Reactor and reaction system containing the same

By designing multiple heat exchange plates and heat exchange medium input and output tubes arranged at intervals in chemical reactors, the problems of small heat exchange area and poor mixing effect in existing reactors are solved, efficient heat exchange and material mixing are achieved, and production efficiency is improved.

CN118527094BActive Publication Date: 2025-04-08ZHONGSHAN ZHIAN CHEM TECH CO
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Patent Information

Application Number
CN202410861224.5
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-06-28
Publication Date
2025-04-08
Estimated Expiration
2044-06-28

AI Technical Summary

Technical Problem

The existing chemical reactors have problems such as small heat exchange area, low heat exchange efficiency, poor material mixing effect and low production efficiency, which cannot meet higher production requirements.

Method used

A reactor is designed, which includes a reactor body and a heat exchange structure. The reactor main body is provided with a reaction tube lumen, an inlet port and an outlet port. The heat exchange structure consists of a plurality of heat exchange plates arranged at intervals along the length of the reaction tube lumen. The heat exchange plate causes the material to form a tortuous flow, and is connected to the heat exchange medium input tube and the output tube through the hollow channel to achieve efficient heat exchange.

Benefits of technology

By increasing the heat exchange area and optimizing material flow, the heat exchange efficiency and material mixing effect are improved, thereby improving production efficiency and achieving continuous and efficient production.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present invention discloses a reactor and a reaction system including the same. The reactor includes a reactor body and a heat exchange structure. The reactor body is provided with a reaction tube cavity, a feed port and a discharge port. The feed port is connected to one end of the reaction tube cavity along the length direction, and the discharge port is connected to the other end of the reaction tube cavity along the length direction. The heat exchange structure is arranged on the reactor body, and the heat exchange structure includes a plurality of heat exchange plates arranged in the reaction tube cavity and arranged at intervals along the length direction of the reaction tube cavity. The heat exchange plates extend radially along the reaction tube cavity, and the heat exchange plates are used to make the material in the reaction tube cavity form a tortuous flow. The reactor of the above structure and the reaction system using the same can carry out continuous production, and have a large heat exchange area, high heat exchange efficiency, good material mixing effect, and high production efficiency.
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Description

Technical Field

[0001] The present invention relates to the field of chemical equipment, and in particular to a reactor and a reaction system comprising the same. Background Art

[0002] In the chemical industry, a reactor is a device that realizes the reaction process and is widely used in the chemical field. Existing reactors mainly include a main body with a reaction chamber. The materials participating in the reaction are input into the reaction chamber for mixing and reaction, and the reactants are output to the outside after being generated. The reactor is usually also equipped with a heat exchange structure to exchange heat with the materials in the reaction chamber to control the temperature of the reaction. However, the current reactors still have the defects of small heat exchange area, low heat exchange efficiency, poor mixing effect and low production efficiency, and cannot meet higher requirements. Summary of the invention

[0003] The present invention aims to solve at least one of the technical problems existing in the prior art. To this end, the present invention provides a reactor that can carry out continuous production, has a large heat exchange area, high heat exchange efficiency, good material mixing effect, and high production efficiency.

[0004] The present invention also provides a reaction system having the reactor.

[0005] According to the first aspect of the present invention, the reactor comprises: a reactor body and a heat exchange structure. The reactor body is provided with a reaction tube cavity, a feed port and a discharge port, the feed port is connected with one end of the reaction tube cavity along the length direction, and the discharge port is connected with the other end of the reaction tube cavity along the length direction. The heat exchange structure is arranged on the reactor body, and the heat exchange structure comprises a plurality of heat exchange plates arranged in the reaction tube cavity and arranged at intervals along the length direction of the reaction tube cavity, the heat exchange plates extend along the radial direction of the reaction tube cavity, and the heat exchange plates are used to make the material in the reaction tube cavity form a tortuous flow.

[0006] The reactor according to the embodiment of the present invention has at least the following beneficial effects: during production, the material is input into one end of the reaction tube cavity through the feed port, the material will move along the reaction tube cavity to the other end, and the product after the material mixing reaction is output through the discharge port, thereby forming continuous production. In the above process, the heat exchange plates of the heat exchange structure form an obstacle to the material, so that the material forms a tortuous flow between the multiple heat exchange plates, and the heat exchange plates also perform heat exchange on the tortuous flow of the material. The above reactor adopts the arrangement of multiple heat exchange plates, the heat exchange area is large, and the material can form a tortuous flow between the heat exchange plates, the heat exchange efficiency is high, and the mixing effect between the materials is good, thereby improving the production efficiency.

