An L-type heating chlorination device
By designing an L-shaped structure and sand-scooping blades in the quartz sand heating and chlorination device, the problem of insufficient contact between quartz sand and chlorine is solved, more efficient impurity removal is achieved, and high-purity quartz sand is obtained.
Patent Information
- Application Number
- CN202410922589.4
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-07-10
- Publication Date
- 2025-09-12
- Estimated Expiration
- 2044-07-10
AI Technical Summary
In existing quartz sand heating and chlorination devices, the contact between quartz sand and chlorine is insufficient, resulting in poor impurity removal and difficulty in obtaining high-purity quartz sand.
An L-shaped heated chlorination device is designed, which includes first-stage and second-stage high-temperature chlorination modules. A rotating shaft and sand-scooping blades are arranged in the drum. The rotating shaft and the drum rotate in opposite directions to drive the quartz sand to roll. The structural design of the sand-scooping blades ensures that the quartz sand is fully in contact with chlorine.
The contact efficiency between quartz sand and chlorine is improved, the reaction effect of impurities is enhanced, and quartz sand of higher purity is obtained.
Smart Images

Figure CN118874347B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of quartz sand purification, in particular to an L-shaped heating chlorination device. Background Art
[0002] After crushing, quartz sand needs to be purified before use in photovoltaic and optoelectronics applications. Currently, high-temperature chlorination is commonly used for purification. This process can further reduce the levels of impurities such as Fe, Na, K, and Ca in the sand, thereby increasing its purity. To ensure sufficient contact between the sand and the hydrogen chloride gas, a sand-scooping mechanism is installed within the reaction chamber to tumble the sand, allowing for a thorough reaction. However, current quartz sand heating and chlorination systems typically use a rotating drum to tumble the sand. Due to its own gravity, the sand remains deposited at the bottom of the drum for most of the time, where it accumulates and hinders sufficient contact with the chlorine gas.
[0003] Therefore, a kind of L-type heating chlorination device is needed to solve the above-mentioned technical problems. Summary of the Invention
[0004] The present invention aims at solving the technical problems in the prior art and provides an L-shaped heating chlorination device.
[0005] The present invention solves the above technical problems with the following technical solutions: an L-shaped heating chlorination device, comprising a first-stage high-temperature chlorination module and a second-stage high-temperature chlorination module, wherein the first-stage high-temperature chlorination module is connected to the second-stage high-temperature chlorination module, and the second-stage high-temperature chlorination module is vertically arranged, the first-stage high-temperature chlorination module comprises a first high-temperature chlorination cylinder, and the second-stage high-temperature chlorination module comprises a second high-temperature chlorination cylinder, and the first high-temperature chlorination cylinder and the second high-temperature chlorination cylinder are both provided with electric auxiliary heating units and microwave heating units at intervals along the axial direction;
[0006] The interior of the first high-temperature chlorination cylinder is rotatably connected to a roller, the exterior of the roller is connected to a drive unit, a feed connecting pipe is inserted into the front end of the roller, an air intake pipe is connected to the upper side of the feed connecting pipe, the feed connecting pipe is sealingly and rotatably connected to the roller, the rear end of the roller is inserted into the discharge connecting cylinder, the top of the discharge connecting cylinder is connected to an exhaust pipe, air valves are installed on the air intake pipe and the exhaust pipe, and the discharge connecting cylinder is rotatably and sealably connected to the roller.
[0007] Preferably, in the above-mentioned L-shaped heating chlorination device, the interior of the drum is rotatably connected to a rotating shaft, a plurality of sand-copying blades are provided on the rotating shaft, a second motor is provided on the outside of the discharge connecting cylinder, the output end of the second motor extends into the discharge connecting cylinder and is connected to the end of the rotating shaft, and the output end of the second motor is rotatably and sealedly connected to the discharge connecting cylinder.
[0008] Preferably, in the above-mentioned L-shaped heating chlorination device, the sand-scooping blades are circumferentially distributed on the outside of the rotating shaft, and the sand-scooping blades are equidistantly distributed in the axial direction of the rotating shaft.
