A kind of hair care peptide essence lotion and preparation method thereof

Abstract

The present application relates to the field of bioactive peptide application technology, and specifically discloses a hair care peptide essence lotion and a preparation method thereof. A hair care peptide essence lotion is made from the following raw materials in parts by weight: 45-65 parts of deionized water; 1-5 parts of emulsifier; 0.1-0.3 parts of preservative; 0.5-2.5 parts of oligopeptide-3; 10-12 parts of hair care extract mixture; 0.5-3 parts of glyceryl stearate; 1-5 parts of cetearyl alcohol polyether-25; 0.5-2.5 parts of stearyl trimethylammonium chloride; 0.8-1 parts of ethanol; 0.05-0.2 parts of fragrance 0.1-1 parts of biotin; 0.1-2 parts of chlorophyll; 0.2-0.6 parts of wheat hydrolyzed protein; 4-8 parts of donkey bone collagen peptide; 0.5-2 parts of green prune fruit oil; 1-3 parts of fermented Dendrobium candidum; Fermented Dendrobium candidum is obtained by: S1, mixing the Dendrobium candidum raw material with distilled water to prepare a fermentation stock solution; S2, inoculating the fermentation stock solution with mixed bacteria for fermentation, adding Ganoderma lucidum polysaccharide during the fermentation process, and then centrifuging to obtain the supernatant. The hair care peptide essence lotion of the present application is not only suitable for people with sensitive skin with damaged skin barrier, but also can bring excellent hair care effects.

Description

Technical Field

[0001] The present application relates to the technical field of bioactive peptide applications, and more specifically, to a hair care peptide essence lotion and a preparation method thereof. Background Art

[0002] Hair care peptide is an active peptide that can quickly repair hair in a short period of time. It is derived from keratin itself, is safe and has no side effects. It can not only strengthen the toughness and elasticity of hair, make hair smooth and enhance its luster, but also reorganize the hair structure by stabilizing the keratin chain, revive damaged hair from the root, and give hair new vitality.

[0003] At present, hair peptides are usually combined with other functional ingredients to prepare an efficient hair care product, such as essence milk. Essence milk has the excellent characteristics of being easy to apply and wash-free. You only need to take an appropriate amount of essence milk and apply it evenly on the hair, and gently massage for 1-3 minutes for complete absorption. Therefore, it is increasingly favored by consumers. However, people with sensitive skin with damaged skin barrier are often greatly restricted in the selection of the above products, because sensitive skin people have poor resistance to external stimuli and weak self-repair ability. At this time, the skin is usually in a highly reactive state. Once the skin barrier is damaged, it is often the skin's sebum membrane or stratum corneum that is damaged. At this time, it will have a great difference in the treatment of some substances that can be absorbed by normal people.

[0004] With respect to the above-mentioned related technologies, the inventor believes that the essence lotion containing hair care peptides currently on the market is often not suitable for people with sensitive skin with damaged skin barrier in order to pursue stronger hair care effects. Because the skin tolerance is too low, excessive reactions often occur, such as scalp itching and scalp redness. Moreover, after long-term and large-scale use, it not only fails to bring the expected hair care effect, but also causes dry and broken hair. Therefore, it is urgent to propose a solution to solve the above technical problems. Summary of the invention

[0005] In order to obtain a hair care peptide product that has excellent hair care effects and is suitable for people with sensitive skin who have damaged skin barriers, the present application provides a hair care peptide essence lotion and a preparation method thereof.

[0006] In the first aspect, the present application provides a hair care peptide essence lotion, which adopts the following technical solution:

[0007] A hair care peptide essence lotion is prepared from the following raw materials in parts by weight:

[0008] 45-65 parts of deionized water;

[0009] Emulsifier 1-5 parts;

[0010] Preservative 0.1-0.3 parts;

[0011] Oligopeptide-3 0.5-2.5 parts;

[0012] 10-12 parts of hair care extract mixture;

[0013] Glyceryl stearate 0.5-3 parts;

[0014] Ceteareth-25 1-5 parts;

[0015] 0.5-2.5 parts of stearyl trimethyl ammonium chloride;

[0016] 0.8-1 part of ethanol;

[0017] Essence 0.05-0.2 parts;

[0018] Biotin 0.1-1 part;

[0019] Chlorophyll 0.1-2 parts;

[0020] 0.2-0.6 parts of hydrolyzed wheat protein;

[0021] 4-8 portions of donkey bone collagen peptide;

[0022] 0.5-2 parts of prickle oil;

[0023] 1-3 parts of fermented Dendrobium officinale;