[0007] According to some embodiments of the present invention, a stirring component is further included, which is arranged on the reactor body. The stirring component includes a stirring shaft, stirring blades and a rotary driver. The stirring shaft is arranged along the length direction of the reaction tube cavity and extends into the reaction tube cavity. The stirring blades are arranged on the stirring shaft, and the rotary driver is used to drive the stirring shaft to rotate.

[0008] According to some embodiments of the present invention, the heat exchange plate is disc-shaped, the heat exchange plate is provided with a central through hole, the stirring shaft is penetrated through the central through hole of each of the heat exchange plates, the heat exchange plate is divided into a larger plate and a smaller plate, the diameter of the larger plate is larger than that of the smaller plate, the diameter of the central through hole of the larger plate is larger than the diameter of the central through hole of the smaller plate, the larger plate and the smaller plate are arranged alternately, and an outer peripheral channel connecting the two sides of the smaller plate is formed between the outer periphery of the smaller plate and the cavity wall of the reaction tube cavity, and an inner channel connecting the two sides of the larger plate is formed between the hole wall of the central through hole of the larger plate and the stirring shaft.

[0009] According to some embodiments of the present invention, the heat exchange structure includes a heat exchange medium input pipe and a heat exchange medium output pipe, the two ends of the heat exchange plate are respectively fixed to the heat exchange medium input pipe and the heat exchange medium output pipe, the heat exchange medium input pipe and the heat exchange medium output pipe form an assembly with the heat exchange plate and are together accommodated in the reaction tube cavity, the heat exchange plate is provided with a hollow channel, the tube cavity of the heat exchange medium input pipe and the tube cavity of the heat exchange medium output pipe are respectively connected to the two ends of the hollow channel of the heat exchange plate, and the heat exchange medium input pipe and the heat exchange medium output pipe are respectively provided with an input port and an output port.

[0010] According to some embodiments of the present invention, the heat exchange structure includes at least two sub-components, each of which includes a row of the heat exchange plates and is provided with a heat exchange medium input pipe and a heat exchange medium output pipe, both ends of the heat exchange plates are respectively fixed to the heat exchange medium input pipe and the heat exchange medium output pipe, the heat exchange plates are provided with hollow channels, the tube lumens of the heat exchange medium input pipe and the tube lumens of the heat exchange medium output pipe are respectively connected to both ends of the hollow channels of each of the heat exchange plates, and the heat exchange medium input pipe and the heat exchange medium output pipe are respectively provided with an input port and an output port; each row of the heat exchange plates of each of the sub-components is arranged around the outer peripheral side of the stirring shaft.

[0011] According to some embodiments of the present invention, the outer peripheral surface of the heat exchange plate includes a tube cavity opposite surface and a stirring shaft opposite surface, the tube cavity opposite surface is adapted to the shape of the tube wall of the reaction tube cavity, the heat exchange plate of the subassembly is divided into a larger plate and a smaller plate, the tube cavity opposite surface of the larger plate is closer to the tube wall of the reaction tube cavity than the tube cavity opposite surface of the smaller plate, the larger plates and the smaller plates are arranged alternately, and a peripheral channel connecting the two sides of the smaller plate is formed between the tube cavity opposite surface of the smaller plate and the cavity wall of the reaction tube cavity, and between the heat exchange plates of different subassemblies, the larger plates are opposite to each other one by one, and the smaller plates are opposite to each other one by one, and an inner channel is formed between the stirring shaft opposite surfaces of the two corresponding larger plates.

[0012] According to some embodiments of the present invention, the reactor body includes an inner shell and an outer shell, the reaction tube cavity is arranged in the inner shell, the heat exchange plate is a hollow shell extending from the shell wall of the inner shell into the reaction tube cavity, the outer shell is sleeved on the outer peripheral side of the inner shell, a heat exchange medium flow channel is formed between the outer shell and the inner shell, the shell inner space of the heat exchange plate is connected with the heat exchange medium flow channel, and the outer shell is provided with an inlet and an outlet connected with the heat exchange medium flow channel; the heat exchange plates are arranged in two rows, and the two rows of heat exchange plates are respectively arranged on both sides of the stirring shaft in the radial direction, and the two rows of heat exchange plates are staggered and arranged relative to each other.

[0013] According to some embodiments of the present invention, the stirring blade is provided between two adjacent heat exchange plates along the length direction of the reaction tube cavity.

