A multi-effect facial mask essence and preparation method thereof

Abstract

The present invention relates to a multi-effect facial mask essence and a preparation method thereof, and belongs to the technical field of skin care products. The multi-effect facial mask essence comprises 0.3-0.6% calcium acetate, 0.3-0.6% magnesium chloride, 2.1-3.6% adenosine triphosphate, 1.5-2.5% sodium hyaluronate cross-linked polymer, 1.5-2.0% pentylene glycol, 1.2-2.6% iota carrageenan, 0.1-0.5% hydrogenated castor oil and the balance deionized water. The present invention also discloses a preparation method of the multi-effect facial mask essence. Beneficial effect: With the high permeability of ions and the catalytic activity of adenosine triphosphate on oils and fatty acids, the two work together to whiten and moisturize, deeply fade acne marks, and are gentle and non-irritating.

Description

Technical Field

[0001] The invention belongs to the technical field of skin care products, and particularly relates to a multi-effect facial mask essence and a preparation method thereof. Background Art

[0002] With the worsening of air pollution, the accelerated pace of life, and the emergence of irregular work and rest, the phenomenon of acne on people's faces has become more and more common. How to remove acne scars has become a problem that often troubles people. Acne scars themselves are a repair response of the human body to tissue damage. The main repair process is that after the acne is inflamed and worn, the skin epidermis is defective. The epidermis in this area cannot regenerate and will be replaced by dermal fibroblasts, collagen, and proliferating blood vessels, thus acne scars appear. People often regard acne scars as unsightly, so they will choose some targeted drugs to eliminate acne scars on the face, but improper use will often have some inevitable effects and allergies on the face.

[0003] In view of this, it is necessary to provide a multi-effect facial mask essence that can deeply fade facial acne marks and can achieve whitening and moisturizing effects. Therefore, this patent relates to a multi-effect facial mask essence and a preparation method thereof to solve the above-mentioned technical gap problem. Summary of the invention

[0004] In order to solve the above technical problems, the present invention provides a multi-effect facial mask essence, which relies on the high permeability of ions and the catalytic activity of adenine nucleoside triphosphate on oils and fatty acids. The two work together to achieve whitening and moisturizing, deeply lighten acne marks, and are gentle and non-irritating.

[0005] The technical solution of the present invention to solve the above technical problems is as follows: a multi-effect facial mask essence liquid comprises 0.3-0.6% calcium acetate, 0.3-0.6% magnesium chloride, 2.1-3.6% adenosine triphosphate, 1.5-2.5% sodium hyaluronate cross-linked polymer, 1.5-2.0% pentylene glycol, 1.2-2.6% iota carrageenan, 0.1-0.5% hydrogenated castor oil and the remainder deionized water.

[0006] Beneficial effects: With the high permeability of ions and the catalytic activity of adenine nucleoside triphosphate on oils and fatty acids, the two work together to achieve whitening and moisturizing effects, deeply lighten acne marks, and are gentle and non-irritating.

[0007] Principle description:

[0008] Calcium acetate and magnesium chloride micron powders are used to provide active ions, and sodium hyaluronate cross-linked polymer, hydrogenated castor oil, and pentylene glycol are added step by step to play the role of film-forming, emulsification, and preservation. 2+ Mg 2+The well-adapted iota carrageenan is used to increase the viscosity of the liquid system, and finally adenosine triphosphate is added as a catalytic activator for facial oils, which can effectively accelerate the metabolism of oils and play a role in whitening, moisturizing, and deeply fading acne marks.

[0009] Based on the above technical solution, the present invention can also be improved as follows.

[0010] Furthermore, it is composed of the following components in mole percentage: 0.4% calcium acetate, 0.4% magnesium chloride, 2.5% adenosine triphosphate, 2.1% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.8% iota carrageenan, 0.3% hydrogenated castor oil and the balance deionized water.

[0011] Beneficial effects: The multi-effect facial mask essence obtained by the above-mentioned composition combination has good effects, and several effective components are fully mixed to exert good effects.

[0012] Furthermore, it is composed of the following components in mole percentage: 0.3% calcium acetate, 0.3% magnesium chloride, 2.1% adenosine triphosphate, 1.5% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.3% iota carrageenan, 0.2% hydrogenated castor oil and the balance deionized water.

