A composite containing soapberry extract and preparation method thereof

Abstract

The present application relates to the field of daily chemical external cleaning products, and more specifically, it relates to a compound containing a soapberry extract and a preparation method thereof. A compound containing a soapberry extract, according to mass percentage, comprises the following components: 1‑5% soapberry extract, 5‑15% Polygonum multiflorum root extract, 1‑10% Nasturtium extract, 1‑5% Black Ganoderma extract, 1‑5% Dendrobium candidum extract, and solvent; the preparation method is: the raw materials are mixed until uniform to obtain a compound containing a soapberry extract. The compound provided in the present application is mainly used in washing or cleaning products such as shampoo and shower gel, and has good effects such as cleaning, antibacterial, moisturizing, and anti-aging.

Description

Technical Field

[0001] The application relates to the field of daily chemical external cleaning products, and more specifically, it relates to a complex containing soapberry extract and a preparation method thereof. Background Art

[0002] In the field of modern personal care, shower gel, shampoo, etc. are necessities for daily cleaning and care. Their performance and quality directly affect the skin health and comfort of users. With the growing pursuit of natural, environmentally friendly and efficient skin care products by consumers, traditional shower gels and shampoos with chemical synthetics as the main ingredients are gradually unable to meet market demand. Therefore, the development of a natural shower gel and shampoo that integrates multiple functions such as cleaning, moisturizing, oil control and antibacterial has become a hot topic in industry research. Sapindus mukorossi, as a natural cleanser with a long history, has broad application prospects in the field of washing and cleaning products due to its unique biological activity and excellent skin care effect.

[0003] There are many kinds of skin care products on the market, but most of them have the following problems: First, they rely too much on chemical surfactants, which result in strong cleaning power but easy to damage the skin barrier, causing dryness, tightness and other discomforts; second, although some products have added moisturizing ingredients, it is often difficult to achieve the ideal water-oil balance effect, especially for oily or combination skin, which is prone to incomplete cleaning or excessive greasiness; third, although some natural skin care products contain natural extracts, the formula design is unreasonable, resulting in unstable product performance and poor use effect. Summary of the invention

[0004] In order to solve the above problems, the present application provides a complex containing soapberry extract and a preparation method thereof, which can not only effectively cleanse the skin, but also provide the skin with necessary moisture while cleansing, regulate sebum secretion, and achieve the effect of water-oil balance.

[0005] In the first aspect, the present application provides a complex containing a soapberry extract, adopting the following technical scheme: a complex containing a soapberry extract, comprising the following components in percentage by mass: 1-5% of a soapberry extract, 5-15% of a Polygonum multiflorum root extract, 1-10% of a Nasturtium officinale extract, 1-5% of a black ganoderma extract, 1-5% of a Dendrobium officinale extract, and a solvent.

[0006] Preferably, the complex containing soapberry extract comprises the following components in percentage by mass: 2-4% soapberry extract, 8-13% Polygonum multiflorum root extract, 3-7% Nasturtium officinale extract, 2-4% Ganoderma lucidum extract, 1-3% Dendrobium officinale extract, and solvent.

[0007] Preferably, the complex containing soapberry extract comprises the following components in percentage by mass: 2% soapberry extract, 10% Polygonum multiflorum root extract, 5% Nasturtium officinale extract, 3% Ganoderma lucidum extract, 2% Dendrobium officinale extract, and solvent.

[0008] The extract of SAPINDUS MUKOROSSI contains saponin. It can produce foam when rubbed with water and can be used for cleaning. It is one of the main cleaning agents in ancient times. It has strong decontamination ability, is easy to degrade, has no harmful residue, is easy to rinse, has no odor, has little irritation to the skin, and can be used for skin cleaning. It has the effects of antibacterial beauty, sterilization and anti-inflammatory, dandruff and itching, freckle and acne removal, whitening, and prevention and treatment of skin diseases on human skin.

[0009] Polygonum multiflorum root extract is derived from the dried root tuber of Polygonum multiflorum, a plant of the Polygonaceae family. Its main functional ingredients are lecithin (good moisturizing effect), rhein, rhein and other ingredients. Main effects: anti-aging effect, influence on the immune system, hypolipidemic and anti-atherosclerotic effects, myocardial protection, liver protection, neuroprotection, and antibacterial effects. It can enhance the activity of SOD. Polygonum multiflorum is widely used as a cosmetic for oral or external use because of its ability to make hair black and shiny.