[0009] Preferably, in the above-mentioned L-shaped heated chlorination device, the sand-making blade includes two parallel blade units, one side of the blade unit is fixedly connected to the rotating shaft, and the two blade units are connected to a shovel plate on one side away from the rotating shaft. The angles between the shovel plate and the blade unit are the same, and the two shovel plates form an expansion mouth shape, and a blanking through hole is provided between the two blade units.
[0010] Preferably, in the above-mentioned L-shaped heating chlorination device, a first through groove is provided through one side of the blade unit close to the rotating shaft, and the first through groove is communicated with the blanking through hole.
[0011] Preferably, in the above-mentioned L-shaped heating chlorination device, the sides of the two blade units facing away from each other are provided with a plurality of equally spaced horizontal bars and vertical bars, the horizontal bars and the vertical bars are perpendicular to each other, and the horizontal bars and the vertical bars form a plurality of rectangular frames.
[0012] Preferably, in the above-mentioned L-shaped heating chlorination device, the ends of the two shovel plates are provided with anti-fall baffles, and the anti-fall baffles are located on the side of the two shovel plates away from each other.
[0013] Preferably, in the above-mentioned L-shaped heating chlorination device, the ends of the two shovel plates are each provided with a hook plate, and the hook plate is located on the side where the two shovel plates are close to each other.
[0014] Preferably, in the above-mentioned L-shaped heating chlorination device, an annular groove is provided on the outside of the feed connecting pipe, and a rubber sealing ring is fixed on the inner side of one end of the drum, and the rubber sealing ring is embedded in the annular groove.
[0015] Preferably, in the above-mentioned L-shaped heating chlorination device, the driving unit includes a first motor, a gear is installed on the output shaft of the first motor, a circle of transmission teeth is provided on the outside of the drum, and the gear is engaged with the transmission teeth.
[0016] The beneficial effects of the present invention are as follows: the present invention rotates a connecting shaft in the drum, and a sand-scooping blade is provided on the shaft. When the shaft and the drum rotate in opposite directions, the quartz sand can be driven to roll. By arranging a first through groove, a blade unit, a horizontal baffle, a vertical baffle, a shovel plate, an anti-fall baffle, a hook plate, and a material-dropping through groove on the sand-scooping blade, the quartz sand can be fully contacted with chlorine gas, and impurities can be fully reacted, thereby obtaining quartz sand of higher purity. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0018] Figure 2 Schematic diagram of the external structure of the first-stage high-temperature chlorination module of the present invention;
[0019] Figure 3 Schematic diagram of the connection structure between the rotating shaft and the sand-scooping blade;
[0020] Figure 4 This is a structural diagram of the sand-copying blade;
[0021] Figure 5 for Figure 4 Schematic diagram of the structure at A-A in the middle;
[0022] Figure 6 This is a schematic diagram of the principle of the sand-copying blade in operation;
[0023] Figure 7 for Figure 6 Schematic diagram of the structure after the middle sand-dusting blade rotates to a certain angle;
[0024] Figure 8 Schematic diagram of the structure of the rotating shaft bracket;
[0025] Figure 9 Schematic diagram of the sealing structure at both ends of the drum.
[0026] In the accompanying drawings, the components represented by the reference numerals are as follows:
[0027] 1. First high-temperature chlorination cylinder, 2. Frame, 3. Feed hopper, 4. Drum, 5. Discharge pipe, 6. Sand-copying blade, 61. Support, 62. First through slot, 63. Blade unit, 64. Horizontal baffle, 65. Vertical baffle, 66. Shovel plate, 67. Anti-fall baffle, 68. Hook plate, 69. Discharge through slot, 7. Feed connecting pipe, 8. Discharge connecting cylinder, 9. First motor, 10. Gear, 11. Transmission gear, 12. Inlet pipe, 13. Exhaust pipe, 14. Second motor, 15. Rotating shaft, 1501, annular protrusion, 16. Second high-temperature chlorination cylinder, 17. Rotating shaft bracket, 18. First bearing, 19. Annular groove, 20. Rubber sealing ring. DETAILED DESCRIPTION
[0028] The principles and features of the present invention are described below with reference to the accompanying drawings. The examples given are only used to explain the present invention and are not used to limit the scope of the present invention.