[0014] According to some embodiments of the present invention, a shear plate is provided at one end of the stirring shaft close to the feed port, and the shear plate includes a fixed plate and a plurality of shear pieces. The fixed plate is arranged perpendicular to the stirring shaft and is fixed to the stirring shaft, and the shear pieces extend along the length direction of the reaction tube cavity. The shear pieces are arranged along the circumference of the reaction tube cavity and are provided on four edges of the fixed plate.

[0015] The reaction system according to the second embodiment of the present invention comprises the reactor according to the first embodiment of the present invention.

[0016] The reaction system according to the embodiment of the present invention has at least the following beneficial effects: due to the use of the reactor of the embodiment of the first aspect of the present invention, the reaction system can carry out continuous production, and has a large heat exchange area, high heat exchange efficiency, good material mixing effect, and high production efficiency.

[0017] Additional aspects and advantages of the present invention will be given in part in the following description and in part will be obvious from the following description, or will be learned through practice of the present invention. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] The above and / or additional aspects and advantages of the present invention will become apparent and easily understood from the description of the embodiments in conjunction with the following drawings, in which:

[0019] Figure 1 A three-dimensional schematic diagram of one embodiment of the present invention;

[0020] Figure 2 for Figure 1 One of the cross-sectional views of the structure shown;

[0021] Figure 3 for Figure 1 A three-dimensional schematic diagram of the heat exchange structure and stirring assembly in FIG.

[0022] Figure 4 for Figure 3 a front view of the structure shown;

[0023] Figure 5 for Figure 1 A second cross-sectional view of the structure shown;

[0024] Figure 6 for Figure 1 A three-dimensional schematic diagram of the structure shown with the outer shell removed;

[0025] Figure 7 It is a three-dimensional schematic diagram of the second embodiment of the present invention;

[0026] Figure 8 for Figure 7 a cross-sectional view of the structure shown;

[0027] Fig. 9 for Figure 7 A three-dimensional schematic diagram of the heat exchange structure and stirring assembly in FIG.

[0028] Fig.10 for Fig. 9 An exploded schematic diagram of the structure shown;

[0029] Fig.11 for Fig. 9 a front view of the structure shown;

[0030] Fig.12 for Figure 7 The structure shown is a three-dimensional schematic diagram after a portion of the outer shell is cut away;

[0031] Fig.13 It is a three-dimensional schematic diagram of the third embodiment of the present invention;

[0032] Fig.14 for Fig.13 a cross-sectional view of the structure shown;

[0033] Fig.15 for Fig.13A partial enlarged cross-sectional view of the structure shown;

[0034] Fig.16 for Fig.13 A three-dimensional schematic diagram of the structure shown with the outer shell removed;

[0035] Fig.17 for Fig.13 The structure shown is a front view with the outer shell removed.

[0036] Figure numerals: reactor body 100, reaction tube cavity 110, feed port 120, discharge port 130, inner shell 140, outer shell 150, inlet port 151, outlet port 152, dividing rib 160; heat exchange structure 200, heat exchange plate 210, hollow channel 211, middle perforation 212, heat exchange medium input pipe 220, heat exchange medium output pipe 230, input port 221, output port 231, subassembly 240, tube cavity opposite surface 213, stirring shaft opposite surface 214; stirring assembly 300, stirring shaft 310, stirring blade 320, rotary drive 330, shear disk 340, fixed plate 341, shear sheet 342; peripheral channel 401, inner channel 402. DETAILED DESCRIPTION

[0037] Embodiments of the present invention are described in detail below, examples of which are shown in the accompanying drawings, wherein the same or similar reference numerals throughout represent the same or similar elements or elements having the same or similar functions. The embodiments described below with reference to the accompanying drawings are exemplary and are only used to explain the present invention, and cannot be understood as limiting the present invention.

[0038] In the description of the present invention, "several" means one or more, "more" means more than two, "greater than", "less than", "exceed" etc. are understood as not including the number itself, and "above", "below", "within" etc. are understood as including the number itself. If there is a description of "first" or "second", it is only used for the purpose of distinguishing the technical features, and cannot be understood as indicating or implying the relative importance or implicitly indicating the number of the indicated technical features or implicitly indicating the order of the indicated technical features.

[0039] In the description of the present invention, unless otherwise clearly defined, terms such as setting, installing, connecting, etc. should be understood in a broad sense, and technicians in the relevant technical field can reasonably determine the specific meanings of the above terms in the present invention in combination with the specific content of the technical solution.

