Method for producing xylooligosaccharides from camellia oleifera shell by buffer catalysis

By combining the hydrolysis of camellia shells catalyzed by citric acid-sodium citrate solution with activated carbon column chromatography, the problem of low yield of xylooligosaccharides was solved, achieving efficient production and environmentally friendly processes, and improving product yield and equipment corrosion resistance.

CN122404430APending Publication Date: 2026-07-17LINYI UNIVERSITY
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
LINYI UNIVERSITY
Filing Date
2026-05-13
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for producing xylooligosaccharides suffer from low yield, numerous byproducts, and poor reaction controllability. In particular, traditional pretreatment methods are insufficient to efficiently break down the structure of raw materials when camellia shells have a dense structure.

Method used

Citric acid-sodium citrate solution was used as the catalytic system to hydrolyze camellia oleifera shells at 150-190℃ for 20-60 minutes. Combined with activated carbon column chromatography and spray drying, the hydrolysis intensity and pH value were precisely controlled to inhibit the further degradation of xylooligosaccharides.

Benefits of technology

It significantly improves the yield of xylooligosaccharides, enhances raw material utilization and equipment corrosion resistance, reduces equipment investment and operation and maintenance costs, and meets the requirements of green chemistry and sustainable development.

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Abstract

本申请提供一种缓冲液催化油茶壳生产低聚木糖的方法,该方法中引入柠檬酸‑柠檬酸钠缓冲体系作为催化体系,利用其共轭酸碱对的协同作用,在提供催化所需H+的同时精确调控水解反应强度,有效抑制低聚木糖的过度降解,显著提升低聚木糖得率;本申请所使用的柠檬酸和柠檬酸钠为食品级,安全可生物降解;本申请中的水解反应在高固液比下操作,提升原料利用率和单位体积产能。
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