Chemical synthetic material powder purification and separation device

Abstract

The utility model relates to the technical field of chemical equipment, and discloses a chemical synthetic material powder purification and separation device which comprises a supporting frame, the top output end of the supporting frame is fixedly connected with a reaction kettle, the top of the reaction kettle is fixedly connected with a motor, and the bottom output end of the motor penetrates through the top of the inner wall of the reaction kettle. The device is compact and reasonable in structural design, efficient mixing and reaction of raw materials and precipitants can be achieved through the integrated stirring and centrifugal separation technology, the raw materials and the precipitants can be efficiently mixed and reacted, the reaction efficiency is improved, the production cost is reduced, and the production efficiency is improved. By adjusting the addition amount of raw materials and precipitants, stirring and separation conditions and the like, different purification and separation requirements can be easily met, the vertical space is fully utilized, the occupied space of the equipment is reduced, and the problems that in the prior art, the process of treating complex mixtures is complex, and when special mixtures are separated, flexible adjustment cannot be conducted, and the separation efficiency is high are solved. And the occupied space is large.

Description

Technical Field

[0001] The utility model relates to the technical field of chemical equipment, in particular to a chemical synthesis material powder purification and separation device. Background Art

[0002] Purification and separation of chemically synthesized material powders is a crucial technology in the chemical industry, aimed at isolating the target product from the reaction mixture, removing impurities, and improving the purity and quality of the product. Traditional purification and separation methods include filtration, distillation, and crystallization, but these methods are often inefficient and complex when dealing with complex mixtures or when high-purity products are required. With the development of the chemical industry, the purity requirements for chemically synthesized material powders are becoming increasingly stringent, necessitating the development of more efficient and automated purification and separation equipment.

[0003] When processing complex mixtures, existing equipment has complicated procedures and cannot be flexibly adjusted when separating special types of mixtures, such as centrifugal speed, dosage of reaction reagents, etc., and existing equipment takes up a large space. For this reason, we propose a chemical synthetic material powder purification and separation device. Utility Model Content

[0004] (1) Technical problems solved

[0005] In view of the deficiencies in the prior art, the present invention provides a chemical synthesis material powder purification and separation device to solve the above-mentioned problems.

[0006] (2) Technical solution

[0007] To achieve the above-mentioned objectives, the present invention provides the following technical solutions: a chemical synthetic material powder purification and separation device, comprising a support frame, the top output end of the support frame is fixedly connected to a reactor, the top of the reactor is fixedly connected to a motor, the bottom output end of the motor passes through the top of the inner wall of the reactor, the bottom output end of the motor is fixedly connected to a stirring roller, and the bottom output end of the reactor is fixedly connected to a connecting valve.

[0008] Preferably, a precipitant box is fixedly connected to the outer wall of one side of the support frame, a water pump is fixedly connected to the top output end of the precipitant box, a connecting pipe is fixedly connected to the top output end of the water pump, a quantitative valve is fixedly connected to the output end of the connecting pipe away from the water pump, a second connecting pipe is fixedly connected to the top output end of the quantitative valve away from the quantitative valve, and the output end of the second connecting pipe on the side away from the quantitative valve is fixedly connected to the output end of the top of the reactor close to the motor.

[0009] Preferably, the support frame is fixedly connected to the outer wall of the side away from the precipitant box, the top output end of the raw material box is fixedly connected to the pressure pump, the top output end of the pressure pump is fixedly connected to the third connecting pipe, the output end of the third connecting pipe away from the pressure pump is fixedly connected to the second metering valve, the top output end of the second metering valve is fixedly connected to the fourth connecting pipe, and the output end of the fourth connecting pipe on the side away from the second metering valve is fixedly connected to the output end of the top of the reactor on the side away from the second connecting pipe.

[0010] Preferably, the bottom of the inner wall of the support frame is fixedly connected to a drain cover, the inner wall of the support frame close to one end of the drain cover is fixedly connected to a second motor, and the top output end of the second motor passes through the bottom of the inner wall of the drain cover, the bottom output end of the connecting valve is sleeved with a bearing, the top output end of the second motor is fixedly connected to a separation drum, and the top output end of the separation drum is sleeved on one end of the outer wall of the bearing.

[0011] Preferably, an injection port is provided on the outer wall of the precipitant box away from the support frame, and a second injection port is provided on the outer wall of the raw material box away from the support frame.

[0012] Preferably, a controller is fixedly connected to the outer wall of one end of the support frame, and a drain valve is fixedly connected to the outer wall of one end of the drain cover.