[0040] Reference Figures 1 to 17, the accompanying drawings illustrate three types of reactors, among which the reactor includes a reactor body 100 and a heat exchange structure 200. The reactor body 100 is provided with a reaction tube cavity 110, a feed port 120 and a discharge port 130, the feed port 120 is connected to one end of the reaction tube cavity 110 along the length direction, and the discharge port 130 is connected to the other end of the reaction tube cavity 110 along the length direction. The heat exchange structure 200 is arranged in the reactor body 100, and the heat exchange structure 200 includes a plurality of heat exchange plates 210 arranged in the reaction tube cavity 110 and arranged at intervals along the length direction of the reaction tube cavity 110, and the heat exchange plates 210 extend along the radial direction of the reaction tube cavity 110, and the heat exchange plates 210 are used to make the material in the reaction tube cavity 110 form a tortuous flow. In the embodiment shown in the accompanying drawings, the length direction of the reaction tube cavity 110 is shown by the double arrow A in the figure, and the radial direction of the reaction tube cavity 110 is the direction of the vertical arrow A.

[0041] During production, the material is input into one end of the reaction tube cavity 110 through the feed port 120, and the material will move along the reaction tube cavity 110 to the other end, and the product after the material mixing reaction is output through the discharge port 130, thereby forming a continuous production. In the above process, the heat exchange plate 210 of the heat exchange structure 200 forms an obstacle to the material, so that the material forms a tortuous flow between the multiple heat exchange plates 210, and the heat exchange plate 210 also performs heat exchange on the tortuous flow of the material. The above reactor adopts the setting of multiple heat exchange plates 210, the heat exchange area is large, and the material can form a tortuous flow between the heat exchange plates 210, the heat exchange efficiency is high, and the mixing effect between the materials is good, thereby improving the production efficiency.

[0042] In each embodiment shown in the drawings, the heat exchange plate 210 is provided with a hollow channel 211, and the heat exchange structure 200 also includes a connecting channel connecting the hollow channels 211 of each heat exchange plate 210, and the connecting channel and each hollow channel 211 together constitute a heat exchange flow channel, and the reactor body 100 or the heat exchange structure 200 is provided with a heat exchange medium inlet and a heat exchange medium outlet connected to the heat exchange flow channel. With the above structure, the heat exchange plate 210 can exchange heat with the material by inputting a heat exchange medium into the heat exchange flow channel. The above heat exchange medium can be, for example, water, oil or other fluids capable of heat exchange.

[0043] It is conceivable that, in certain embodiments, the heat exchange plate 210 may also have heat exchange capabilities other than limited to the above-mentioned structure, for example, it may be made of a material with good heat dissipation and conduct heat outwardly through a heat-conducting structure; it is understandable that in this field, there are many specific implementations of the heat exchange plate 210, and those skilled in the art may reasonably configure its structure according to actual conditions without being limited to the above-mentioned implementations.

[0044] In the embodiment, several feed ports 120 may be provided, and different materials may be input simultaneously; of course, it is conceivable that in certain embodiments, if some premixing structures are additionally adopted, only a single feed port 120 may be provided.

[0045] In each embodiment shown in the drawings, the reactor further includes a stirring assembly 300, which is disposed on the reactor body 100. The stirring assembly 300 includes a stirring shaft 310, a stirring blade 320, and a rotary driver 330. The stirring shaft 310 is disposed along the length direction of the reaction lumen 110 and extends into the reaction lumen 110. The stirring blade 320 is disposed on the stirring shaft 310, and the rotary driver 330 is used to drive the stirring shaft 310 to rotate. When the rotary driver 330 drives the stirring shaft 310 to rotate, the mixed material can be stirred by the stirring blade 320.

[0046] Reference Figures 1 to 6 , which is one of the implementation structures of the present invention. In this embodiment, the heat exchange plate 210 of the heat exchange structure 200 is disc-shaped, and the heat exchange plate 210 is provided with a central through hole 212. The stirring shaft 310 is provided through the central through hole 212 of each heat exchange plate 210. The heat exchange plate 210 is divided into a larger plate and a smaller plate. The diameter of the larger plate is larger than that of the smaller plate. The diameter of the central through hole 212 of the larger plate is larger than that of the central through hole 212 of the smaller plate. The larger plate and the smaller plate are arranged alternately. The outer periphery of the smaller plate and the cavity wall of the reaction tube cavity 110 form an outer peripheral channel 401 connecting the two sides of the smaller plate. The hole wall of the central through hole 212 of the larger plate and the stirring shaft 310 form an inner channel 402 connecting the two sides of the larger plate. With the above structure, when the material encounters a smaller plate in the process of moving from one end of the reaction tube cavity 110 to the other end, it can be stopped and guided to the outer periphery of the smaller plate, and the material continues to flow forward through the outer peripheral channel 401. After passing through the peripheral channel 401, the material can be stopped by the larger plate and guided to the middle perforation 212 of the larger plate, and continue to flow forward through the inner channel 402; this is repeated, and during the forward movement of the material, the material can form a tortuous flow that first moves radially outward and then radially inward, and so on, which has a better material mixing effect and more sufficient heat exchange. The flow mode of the above-mentioned material can be referred to Figure 2 As indicated by the arrow in .

