Automatic purification device for zirconium oxide
By introducing a rotating plate and a deflecting plate design into the automated purification unit for zirconium oxide, the problem of insufficient contact between hydrogen and solid impurities was solved, resulting in more thorough impurity reduction and higher purification efficiency.
Patent Information
- Application Number
- CN202311331036.3
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2023-10-13
- Publication Date
- 2025-12-26
- Estimated Expiration
- 2043-10-13
AI Technical Summary
In existing automated zirconium oxide purification equipment, during the zirconium chloride impurity removal operation, the contact between hydrogen and solid impurities is insufficient, resulting in some impurities not being reduced. As the temperature rises, these impurities vaporize and mix into the zirconium chloride, reducing the purification effect.
Purification auxiliary components, including a rotating plate and a deflecting plate, are used. The rotating plate is driven by a drive motor to flip and the deflecting plate is separated to ensure that hydrogen and solid impurities are in full contact. The solid is flipped and diverted in all directions by a hydraulic cylinder and a sealing strip, thereby improving the reaction efficiency of hydrogen.
It effectively increases the contact area and reaction completeness between hydrogen and solid impurities, reduces impurity residue, and improves the purification effect of zirconium oxide.
Smart Images
Figure CN117509726B_ABST
Abstract
Description
TECHNICAL FIELD
[0001] The application relates to the technical field of zirconia purification, and in particular to an automatic zirconia purification device. BACKGROUND
[0002] In the zirconia purification process, the zirconia is first made into a briquette and dried, then the inside of the briquette is passed through chlorine gas, and the zirconia reacts with the chlorine gas to generate zirconium chloride; in the impurity removal process of the zirconium chloride, a large amount of hydrogen gas needs to be passed through the zirconium chloride to reduce part of the impurities, and then separation is realized through high-temperature mode; after the zirconia is operated step by step, the purification is completed.
[0003] In the existing automatic zirconia purification device, a large amount of hydrogen gas needs to be passed through in the impurity removal operation of the zirconium chloride; in the process of introducing the hydrogen gas into the zirconium chloride, the zirconium chloride and solid impurities are accumulated together, the hydrogen gas cannot fully react with the solid impurities, part of the solid impurities cannot be reduced, and the solid impurities are mixed with the vaporized zirconium chloride and discharged as the temperature rises, so that a small amount of impurities are still mixed in the zirconium chloride after impurity removal, and the use value of the automatic purification device is reduced. SUMMARY
[0004] The application discloses an automatic zirconia purification device, which aims to solve the technical problem that in the existing automatic zirconia purification device, a large amount of hydrogen gas needs to be passed through in the impurity removal operation of the zirconium chloride; in the process of introducing the hydrogen gas into the zirconium chloride, the zirconium chloride and solid impurities are accumulated together, the hydrogen gas cannot fully react with the solid impurities, part of the solid impurities cannot be reduced, and the solid impurities are mixed with the vaporized zirconium chloride and discharged as the temperature rises, so that a small amount of impurities are still mixed in the zirconium chloride after impurity removal.
[0005] In order to achieve the above-mentioned purpose, the application adopts the following technical scheme:
[0006] The application discloses an automatic purification device for zirconium oxide, which comprises a base, two fixed rods are fixedly connected to the top of the base, and a same treatment chamber is fixedly connected to the opposite side of the two fixed rods; an inlet hole is formed in the outer side of the treatment chamber located at the upper portion; an inlet frame is fixedly connected to the inside of the inlet hole; an inner connecting column is fixedly connected to the inner wall of each side of the treatment chamber located below the inlet frame; a same purification frame is fixedly connected to the opposite side of the two inner connecting columns; a purification auxiliary assembly is arranged on the purification frame; a gas passing hole is formed in each side of the purification frame at equal intervals; the purification auxiliary assembly comprises two shaft sleeves; the two shaft sleeves are respectively and slidably connected to the inside of adjacent sliding holes; a same intermediate shaft is connected to the inside of the two shaft sleeves through bearings; one of the shaft sleeves is fixedly connected to an accommodation rack on the outer side located below; a driving motor two is fixedly connected to the accommodation rack; and the output shaft of the driving motor two is connected to the intermediate shaft through a shaft coupling.