[0024] The fermented Dendrobium officinale is prepared by the following steps:

[0025] S1. Grind the raw material of Dendrobium officinale and mix it with distilled water at a ratio of 1: (25-35), extract it at 85-90° C. for 2-3 hours, and take the supernatant after centrifugation to obtain the fermentation stock solution;

[0026] S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate 4-7% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 30-35°C and a fermentation speed of 150-170r / min for 2-3 days, and add 5-10 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

[0027] By adopting the above technical scheme, a large number of polar and charged groups are exposed in the oligopeptide-3 molecules, which can combine with water molecules to form hydrogen bonds, which is beneficial to maintaining the watery environment of the skin, and can also penetrate the dermis through the skin's stratum corneum to exert its effect, bringing anti-aging, promoting skin collagen metabolism, whitening and repairing effects; the hair care extract mixture is composed of a variety of natural plant extracts, which can not only enhance the activity of tyrosinase, but also promote the absorption of nutrients, thereby promoting the formation of melanin, promoting hair growth, and making the hair black and moisturizing; biotin can improve hair quality, reduce hair loss, hair breakage, and frizzy hair, and make hair more shiny; in the hair care peptide essence lotion, the combination of the above oligopeptide-3, hair care extract mixture and biotin can bring stronger hair care effects.

[0028] At the same time, in order to make the hair care peptide essence lotion more suitable for people with sensitive skin with damaged skin barrier and bring positive hair care effects, it is mainly achieved through the combination of donkey bone collagen peptides, prickly ash oil and fermented Dendrobium officinale. In addition to removing impurities and strengthening proteins, donkey bone collagen peptides can also promote the proliferation and migration of keratinocytes, thereby accelerating the repair of the epidermal barrier; prickle fruit oil can increase tight junction proteins at the protein level, and by accelerating the expression of intercellular lipid synthase in the epidermal permeability barrier, improve lipid synthesis, and thus bring about a repair effect on the skin barrier; fermented Dendrobium officinale is obtained by double-bacteria fermentation and the use of Ganoderma lucidum polysaccharide for stimulation and regulation during the fermentation process. It is rich in sugars, proteins, amino acids, fatty acids, polyphenols and other ingredients, which can play an excellent balancing and regulating role in the complex micro-ecological system of the scalp; and the combination of donkey bone collagen peptides, prickle fruit oil and fermented Dendrobium officinale can play an excellent compound synergistic role, especially for people with sensitive skin with damaged skin barriers, can form a coordinated mechanism of internal repair and external recovery, while improving the skin barrier function, it can also assist the skin in absorbing and transforming high-efficiency hair care ingredients, and in the process can also improve skin tolerance and reduce irritation, so that the hair care peptide essence lotion can play an excellent hair care effect after application.

[0029] Preferably, the fermented Dendrobium officinale is prepared by the following steps:

[0030] S1. Grind the raw material of Dendrobium officinale and mix it with distilled water at a ratio of 1:30, extract it at 90° C. for 2 h, and take the supernatant after centrifugation to obtain the fermentation stock solution;

[0031] S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate it with 5% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 30°C and a fermentation speed of 150r / min for 2 days, and add 10 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

[0032] By adopting the above technical scheme and controlling the above parameters in the preparation of fermented Dendrobium officinale, reducing sugars can be fully decomposed and utilized by microorganisms during the process, large molecular polysaccharides are decomposed into small molecules, and some small molecular polysaccharides are decomposed into diversified monosaccharides; at the same time, the contents of protein, amino acids, short-chain fatty acids and polyphenols are also relatively high; the fermented Dendrobium officinale obtained at this time contains a relatively rich ingredient system, which can not only exert better its own efficacy during the application process, but also have a relatively excellent coordination effect with donkey bone collagen peptides and prickle oil, thereby making the final hair care peptide essence milk more suitable for people with sensitive skin with damaged skin barrier, and the hair care effect it brings is also relatively excellent.

[0033] Preferably, the ratio of the combined fermentation of yeast and lactic acid bacteria is 3:7.

[0034] By adopting the above technical scheme and selecting the above fermentation ratio, better cooperation can be exerted between each other, and the stability of the fermentation system can be increased to ensure the smooth progress of the fermentation process. At the same time, the mixed bacteria and the added Ganoderma lucidum polysaccharide have a better cooperative effect during the fermentation process, so that the obtained fermented Dendrobium officinale has better application quality, and the overall application effect of the hair care peptide essence lotion is also relatively excellent.