[0013] Beneficial effects: The above composition is the best combination, and the obtained multi-effect facial mask essence has the best effect, so that several effective components are fully mixed to exert the best effect.

[0014] To achieve the second purpose of the present invention, a method for preparing a multi-effect facial mask essence is provided, comprising the following steps:

[0015] S1: adding 0.3-0.6 mol% of calcium acetate and 0.3-0.6 mol% of magnesium chloride into a planetary ball mill to obtain a micron-sized mixed powder, and then adding the obtained mixed powder into deionized water, stirring until the solid matter is completely dissolved, to obtain a solution A;

[0016] S2: adding 1.5-2.5 mol% of sodium hyaluronate cross-linked polymer and 0.1-0.5 mol% of hydrogenated castor oil to the solution A obtained in step S1, transferring to a high-pressure reactor, reacting for 3-4 hours at 75-90° C. and 5-10 MPa, then lowering the temperature to 45° C.-55° C., slowly adding 1.5-2.0 mol% of pentanediol, and stirring thoroughly until the solution becomes transparent, thereby obtaining a solution B;

[0017] S3: adding 1.2-2.6 mol% of iota carrageenan to the solution B obtained in step S2, mixing and stirring to obtain solution C;

[0018] S4: adding 2.1-3.6 mol% of adenine nucleoside triphosphate to the solution C obtained in step S3, and slowly stirring until the solid powder is completely dissolved to prepare a multi-effect facial mask essence.

[0019] Beneficial effects: The prepared facial mask essence can effectively accelerate oil metabolism, play the role of whitening, moisturizing, and deeply fading acne marks; the preparation method is simple, low-cost, and convenient for mass production. Furthermore, in step S1, the orbital speed of the planetary ball mill is 100 to 200 revolutions, the rotation speed is 150 to 250 revolutions, and the time is 10 to 20 minutes.

[0020] Beneficial effect: In the above steps, a planetary ball mill is used to grind calcium acetate and magnesium chloride solids under the parameter conditions, so that the solid powder reaches a micrometer scale, which is helpful for the subsequent dissolution and subsequent reactions.

[0021] Further, in step S3, the stirring rate is 800 to 1000 revolutions per minute, and the time is 0.5 to 1 hour.

[0022] Beneficial effects: Use with Ca 2+ Mg 2+ The iota carrageenan with good adaptability is used as a thickener, so that it can be evenly mixed with the above solution without destroying the ion activity, and its thickening effect can be fully exerted. Stirring under this parameter is helpful for the subsequent dissolution and subsequent reaction.

[0023] Furthermore, the method further comprises a degassing process, wherein the multi-effect facial mask essence is added into a vacuum degassing tank for liquid degassing.

[0024] Beneficial effects: Remove the bubbles remaining in the mask essence and ensure the uniform stability within the essence system to facilitate bottling in the subsequent process.

[0025] Furthermore, the vacuum degree of the vacuum degassing tank is 0.08Mpa to 0.095Mpa.

[0026] Beneficial Effects: Guaranteed to effectively remove residual bubbles in the mask essence. DETAILED DESCRIPTION

[0027] The principles and features of the present invention are described below. The examples given are only used to explain the present invention and are not used to limit the scope of the present invention.

[0028] Example 1

[0029] The multi-effect facial mask essence of this embodiment is prepared from the following components in molar percentage: 0.4% calcium acetate, 0.4% magnesium chloride, 2.5% adenosine triphosphate, 2.1% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.8% iota carrageenan, 0.3% hydrogenated castor oil and the balance deionized water.

[0030] The above-mentioned calcium acetate and magnesium chloride are added to a planetary ball mill, and the revolution speed is set to 150 rpm, the rotation speed is set to 200 rpm, and the time is controlled at 15 min to obtain a micron-sized mixed powder and add it to deionized water, and stir until the solid is completely dissolved; then sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the solution and transferred to a high-pressure reactor, the pressure of which is controlled at 8 MPa, and the reactor is placed in an oven, the temperature is controlled at 80°C, and the reaction lasts for 3 hours; after the reaction is completed, the temperature is lowered to 45°C, pentanediol is slowly added, and the mixture is fully stirred until the solution becomes transparent; iota carrageenan is added to the transparent solution, and a magnetic stirrer is used to mix, the stirring rate is controlled at 850 rpm, and the stirring time is controlled at 0.5 h; when the viscosity of the solution is 250 mPa·s, adenosine triphosphate is added, and the mixture is slowly stirred until the solid powder is completely dissolved to obtain a multi-effect facial mask essence. Finally, the essence is placed in a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085Mpa, and finally a finished product of a multi-effect facial mask essence is obtained.