[0010] Tropaeolum majus extract, because it contains benzyl thiocyanate, has antibacterial properties and has antibacterial effects on Staphylococcus aureus, Streptococcus, Escherichia coli, Bacillus subtilis and some fungi. It also has anti-inflammatory effects. It can promote hair growth and can be used to prevent hair loss and nourish hair. It can eliminate free radicals and has anti-aging effects.

[0011] Black Ganoderma (GANODERMA ATRUM) extract, the polysaccharides and peptides contained in Ganoderma have obvious anti-aging effects. Promote and adjust immune function. Regulate metabolic balance and promote the synthesis of nucleic acids and proteins. Ganoderma polysaccharides have significant pseudo-SOD activity, which can significantly remove free radicals produced by the body, thereby preventing free radicals from damaging the body, preventing lipid peroxidation, protecting cells, and delaying cell aging.

[0012] Dendrobium officinale extract can increase capillary blood flow and can be used in hair, anti-aging and other cosmetics that require blood circulation; it can eliminate a variety of free radicals and can be used as an antioxidant; it has the function of absorbing water under low humidity and has a moisturizing effect.

[0013] By adopting the above technical scheme, five raw materials, namely, soapberry extract, Polygonum multiflorum root extract, Nasturtium extract, black ganoderma extract, and Dendrobium officinale extract, are specially selected to work together. The soapberry extract first removes the grease and dirt on the skin surface, laying the foundation for subsequent nutrient absorption; the Dendrobium officinale extract and Polygonum multiflorum root extract are responsible for moisturizing and nourishing to prevent dry skin; the black ganoderma extract and Nasturtium extract further consolidate the effect of water-oil balance by regulating sebum secretion, anti-inflammatory and repair effects. These ingredients work together to act on the skin to achieve the goal of water-oil balance.

[0014] Soapberry extract is rich in saponins and has good foaming and detergency properties. It can deeply clean the scalp and skin and remove excess oil and dirt. Dendrobium officinale extract and Polygonum multiflorum root extract do not have as significant direct cleaning effects as Soapberry, but the polysaccharide components of both help keep the skin moisturized. When used in combination with Soapberry extract, they can maintain the water and oil balance of the skin while cleaning and quickly replenish the nutrients needed by the skin. Black Ganoderma lucidum extract and Nasturtium extract can effectively work together to assist in regulating the skin microenvironment, thereby facilitating the balance of water and oil.

[0015] Preferably, the complex containing soapberry extract comprises the following components in percentage by mass: 2-4% soapberry extract, 8-13% Polygonum multiflorum root extract, 3-7% Nasturtium officinale extract, 2-4% Ganoderma lucidum extract, 1-3% Dendrobium officinale extract, and solvent.

[0016] Preferably, the complex containing soapberry extract comprises the following components in percentage by mass: 2% soapberry extract, 10% Polygonum multiflorum root extract, 5% Nasturtium officinale extract, 3% Ganoderma lucidum extract, 2% Dendrobium officinale extract, and solvent.

[0017] By adopting the above technical scheme, the dosage and coordination relationship of Sapindus mukorossi extract, Polygonum multiflorum root extract, Nasturtium officinale extract, Ganoderma lucidum extract and Dendrobium officinale extract in the system are further limited, so that the synergistic coordination relationship of the five can be more fully exerted, which can better improve the skin care effect of the product, find a good balance between cleansing and moisturizing, and achieve water-oil balance.

[0018] Preferably, the complex containing the soapberry extract further comprises 0.01-1% of a preservative.

[0019] Preferably, the preservative comprises a mixture of one or more of p-hydroxyacetophenone and 1,2-hexanediol.

[0020] Preferably, the solvent is water.

[0021] In a second aspect, the present application provides a method for preparing a composite containing a soapberry extract, using the following technical solution:

[0022] A method for preparing a compound containing a soapberry extract comprises the following steps: mixing raw materials until they are uniform to obtain the compound containing the soapberry extract.

[0023] Preferably, the soapberry extract, polygonum multiflorum root extract, nasturtium extract, black ganoderma extract, dendrobium officinale extract and solvent are mixed at 1500-2000r / min for 10-20min, then microwaved at 30-50W for 3-5min, and then mixed with the remaining raw materials until uniform.