[0013] Preferably, a plurality of holes are opened on the outer wall of one end of the separation drum and pass through one end of the inner wall of the separation drum.

[0014] (3) Beneficial effects

[0015] Compared with the prior art, the present invention provides a chemical synthesis material powder purification and separation device with the following features:

[0016] Beneficial effects:

[0017] 1. This chemical synthetic material powder purification and separation device integrates stirring and centrifugal separation technologies. The device can achieve efficient mixing and reaction of raw materials and precipitants, as well as rapid separation of solids and liquids in the mixture, significantly improving the purification and separation efficiency.

[0018] 2. This chemical synthetic material powder purification and separation device is suitable for processing different types of chemical synthetic material powder mixtures. By adjusting the amount of raw materials and precipitants added, stirring and separation conditions, etc., it can easily adapt to different purification and separation needs.

[0019] 3. The chemical synthetic material powder purification and separation device fully utilizes the upper and lower spaces and reduces the space occupied by the equipment. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] Figure 1 This is a schematic cross-sectional view of the structure of the utility model;

[0021] Figure 2 This is a front view schematic diagram of the utility model;

[0022] Figure 3 It is a rear schematic diagram of the utility model.

[0023] In the figure: 1. Support frame; 2. Reactor; 3. Motor; 4. Stirring roller; 5. Connecting valve; 6. Precipitant tank; 7. Water pump; 8. Connecting pipe; 9. Dosing valve; 10. Second connecting pipe; 11. Raw material tank; 12. Pressure pump; 13. Third connecting pipe; 14. Second dosing valve; 15. Fourth connecting pipe; 16. Drain cover; 17. Second motor; 18. Bearing; 19. Separation drum; 20. Injection port; 21. Second injection port; 22. Controller; 23. Drain valve; 24. Round hole. DETAILED DESCRIPTION

[0024] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.

[0025] See also Figure 1-3 A chemical synthetic material powder purification and separation device includes a support frame 1, the top output end of the support frame 1 is fixedly connected to a reactor 2, the top of the reactor 2 is fixedly connected to a motor 3, the bottom output end of the motor 3 passes through the top of the inner wall of the reactor 2, the bottom output end of the motor 3 is fixedly connected to a stirring roller 4, and the bottom output end of the reactor 2 is fixedly connected to a connecting valve 5.

[0026] Furthermore, a precipitant tank 6 is fixedly connected to the outer wall of one side of the support frame 1, a water pump 7 is fixedly connected to the top output end of the precipitant tank 6, a connecting pipe 8 is fixedly connected to the top output end of the water pump 7, the connecting pipe 8 is fixedly connected to the output end away from the water pump 7, a metering valve 9 is fixedly connected to the top output end of the metering valve 9, and a second connecting pipe 10 is fixedly connected to the output end of the second connecting pipe 10 away from the metering valve 9 on the side fixedly connected to the output end of the top of the reactor 2 near the motor 3.

[0027] Furthermore, the outer wall of the support frame 1 away from the precipitant tank 6 is fixedly connected to a raw material box 11, the top output end of the raw material box 11 is fixedly connected to a pressure pump 12, the top output end of the pressure pump 12 is fixedly connected to a third connecting pipe 13, the output end of the third connecting pipe 13 away from the pressure pump 12 is fixedly connected to a second metering valve 14, the top output end of the second metering valve 14 is fixedly connected to a fourth connecting pipe 15, and the output end of the fourth connecting pipe 15 away from the second metering valve 14 is fixedly connected to the output end of the top of the reactor 2 away from the second connecting pipe 10.

[0028] Furthermore, a drainage cover 16 is fixedly connected to the bottom of the inner wall of the support frame 1, and a second motor 17 is fixedly connected to the inner wall of one end of the support frame 1 close to the drainage cover 16, and the top output end of the second motor 17 passes through the bottom of the inner wall of the drainage cover 16, and the bottom output end of the connecting valve 5 is sleeved with a bearing 18, and the top output end of the second motor 17 is fixedly connected to a separation drum 19, and the top output end of the separation drum 19 is sleeved on one end of the outer wall of the bearing 18.

[0029] Furthermore, an injection port 20 is provided on the outer wall of the precipitant box 6 away from the support frame 1 , and a second injection port 21 is provided on the outer wall of the raw material box 11 away from the support frame 1 .

[0030] Furthermore, a controller 22 is fixedly connected to the outer wall of one end of the support frame 1 , and a drain valve 23 is fixedly connected to the outer wall of one end of the drain cover 16 .