[0007] By arranging the purification auxiliary assembly, after preliminary heating, the hydrogen is introduced into the purification frame, the heating assembly increases the temperature inside the treatment chamber, the driving motor two is started, the driving motor two drives the rotation of the rotating plates to turn the solid in the purification frame, when the rotating plates rotate from the lower portion to the upper portion, the positive and negative rotation motor is started to drive the contact arc rod on the deflection plate to separate from the rotating plates, the rotating plates are deflected under the gravity of the solid, the solid above the rotating plates gradually falls to the lower portion, the hydrogen fully contacts with the solid, the incomplete contact of the hydrogen does not cause the incomplete reduction of the impurities, after the rotating plates rotate by 180 degrees, the positive and negative rotation motor drives the contact arc rod to reset, the continuous rotation of the driving motor drives the remaining solid on the rotating plates to fall from another direction, the solid is separated and poured, the hydrogen introduction effect is further improved, and the purification effect is improved.
[0008] In a preferred scheme, the shaft sleeve is fixedly connected with a sealing belt at the upper portion and the lower portion, the two sealing belts are arranged on the inner wall of the sliding hole, two supporting blocks are fixedly connected to each side of the purification frame close to the bottom end, a hydraulic cylinder three is fixedly connected to the top of each supporting block, an outer spreading rod is fixedly connected to the output end of each hydraulic cylinder three and the outer side of the shaft sleeve.
[0009] In an preferred scheme, the outer side of the intermediate rotating shaft is annularly distributed with an outer frame, and each outer frame is connected with the same inner connecting shaft through bearings near the two inner walls of the intermediate rotating shaft, the outer side of the inner connecting shaft is sleeved with a rotating plate, the outer side of the rotating plate is provided with a groove, the inner side of the groove is fixedly connected with dispersion rods at equal intervals, the outer side of the outer frame at each dispersion rod is fixedly connected with a limiting plate, the limiting plate is located at the inner connecting shaft, the side of the outer frame away from the dispersion rod is fixedly connected with a motor plate, the side of the motor plate is fixedly connected with a forward and reverse motor, the output shaft of the forward and reverse motor is fixedly connected with a deflection plate through a shaft coupling, the outer side of the deflection plate near the rotating plate is fixedly connected with a contact arc rod, and the outer side of the contact arc rod is in contact with the rotating plate.
[0010] In an preferred scheme, the bottom of the purification frame is provided with a slag discharge hole, and the bottom of the purification frame is fixedly connected with two intermediate blocks, the two sides of the two intermediate blocks are fixedly connected with two hydraulic cylinders two, the output ends of the two hydraulic cylinders two on one side are fixedly connected with the same push plate, the side of the push plate facing the slag discharge hole is fixedly connected with a blocking plate, and the blocking plate is matched with the slag discharge hole.
[0011] In an preferred scheme, the two open ends of the purification frame are fixedly connected with hydrogen accumulation plates, the opposite sides of the two hydrogen accumulation plates are equally provided with hydrogen discharge holes, the opposite sides of the two hydrogen accumulation plates are provided with connecting holes and butt joints, the inner sides of the two connecting holes are fixedly connected with the same connecting pipe, the inner sides of the two butt joints are fixedly connected with hydrogen inlet pipes, and the inlet ends of the hydrogen inlet pipes are located on the outer side of the treatment chamber.
[0012] In an preferred scheme, the outer side of the bottom of the treatment chamber is provided with a discharging hole, and the treatment chamber is provided with an electric control door at the discharging hole.
[0013] In an preferred scheme, the outer side of the treatment chamber is fixedly connected with a support frame, and the top of the support frame is fixedly connected with a condensation box, one side of the condensation box is provided with a drainage hole, the inner wall of the drainage hole is fixedly connected with a drainage pipe, and the outer side of the drainage pipe is connected with an electromagnetic valve through a flange.
[0014] In an preferred scheme, the top of the condensation box is fixedly connected with an adsorption pump, one side of the condensation box facing the feeding frame is fixedly connected with a hydraulic cylinder one, the output end of the hydraulic cylinder one is fixedly connected with an external connecting block, the outer side of the external connecting block is fixedly connected with a hollow adsorption plate, the bottom of the hollow adsorption plate is equally provided with adsorption holes, the adsorption end of the adsorption pump is fixedly connected with a telescopic adsorption pipe, the telescopic adsorption pipe is inserted into the hollow adsorption plate, and the conveying end of the adsorption pump is connected to the inner side of the condensation box through a pipeline.
[0015] In an preferred scheme, the outer side of the feeding frame is provided with a gas impurity collecting assembly, and the gas impurity collecting assembly comprises a filter chamber, two mounting rods are fixedly connected to one side of the filter chamber and are fixedly connected to the outer side of the feeding frame, a filter screen is fixedly connected to the inside of the filter chamber, a suction box is fixedly connected to the inside of the feeding frame, a plurality of suction holes two are equidistantly formed in the bottom of the suction box, a mounting hole one is formed in the bottom of the suction box, a C-shaped suction pipe is fixedly connected to the inside of the mounting hole one and is located at the outer side of the purification frame, a suction hole one is formed in the outer side of the C-shaped suction pipe facing the purification frame, a mounting hole two is formed in the outer side of the filter chamber and the suction box, and the same connecting elbow is fixedly connected to the inside of the two mounting holes two.
