A netted relief glaze and a method for preparing the same

By combining three layers of glaze and controlling the component ratio, a textured relief glaze with low lead and cadmium content, high thermal stability, warm luster, and delicate touch was prepared. This solved the problems of excessive lead content and poor relief effect in existing technologies, and realized the combination of daily-use ceramics and art ceramics.

CN119285232BActive Publication Date: 2025-12-26HUNAN HUALIAN CHINA IND
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Patent Information

Application Number
CN202411407400.4
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-10-10
Publication Date
2025-12-26
Estimated Expiration
2044-10-10

AI Technical Summary

Technical Problem

Existing technologies struggle to produce textured embossed glazes with low lead and cadmium content, high thermal stability, a warm luster, and a delicate feel. Furthermore, traditional embossed glaze production processes suffer from issues such as excessive lead content and a lack of complex embossed effects.

Method used

It adopts a three-layer glaze, including base glaze, top glaze and spray glaze. By strictly controlling the proportion of each component and additives such as vanadium pentoxide and zirconium silicate, a net-like relief effect is formed. Combined with a specific firing process, the relief effect and gloss are achieved.

Benefits of technology

It achieves a textured relief glaze with low lead and cadmium content, high thermal stability, warm luster, and delicate touch, meeting market demands and relevant standards, and is suitable for the artistic transformation of daily-use ceramics and the daily-use transformation of artistic ceramics.

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Abstract

The application discloses a net-shaped relief glaze and a preparation method thereof, and comprises a base glaze, a surface glaze and a spraying point glaze. The surface glaze comprises 8-15 parts of 2# frit, 38-42 parts of potassium feldspar, 14-20 parts of quartz, 13-17 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of zinc ash, 8-12 parts of Longyan clay, 15-22 parts of zirconium silicate, 3-7 parts of titanium white, 1-3 parts of calcined bone carbon and 0-10 parts of synthetic colorant. The spraying point glaze comprises 14-18 parts of 3# frit, 38-42 parts of potassium feldspar, 8-12 parts of quartz, 10-14 parts of calcite, 3-7 parts of barium carbonate, 1-3 parts of calcined talc, 3-7 parts of zinc ash, 8-12 parts of Longyan clay and 6-10 parts of vanadic oxide. The base glaze formula is further included. The net-shaped relief glaze prepared through the unique three-layer glaze formula has low lead and cadmium contents, high thermal stability, warm luster, and delicate touch.
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Description

TECHNICAL FIELD

[0001] The application belongs to the technical field of daily-use stoneware glaze, and particularly relates to a net-shaped relief glaze and a preparation method thereof. BACKGROUND

[0002] Daily-use ceramic mainly includes four categories of fine porcelain, stoneware, fine pottery and coarse pottery, and the main difference lies in the water absorption rate of ceramic formation. The water absorption rate of stoneware is between 0.5% and 3%, and the firing temperature is between 1160 and 1260 degrees Celsius. The stoneware is mainly decorated with color glaze, because the firing temperature is relatively low, and various inorganic ceramic pigments can be used, so the color glaze stoneware is popular in the world. The color glaze stoneware pursues new, strange and special decoration, and gives certain cultural connotation or other aesthetic will. The color glaze stoneware truly makes daily-use ceramic artistic, and makes artistic ceramic daily-used.

[0003] The patent application with the patent publication number CN104016722A discloses a reaction glaze with a relief effect, which comprises a base glaze and a surface glaze, and is characterized in that the base glaze comprises the following components and the mass fraction of each component is as follows: feldspar 31-35 parts, quartz 20-23 parts, calcite 12-15 parts, Guizhou soil 4-5 parts, zinc oxide 2.5-5 parts, zirconium silicate 8-10 parts, strontium carbonate 5-8 parts; the surface glaze comprises the following components and the mass fraction of each component is as follows: feldspar 23-25 parts, borax 20-25 parts, quartz 12-15 parts, calcite 15-18 parts, Guizhou soil 3-5 parts, zinc oxide 15-17 parts, zirconium silicate 8-10 parts, titanium oxide 9-10 parts, and color base 11-15 parts. The technical scheme can make the glaze surface present concave-convex feeling and have simple relief effect, but cannot realize complex relief effect and has limitations.

[0004] The patent application with the patent publication number CN104909832A discloses a gold metal glaze and a preparation method thereof, and the components of the gold metal glaze and the mass fraction of each component are as follows: potassium feldspar 35-40 parts, kaolin 5-8 parts, quartz 8-12 parts, high-expansion coefficient frit 3-5 parts, barium carbonate 4-7 parts, high-lead frit 15-25 parts, vanadium pentoxide 1-2 parts, manganese dioxide 10-12 parts, copper oxide 1-3 parts, and talc 1-2 parts. The patent is a surface glaze formula, high-lead powder is added to break the traditional lead-free metal glaze mode, the metal luster of the oxide can be more stable, but the relief effect is not achieved. Because of the lead content, the product is not suitable for export daily-use ceramic production, that is, the quality standard for export is not reached.