[0031] The following method was used to test the performance of the multi-effect facial mask essence:

[0032] A group of three volunteers were used as a reference. The same amount of multi-effect mask essence was evenly applied to the designated areas of the volunteers' faces (including acne marks) once a day for seven days. The time it took for the essence to be completely absorbed each time, the facial moisturizing effect reported by the volunteers, and the fading of acne marks after seven days were recorded.

[0033]

[0034] Example 2

[0035] This embodiment is different from embodiment 1 in that the multi-effect facial mask essence is prepared by changing the amount of each component in the experimental steps. The main process is as follows:

[0036] The multi-effect facial mask essence is prepared from the following components in molar percentage: 0.3% calcium acetate, 0.3% magnesium chloride, 2.1% adenosine triphosphate, 1.5% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.3% iota carrageenan, 0.2% hydrogenated castor oil and the balance deionized water.

[0037] The preparation process and parameters of this embodiment are:

[0038] Calcium acetate and magnesium chloride are added to a planetary ball mill, the orbital speed is set to 150 rpm, the rotation speed is set to 200 rpm, the running time is 15 min, and then deionized water is added and stirred until dissolved; sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the above solution and transferred to a high-pressure reactor, the internal pressure of which is controlled at 8 MPa, the oven temperature is set at 80°C, and the reaction is continued for 3 hours; after the reaction is completed, the temperature is lowered to 45°C, pentanediol is slowly added and dissolved; iota carrageenan is added to the above solution, the magnetic stirrer speed is 850 rpm, and the stirring time is 0.5 h; when the solution viscosity is 250 mPa·s, adenosine triphosphate is added, and it is slowly stirred until it is completely dissolved to obtain a multi-effect facial mask essence; finally, it is loaded into a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085 MPa to finally obtain a finished multi-effect facial mask essence.

[0039] The multi-effect facial mask essence of this embodiment is prepared according to the steps of the present invention, and its performance test method is the same as that of Example 1, and the test results are as follows:

[0040]

[0041] Example 3

[0042] This embodiment is different from embodiment 1 in that the multi-effect facial mask essence is prepared by changing the amount of each component in the experimental steps. The main process is as follows:

[0043] The multi-effect facial mask essence is prepared from the following components in molar percentage: 0.6% calcium acetate, 0.6% magnesium chloride, 3.5% adenosine triphosphate, 2.4% sodium hyaluronate cross-linked polymer, 2.0% pentylene glycol, 2.4% iota carrageenan, 0.2% hydrogenated castor oil and the balance deionized water.

[0044] The preparation process and parameters of this embodiment are:

[0045] Calcium acetate and magnesium chloride are added to a planetary ball mill, the orbital speed is set to 150 rpm, the rotation speed is set to 200 rpm, the running time is 15 min, and then deionized water is added and stirred until dissolved; sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the above solution and transferred to a high-pressure reactor, the internal pressure of which is controlled at 8 MPa, the oven temperature is set at 80°C, and the reaction is continued for 3 hours; after the reaction is completed, the temperature is lowered to 45°C, pentanediol is slowly added and dissolved; iota carrageenan is added to the above solution, the magnetic stirrer speed is 850 rpm, and the stirring time is 0.5 h; when the solution viscosity is 250 mPa·s, adenosine triphosphate is added, and it is slowly stirred until it is completely dissolved to obtain a multi-effect facial mask essence; finally, it is loaded into a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085 MPa to finally obtain a finished multi-effect facial mask essence.

[0046] The multi-effect facial mask essence of this embodiment is prepared according to the steps of the present invention, and its performance test method is the same as that of Example 1, and the test results are as follows:

[0047]

[0048]

[0049] Example 4

[0050] The difference between this embodiment and embodiment 1 is that the multi-effect facial mask essence is prepared by changing the temperature during the experiment. The main process is as follows:

[0051] The multi-effect facial mask essence is prepared from the following components in molar percentage: 0.4% calcium acetate, 0.4% magnesium chloride, 2.5% adenosine triphosphate, 2.1% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.8% iota carrageenan, 0.3% hydrogenated castor oil and the balance deionized water.