[0016] In an preferred scheme, one side of the filter chamber is fixedly connected with a motor bracket, and a driving motor one is fixedly connected to the outer side of the motor bracket, the output shaft of the driving motor one is fixedly connected with a rotating shaft through a shaft coupling, the end of the rotating shaft is fixedly connected with a scraping bracket, the scraping bracket is in contact with the outer side of the filter screen, the bottom of the filter chamber below the scraping bracket is fixedly connected with an impurity collecting box, one side of the filter chamber away from the suction box is fixedly connected with a gas impurity storage tank, an exhaust hole is formed in one side of the gas impurity storage tank, an exhaust pipe is fixedly connected to the inside of the exhaust hole, the outer side of the exhaust pipe is connected with a pipe valve through a flange, one side of the filter chamber is fixedly connected with a collecting pump, the collecting end of the collecting pump is connected to the inside of the filter chamber through a pipeline, the conveying end of the collecting pump is fixedly connected with an air guide pipe, and the air guide pipe is inserted into the inside of the gas impurity storage tank.
[0017] By arranging the gas impurity collecting assembly, when the impurities in the zirconium chloride are treated, the zirconium chloride is first subjected to low-temperature treatment, during the low-temperature treatment process, the impurities in the zirconium chloride are vaporized, the collecting pump is started, and the collecting pump collects the gas impurities in the treatment chamber through the suction hole one on the C-shaped suction pipe and the suction hole two below the suction box, thereby improving the impurity collection efficiency. When the gas impurities carrying dust and other small-particle impurities enter the filter chamber, the filter screen filters the dust and other small-particle impurities, the gas impurities enter the gas impurity storage tank through the filter screen, the driving motor one is started, the driving motor one drives the scraping bracket to rotate, thereby guiding the dust and other small-particle impurities attached to the filter screen into the impurity collecting box below, facilitating the classified treatment of the impurities, and improving the use value of the purification device.
[0018] From the above, the automatic purification device for zirconium oxide provided by the application has the advantages that after preliminary heating, part of impurities in the zirconium chloride is vaporized and collected, then hydrogen is introduced, the temperature inside the processing chamber is increased by the heating assembly during the hydrogen introduction process, the second driving motor is started, the driving motor drives each rotating plate to overturn the solid inside the purification frame, when the rotating plate rotates from the lower direction to the upper direction, the reversing motor is started to drive the contact arc rod on the deflection plate to separate from the rotating plate, then the rotating plate deflects under the gravity of the solid, the solid above the rotating plate gradually pours to the lower direction, then the hydrogen fully contacts with the solid, avoids incomplete reduction of part of impurities due to incomplete contact of the hydrogen introduction, after the same rotating plate rotates 180 degrees, the reversing motor drives the contact arc rod to reset, then the continuous rotation of the driving motor drives the remaining solid on the rotating plate to fall from another direction, realizes the shunt pouring of the solid, and further improves the technical effect of the hydrogen introduction. BRIEF DESCRIPTION OF DRAWINGS
[0019] Figure 1 The overall structure of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0020] Figure 2 The processing chamber structure of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0021] Figure 3 The purification frame structure of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0022] Figure 4 The internal structure of the purification frame of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0023] Figure 5 The purification auxiliary assembly of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0024] Figure 6 The rotating plate and outer frame combined structure of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0025] Figure 7 The gas impurity collection assembly of the automatic purification device for zirconium oxide provided by the application is shown in the figure.