[0047] exist Figures 1 to 6In the embodiment of the present invention, the heat exchange structure 200 includes a heat exchange medium input pipe 220 and a heat exchange medium output pipe 230. The two ends of the heat exchange plate 210 are respectively fixed to the heat exchange medium input pipe 220 and the heat exchange medium output pipe 230. The heat exchange medium input pipe 220 and the heat exchange medium output pipe 230 form an assembly with the heat exchange plate 210 and are accommodated together in the reaction tube cavity 110. The tube cavity of the heat exchange medium input pipe 220 and the tube cavity of the heat exchange medium output pipe 230 are respectively connected to the two ends of the hollow channel 211 of the heat exchange plate 210. The heat exchange medium input pipe 220 and the heat exchange medium output pipe 230 are respectively provided with an input port 221 and an output port 231. With the above structure, through the arrangement of the heat exchange medium input pipe 220 and the heat exchange medium output pipe 230, each heat exchange plate 210 can be connected together to form an assembly, which is easy to install and has a stable overall structure. When in use, the heat exchange medium can be input through the input port 221, and after exchanging heat through each heat exchange plate 210, it can be output through the output port 231. The flow mode of the heat exchange medium inside the heat exchange structure 200 can be seen in Figure 4 As indicated by the arrow in .

[0048] In the embodiment, the plate surface of the heat exchange plate 210 can be set to a wave shape, so that the heat exchange area is larger. Of course, it is conceivable that the plate surface of the heat exchange plate 210 can also be set to a plane or other suitable shape, which can be configured according to actual conditions.

[0049] Reference Figures 7 to 12 , which is one of the implementation structures of the present invention. In this embodiment, the heat exchange structure 200 includes two subassemblies 240, and the subassembly 240 includes a row of heat exchange plates 210 and is provided with a heat exchange medium input pipe 220 and a heat exchange medium output pipe 230. The two ends of the heat exchange plate 210 are respectively fixed to the heat exchange medium input pipe 220 and the heat exchange medium output pipe 230. The lumen of the heat exchange medium input pipe 220 and the lumen of the heat exchange medium output pipe 230 are respectively connected to the two ends of the hollow channel 211 of each heat exchange plate 210. The heat exchange medium input pipe 220 and the heat exchange medium output pipe 230 are respectively provided with an input port 221 and an output port 231; each row of heat exchange plates 210 of each subassembly 240 is arranged around the outer peripheral side of the stirring shaft 310. In the embodiment shown in the drawings, the heat exchange structure 200 is divided into two subassemblies 240. It is conceivable that in some embodiments, the heat exchange structure 200 can also be divided into more than two subassemblies 240, which can be specifically configured according to actual conditions. In the above structure, each subassembly 240 is formed with an independent heat exchange flow channel, and the heat exchange medium can be input and output through the respective heat exchange medium input pipe 220 and heat exchange medium output pipe 230, thereby realizing the corresponding heat exchange function. The flow mode of the heat exchange medium in the subassembly 240 can be referred to Fig.11 As indicated by the arrow in .

[0050] By adopting the above structure, the heat exchange structure 200 is divided into at least two sub-assemblies 240. Compared with the single integral assembly, the heat exchange medium flow rate of each sub-assembly 240 is relatively small, and the diameters of the heat exchange medium input pipe 220 and the heat exchange medium output pipe 230 of the sub-assembly 240 are allowed to be made smaller, which is conducive to reducing the volume. In addition, compared with the heat exchange structure 200 adopting a single integral assembly, the design of the sub-assembly 240 does not require the stirring shaft 310 to be inserted into each heat exchange plate 210, and the sub-assembly 240 can be conveniently combined with the stirring shaft 310, which is conducive to simplifying the assembly of the reactor.