[0052] The preparation process and parameters of this embodiment are:

[0053] Calcium acetate and magnesium chloride are added to a planetary ball mill, the orbital speed is set to 150 rpm, the rotation speed is set to 200 rpm, the running time is 15 min, and then deionized water is added and stirred until dissolved; sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the above solution and transferred to a high-pressure reactor, the internal pressure of which is controlled at 8 MPa, the oven temperature is set at 115°C, and the reaction is continued for 3 hours; after the reaction is completed, the temperature is lowered to 65°C, pentanediol is slowly added and dissolved; iota carrageenan is added to the above solution, the magnetic stirrer speed is 850 rpm, and the stirring time is 0.5 h; when the solution viscosity is 250 mPa·s, adenosine triphosphate is added, and it is slowly stirred until it is completely dissolved to obtain a multi-effect facial mask essence; finally, it is loaded into a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085 MPa to finally obtain a finished multi-effect facial mask essence.

[0054] The multi-effect facial mask essence of this embodiment is prepared according to the steps of the present invention, and its performance test method is the same as that of Example 1, and the test results are as follows:

[0055]

[0056] It can be concluded from the above Examples 1 and 4 that if the reaction temperature is increased and exceeds the specified temperature of the present invention, the activity of the ions will not be increased, but the actual moisturizing effect of the multi-effect facial mask essence will be affected.

[0057] Example 5

[0058] The difference between this embodiment and embodiment 1 is that the multi-effect facial mask essence is prepared by changing the pressure in the high-pressure reactor, and the main process is as follows:

[0059] The multi-effect facial mask essence is prepared from the following components in molar percentage: 0.4% calcium acetate, 0.4% magnesium chloride, 2.5% adenosine triphosphate, 2.1% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.8% iota carrageenan, 0.3% hydrogenated castor oil and the balance deionized water.

[0060] The preparation process and parameters of this embodiment are:

[0061] Calcium acetate and magnesium chloride are added to a planetary ball mill, the orbital speed is set to 150 rpm, the rotation speed is set to 200 rpm, the running time is 15 min, and then deionized water is added and stirred until dissolved; sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the above solution and transferred to a high-pressure reactor, the internal pressure of which is controlled at 3 MPa, the oven temperature is set at 80°C, and the reaction is continued for 3 hours; after the reaction is completed, the temperature is lowered to 45°C, pentanediol is slowly added and dissolved; iota carrageenan is added to the above solution, the magnetic stirrer speed is 850 rpm, and the stirring time is 0.5 h; when the solution viscosity is 250 mPa·s, adenosine triphosphate is added, and it is slowly stirred until it is completely dissolved to obtain a multi-effect facial mask essence; finally, it is loaded into a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085 MPa to finally obtain a finished multi-effect facial mask essence.

[0062] The multi-effect facial mask essence of this embodiment is prepared according to the steps of the present invention, and its performance test method is the same as that of Example 1, and the test results are as follows:

[0063]

[0064] It can be concluded from the above Examples 1 and 5 that if the pressure in the high-pressure reactor is reduced, the contact between the reactants will be insufficient and the reaction will be insufficient, which will affect the subsequent processes and the actual moisturizing and acne scar fading effects will be difficult to achieve.

[0065] Example 6

[0066] The difference between this embodiment and embodiment 1 is that the multi-effect facial mask essence is prepared by changing the reaction time in the experiment, and the main process is as follows:

[0067] The multi-effect facial mask essence is prepared from the following components in molar percentage: 0.4% calcium acetate, 0.4% magnesium chloride, 2.5% adenosine triphosphate, 2.1% sodium hyaluronate cross-linked polymer, 1.6% pentylene glycol, 1.8% iota carrageenan, 0.3% hydrogenated castor oil and the balance deionized water.