[0026] Figure 8 The overall structure of the automatic purification device for zirconium oxide provided by the application is shown in the figure. Figure 7
[0027] In the figure: 1, base; 2, fixed rod; 3, processing chamber; 4, feeding frame; 5, gas impurity collection assembly; 501, filter chamber; 502, gas impurity storage tank; 503, air exhaust tank; 504, exhaust pipe; 505, pipe valve; 506, collection pump; 507, connecting elbow; 508, mounting rod; 509, C-shaped air exhaust pipe; 510, air exhaust hole one; 511, air guide pipe; 512, filter screen; 513, motor frame; 514, driving motor one; 515, air exhaust hole two; 516, rotating shaft; 517, scraping frame; 518, impurity collection tank; 6, hollow adsorption plate; 7, external block; 8, telescopic adsorption pipe; 9, adsorption pump; 10, condensation tank; 11, liquid discharge pipe; 12, electromagnetic valve; 13, hydrogen inlet pipe; 14, hydraulic cylinder one; 15, adsorption hole; 16, support frame; 17, electric control door; 18, heating assembly; 19, connecting pipe; 20, purification frame; 21, air passing hole; 22, internal connecting column; 23, hydrogen discharge hole; 24, hydrogen accumulation plate; 25, pushing plate; 26, intermediate block; 27, hydraulic cylinder two; 28, blocking plate; 29, purification auxiliary assembly; 2901, rotating plate; 2902, outer frame; 2903, shaft sleeve; 2904, outward extending rod; 2905, driving motor two; 2906, placing frame; 2907, sealing belt; 2908, hydraulic cylinder three; 2909, support block; 2910, dispersing rod; 2911, limiting plate; 2912, intermediate rotating shaft; 2913, motor plate; 2914, forward and reverse motor; 2915, deflection plate; 2916, contact arc rod; 2917, internal connecting shaft. DETAILED DESCRIPTION
[0028] The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application. Obviously, the described embodiments are only part of the embodiments of the present application, not all the embodiments.
[0029] The automatic purification device for zirconium oxide disclosed in the present application is mainly applied to the existing automatic purification device for zirconium oxide in the process of use, and needs to introduce a large amount of hydrogen during the impurity removal operation of zirconium chloride. During the introduction of hydrogen into zirconium chloride, zirconium chloride and solid impurities are accumulated together, hydrogen cannot fully react with solid impurities, part of the solid impurities cannot be reduced, and thus the part of the impurities are vaporized along with the increase of temperature, mixed with the vaporized zirconium chloride and discharged, resulting in the scene that a small amount of impurities are still mixed in the zirconium chloride after impurity removal.
[0030] REFERENCE Figures 1-8The utility model provides an automatic purification device of zirconium oxide, which comprises a base 1, two fixed rods 2 fixedly connected to the top of the base 1, and a same treatment chamber 3 fixedly connected to the opposite side of the two fixed rods 2, a feeding hole is formed in the outer side of the upper part of the treatment chamber 3, a feeding frame 4 is fixedly connected to the inside of the feeding hole, an inner connecting column 22 is fixedly connected to the inner wall of the two sides below the feeding frame 4, a same purification frame 20 is fixedly connected to the opposite side of the two inner connecting columns 22, a purification auxiliary assembly 29 is arranged on the purification frame 20, a gas passing hole 21 is formed in the two sides of the purification frame 20 at equal intervals, the purification auxiliary assembly 29 comprises two shaft sleeves 2903, sliding holes are formed in the two sides of the purification frame 20, the two shaft sleeves 2903 are respectively slidably connected to the inside of the adjacent sliding holes, a same intermediate shaft 2912 is connected to the inside of the two shaft sleeves 2903 through bearings, the outer side of one of the shaft sleeves 2903 below is fixedly connected to a placing frame 2906, the placing frame 2906 is fixedly connected to a driving motor two 2905, and the output shaft of the driving motor two 2905 is connected to the intermediate shaft 2912 through a shaft coupling.
[0031] Referring to Figures 1-6 In a preferred embodiment, the shaft sleeve 2903 is fixedly connected to a sealing band 2907 at the upper part and the lower part, the two sealing bands 2907 are arranged on the inner wall of the sliding hole, the two sides of the purification frame 20 close to the bottom end are fixedly connected to two support blocks 2909, the top of each support block 2909 is fixedly connected to a hydraulic cylinder three 2908, the output end of each hydraulic cylinder three 2908 is fixedly connected to an outward extending rod 2904, the outward extending rod 2904 is fixedly connected to the outer side of the shaft sleeve 2903, the outer side of the intermediate shaft 2912 is annularly distributed with an outer frame 2902, the two inner walls of each outer frame 2902 close to the intermediate shaft 2912 are connected to a same inner connecting shaft 2917 through bearings, the outer side of the inner connecting shaft 2917 is sleeved with a rotating plate 2901, the outer side of the rotating plate 2901 is provided with a groove, the inside of the groove is fixedly connected to a dispersing rod 2910 at equal intervals, the outer side of the outer frame 2902 at each dispersing rod 2910 is fixedly connected to a limiting plate 2911, the limiting plate 2911 is located at the inner connecting shaft 2917, the outer frame 2902 is fixedly connected to a motor plate 2913 away from the dispersing rod 2910, one side of the motor plate 2913 is fixedly connected to a forward and reverse motor 2914, the output shaft of the forward and reverse motor 2914 is fixedly connected to a deflection plate 2915 through a shaft coupling, the outer side of the deflection plate 2915 close to the rotating plate 2901 is fixedly connected to a contact arc rod 2916, and the outer side of the contact arc rod 2916 is in contact with the rotating plate 2901.