[0035] Preferably, the weight ratio of the donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium officinale is 6:1:1.5.

[0036] By adopting the above technical scheme, when the donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium officinale in the above weight ratio are combined, the corresponding effects exerted are relatively excellent, making the hair care peptide essence lotion not only more suitable for people with sensitive skin with damaged skin barrier, but also able to show relatively excellent hair care effects.

[0037] Preferably, 3-5 parts by weight of auxiliary functional additives are added to the raw materials of the hair care peptide essence lotion, and the auxiliary functional additives are composed of citrus hydrosol pectin, fish sauce and tea bran powder, and the weight ratio of citrus hydrosol, fish sauce and tea bran powder is (3-5):1:(0.4-0.7).

[0038] By adopting the above technical scheme, citrus water-soluble pectin is a water-soluble colloid gradient extract obtained by mixing citrus peel and water and then heating and filtering, which is not only beneficial to maintaining the stability of skin and mucous membranes, but also has a good emulsification stabilization effect; fish sauce is rich in nutrients such as protein, amino acids, vitamins, minerals, etc., and can be used as a nutritional supplement; tea bran micropowder is rich in tea polyphenols, catechins and other antioxidant substances, which can effectively remove free radicals and prevent the occurrence of oxidation reactions, thereby achieving antioxidant and anti-aging effects; and citrus water-soluble pectin, fish sauce and tea bran micropowder are mixed according to the conditions of the invention. When the functional additives composed within a specific weight ratio range are used, through the compounding of the three, firstly, when the sensitive skin with damaged skin barrier absorbs the effective ingredients, the positive and negative charge balance of the skin can be maintained, which is conducive to achieving better absorption and conversion effects of the effective ingredients; secondly, in the process of micro-ecological system recovery and skin barrier repair, a rich supply of materials is provided to maintain cell homeostasis, which is conducive to avoiding the occurrence of greater stimulation. Therefore, the process is more conducive to donkey bone collagen peptides, prickle oil and fermented Dendrobium officinale to play a more powerful role, so that the overall quality of the hair care peptide essence lotion is significantly improved.

[0039] Preferably, the weight ratio of the citrus hydrosol, fish sauce and tea bran powder is 4.5:1:0.5.

[0040] By adopting the above technical scheme, the auxiliary functional additives composed of citrus hydrosol, fish sauce and tea bran powder in the above weight ratio have better effects when used, and the hair care peptide essence lotion finally obtained has better applicability and hair care effect for people with sensitive skin with damaged skin barrier.

[0041] Preferably, the emulsifier is one or a combination of cetearyl alcohol, polysorbate-20, alkyl polyglucoside, lecithin and steareth-6.

[0042] By adopting the above technical scheme, the above types of emulsifiers are all suitable for the preparation of hair care peptide essence lotion, which can make the various component raw materials fully combined and form a stable combination state. The hair care peptide essence lotion obtained by application not only has a lighter and more delicate texture, but is also easier to spread and apply evenly during use.

[0043] Preferably, the preservative is one or a combination of p-hydroxyacetophenone, phenoxyethanol, caprylyl glycol and hydroquinone.

[0044] By adopting the above technical solution, the above types of preservatives can prevent the growth of bacteria and enable the hair care peptide essence lotion to maintain excellent product stability during storage.

[0045] Preferably, the hair care extract mixture is a combination of angelica extract, black ganoderma extract, polygonum multiflorum extract, ginseng extract, black mulberry extract, Polygonum multiflorum vine extract, European larch wood extract, tea extract, Panax notoginseng extract, gallnut extract, ginger root extract, Platycladus orientalis leaf extract, black sesame extract, and South American annatto seed extract.

[0046] By adopting the above technical solutions, angelica extract can increase the oxygen and nutrient supply of the skin, relieve skin fatigue, and improve the skin's self-repair ability; black ganoderma extract is rich in vitamins and minerals, which can nourish hair and make hair healthier; Polygonum multiflorum extract has the effect of promoting melanin synthesis and activating tyrosinase, which can nourish hair and increase melanin; ginseng extract is rich in various active ingredients and can provide the nutrients and antioxidant protection required by the skin; black mulberry extract has a significant effect on promoting hair growth and improving hair quality; Polygonum multiflorum vine extract has certain skin conditioning effects and can help balance oil secretion; European larch wood extract has moisturizing, soothing and anti-allergic effects; tea The extract has a strong anti-oxidation ability and can promote the production of collagen; Panax notoginseng extract not only has a strong ability to scavenge free radicals, but also can regulate the skin's immunity and has a good antioxidant effect; Gallnut extract has good whitening, astringent, anti-inflammatory, antioxidant, antibacterial and other effects; Ginger root extract can promote hair growth and bring anti-inflammatory effects; Platycladus orientalis leaf extract can provide sufficient nutrition and control sebum secretion; Black sesame extract enhances the brightness and softness of hair and provides the necessary nutrition for hair roots; South American Annatto seed extract can strengthen hair and resist ultraviolet rays and heat damage; and applying the above ingredients to form a hair care extract mixture and applying it to hair care peptide essence lotion can bring more excellent hair care effects.