[0051] exist Figures 7 to 12 In the illustrated embodiment, the outer peripheral surface of the heat exchange plate 210 includes a tube cavity opposite surface 213 and a stirring shaft opposite surface 214, the tube cavity opposite surface 213 is adapted to the tube wall shape of the reaction tube cavity 110, the heat exchange plate 210 of the subassembly 240 is divided into a larger plate and a smaller plate, the tube cavity opposite surface 213 of the larger plate is closer to the tube wall of the reaction tube cavity 110 than the tube cavity opposite surface 213 of the smaller plate, the larger plates and the smaller plates are arranged alternately, and a peripheral channel 401 connecting the two sides of the smaller plate is formed between the tube cavity opposite surface 213 of the smaller plate and the cavity wall of the reaction tube cavity 110, and between the heat exchange plates 210 of different subassemblies 240, the larger plates are opposite to each other one by one, and the smaller plates are opposite to each other one by one, and an inner channel 402 is formed between the stirring shaft opposite surfaces 214 of the two corresponding larger plates. With the above structure, similar to the first embodiment of the present invention, when the material flows from one end to the other end of the reaction tube cavity 110, the material alternately flows between the outer peripheral channel 401 and the inner channel 402, so that the material can form a tortuous flow from radially outward to radially inward and then to radially outward repeatedly, and the mixing effect and heat exchange effect are good. The above flow mode of the material can be referred to Figure 8 As indicated by the arrow in .

[0052] exist Figures 1 to 6 , Figures 7 to 12 In the two embodiments, the reactor body 100 includes an inner shell 140 and an outer shell 150, the reaction tube cavity 110 is arranged in the inner shell 140, and the outer shell 150 and the inner shell 140 are enclosed to form an outer heat exchange channel, and the outer shell 150 is provided with an inlet 151 and an outlet 152 connected to the outer heat exchange channel. The heat exchange medium can be input into the outer heat exchange channel through the inlet 151 to exchange heat of the material, and the heat exchange medium that has completed the heat exchange can be output through the outlet 152, so that the heat exchange of the material can be carried out on the outer peripheral side of the reaction tube cavity 110, further improving the heat exchange effect. The flow mode of the outer heat exchange channel can be referred to Figure 6 and Fig.12 As indicated by the arrow in .

[0053] Reference Figures 13 to 17, which is one of the implementation structures of the present invention, in this embodiment, the reactor body 100 also includes an inner shell 140 and an outer shell 150, the reaction tube cavity 110 is arranged in the inner shell 140, the heat exchange plate 210 is a hollow shell extending from the shell wall of the inner shell 140 into the reaction tube cavity 110, the outer shell 150 is sleeved on the outer peripheral side of the inner shell 140, a heat exchange medium flow channel is formed between the outer shell 150 and the inner shell 140, the shell space of the heat exchange plate 210 is connected with the heat exchange medium flow channel, and the outer shell 150 is provided with an inlet 151 and an outlet 152 connected with the heat exchange medium flow channel. In the above structure, the inner shell 140 extends inward to form the heat exchange plate 210, and the heat exchange medium flow channel is formed between the outer shell 150 and the inner shell 140. The heat exchange medium can flow through the inner side of the heat exchange plate 210 through the inlet 151, thereby realizing its heat exchange function. The above structure is simple, and there is no need to install a heat exchange plate group in the reaction tube cavity 110, which is easy to produce and implement. The flow mode of the heat exchange medium in the above heat exchange medium flow channel can be referred to Fig.17 As indicated by the arrow in .

[0054] exist Figures 13 to 17 In the embodiment, the heat exchange plates 210 are arranged in two rows, and the two rows of heat exchange plates 210 are respectively arranged on both sides of the stirring shaft 310 in the radial direction. The two rows of heat exchange plates 210 are arranged relative to each other in a staggered manner, so that the number of heat exchange plates 210 can be reduced while ensuring that the material forms a tortuous flow, thereby reducing resistance, and is suitable for materials with high viscosity. The flow mode of the above-mentioned materials can be referred to Fig.14 As indicated by the arrow in .

[0055] In some implementations, such as Figures 1 to 6 In the illustrated embodiment, a shearing disk 340 is provided at one end of the stirring shaft 310 near the feed port 120. The shearing disk 340 includes a fixed plate 341 and a plurality of shearing pieces 342. The fixed plate 341 is provided perpendicular to the stirring shaft 310 and fixed to the stirring shaft 310. The shearing pieces 342 extend along the length direction of the reaction lumen 110. The shearing pieces 342 are arranged along the circumference of the reaction lumen 110 and are provided on the four edges of the fixed plate 341. By providing the shearing disk 340, the material can be pre-sheared and mixed in the front section of the reaction lumen 110, and the mixing effect is better with the mixing of the stirring paddle in the rear section. It can be understood that the above-mentioned setting of the shearing disk 340 can also be applied to other embodiments in the accompanying drawings according to actual needs.