[0024] By adopting the above technical solution, the preliminary mixing at a specific speed (1500-2000r / min) and time (10-20min) ensures the uniform distribution of active ingredients in each extract. Subsequently, microwave treatment further promotes the interaction and fusion between molecules, making the final product more uniform and stable, and improving the overall quality of the product. Microwave treatment at moderate power (30-50W) and time (3-5min) can selectively excite and retain more bioactive ingredients, avoiding degradation and destruction caused by high temperature. At the same time, the non-thermal effect of microwaves may also promote the transformation and enhancement of certain active ingredients, improve the bioavailability and efficacy of the product, and make the synergy of the five more fully exerted.

[0025] In summary, this application has the following beneficial effects:

[0026] 1. Specially selected soapberry extract, polygonum multiflorum root extract, nasturtium extract, black ganoderma extract, and dendrobium candidum extract as the active ingredients of the complex, which are mainly used in washing or cleaning products such as shampoo and shower gel, and have good cleaning, antibacterial, moisturizing, and anti-aging effects.

[0027] 2. Five ingredients, namely, Soapberry extract, Polygonum multiflorum root extract, Nasturtium extract, Black Ganoderma extract, and Dendrobium officinale extract, are specially selected to work together. Soapberry extract first removes grease and dirt on the skin surface, laying the foundation for subsequent nutrient absorption; Dendrobium officinale extract and Polygonum multiflorum root extract are responsible for moisturizing and nourishing to prevent dry skin; Black Ganoderma extract and Nasturtium extract further consolidate the effect of water-oil balance by regulating sebum secretion, anti-inflammatory and repairing effects. These ingredients work together to act on the skin to achieve the goal of water-oil balance. DETAILED DESCRIPTION

[0028] The present application is further described in detail below with reference to the embodiments.

[0029] The raw materials used in the following examples and comparative examples are all commercially available products.

[0030] Example

[0031] Example 1

[0032] A compound containing soapberry extract comprises the following components: soapberry extract, polygonum multiflorum root extract, nasturtium extract, black ganoderma extract, dendrobium officinale extract, solvent and preservative.

[0033] Soapberry extract, Polygonum multiflorum root extract, Nasturtium officinale extract, Ganoderma lucidum extract, and Dendrobium officinale extract were all purchased from Guangzhou Fuzhilin Biotechnology Co., Ltd.

[0034] The solvent is water.

[0035] Preservatives include p-hydroxyacetophenone and 1,2-hexanediol.

[0036] The specific content of each component is shown in Table 1.

[0037] The present application also provides a method for preparing a complex containing a soapberry extract, comprising the following steps:

[0038] Step 1: at 1800 r / min, mix the extract of Sapindus mukorossi, the extract of Polygonum multiflorum root, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, the extract of Dendrobium officinale and the solvent for 15 minutes to obtain a first mixture.

[0039] Step 2: The first mixture was subjected to microwave treatment at 40 W for 4 min to obtain a second mixture.

[0040] Step 3: The remaining raw materials are mixed with the second mixture until uniform, to obtain a complex containing the soapberry extract.

[0041] Example 2

[0042] A complex containing a soapberry extract, which is different from Example 1 in that the specific content of each component is different, see Table 1 for details.

[0043] The present application also provides a method for preparing a complex containing a soapberry extract, comprising the following steps:

[0044] Step 1: at 1500 r / min, mix the extract of Sapindus mukorossi, the extract of Polygonum multiflorum root, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, the extract of Dendrobium officinale and the solvent for 20 minutes to obtain a first mixture.

[0045] Step 2: The first mixture was subjected to microwave treatment at 30 W for 5 min to obtain a second mixture.

[0046] Step 3: The remaining raw materials are mixed with the second mixture until uniform, to obtain a complex containing the soapberry extract.

[0047] Example 3

[0048] A complex containing a soapberry extract, which is different from Example 1 in that the specific content of each component is different, see Table 1 for details.

[0049] The present application also provides a method for preparing a complex containing a soapberry extract, comprising the following steps:

[0050] Step 1: at 2000 r / min, mix the extract of Sapindus mukorossi, the extract of Polygonum multiflorum root, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, the extract of Dendrobium officinale and the solvent for 10 minutes to obtain a first mixture.

[0051] Step 2: The first mixture was subjected to microwave treatment at 50 W for 3 min to obtain a second mixture.

[0052] Step 3: The remaining raw materials are mixed with the second mixture until uniform, to obtain a complex containing the soapberry extract.

[0053] Example 4

[0054] A complex containing a soapberry extract, which is different from Example 1 in that the specific content of each component is different, see Table 1 for details.