[0047] In a second aspect, the present application provides a method for preparing a hair care peptide essence lotion, using the following technical solution:

[0048] A method for preparing a hair care peptide essence lotion comprises the following steps:

[0049] (1) preparing raw materials including deionized water, emulsifier, preservative, oligopeptide-3, hair care extract mixture, glyceryl stearate, ceteareth-25, stearyl trimethyl ammonium chloride, ethanol, flavor, biotin, donkey bone collagen peptide, prune fruit oil and fermented Dendrobium officinale according to the ratio;

[0050] (2) The water, emulsifier, oligopeptide-3, hair care extract mixture, glyceryl stearate and prickle oil in step (1) are stirred and mixed at 65-75° C., and then vacuum homogenized at 5000-7000 rpm for 3-5 min. Then, the mixture is cooled to 45-55° C. and ceteareth-25, stearyl trimethylammonium chloride, donkey bone collagen peptide and fermented dendrobium officinale are added and stirred and mixed evenly. Then, the mixture is cooled to 30-40° C. and ethanol, essence and biotin are added and stirred and mixed evenly. After natural cooling, a hair care peptide essence lotion can be obtained.

[0051] By adopting the above technical scheme, the above preparation method is simple to operate, and can obtain a hair care peptide essence milk with excellent and stable quality on the basis of fully mixing and combining the raw materials, which is convenient for large-scale industrial production; at the same time, different addition orders and temperature changes are adopted in the use of each raw material, which is convenient for quality control in the production process, and is conducive to ensuring that the obtained hair care peptide essence milk has high quality.

[0052] In summary, this application has the following beneficial effects:

[0053] 1. The present application adopts the combination of donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium candidum. Through the excellent compound synergistic effect among the three, it can form a coordination mechanism of internal repair and external recovery for people with sensitive skin whose skin barrier is damaged. While improving the skin barrier function, it can also assist the skin in absorbing and transforming high-efficiency hair care ingredients. In the process, it can also improve skin tolerance and reduce irritation, so that the hair care peptide essence lotion can play an excellent hair care effect;

[0054] 2. In the present application, citrus water-soluble pectin, fish sauce and tea bran powder are used as functional additives in a specific weight ratio range and applied to the hair care peptide essence lotion. Not only can it maintain the positive and negative charge balance of the skin when the effective ingredients are absorbed by sensitive skin with damaged skin barrier, which is conducive to achieving better absorption and conversion effects of the effective ingredients, but it also provides a rich supply of materials in the process of micro-ecological system recovery and skin barrier repair, maintains cell homeostasis, and helps avoid the occurrence of greater stimulation, so that the hair care peptide essence lotion is more suitable for people with sensitive skin with damaged skin barrier, and the hair care effect it brings is also relatively excellent. DETAILED DESCRIPTION

[0055] The present application is further described in detail below with reference to the embodiments.

[0056] Unless otherwise specified, the raw materials used in the preparation examples, embodiments and comparative examples of the present application are commercially available.

[0057] Donkey bone collagen peptide was purchased from Gansu Yishengxiang Biotechnology Co., Ltd., with a specification of 80 mesh and a molecular weight of 500 Daltons;

[0058] Citrus water-soluble pectin was purchased from Mufan Biotechnology's 96% low-molecular-weight citrus pectin;

[0059] Tea bran powder is provided by Waterless Bio, and is spray-dried powder extracted from raw materials at a ratio of 20:1.

[0060] Preparation examples of raw materials and / or intermediates

[0061] Preparation Example 1

[0062] A fermented Dendrobium officinale is prepared by the following steps:

[0063] S1. Grind the raw material of Dendrobium officinale into 800 meshes and mix it with distilled water at a ratio of 1:30, extract at 90° C. for 2 h, centrifuge and take the supernatant to obtain a fermentation stock solution;

[0064] S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate it with 5% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 30°C and a fermentation speed of 150r / min for 2 days, and add 10 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

[0065] Note: In the above operation, the ratio of the combined fermentation of yeast and lactic acid bacteria is 3:7.

