtain the test data, and calibrate and check the test data; Analyze the test data after calibration and generate an analysis report for the target sample based on the analysis results.
7. The GM806 gas chromatograph operating method according to claim 6, characterized in that: The method of collecting the target sample by the automated sampling device and selecting a separation column for accurate sampling comprises: Determine the sample form and analytical properties of the target sample, and determine the sample collection conditions and sample collection volume requirements based on the sample form and analytical properties of the sample; Based on the sample collection condition requirements and sample collection volume requirements, target samples are collected through an automated sampling device; Determine the sample properties of the target sample, select the target separation column according to the sample properties, and accurately inject the target sample into the target separation column.
8. The GM806 gas chromatograph operating method according to claim 6, characterized in that: The component separation of the target sample by the separation column comprises: Determine the solubility parameters of the target sample and configure the mobile phase carrier of the target separation column according to the solubility parameters; A stationary phase carrier loaded into a target separation column; Determine the high temperature tolerance of the target separation column, determine the temperature rise threshold range based on the high temperature tolerance, obtain the separation efficiency requirement for the target sample, select a target temperature value from the temperature rise threshold range based on the separation efficiency requirement, and optimize the current heating parameters based on the target temperature value; The optimized heating parameters are used to heat the sample to assist the mobile phase carrier in flushing the target sample for component separation, and the component distribution of the multiple components of the target sample between the mobile phase and the stationary phase is obtained.
9. The GM806 gas chromatograph operating method according to claim 6, characterized in that: The detecting of the separated sample components, obtaining the detection data, and calibrating and checking the detection data include: Determine the separation target for the target sample, select the detector type based on the separation target, determine the concentration parameters of each sample component, and determine the detection accuracy requirements for each sample component based on the concentration parameters; Determine the detection sensitivity requirements of the detector corresponding to each sample component based on the detection accuracy requirements for each sample component; Setting detection parameters for the target type detector based on the detection sensitivity requirements, and detecting each sample component through the set target type detector; The detection data of each sample component is obtained based on the detection results, mass spectrometry verification and quantitative analysis are performed on each sample component, and the detection data is calibrated and checked based on the analysis results.
10. The GM806 gas chromatograph operating method according to claim 6, characterized in that: The analysis of the calibration and verification test data and the generation of an analysis report of the target sample based on the analysis results include: Determine the ratio parameter of each sample component based on the calibration and verification test data, and perform quantitative analysis based on the ratio parameter; Determine the qualified conclusion of the labeled amount of each sample component based on the analysis results and preset requirements, and determine the compatibility of the target sample with the sample regulations based on the qualified conclusion of the labeled amount; Screen out unqualified sample components based on the compatibility between the target sample and the sample requirements, and generate optimization suggestions based on the unqualified sample components; Generate an analysis and optimization report for the target sample based on the optimization suggestions and upload it to the server terminal.