[0055] The preparation method of a composite containing a soapberry extract is the same as that in Example 1 and is not described herein.

[0056] Example 5

[0057] A complex containing a soapberry extract, which is different from Example 1 in that the specific content of each component is different, see Table 1 for details.

[0058] The preparation method of a composite containing a soapberry extract is the same as that in Example 1 and is not described herein.

[0059] Table 1

[0060]

[0061] Example 6

[0062] A method for preparing a composite containing a soapberry extract, which is different from that in Example 1, comprises the following steps:

[0063] Step 1: Mix the extract of Sapindus mukorossi, the extract of Polygonum multiflorum root, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, the extract of Dendrobium officinale and the solvent at 500 r / min for 15 minutes to obtain a first mixture.

[0064] Step 2: The first mixture was subjected to microwave treatment at 10 W for 4 min to obtain a second mixture.

[0065] Step 3: The remaining raw materials are mixed with the second mixture until uniform, to obtain a complex containing the soapberry extract.

[0066] Example 7

[0067] A method for preparing a complex containing a soapberry extract, which differs from Example 1 in that it comprises the following steps: Step 1: Mixing a soapberry extract, a Polygonum multiflorum root extract, a Nasturtium extract, a Black Ganoderma extract, a Dendrobium officinale extract, and a solvent at 2500 r / min for 15 minutes to obtain a first mixture.

[0068] Step 2: The first mixture was subjected to microwave treatment at 100 W for 4 min to obtain a second mixture.

[0069] Step 3: The remaining raw materials are mixed with the second mixture until uniform, to obtain a complex containing the soapberry extract.

[0070] Comparative Example

[0071] Comparative Example 1

[0072] A composite material, which is different from Example 1 in that the soapberry extract is replaced by the purslane (PORTULACA OLERACEA) extract.

[0073] Purslane extract was purchased from Shaanxi Junhe Biotechnology Co., Ltd.

[0074] Comparative Example 2

[0075] A composite containing a soapberry extract, which is different from Example 1 in that the Polygonum multiflorum root extract is replaced by a black sesame (SESAMUM INDICUM) extract.

[0076] Black sesame extract was purchased from Shaanxi Sinuote Biotechnology Co., Ltd.

[0077] Comparative Example 3

[0078] A composite containing a soapberry extract, which is different from Example 1 in that the nasturtium extract is replaced by a grape seed (Vitis vinifera) extract.

[0079] Grape seed extract was purchased from Baoji Runmu Agricultural Development Co., Ltd.

[0080] Comparative Example 4

[0081] A composite containing a soapberry extract, which is different from Example 1 in that the black ganoderma extract is replaced by a witch hazel (HAMAMELIS VIRGINIANA) extract.

[0082] North American witch hazel extract was purchased from Xi'an Anao Biotechnology Co., Ltd.

[0083] Comparative Example 5

[0084] A composite containing a soapberry extract, which is different from Example 1 in that the Dendrobium officinale extract is replaced by a green tea (Camellia Sinensis) extract.

[0085] Green tea extract was purchased from Hubei Sanxin Biotechnology Co., Ltd.

[0086] Performance testing

[0087] Preparation of test samples: The composites of Examples 1-7 and Comparative Examples 1-5 were mixed with water until uniform, and a 10% test solution was prepared.

[0088] Volunteer selection: 10 volunteers who self-assessed as having oily skin and were aged 25-35 years with healthy skin were selected.

[0089] Ten volunteers underwent a 12-day test, testing one solution each day.

[0090] Testing method: Use a skin water-oil test pen to detect the initial skin water content and initial skin oil content of the test area on the volunteer's arm.

[0091] Then soak the area of ​​your arm to be tested in the test solution for half a minute, rubbing gently in circles while soaking.

[0092] Take the arm out of the test solution, wipe it dry with paper, and wait for 3 minutes.

[0093] Then, the skin water and oil test pen was used again to detect the treated skin water content and treated skin oil content in the test area of ​​the volunteer's arm.

[0094] Calculate the moisture change rate and oil change rate according to the following formula, and take the average value of the volunteers as the test data of the solution to be tested, which is recorded in Table 2.

[0095]

[0096] Table 2

[0097]

[0098]

[0099] After each test, a questionnaire was distributed to record the volunteers' feelings. The content of the questionnaire is as follows:

[0100] Question 1: How moisturizing is the product? The options include "good", "average", and "poor".

[0101] Question 2: How effective is the product in controlling oil? The options include "good", "average", and "poor".