[0066] Preparation Example 2

[0067] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that it is prepared by the following steps:

[0068] S1. Grind the raw material of Dendrobium officinale into 800 meshes and mix it with distilled water at a ratio of 1:25, extract it at 85° C. for 3 h, and take the supernatant after centrifugation to obtain the fermentation stock solution;

[0069] S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate it with 4% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 35°C and a fermentation speed of 170r / min for 3 days, and add 5 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

[0070] Preparation Example 3

[0071] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that it is prepared by the following steps:

[0072] S1. Grind the raw material of Dendrobium officinale into 800 meshes and mix it with distilled water at a ratio of 1:35, extract it at 90° C. for 2.5 h, centrifuge it and take the supernatant to obtain the fermentation stock solution;

[0073] S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate it with 7% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 30°C and a fermentation speed of 160r / min for 2.5, and add 7.5 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

[0074] Preparation Example 4

[0075] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that the ratio of the combined fermentation of yeast and lactic acid bacteria is 3.5:7.

[0076] Preparation Example 5

[0077] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that the ratio of the combined fermentation of yeast and lactic acid bacteria is 3:7.5.

[0078] Preparation Example 6

[0079] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that only yeast is used in the fermentation process.

[0080] Preparation Example 7

[0081] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that only lactic acid bacteria are used in the fermentation process.

[0082] Preparation Example 8

[0083] A fermented Dendrobium officinale, which is different from Preparation Example 1 in that no Ganoderma lucidum polysaccharide is added to the fermentation mixture during the fermentation process.

[0084] Example

[0085] Example 1

[0086] A hair care peptide essence lotion, the raw materials used and their corresponding weight parts are shown in Table 1, and is prepared by the following method:

[0087] (1) preparing raw materials including deionized water, emulsifier, preservative, oligopeptide-3, hair care extract mixture, glyceryl stearate, ceteareth-25, stearyl trimethyl ammonium chloride, ethanol, flavor, biotin, donkey bone collagen peptide, prune fruit oil and fermented Dendrobium officinale according to the ratio;

[0088] (2) The water, emulsifier, oligopeptide-3, hair care extract mixture, glyceryl stearate and utila utila oil in step (1) are stirred and mixed uniformly at 65-75° C. (70° C. is selected in this embodiment), and then vacuum homogenized at 5000-7000 rpm (6000 rpm is selected in this embodiment) for 3-5 min (5 min is selected in this embodiment), and then the temperature is lowered to 45-55° C. (50° C. is selected in this embodiment), and then cetearyl alcohol polyether-25, stearyl trimethyl ammonium chloride, donkey bone collagen peptide and fermented dendrobium officinale are added and stirred and mixed uniformly, and then the temperature is lowered to 30-40° C. (35° C. is selected in this embodiment), and then ethanol, essence and biotin are added and stirred and mixed uniformly, and after natural cooling, a hair care peptide essence lotion can be obtained.

[0089] Note: In the above operation, the fermented Dendrobium officinale is the one obtained in Preparation Example 1; the biotin is D-biotin; the essence is cinnamaldehyde; the emulsifier is cetearyl alcohol; the preservative is phenoxyethanol; the hair care extract mixture is a composition of angelica extract, black ganoderma extract, Polygonum multiflorum extract, ginseng extract, black mulberry extract, Polygonum multiflorum vine extract, European larch wood extract, tea extract, Panax notoginseng extract, Galla chinensis extract, ginger root extract, Platycladus orientalis leaf extract, black sesame extract, and South American Annatto seed extract, and the ratio is 13:7.5:6:5:4.5:3:2:1.5:1:0.8:0.7:0.5:0.3:0.1.

[0090] Example 2-3

[0091] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials used and their corresponding weight parts are as shown in Table 1.

[0092] Table 1 Raw materials and their weight parts in Examples 1-3 (kg / part)

[0093]

[0094]

[0095] Example 4

[0096] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 2.

[0097] Example 5

[0098] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 3.

[0099] Example 6

[0100] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 4.

[0101] Example 7

[0102] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 5.

[0103] Example 8

[0104] A hair care peptide essence lotion is different from Example 1 in that the total amount of donkey bone collagen peptide, prickle fruit oil and fermented dendrobium officinale remains unchanged, and the weight ratio of the three is adjusted to 6:1:1.5.