[0056] In each embodiment shown in the drawings, a stirring blade 320 is provided between two adjacent heat exchange plates 210 along the length direction of the reaction tube cavity 110, so that the material can be fully stirred when the material passes through the stirring shaft 310, thereby achieving a better mixing effect.

[0057] In each embodiment shown in the drawings, the rotary driver 330 driving the stirring shaft 310 to rotate is specifically a motor, and the output shaft of the motor is connected to the stirring shaft 310, so as to drive the stirring shaft 310 to rotate. Of course, it is understandable that the rotary driver 330 is not limited to using a motor, for example, a rotary cylinder, or a connecting rod mechanism driven by a motor, etc., can also be used, as long as it can drive the stirring shaft 310 to rotate.

[0058] In each embodiment shown in the drawings, a separation rib 160 is provided in the heat exchange medium flow channel formed between the inner shell 140 and the outer shell 150. The separation rib 160 separates and forms a tortuous heat exchange flow channel, thereby improving the heat exchange effect.

[0059] The present invention provides a reaction system, which includes the above-mentioned reactor. The reaction system can be any of the following structures:

[0060] Normal pressure reaction system: It includes a pretreatment microreactor, which inputs materials through a plurality of material pumps, and the material outlet of the pretreatment microreactor is connected to the feed port 120 of the reactor. The reactor is provided with an exhaust channel connected to the reaction tube cavity 110, and the discharge port 130 of the reactor directly discharges materials or is connected to the post-processing equipment.

[0061] Reflux reaction system: It includes a pretreatment microreactor and a reflux separation component. The pretreatment microreactor inputs materials through a plurality of material pumps. The material outlet of the pretreatment microreactor is connected to the feed inlet 120 of the reactor. The reflux separation component is connected to the reactor and is used to reflux the unreacted materials to one end of the reaction tube cavity 110.

[0062] The above reaction systems are only some examples, and those skilled in the art can also reasonably combine them to form different reaction systems according to actual conditions.

[0063] The above-mentioned reactor and reaction system can be used for production of liquid-liquid, gas-liquid, liquid-solid, gas-liquid-solid and other systems, and is particularly suitable for solid-containing systems with a solid content of <50%.

[0064] The technical features of the above embodiments can be combined arbitrarily. To make the description concise, not all possible combinations of the technical features in the above embodiments are described. However, as long as there is no contradiction in the combination of these technical features, they should be considered to be within the scope of this specification. The embodiments of the present invention are described in detail above in conjunction with the accompanying drawings, but the present invention is not limited to the above embodiments. Various changes can be made within the knowledge of ordinary technicians in the technical field without departing from the purpose of the present invention.

Claims

1. A reactor, characterized in that: include: The reactor body is provided with a reaction tube cavity, a feed port and a discharge port, wherein the feed port is connected to one end of the reaction tube cavity along the length direction, and the discharge port is connected to the other end of the reaction tube cavity along the length direction; a heat exchange structure, arranged in the reactor body, comprising a plurality of heat exchange plates arranged in the reaction tube cavity and arranged at intervals along the length direction of the reaction tube cavity, the heat exchange plates extending in the radial direction of the reaction tube cavity, and used to make the material in the reaction tube cavity form a zigzag flow; A stirring assembly, the stirring assembly is arranged on the reactor body, the stirring assembly comprises a stirring shaft, a stirring blade and a rotary driver, the stirring shaft is arranged along the length direction of the reaction tube cavity and extends into the reaction tube cavity, the stirring blade is arranged on the stirring shaft, and the rotary driver is used to drive the stirring shaft to rotate; The heat exchange plate is disc-shaped, and is provided with a central through hole. The stirring shaft is passed through the central through hole of each heat exchange plate. The heat exchange plate is divided into a larger plate and a smaller plate. The diameter of the larger plate is larger than that of the smaller plate. The diameter of the central through hole of the larger plate is larger than that of the smaller plate. The larger plate and the smaller plate are arranged alternately. A peripheral channel connecting the two sides of the smaller plate is formed between the periphery of the smaller plate and the cavity wall of the reaction tube cavity, and a channel connecting the larger plate is formed between the hole wall of the central through hole of the larger plate and the stirring shaft. The inner channels on both sides; the heat exchange structure includes a heat exchange medium input pipe and a heat exchange medium output pipe, the two ends of the heat exchange plate are respectively fixed to the heat exchange medium input pipe and the heat exchange medium output pipe, the heat exchange medium input pipe and the heat exchange medium output pipe form an assembly with the heat exchange plate and are accommodated in the reaction tube cavity together, the heat exchange plate is provided with a hollow channel, the tube cavity of the heat exchange medium input pipe and the tube cavity of the heat exchange medium output pipe are respectively connected to the two ends of the hollow channel of the heat exchange plate, and the heat exchange medium input pipe and the heat exchange medium output pipe are respectively provided with an input port and an output port.