[0102] Question 3: After using the product, do you feel tightness, greasiness, or other discomfort? If you experience any of these, select “yes”.

[0103] Question 4: Give the product an overall score from 0 to 10. The closer to 10, the better and more satisfactory the product experience is; the closer to 0, the worse and less satisfactory the product experience is.

[0104] For questions 1 and 2, record the number of people who chose each option, for question 3, record the number of people who chose "yes", and for question 4, record the average score of the total score. Record the results in Table 3.

[0105] Table 3

[0106]

[0107] According to the test data in Table 2, Examples 1-7 can effectively increase the water content of the skin after treatment and reduce the oil content of the skin after treatment. Combined with the data in Table 3, it can be seen that the hydrating and degreasing effect is within a good range, and there will be no excessive degreasing, causing any discomfort to the volunteers. In other words, the composites containing the soapberry extract of Examples 1-7 can achieve good cleaning and water-oil balance effects when used on the skin. Comparative Examples 1-5 are based on Example 1, and any of the soapberry extract, the root extract of Polygonum multiflorum, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, and the extract of Dendrobium officinale is replaced with other plant extracts. Although the prepared composites still have a certain hydrating and degreasing effect, the water change rate and the oil change rate are significantly lower than those of Example 1, and the sensory evaluation of the questionnaire is not as good as that of Example 1. It shows that there is a special coordination effect between the soapberry extract, the root extract of Polygonum multiflorum, the extract of Nasturtium officinale, the extract of Ganoderma lucidum, and the extract of Dendrobium officinale. Randomly splitting the special combination will destroy the coordination effect, thereby failing to achieve ideal performance.

[0108] Examples 6 and 7 are based on Example 1, but the parameters in the preparation method are changed. According to the test data in Tables 2 and 3, the performance of Examples 6 and 7 in terms of water replenishment and oil removal is not as good as that of Example 1, and the sensory performance is also slightly worse than that of Example 1. This shows that if the parameters of the preparation method can be further limited, the extract of Sapindus mukorossi, the extract of Polygonum multiflorum root, the extract of Nasturtium officinale, the extract of Ganoderma lucidum and the extract of Dendrobium candidum can be more fully promoted to cooperate with each other and mix fully, thereby giving the composite a more excellent effect.

[0109] This specific embodiment is merely an explanation of the present application and is not a limitation of the present application. After reading this specification, those skilled in the art may make modifications to the present embodiment without any creative contribution as needed, but such modifications are protected by the patent law as long as they are within the scope of the claims of the present application.

Claims

1. A composite containing a soapberry extract, characterized in that The composition is composed of the following components according to mass percentage: 1-5% of soapberry extract, 5-15% of Polygonum multiflorum root extract, 1-10% of Nasturtium officinale extract, 1-5% of black ganoderma extract, 1-5% of Dendrobium officinale extract, solvent, and preservative; The solvent is water.

2. The complex containing the soapberry extract according to claim 1, characterized in that: The complex containing soapberry extract is composed of the following components according to mass percentage: 2-4% soapberry extract, 8-13% Polygonum multiflorum root extract, 3-7% Nasturtium extract, 2-4% Ganoderma lucidum extract, 1-3% Dendrobium officinale extract, solvent, and preservative.

3. The complex containing the soapberry extract according to claim 2, characterized in that: The complex containing the soapberry extract is composed of the following components in percentage by mass: 2% soapberry extract, 10% Polygonum multiflorum root extract, 5% Nasturtium officinale extract, 3% black ganoderma extract, 2% Dendrobium officinale extract, solvent, and preservative.

4. The complex containing the soapberry extract according to claim 1, characterized in that: According to mass percentage, the preservative in the complex containing the soapberry extract is 0.01-1%.

5. The complex containing the soapberry extract according to claim 4, characterized in that: The preservative comprises a mixture of one or more of p-hydroxyacetophenone and 1,2-hexanediol.

6. A method for preparing a complex containing a soapberry extract according to any one of claims 1 to 5, characterized in that: The method comprises the following steps: mixing the raw materials until they are uniform to obtain a complex containing the soapberry extract.

7. The method for preparing the composite containing the soapberry extract according to claim 6, characterized in that: The soapberry extract, polygonum multiflorum root extract, nasturtium extract, black ganoderma extract, dendrobium officinale extract and solvent are mixed at 1500-2000r / min for 10-20min, then microwaved at 30-50W for 3-5min, and then mixed with the remaining raw materials until uniform.

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