[0029] like Figure 1As shown, an L-shaped heated chlorination unit comprises a first-stage high-temperature chlorination module and a second-stage high-temperature chlorination module, connected by a feed pipe 5. The second-stage high-temperature chlorination module is arranged vertically, while the first-stage module is slightly tilted horizontally, forming an "L" shape. The first-stage high-temperature chlorination module comprises a first high-temperature chlorination cylinder 1, and the second-stage high-temperature chlorination module comprises a second high-temperature chlorination cylinder 16. A drum 4 is rotatably connected to the first drum 1 via a second bearing. A feed barrel is located within the second drum 16. Both the first and second drums 1, 16 are axially spaced apart with electric auxiliary heating units and microwave heating units. These units heat the drum 4 and feed barrel, providing the necessary temperature for the impurity chlorination reaction. Quartz sand first passes through the first-stage high-temperature chlorination module before entering the second-stage high-temperature chlorination module. Both the first and second drums 1, 16 are fixedly mounted on a frame 2.
[0030] like Figures 2 to 9 As shown, the outside of the drum 4 is connected to a drive unit, which includes a first motor 9. A gear 10 is mounted on the output shaft of the first motor 9. A circle of transmission teeth 11 is provided on the outside of the drum 4, and the gear 10 meshes with the transmission teeth 11. When the first motor 9 rotates, the gear 10 rotates, and the rotation of the gear 10 drives the drum 4 to rotate through the transmission teeth 11.
[0031] A feed connection pipe 7 is inserted into the front end of the drum 4, which is connected to the feed hopper 3. Quartz sand is added from the feed hopper 3 and enters the drum 4 through the connection pipe 7. Both the feed connection pipe 7 and the drum 4 are arranged at an angle. An air inlet pipe 12 is connected to the upper side of the feed connection pipe 7, which continuously introduces chlorine gas into the drum 4. The rear end of the drum 4 is inserted into the discharge connection barrel 8, and an exhaust pipe 13 is connected to the top of the discharge connection barrel 8. Exhaust pipe 13 is used to exhaust the reacted gas, thereby ensuring a stable air pressure in the drum 4. Both the air inlet pipe 12 and the exhaust pipe 13 are equipped with air valves. By adjusting these two valves, the chlorine content in the drum 4 can be controlled to ensure the reaction and purification effect.
[0032] like Figure 9 As shown, the feed connecting pipe 7 is sealed and rotatably connected to the drum 4, and the discharge connecting pipe 8 is rotatably and sealably connected to the drum 4. An annular groove 19 is provided on the outside of the feed connecting pipe 7. A rubber sealing ring 20 is fixed to the inside of one end of the drum 4, embedded in the annular groove 19, and rotatably connected to the annular groove 19. An annular groove is provided on the other end of the drum 4, and a rubber sealing ring is fixed to the inside of one end of the discharge connecting pipe 8, embedded in the annular groove, and rotatably connected to the annular groove, thereby forming a good sealing effect and reducing the leakage of chlorine gas.
[0033] A rotating shaft 15 is rotatably connected to the interior of the drum 4. Specifically, a rotating shaft bracket 17 is fixed to the interior of the drum 4 and rotatably connected to the rotating shaft 15 via a first bearing 18. Multiple sand-splitting blades 6 are mounted on the rotating shaft 15. A second motor 14 is mounted outside the discharge connection barrel 8. The output end of the second motor 14 extends into the discharge connection barrel 8 and connects to the end of the rotating shaft 15. The output end of the second motor 14 is rotatably and sealedly connected to the discharge connection barrel 8. Both the first motor 9 and the second motor 14 are fixed to the frame 2. The sand-splitting blades 6 are circumferentially distributed outside the rotating shaft 15, and the blades 6 are evenly spaced axially along the rotating shaft 15. Rotation of the second motor 14 drives the rotating shaft 15. During operation, the second motor 14 rotates in the opposite direction to that of the first motor 9, meaning that the rotating shaft 15 rotates in the opposite direction to that of the drum 4. Rotation of the rotating shaft 15 causes the quartz sand to tumble through the sand-splitting blades 6.