[0105] Example 9

[0106] A hair care peptide essence lotion, which is different from Example 1 in that 4 parts by weight of an auxiliary functional additive are also added to the raw materials, the auxiliary functional additive is composed of citrus water-soluble pectin, fish sauce and tea bran powder in a weight ratio of 4.5:1:0.5, and in the preparation process of the hair care peptide essence lotion, the auxiliary functional additive is added together with fermented Dendrobium officinale.

[0107] Example 10

[0108] A hair care peptide essence lotion, which is different from Example 9 in that the weight parts of the auxiliary functional additives added are 3 parts.

[0109] Embodiment 11

[0110] A hair care peptide essence lotion, which is different from Example 9 in that the weight parts of the auxiliary functional additives added are 5 parts.

[0111] Example 12

[0112] A hair care peptide essence lotion, which is different from Example 9 in that the auxiliary functional additive is composed of citrus water-soluble pectin, fish sauce and tea bran powder in a weight ratio of 3:1:0.4.

[0113] Example 13

[0114] A hair care peptide essence lotion, which is different from Example 9 in that the auxiliary functional additive is composed of citrus water-soluble pectin, fish sauce and tea bran powder in a weight ratio of 5:1:0.7.

[0115] Embodiment 14

[0116] A hair care peptide essence lotion, which is different from Example 9 in that the auxiliary functional additive is composed of citrus water-soluble pectin, fish sauce and tea bran powder in a weight ratio of 4:1:0.55.

[0117] Embodiment 15

[0118] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain citrus water-soluble pectin.

[0119] Example 16

[0120] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain fish sauce.

[0121] Embodiment 17

[0122] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain tea bran powder.

[0123] Embodiment 18

[0124] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain citrus water-soluble pectin and fish sauce.

[0125] Embodiment 19

[0126] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain tea bran powder and fish sauce.

[0127] Embodiment 20

[0128] A hair care peptide essence lotion, which is different from Example 9 in that the raw materials do not contain citrus water-soluble pectin and tea bran powder.

[0129] Comparative Example

[0130] Comparative Example 1

[0131] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 6.

[0132] Comparative Example 2

[0133] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 7.

[0134] Comparative Example 3

[0135] A hair care peptide essence lotion, which is different from Example 1 in that the fermented Dendrobium officinale is obtained in Preparation Example 8.

[0136] Comparative Example 4

[0137] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain donkey bone collagen peptide.

[0138] Comparative Example 5

[0139] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain prickle fruit oil.

[0140] Comparative Example 6

[0141] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain fermented Dendrobium officinale.

[0142] Comparative Example 7

[0143] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain donkey bone collagen peptide and prickle fruit oil.

[0144] Comparative Example 8

[0145] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain donkey bone collagen peptides and fermented Dendrobium officinale.

[0146] Comparative Example 9

[0147] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain prickle oil and fermented dendrobium officinale.

[0148] Comparative Example 10

[0149] A hair care peptide essence lotion, which is different from Example 1 in that the raw materials do not contain donkey bone collagen peptide, prickle fruit oil and fermented dendrobium officinale.

[0150] Performance testing

[0151] Test samples: The hair care peptide essence milk obtained in Examples 1-20 was used as test samples 1-20, and the hair care peptide essence milk obtained in Comparative Examples 1-10 was used as control samples 1-10.

[0152] Test method: 60 people with sensitive skin and damaged skin barrier, aged 18-30 years old, were selected for the experiment and divided into 30 groups, with one male and one female in each group, and test samples 1-20 and control samples 1-10 were used respectively.

[0153] Before use, clean the test area with clean water, apply 0.5ml of hair peptide essence milk to the test area of ​​4cm*4cm, and massage with your hands in circles for 3 minutes, once in the morning and once in the evening, apply to the same area, and do the following test after 5 days:

[0154] (1) Transepidermal water loss reduction rate test. Transepidermal water loss (TEWL) is a physical parameter that indicates the normal and continuous diffusion of water through the stratum corneum of the skin. It represents the loss of water in the stratum corneum of the skin and is a common indicator of skin barrier function. When the skin barrier function is damaged, the water content of the stratum corneum of the skin will decrease and the transepidermal water loss (TEWL) will increase. The German CK skin tester Tewameter TM Hex was used to test the transepidermal water loss of the subjects before and after using the hair peptide essence lotion. The transepidermal water loss reduction rate = (pre-test value - post-test value) / pre-test value. Among them, the higher the transepidermal water loss reduction rate, the better the application effect of the hair peptide essence lotion.