2. The reactor according to claim 1, characterized in that: The stirring blade is arranged between two adjacent heat exchange plates along the length direction of the reaction tube cavity.

3. The reactor according to claim 1, characterized in that: A shear plate is arranged at one end of the stirring shaft close to the feed port, and the shear plate includes a fixed plate and a plurality of shear pieces. The fixed plate is arranged perpendicular to the stirring shaft and fixed to the stirring shaft, and the shear pieces extend along the length direction of the reaction tube cavity. The shear pieces are arranged along the circumference of the reaction tube cavity and are arranged on four edges of the fixed plate.

4. A reactor, characterized in that: include: The reactor body is provided with a reaction tube cavity, a feed port and a discharge port, wherein the feed port is connected to one end of the reaction tube cavity along the length direction, and the discharge port is connected to the other end of the reaction tube cavity along the length direction; a heat exchange structure, arranged in the reactor body, comprising a plurality of heat exchange plates arranged in the reaction tube cavity and arranged at intervals along the length direction of the reaction tube cavity, the heat exchange plates extending in the radial direction of the reaction tube cavity, and used to make the material in the reaction tube cavity form a zigzag flow; A stirring assembly, the stirring assembly is arranged on the reactor body, the stirring assembly comprises a stirring shaft, a stirring blade and a rotary driver, the stirring shaft is arranged along the length direction of the reaction tube cavity and extends into the reaction tube cavity, the stirring blade is arranged on the stirring shaft, and the rotary driver is used to drive the stirring shaft to rotate; Wherein, the heat exchange structure includes at least two sub-components, and the sub-component includes a row of the heat exchange plates and is provided with a heat exchange medium input pipe and a heat exchange medium output pipe, the two ends of the heat exchange plate are respectively fixed to the heat exchange medium input pipe and the heat exchange medium output pipe, the heat exchange plate is provided with a hollow channel, the tube cavity of the heat exchange medium input pipe and the tube cavity of the heat exchange medium output pipe are respectively connected to the two ends of the hollow channel of each heat exchange plate, and the heat exchange medium input pipe and the heat exchange medium output pipe are respectively configured with an input port and an output port; each row of the heat exchange plates of each sub-component is arranged around the outer peripheral side of the stirring shaft.

5. The reactor according to claim 4, characterized in that: The outer peripheral surface of the heat exchange plate includes a tube cavity opposite surface and a stirring shaft opposite surface, the tube cavity opposite surface is adapted to the tube wall shape of the reaction tube cavity, the heat exchange plate of the subassembly is divided into a larger plate and a smaller plate, the tube cavity opposite surface of the larger plate is closer to the tube wall of the reaction tube cavity than the tube cavity opposite surface of the smaller plate, the larger plate and the smaller plate are arranged alternately, and a peripheral channel connecting the two sides of the smaller plate is formed between the tube cavity opposite surface of the smaller plate and the cavity wall of the reaction tube cavity. Between the heat exchange plates of different subassemblies, the larger plates are opposite to each other one by one, and the smaller plates are opposite to each other one by one, and an inner channel is formed between the stirring shaft opposite surfaces of the two corresponding larger plates.

6. The reactor according to claim 4, characterized in that: The stirring blade is arranged between two adjacent heat exchange plates along the length direction of the reaction tube cavity.

7. The reactor according to claim 4, characterized in that: A shear plate is arranged at one end of the stirring shaft close to the feed port, and the shear plate includes a fixed plate and a plurality of shear pieces. The fixed plate is arranged perpendicular to the stirring shaft and fixed to the stirring shaft, and the shear pieces extend along the length direction of the reaction tube cavity. The shear pieces are arranged along the circumference of the reaction tube cavity and are arranged on four edges of the fixed plate.

8. A reaction system, characterized in that: include: The reactor according to any one of claims 1 to 7.

Citation Information

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