[0034] The sand-scooping blades 6 comprise two parallel blade units 63, one side of which is fixedly connected to the rotating shaft 15 via two supports 61. A shovel plate 66 is connected to each blade unit 63 on the side facing away from the rotating shaft 15. The shovel plates 66 and blade units 63 are arranged at the same angle, forming an expanded opening. A material-dropping hole 69 is provided between the blade units 63. As the rotating shaft 15 rotates, the shovel plate 66 on one side scoops up the quartz sand. As the rotating shaft 15 continues to rotate in that direction, the quartz sand falls onto the blade unit 63 on that side. To prevent the quartz sand from sliding off the ends of the shovel plates 66 during this process, anti-drop baffles 67 are provided at the ends of each blade unit 66. These baffles 67 are located on the side facing away from each other to prevent the sand from sliding off the ends of the blade units 66.
[0035] A first through-slot 62 is provided on one side of the blade unit 63 near the rotating shaft 15. The first through-slot 62 communicates with the blanking hole 69. As the blade unit 63 rotates upward from a horizontal position, the quartz sand slides down the blade unit 63 under its own gravity, passes through the first through-slot 62, and falls onto the rotating shaft 15. From there, it falls along the rotating shaft 15 to the bottom of the drum 4, allowing the quartz sand to fully come into contact with the chlorine gas and allow the impurities to react fully.
[0036] The sides of the two blade units 63 facing away from each other are each equipped with a plurality of equally spaced horizontal bars 64 and vertical bars 65. The horizontal bars 64 and vertical bars 65 are perpendicular to each other and form a plurality of rectangular frames. When the blade units 63 rotate upward from a horizontal position, the quartz sand slides down along the blade units 63 under its own gravity. The rectangular frames formed by the horizontal and vertical bars 64 and 65 retain some of the quartz sand within the rectangular frames, preventing it from falling out. This helps the thin layer of quartz sand fully contact the chlorine gas. The quartz sand in the rectangular frames will not be poured out until the blade units 63 rotate downward from the top.
[0037] Furthermore, each shovel blade 66 is provided with a hook plate 68 at its end, located on the side where the two shovel blades 66 are close to each other. When the blade units 63 rotate in one direction, the shovel plate 66 on one blade unit 63 scoops up some quartz sand, while the hook plate 68 on the adjacent blade unit 63 also scoops up some quartz sand. During the upward rotation, the quartz sand on the inner side of the hook plate 68 slides along the drop groove 69 to the first groove 62, falls onto the rotating shaft 15, and finally falls to the bottom of the drum 4. In this process, the quartz sand is picked up and scattered, thereby facilitating sufficient contact between the quartz sand and the chlorine gas. Similarly, when the rotating shaft 15 rotates in the opposite direction, the blade units 63 on both sides have the same structure, so the effect is the same.
[0038] A plurality of annular protrusions 1501 are equidistantly arranged on the rotating shaft 15 to prevent the quartz sand from sliding down along the rotating shaft 15 when the quartz sand falls onto the rotating shaft 15 , thereby increasing the contact time between the quartz sand and the chlorine gas and improving the purification effect of the quartz sand.
[0039] In the description of the present invention, it should be understood that the terms "upper", "lower", "left", "right" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, and a specific orientation structure and operation, and therefore, cannot be understood as limiting the present invention. In addition, "first" and "second" are only used for descriptive purposes and cannot be understood as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Therefore, the features defined as "first" and "second" may explicitly or implicitly include one or more of the features. In the description of the present invention, unless otherwise specified, "multiple" means two or more.
[0040] In the description of the present invention, it should be noted that, unless otherwise expressly specified or limited, the terms "mounted," "connected," and "connected" should be understood in a broad sense. For example, they may refer to fixed connections, detachable connections, or integral connections; mechanical connections or electrical connections; direct connections or indirect connections through an intermediate medium; and internal communication between two components. Those skilled in the art will understand the specific meanings of the above terms in the present invention based on the specific circumstances.