[0155] (2) Rating of irritation: observe the test skin of the subject to check for the presence of erythema, and record the subject's feelings about the test skin during use, mainly focusing on stinging, burning and tightness, and divide the severity into 0-10 levels, where 0 is a negative reaction, no erythema, no stinging, burning and tightness; 10 is a severe positive reaction, obvious erythema, stinging, burning and tightness, and the reaction exceeds the skin test area; the test result of each group is the average of the ratings of the two people in each group.

[0156] (3) Evaluation of scalp ecological balance. As the soil for hair growth, the scalp's micro-ecological environment is crucial. This benign ecological system is maintained by the balance of oil, bacteria, and metabolism. Once this ecological environment is out of balance, problems such as oily scalp, itching, and dandruff will occur. Oily scalp is mainly caused by abnormal oil secretion, itching is caused by the proliferation of harmful bacteria, and dandruff is caused by metabolic imbalance. The severity of oily scalp, itching, and dandruff is evaluated on a scale of 0-10, with 10 being the best and 0 being the worst. The test result of each group is the average of the evaluation scores of the two people in each group.

[0157] (4) Glossiness improvement rate test: When light is irradiated on the hair, part of the light will enter the hair fiber; part of the light will be reflected or refracted on the surface of the hair cuticle composed of dense keratin. Healthy hair often emits stronger gloss, so the hair care, repair, and nourishment effects of the hair care peptide essence can be evaluated by measuring the hair glossiness. The hair glossiness of the subjects was measured before and after using the hair care peptide essence using the hair glossiness tester SAMBA HAIR, and the glossiness improvement rate = (post-test value - pre-test value) / pre-test value. The higher the glossiness improvement rate, the better the application effect of the hair care peptide essence.

[0158] Table 2 Application test results of test samples 1-20 and control samples 1-10

[0159]

[0160]

[0161] Combining Example 1 and Comparative Examples 4-10 with Table 2, it can be seen that the combination of donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium candidum can make the hair care peptide essence lotion perform better in terms of transepidermal water loss reduction rate, irritation rating, scalp ecological balance evaluation and gloss improvement rate after being applied to sensitive skin groups with damaged skin barrier; if only any one or two of donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium candidum are used, the effect brought is limited, and the effects between them are only simply superimposed. It can be seen that only when the three are combined can they bring about an outstanding synergistic effect; among them, when donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium candidum are not used, it is found that the transepidermal water loss reduction rate is negative, indicating that the skin barrier is severely damaged. It may be that other effective ingredients have brought about stimulation during the absorption process, and the irritation relief effect of any one or two of donkey bone collagen peptide, prickle fruit oil and fermented Dendrobium candidum is also extremely limited. Only when the three are combined can they bring about a greater effect in this regard.

[0162] In combination with Example 1 and Comparative Examples 1-3 and Table 2, it can be seen that the fermented Dendrobium officinale is obtained by double-bacteria fermentation and stimulation and regulation by Ganoderma lucidum polysaccharide during the fermentation process, so that the obtained fermented Dendrobium officinale can exert a better coordination effect with donkey bone collagen peptide and prune thorn fruit oil after application, while the fermented Dendrobium officinale obtained by single-bacteria fermentation or lack of Ganoderma lucidum polysaccharide for stimulation and regulation, it is found that the hair care peptide essence lotion has obvious losses in transepidermal water loss reduction rate, scalp ecological balance evaluation and gloss improvement rate; combined with Implementation 6-7 and Table 2, it can be seen that when the ratio of the combined fermentation of yeast and lactic acid bacteria is 3:7, the effect of the hair care peptide essence lotion on sensitive skin people with damaged skin barrier is relatively excellent.

[0163] Combining Examples 1-3 and Example 8 with Table 2, it can be seen that when the weight ratio of donkey bone collagen peptide, prickle oil and fermented Dendrobium officinale is 6:1:1.5, the hair care peptide essence lotion can not only be more suitable for people with sensitive skin with damaged skin barrier, but also can show a relatively excellent hair care effect.

[0164] In combination with Example 1 and Example 9-14 and Table 2, it can be seen that the application of citrus water-soluble pectin, fish sauce and tea bran powder in a specific weight ratio range as functional additives in the hair care peptide essence milk can bring about a positive improvement in the transdermal water loss reduction rate, scalp ecological balance evaluation and glossiness improvement rate. Among them, when the weight ratio of citrus water sol, fish sauce and tea bran powder is 4.5:1:0.5, the improvement effect is relatively excellent. In combination with Examples 15-20 and Table 2, it can be seen that if only any one or two of citrus water-soluble pectin, fish sauce and tea bran powder are added, although a simple improvement in the corresponding effect can be brought, the improvement space is limited, and it is only a simple superposition of the effect. Only when the three ingredients are used together can a more prominent and significant coordination effect be brought, so that the hair care peptide essence milk is more suitable for sensitive skin people with damaged skin barriers, and the hair care effect brought is also relatively excellent.