[0032] In a specific application scenario, after preliminary heating, part of the impurities in the zirconium chloride are vaporized and collected, and then hydrogen is introduced. During the hydrogen introduction process, the temperature inside the treatment chamber 3 is raised by the heating assembly 18, the driving motor two 2905 is started, and the driving motor two 2905 drives each rotating plate 2901 to rotate and drive the solid inside the purification frame 20. When the rotating plate 2901 rotates from the bottom to the top, the positive and negative rotation motor 2914 is started to drive the contact arc rod 2916 on the deflection plate 2915 to separate from the rotating plate 2901. Then, the rotating plate 2901 deflects under the action of the gravity of the solid, and the solid above the rotating plate 2901 gradually pours down. Therefore, the hydrogen fully contacts with the solid, avoiding incomplete reduction of part of the impurities due to incomplete contact during hydrogen introduction. After the same rotating plate 2901 rotates by 180°, the positive and negative rotation motor 2914 drives the contact arc rod 2916 to reset. The continuous rotation of the driving motor drives the remaining solid on the rotating plate 2901 to fall from the other direction, realizing the diversion of the solid and further improving the effect of hydrogen introduction, thereby improving the purification effect.
[0033] Specifically, during the working process of the purification auxiliary assembly 29, the adjusting hydraulic cylinder three 2908 drives the two shaft sleeves 2903 to slide inside the sliding hole, thereby adjusting the height of the rotating plate 2901, realizing the omnidirectional rotation of the solid inside the purification frame 20, and further improving the purification effect. Meanwhile, during the up-down adjustment of the shaft sleeve 2903, the sealing band 2907 realizes the sealing of the sliding hole, preventing the solid from sliding into the treatment chamber 3 from the sliding hole.
[0034] Referring to Figure 1 , Figure 3 and Figure 4 , in a preferred embodiment, the bottom of the purification frame 20 is provided with a slag discharge hole, and the bottom of the purification frame 20 is fixedly connected with two intermediate blocks 26. The two intermediate blocks 26 are fixedly connected with two hydraulic cylinders two 27 on both sides. The output ends of the two hydraulic cylinders two 27 on one side are fixedly connected with the same push plate 25. The side of the push plate 25 facing the slag discharge hole is fixedly connected with the blocking plate 28, and the blocking plate 28 is matched with the slag discharge hole.
[0035] Referring to Figure 1 , Figure 2 and Figure 3 , in a preferred embodiment, the two open ends of the purification frame 20 are fixedly connected with hydrogen accumulation plates 24, and the opposite sides of the two hydrogen accumulation plates 24 are equally provided with hydrogen discharge holes 23. The opposite sides of the two hydrogen accumulation plates 24 are provided with connecting holes and counter holes. The inside of the two connecting holes is fixedly connected with the same connecting pipe 19, and the inside of the two counter holes is fixedly connected with hydrogen inlet pipes 13. The inlet ends of the hydrogen inlet pipes 13 are located on the outside of the treatment chamber 3.
[0036] Referring toFigure 1 And Figure 2 In a preferred embodiment, the processing chamber 3 is provided with a discharging hole on the outer side of the bottom, and the processing chamber 3 is provided with an electric control door 17 at the discharging hole, and the processing chamber 3 is provided with a heating assembly 18 on the inner side of both sides of the purification frame 20.
[0037] Referring to Figure 1 And Figure 2 In a preferred embodiment, the processing chamber 3 is fixedly connected with a support frame 16 on the outer side, and the support frame 16 is fixedly connected with a condensation box 10 on the top, and the condensation box 10 is provided with a liquid discharging hole on one side, and the inner wall of the liquid discharging hole is fixedly connected with a liquid discharging pipe 11, and the outer side of the liquid discharging pipe 11 is connected with an electromagnetic valve 12 through a flange.
[0038] In the present application, the condensation box 10 is fixedly connected with a suction pump 9 on the top, and the condensation box 10 is fixedly connected with a hydraulic cylinder one 14 on the side facing the feeding frame 4, and the output end of the hydraulic cylinder one 14 is fixedly connected with an external connecting block 7, and the outer side of the external connecting block 7 is fixedly connected with a hollow suction plate 6, and the bottom of the hollow suction plate 6 is provided with a suction hole 15 at equal intervals, and the suction end of the suction pump 9 is fixedly connected with a telescopic suction pipe 8, and the telescopic suction pipe 8 is inserted into the inside of the hollow suction plate 6, and the conveying end of the suction pump 9 is connected with the inside of the condensation box 10 through a pipeline.