[0031] Furthermore, a plurality of openings 24 are formed on the outer wall of one end of the separation drum 19 , and the openings 24 penetrate through one end of the inner wall of the separation drum 19 .

[0032] Working principle: First, the raw materials are quantitatively added to the reactor 2 through the raw material box 11, the pressure pump 12, the third connecting pipe 13, the second metering valve 14 and the fourth connecting pipe 15. The precipitant is quantitatively added to the reactor 2 through the precipitant box 6, the water pump 7, the connecting pipe 8, the metering valve 9 and the second connecting pipe 10. The motor 3 drives the stirring roller 4 to rotate in the reactor 2, so that the raw materials and the precipitant are fully mixed and react. After the reaction is completed, the mixture enters the separation drum 19 through the connecting valve 5, and the separation drum 19 is driven to rotate by the second motor 17 and the bearing 18 at the output end of the top of the separation drum 19. The solid and liquid in the mixture are separated by centrifugal force. The separated liquid is discharged through the drain cover 16 and the drain valve 23, and the solid part remains in the separation drum 19 and is further dried or processed through a number of holes 24 opened therein. The controller 22 is used to control the operation of the entire device, including the amount of raw materials and precipitant added, the stirring speed, the rotation speed of the separation drum, etc.

[0033] Although the embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and variations may be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A chemical synthesis material powder purification and separation device, comprising a support frame (1), characterized in that: The top output end of the support frame (1) is fixedly connected to a reactor (2), the top of the reactor (2) is fixedly connected to a motor (3), the bottom output end of the motor (3) passes through the top of the inner wall of the reactor (2), the bottom output end of the motor (3) is fixedly connected to a stirring roller (4), and the bottom output end of the reactor (2) is fixedly connected to a connecting valve (5).

2. The chemical synthesis material powder purification and separation device according to claim 1, characterized in that: A precipitant box (6) is fixedly connected to an outer wall of one side of the support frame (1), a water pump (7) is fixedly connected to the top output end of the precipitant box (6), a connecting pipe (8) is fixedly connected to the top output end of the water pump (7), an output end of the connecting pipe (8) away from the water pump (7) is fixedly connected to a quantitative valve (9), a second connecting pipe (10) is fixedly connected to the top output end of the quantitative valve (9), and an output end of the second connecting pipe (10) away from the quantitative valve (9) is fixedly connected to an output end of the top of the reactor (2) near the motor (3).

3. The chemical synthesis material powder purification and separation device according to claim 2, characterized in that: The outer wall of the support frame (1) on the side away from the precipitant tank (6) is fixedly connected to a raw material box (11), the top output end of the raw material box (11) is fixedly connected to a pressure pump (12), the top output end of the pressure pump (12) is fixedly connected to a third connecting pipe (13), the output end of the third connecting pipe (13) on the side away from the pressure pump (12) is fixedly connected to a second metering valve (14), the top output end of the second metering valve (14) is fixedly connected to a fourth connecting pipe (15), and the output end of the fourth connecting pipe (15) on the side away from the second metering valve (14) is fixedly connected to the output end of the top of the reactor (2) on the side away from the second connecting pipe (10).

4. The chemical synthesis material powder purification and separation device according to claim 1, characterized in that: The bottom of the inner wall of the support frame (1) is fixedly connected to a drainage cover (16), the inner wall of one end of the support frame (1) close to the drainage cover (16) is fixedly connected to a second motor (17), and the top output end of the second motor (17) passes through the bottom of the inner wall of the drainage cover (16), the bottom output end of the connecting valve (5) is sleeved with a bearing (18), the top output end of the second motor (17) is fixedly connected to a separation drum (19), and the top output end of the separation drum (19) is sleeved on one end of the outer wall of the bearing (18).

5. The chemical synthesis material powder purification and separation device according to claim 3, characterized in that: An injection port (20) is provided on the outer wall of the precipitant box (6) on the side away from the support frame (1), and a second injection port (21) is provided on the outer wall of the raw material box (11) on the side away from the support frame (1).

6. The chemical synthesis material powder purification and separation device according to claim 4, characterized in that: A controller (22) is fixedly connected to the outer wall of one end of the support frame (1), and a drain valve (23) is fixedly connected to the outer wall of one end of the drain cover (16).

7. The chemical synthesis material powder purification and separation device according to claim 4, characterized in that: A plurality of (24) are provided on the outer wall of one end of the separation drum (19), and the (24) penetrates one end of the inner wall of the separation drum (19).

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