[0165] This specific embodiment is merely an explanation of the present application and is not a limitation of the present application. After reading this specification, those skilled in the art may make modifications to the present embodiment without any creative contribution as needed. However, as long as it is within the scope of the claims of the present application, it shall be protected by the patent law.

Claims

1. A hair care peptide essence lotion, characterized in that: Made from the following raw materials in parts by weight: 45-65 parts of deionized water; Emulsifier 1-5 parts; Preservative 0.1-0.3 parts; Oligopeptide-3 0.5-2.5 parts; 10-12 parts of hair care extract mixture; Glyceryl stearate 0.5-3 parts; Ceteareth-25 1-5 parts; 0.5-2.5 parts of stearyl trimethyl ammonium chloride; 0.8-1 part of ethanol; Essence 0.05-0.2 parts; Biotin 0.1-1 part; Chlorophyll 0.1-2 parts; 0.2-0.6 parts of hydrolyzed wheat protein; 4-8 portions of donkey bone collagen peptide; 0.5-2 parts of prickle oil; 1-3 parts of fermented Dendrobium officinale; The fermented Dendrobium officinale is prepared by the following steps: S1. Grind the raw material of Dendrobium officinale and mix it with distilled water at a ratio of 1: (25-35), extract it at 85-90° C. for 2-3 hours, and take the supernatant after centrifugation to obtain the fermentation stock solution; S2, sterilizing the fermentation stock solution at high temperature, cooling it and placing it in a fermentation container, inoculating 4-7% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then fermenting it at 30-35° C. and a fermentation speed of 150-170 r / min for 2-3 days, and adding 5-10 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process, and centrifuging and taking the supernatant after the fermentation is completed to obtain the fermented Dendrobium officinale; The hair care extract mixture is a composition of angelica extract, black ganoderma extract, polygonum multiflorum extract, ginseng extract, black mulberry extract, Polygonum multiflorum vine extract, European larch wood extract, tea extract, Panax notoginseng extract, gallnut extract, ginger root extract, Platycladus orientalis leaf extract, black sesame extract, and South American annatto seed extract.

2. The hair care peptide essence lotion according to claim 1, characterized in that: The fermented Dendrobium officinale is prepared by the following steps: S1. Grind the raw material of Dendrobium officinale and mix it with distilled water at a ratio of 1:30, extract it at 90° C. for 2 h, and take the supernatant after centrifugation to obtain the fermentation stock solution; S2. After high-temperature sterilization of the fermentation stock solution, cool it and place it in a fermentation container, inoculate it with 5% of a mixed bacteria obtained by mixing yeast and lactic acid bacteria, and then ferment it at 30°C and a fermentation speed of 150r / min for 2 days, and add 10 / L of Ganoderma lucidum polysaccharide to the fermentation mixture during the fermentation process. After the fermentation is completed, centrifuge and take the supernatant to obtain the fermented Dendrobium officinale.

3. The hair care peptide essence lotion according to claim 1, characterized in that: The ratio of the combined fermentation of yeast and lactic acid bacteria is 3:

7.

4. The hair care peptide essence lotion according to claim 1, characterized in that: The weight ratio of the donkey bone collagen peptide, prickle fruit oil and fermented dendrobium officinale is 6:1:1.

5.

5. The hair care peptide essence lotion according to claim 1, characterized in that: The raw materials of the hair care peptide essence milk are further added with 3-5 parts by weight of auxiliary functional additives, which are composed of citrus water-soluble pectin, fish sauce and tea bran powder, and the weight ratio of citrus water-soluble pectin, fish sauce and tea bran powder is (3-5):1:(0.4-0.7).

6. The hair care peptide essence lotion according to claim 5, characterized in that: The weight ratio of the citrus water-soluble pectin, fish sauce and tea bran powder is 4.5:1:0.

5.

7. The hair care peptide essence lotion according to claim 1, characterized in that: The emulsifier is one or a combination of cetearyl alcohol, polysorbate-20, alkyl polyglucoside, lecithin and steareth-6.

8. The hair care peptide essence lotion according to claim 1, characterized in that: The preservative is one or a combination of p-hydroxyacetophenone, phenoxyethanol, caprylyl glycol and hydroquinone.

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