[0039] Referring to Figure 1 , Figure 2 , Figure 7 And Figure 8In one preferred implementation, the outer side of the feeding frame 4 is provided with a gas impurity collecting assembly 5, and the gas impurity collecting assembly 5 comprises a filtering chamber 501, one side of the filtering chamber 501 is fixedly connected with two mounting rods 508, the two mounting rods 508 are both fixedly connected to the outer side of the feeding frame 4, the inside of the filtering chamber 501 is fixedly connected with a filter screen 512, the inside of the feeding frame 4 is fixedly connected with a suction box 503, the bottom of the suction box 503 is provided with a plurality of equidistant suction holes two 515, the bottom of the suction box 503 is provided with a mounting hole one, the inside of the mounting hole one is fixedly connected with a C-shaped suction pipe 509, the C-shaped suction pipe 509 is located at the outer side of the purification frame 20, the outer side of the C-shaped suction pipe 509 is provided with a suction hole one 510 which faces the outer side of the purification frame 20, the outer sides of the filtering chamber 501 and the suction box 503 are both provided with mounting holes two, the inside of the two mounting holes two is fixedly connected with the same connecting elbow 507, one side of the filtering chamber 501 is fixedly connected with a motor bracket 513, and the outer side of the motor bracket 513 is fixedly connected with a driving motor one 514, the output shaft of the driving motor one 514 is fixedly connected with a rotating shaft 516 through a shaft coupling, the end of the rotating shaft 516 is fixedly connected with a scraping bracket 517, the scraping bracket 517 is in contact with the outer side of the filter screen 512, the bottom of the filtering chamber 501 located below the scraping bracket 517 is fixedly connected with an impurity collecting box 518, one side of the filtering chamber 501 away from the suction box 503 is fixedly connected with a gas impurity storage box 502, one side of the gas impurity storage box 502 is provided with an exhaust hole, the inside of the exhaust hole is fixedly connected with an exhaust pipe 504, the outer side of the exhaust pipe 504 is connected with a pipe valve 505 through a flange, one side of the filtering chamber 501 is fixedly connected with a collecting pump 506, the collecting end of the collecting pump 506 is connected to the inside of the filtering chamber 501 through a pipeline, the conveying end of the collecting pump 506 is fixedly connected with a gas guide pipe 511, and the gas guide pipe 511 is inserted into the inside of the gas impurity storage box 502.
[0040] It should be noted that when the impurities in the zirconium chloride are treated, the zirconium chloride is first subjected to low-temperature treatment. During the low-temperature treatment process, the impurities in the zirconium chloride are vaporized. The collecting pump 506 is started to collect the gas impurities in the treatment chamber 3 through the suction hole one 510 on the C-shaped suction pipe 509 and the suction hole two 515 below the suction box 503, thereby improving the impurity collection efficiency. When the gas impurities carrying dust and other small-particle impurities enter the filtering chamber 501, the filter screen 512 filters the dust and other small-particle impurities. The gas impurities enter the gas impurity storage box 502 through the filter screen 512. The driving motor one 514 is started to drive the scraping bracket 517 to rotate, thereby guiding the dust and other small-particle impurities attached to the filter screen 512 into the impurity collecting box 518 below, facilitating the classified treatment of the impurities, and improving the use value of the purification device.
[0041] Working principle: when using, when the impurities in zirconium chloride are treated, first, low temperature treatment is carried out, during the low temperature treatment process, the impurities in zirconium chloride are vaporized, the collecting pump 506 is started, the collecting pump 506 collects the gas impurities in the treatment chamber 3 through the gas suction hole one 510 on the C-shaped gas suction pipe 509 and the gas suction hole two 515 below the gas suction box 503, when the gas impurities carrying dust and other small particle impurities enter the filter chamber 501, the filter screen 512 filters the dust and other small particle impurities, the gas impurities enter the gas impurity storage box 502 through the filter screen 512, the driving motor one 514 is started, the driving motor one 514 drives the scraping frame 517 to rotate, so that the dust and other small particle impurities attached to the filter screen 512 are introduced into the impurity collecting box 518 below, which is convenient for classified treatment of impurities, after preliminary impurity removal, hydrogen is introduced, during the hydrogen introduction process, the heating assembly 18 increases the temperature in the treatment chamber 3, the driving motor two 2905 is started, the driving motor two 2905 drives each rotating plate 2901 to rotate and drive the solid in the purification frame 20, when the rotating plate 2901 rotates from the lower direction to the upper direction, the forward and reverse motor 2914 drives the contact arc rod 2916 on the deflection plate 2915 to separate from the rotating plate 2901, then the rotating plate 2901 deflects under the action of the gravity of the solid, the solid above the rotating plate 2901 gradually pours down to the lower direction, then the hydrogen is in full contact with the part of the solid, avoiding incomplete contact of the hydrogen introduction causing incomplete reduction of part of the impurities, after the same rotating plate 2901 rotates 180°, the forward and reverse motor 2914 drives the contact arc rod 2916 to reset, then the continuous rotation of the driving motor drives the remaining solid on the rotating plate 2901 to fall from the other direction, realizing the shunt pouring of the solid, the continuous increase of the temperature makes the zirconium chloride vaporization be adsorbed to the condensing box 10 for liquefaction treatment, the remaining solid impurities are retained in the purification frame 20 for collection, and the operation is introduced.