[0068] The preparation process and parameters of this embodiment are:

[0069] Calcium acetate and magnesium chloride are added to a planetary ball mill, the orbital speed is set to 150 rpm, the rotation speed is set to 200 rpm, the running time is 5 min, and then deionized water is added and stirred until dissolved; sodium hyaluronate cross-linked polymer and hydrogenated castor oil are added to the above solution and transferred to a high-pressure reactor, the internal pressure of which is controlled at 8 MPa, the oven temperature is set at 80°C, and the reaction lasts for 1 hour; after the reaction is completed, the temperature is lowered to 45°C, pentanediol is slowly added and dissolved; ι-type carrageenan is added to the above solution, the magnetic stirrer speed is 850 rpm, and the stirring time is 0.2 h; when the solution viscosity is 250 mPa·s, adenosine triphosphate is added, and it is slowly stirred until it is completely dissolved to obtain a multi-effect facial mask essence; finally, it is loaded into a vacuum degassing tank for liquid degassing, and the vacuum degree is set to 0.085 MPa to finally obtain a finished multi-effect facial mask essence.

[0070] The multi-effect facial mask essence of this embodiment is prepared according to the steps of the present invention, and its performance test method is the same as that of Example 1, and the test results are as follows:

[0071]

[0072] It can be concluded from the above Examples 1 and 6 that if the reaction time of each step in preparing the multi-effect facial mask essence is reduced, the main active ingredients will not fully participate in the reaction or the preparation will be incomplete, and the actual moisturizing and fading of acne marks will not be reflected.

[0073] In the description of this specification, the description with reference to the terms "one embodiment", "some embodiments", "example", "specific example", or "some examples" etc. means that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment or example of the present invention. In this specification, the schematic representations of the above terms do not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described may be combined in any one or more embodiments or examples in a suitable manner. In addition, those skilled in the art may combine and combine the different embodiments or examples described in this specification and the features of the different embodiments or examples, without contradiction.

[0074] The above are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A multi-effect facial mask essence, characterized in that: It is composed of the following components in mole percentages: 0.3-0.6% calcium acetate, 0.3-0.6% magnesium chloride, 2.1-3.6% adenosine triphosphate, 1.5-2.5% sodium hyaluronate cross-linked polymer, 1.5-2.0% pentylene glycol, 1.2-2.6% iota carrageenan, 0.1-0.5% hydrogenated castor oil and the balance deionized water; The method for preparing the multi-effect facial mask essence is characterized by comprising the following steps: S1: adding 0.3-0.6 mol% of calcium acetate and 0.3-0.6 mol% of magnesium chloride into a planetary ball mill to obtain a micron-sized mixed powder, and then adding the obtained mixed powder into deionized water, stirring until the solid matter is completely dissolved, to obtain a solution A; S2: adding 1.5-2.5 mol% of sodium hyaluronate cross-linked polymer and 0.1-0.5 mol% of hydrogenated castor oil to the solution A obtained in step S1, transferring to a high-pressure reactor, reacting for 3-4 hours, cooling, slowly adding 1.5-2.0 mol% of pentanediol, stirring thoroughly, until the solution becomes transparent, to obtain solution B; S3: adding 1.2-2.6 mol% of iota carrageenan to the solution B obtained in step S2, mixing and stirring to obtain solution C; S4: adding 2.1-3.6 mol% of adenine nucleoside triphosphate to the solution C obtained in step S3, and slowly stirring until the solid powder is completely dissolved to prepare a multi-effect facial mask essence; In step S2, the internal pressure of the high-pressure reactor is 5-10 MPa, the reaction temperature is 75-90°C, and then the temperature is reduced to 45-55°C.

2. The multi-effect facial mask essence according to claim 1, characterized in that: In step S1, the planetary ball mill has an orbital speed of 100 to 200 revolutions, a rotational speed of 150 to 250 revolutions, and a time of 10 to 20 minutes.

3. The multi-effect facial mask essence according to claim 1, characterized in that: In step S3, the stirring rate is 800-1000 rpm and the time is 0.5-1 h.

4. The multi-effect facial mask essence according to claim 1, characterized in that: After step S4, a degassing process is also included, in which the multi-effect facial mask essence is added into a vacuum degassing tank for liquid degassing.

5. The multi-effect facial mask essence according to claim 4, characterized in that: The vacuum degree of the vacuum degassing tank is 0.08Mpa to 0.095Mpa.

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