[0041] The above is a detailed description of an embodiment of the present invention. However, the content described is only a preferred embodiment of the present invention and should not be considered to limit the scope of the present invention. All equivalent changes and improvements made within the scope of the present invention should still fall within the scope of the patent coverage of the present invention.
Claims
1. An L-type heating chlorination device, characterized in that: The invention comprises a first-stage high-temperature chlorination module and a second-stage high-temperature chlorination module, wherein the first-stage high-temperature chlorination module is connected to the second-stage high-temperature chlorination module, and the second-stage high-temperature chlorination module is vertically arranged, the first-stage high-temperature chlorination module comprises a first high-temperature chlorination cylinder (1), and the second-stage high-temperature chlorination module comprises a second high-temperature chlorination cylinder (16), and the first high-temperature chlorination cylinder (1) and the second high-temperature chlorination cylinder (16) are both provided with electric auxiliary heating units and microwave heating units at intervals along the axial direction; The interior of the first high-temperature chlorination cylinder (1) is rotatably connected to a roller (4), the exterior of the roller (4) is connected to a drive unit, a feed connecting pipe (7) is inserted into the front end of the roller (4), an air intake pipe (12) is connected to the upper side of the feed connecting pipe (7), the feed connecting pipe (7) is sealed and rotatably connected to the roller (4), the rear end of the roller (4) is inserted into the discharge connecting cylinder (8), the top of the discharge connecting cylinder (8) is connected to an exhaust pipe (13), air valves are installed on both the air intake pipe (12) and the exhaust pipe (13), and the discharge connecting cylinder (8) is rotatably and tightly connected to the roller (4). The roller (4) is internally rotatably connected to a rotating shaft (15), and a plurality of sand-scooping blades (6) are provided on the rotating shaft (15). A second motor (14) is provided on the outside of the discharge connecting cylinder (8), and the output end of the second motor (14) extends into the discharge connecting cylinder (8) and is connected to the end of the rotating shaft (15). The output end of the second motor (14) is rotatably and sealably connected to the discharge connecting cylinder (8). The sand-scooping blades (6) are circumferentially distributed on the outside of the rotating shaft (15), and the sand-scooping blades (6) are equidistantly distributed in the axial direction of the rotating shaft (15). The sand-scooping blades (6) The invention comprises two blade monomers (63) arranged in parallel, one side of the blade monomer (63) is fixedly connected to the rotating shaft (15), and the sides of the two blade monomers (63) away from the rotating shaft (15) are connected with a shovel plate (66), the angles between the shovel plate (66) and the blade monomer (63) are the same, and the two shovel plates (66) form an expansion mouth shape, a blanking through hole (69) is provided between the two blade monomers (63), and a first through groove (62) is provided through the side of the blade monomer (63) close to the rotating shaft (15), and the first through groove (62) is connected to the blanking through hole (69). The two blade monomers (63) are provided with a plurality of equally spaced transverse bars (64) and vertical bars (65) on a side away from each other, the transverse bars (64) and the vertical bars (65) are perpendicular to each other, and the transverse bars (64) and the vertical bars (65) form a plurality of rectangular frames, and the ends of the two shovel plates (66) are provided with anti-fall baffles (67), and the anti-fall baffles (67) are located on the side where the two shovel plates (66) are away from each other, and the ends of the two shovel plates (66) are provided with hook plates (68), and the hook plates (68) are located on the side where the two shovel plates (66) are close to each other.
2. L-type heating chlorination device according to claim 1, characterized in that: An annular groove (19) is provided on the outer side of the feed connecting pipe (7), and a rubber sealing ring (20) is fixed on the inner side of one end of the roller (4), and the rubber sealing ring (20) is embedded in the annular groove (19).
3. The L-type heating chlorination device according to claim 1, wherein: The driving unit comprises a first motor (9), a gear (10) is mounted on the output shaft of the first motor (9), a circle of transmission teeth (11) is provided on the outside of the drum (4), and the gear (10) is meshed with the transmission teeth (11).
Citation Information
Patent Citations
High-low temperature chlorination extraction device for quartz purification
CN114751420A
method and apparatus for carrying out reactions at high temperature, in particular for chlorinating ores
FR1266944A