[0042] The above merely illustrates the preferred embodiments of the present application, but the protection scope of the present application is not limited to this, any person skilled in the art can make equivalent replacement or change according to the technical scheme and the inventive concept of the present application within the technical range disclosed by the present application, which should be covered in the protection scope of the present application.
Claims
1. An automated purification device of zirconium oxide comprising a base (1), characterized in that, The top of the base (1) is fixedly connected with two fixed rods (2), and the opposite sides of the two fixed rods (2) are fixedly connected with the same treatment chamber (3), the upper outer side of the treatment chamber (3) is provided with an inlet hole, the inside of the inlet hole is fixedly connected with an inlet frame (4), the inside walls of the two sides of the treatment chamber (3) below the inlet frame (4) are fixedly connected with inner connecting columns (22), the opposite sides of the two inner connecting columns (22) are fixedly connected with the same purification frame (20), the purification frame (20) is provided with a purification auxiliary assembly (29), the two sides of the purification frame (20) are equidistantly provided with air passing holes (21), the purification auxiliary assembly (29) comprises two shaft sleeves (2903), the two sides of the purification frame (20) are provided with sliding holes, the two shaft sleeves (2903) are respectively and slidably connected in the inside of the adjacent sliding holes, the inside of the two shaft sleeves (2903) is connected with the same intermediate shaft (2912) through a bearing, and one of the shaft sleeves (2903) is fixedly connected with a placing frame (2906) on the outer side below, a driving motor two (2905) is fixedly connected at the placing frame (2906), and the output shaft of the driving motor two (2905) is connected with the intermediate shaft (2912) through a shaft coupling. The shaft sleeve (2903) is fixedly connected with a sealing band (2907) on the upper side and the lower side, the two sealing bands (2907) are arranged on the inner walls of the sliding holes, the two sides of the purification frame (20) close to the bottom are fixedly connected with two supporting blocks (2909), the top of each supporting block (2909) is fixedly connected with a hydraulic cylinder three (2908), the output end of each hydraulic cylinder three (2908) is fixedly connected with an outward extending rod (2904), and the outward extending rod (2904) is fixedly connected to the outer side of the shaft sleeve (2903). The outer side of the intermediate shaft (2912) is annularly provided with an outer frame (2902), the two inner walls of each outer frame (2902) close to the intermediate shaft (2912) are connected with the same inner connecting shaft (2917) through a bearing, the outer side of the inner connecting shaft (2917) is sleeved with a rotating plate (2901), the outer side of the rotating plate (2901) is provided with a groove, the inside of the groove is fixedly connected with dispersion rods (2910) at equal intervals, the outer side of the outer frame (2902) at each dispersion rod (2910) is fixedly connected with a limiting plate (2911), the limiting plate (2911) is located at the inner connecting shaft (2917), one side of the outer frame (2902) away from the dispersion rod (2910) is fixedly connected with a motor plate (2913), one side of the motor plate (2913) is fixedly connected with a forward and reverse motor (2914), the output shaft of the forward and reverse motor (2914) is fixedly connected with a deflection plate (2915) through a shaft coupling, the outer side of the deflection plate (2915) close to the rotating plate (2901) is fixedly connected with a contact arc rod (2916), and the outer side of the contact arc rod (2916) is in contact with the rotating plate (2901).
2. The apparatus for automated purification of zirconium oxide according to claim 1, characterized in that, The bottom of the purification frame (20) is provided with a slag hole, and the bottom of the purification frame (20) is fixedly connected with two intermediate blocks (26), the two sides of the two intermediate blocks (26) are fixedly connected with hydraulic cylinders two (27), the output ends of the two hydraulic cylinders two (27) on one side are fixedly connected with the same push plate (25), one side of the push plate (25) facing the slag hole is fixedly connected with a blocking plate (28), and the blocking plate (28) is matched with the slag hole.
3. The apparatus for automated purification of zirconium oxide according to claim 2, characterized in that, The two sides of the purification frame (20) are fixedly connected with hydrogen accumulation plates (24), and the opposite sides of the two hydrogen accumulation plates (24) are equally provided with hydrogen discharge holes (23), the opposite sides of the two hydrogen accumulation plates (24) are provided with connecting holes and butt joints, the inside of the two connecting holes is fixedly connected with the same connecting pipe (19), the inside of the two butt joints is fixedly connected with hydrogen inlet pipes (13), and the inlet end of the hydrogen inlet pipe (13) is located outside the treatment chamber (3).
4. The apparatus for automated purification of zirconium oxide according to claim 1, characterized in that, The bottom of the treatment chamber (3) is provided with a discharging hole, and the treatment chamber (3) is provided with an electric control door (17) at the discharging hole, and the inside of the treatment chamber (3) is provided with a heating assembly (18) on both sides of the purification frame (20).
5. The apparatus for automated purification of zirconium oxide according to claim 4, characterized in that, The outside of the treatment chamber (3) is fixedly connected with a support frame (16), and the top of the support frame (16) is fixedly connected with a condensation box (10), one side of the condensation box (10) is provided with a drainage hole, the inner wall of the drainage hole is fixedly connected with a drainage pipe (11), and the outside of the drainage pipe (11) is connected with an electromagnetic valve (12) through a flange.
6. The apparatus for automated purification of zirconium oxide according to claim 5, characterized in that, The top of the condensation box (10) is fixedly connected with an adsorption pump (9), and one side of the condensation box (10) facing the feeding frame (4) is fixedly connected with a hydraulic cylinder one (14), the output end of the hydraulic cylinder one (14) is fixedly connected with an external block (7), the outside of the external block (7) is fixedly connected with a hollow adsorption plate (6), the bottom of the hollow adsorption plate (6) is equally provided with adsorption holes (15), the adsorption end of the adsorption pump (9) is fixedly connected with a telescopic adsorption pipe (8), the telescopic adsorption pipe (8) is inserted into the inside of the hollow adsorption plate (6), and the conveying end of the adsorption pump (9) is connected to the inside of the condensation box (10) through a pipeline.
7. The apparatus for automated purification of zirconium oxide according to claim 1, characterized by The outer side of the feeding frame (4) is provided with a gas impurity collecting assembly (5), and the gas impurity collecting assembly (5) comprises a filter chamber (501), two mounting rods (508) are fixedly connected to one side of the filter chamber (501), the two mounting rods (508) are fixedly connected to the outer side of the feeding frame (4), a filter screen (512) is fixedly connected to the inside of the filter chamber (501), a gas suction box (503) is fixedly connected to the inside of the feeding frame (4), a plurality of gas suction holes two (515) are equidistantly formed in the bottom of the gas suction box (503), a mounting hole one is formed in the bottom of the gas suction box (503), a C-shaped gas suction pipe (509) is fixedly connected to the inside of the mounting hole one, the C-shaped gas suction pipe (509) is located on the outer side of the purification frame (20), a gas suction hole one (510) is formed in the outer side of the C-shaped gas suction pipe (509) facing the purification frame (20), mounting holes two are formed in the outer sides of the filter chamber (501) and the gas suction box (503), and the same connecting elbow (507) is fixedly connected to the inside of the two mounting holes two.
8. The apparatus for automated purification of zirconium oxide according to claim 7, characterized in that, One side of the filter chamber (501) is fixedly connected with a motor bracket (513), and a driving motor one (514) is fixedly connected to the outer side of the motor bracket (513). The output shaft of the driving motor one (514) is fixedly connected with a rotating shaft (516) through a shaft coupling. The end of the rotating shaft (516) is fixedly connected with a scraping frame (517). The scraping frame (517) is in contact with the outer side of the filter screen (512). The bottom of the filter chamber (501) below the scraping frame (517) is fixedly connected with an impurity collecting box (518). One side of the filter chamber (501) away from the gas suction box (503) is fixedly connected with a gas impurity storage tank (502). One side of the gas impurity storage tank (502) is provided with an exhaust hole. The inside of the exhaust hole is fixedly connected with an exhaust pipe (504). The outer side of the exhaust pipe (504) is connected with a pipe valve (505) through a flange. One side of the filter chamber (501) is fixedly connected with a collecting pump (506). The collecting end of the collecting pump (506) is connected to the inside of the filter chamber (501) through a pipeline. The conveying end of the collecting pump (506) is fixedly connected with an air guide pipe (511). The air guide pipe (511) is inserted into the inside of the gas impurity storage tank (502).
Citation Information
Patent Citations
Multi-functional stirring equipment for factories
CN112221414A
Waste gas treatment device for tantalum powder production
CN116585815A