[0005] The special rubber roller or the printing screen plate with optimized screen mesh number is used in the prior art to print the special glaze on the body with the base glaze and the surface glaze, and the special glaze pattern is sunk in the common surface glaze after high-temperature firing. In view of the defects of the prior art, it is of great significance to research and develop a net-texture relief glaze to meet the current market demand. SUMMARY

[0006] The technical problem to be solved by the present application is to provide a net-texture relief glaze and a preparation method thereof, so as to obtain the net-texture relief glaze with low lead and cadmium content, high thermal stability, warm luster and delicate touch.

[0007] The present application includes the following contents:

[0008] A net-texture relief glaze comprises a base glaze, a surface glaze and a spray point glaze, wherein the base glaze comprises the following raw materials in parts by weight: 3# frit 13-17 parts, potassium feldspar 38-42 parts, quartz 14-20 parts, calcite 10-15 parts, barium carbonate 2-6 parts, calcined talc 3-7 parts, burned zinc 3-7 parts, Guizhou soil 3-7 parts, zirconium silicate 1-5 parts and synthetic colorant 0.1-10 parts.

[0009] The surface glaze comprises the following raw materials in parts by weight: 2# frit 8-15 parts, potassium feldspar 38-42 parts, quartz 14-20 parts, calcite 13-17 parts, barium carbonate 3-7 parts, calcined talc 1-3 parts, burned zinc 3-7 parts, Longyan mud 8-12 parts, zirconium silicate 15-22 parts, titanium white 3-7 parts, calcined bone carbon 1-3 parts and synthetic colorant 0-10 parts.

[0010] The spray point glaze comprises the following raw materials in parts by weight: 3# frit 14-18 parts, potassium feldspar 38-42 parts, quartz 8-12 parts, calcite 10-14 parts, barium carbonate 3-7 parts, calcined talc 1-3 parts, burned zinc 3-7 parts, Longyan mud 8-12 parts and vanadium pentoxide 6-10 parts.

[0011] In one embodiment, the base glaze comprises the following raw materials in parts by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, burned zinc 5 parts, Guizhou soil 5 parts, zirconium silicate 3 parts and synthetic colorant 7 parts.

[0012] The surface glaze comprises the following raw materials in parts by weight: 2# frit 10 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, burned zinc 5 parts, Longyan mud 10 parts, zirconium silicate 20 parts, titanium white 5 parts, calcined bone carbon 2 parts and synthetic colorant 10 parts.

[0013] The spray point glaze comprises the following raw materials by weight: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, and vanadium pentoxide 8 parts.

[0014] Another object of the present application is to provide a preparation method of the above-mentioned net-patterned relief glaze, comprising the following steps:

[0015] (1) preparing a ceramic wet body, drying to form a ceramic dry body;

[0016] (2) applying a base glaze on the surface of the ceramic dry body, then applying a surface glaze, and finally applying a spray point glaze with appropriate size to form a ceramic glaze body;

[0017] (3) drying the ceramic glaze body so that the water content of the body is less than 1%;

[0018] (4) firing the dried body in a kiln to obtain a net-patterned relief glaze product.

[0019] In one embodiment, the thickness of the base glaze in step (2) is 0.10-0.25 mm.

[0020] In one embodiment, the thickness of the surface glaze in step (2) is 0.10-0.15 mm.

[0021] In one embodiment, the average particle size of the slurry of the base glaze and the surface glaze in step (2) is 40-60 μm.

[0022] In one embodiment, the drying temperature of the ceramic wet body in step (1) is 100-120℃, and the drying time is 70-90 min.

[0023] In one embodiment, the drying temperature of the ceramic glaze body in step (3) is 100-120℃, and the drying time is 30-50 min.

[0024] In one embodiment, the firing atmosphere in step (4) is an oxidizing atmosphere.

[0025] In one embodiment, the firing temperature in step (4) is 1170-1210℃.

[0026] The composition of the 2# frit and the 3# frit is as follows:

[0027] SiO2 Al2O3 B2O3 CaO MgO [K2O] Na2O Li2O 2# frit 58 7.2 13 6.8 1.5 6.2 7 / 3# frit 56.2 14 8.1 9.4 / 2 9.5 0.5

[0028] The present application has the following beneficial effects:

[0029] (1) The present application is in the form of three-layer glaze, the base glaze is mainly bright glaze; the surface glaze (middle layer) is mainly bright glaze with certain viscosity, maintains certain fluidity, combines well with the base glaze but has obvious levels without mutual fusion or reaction; then uniform coarse point glaze is sprayed on the two layers of glaze, the recess is generated from the uppermost coarse point glaze, the surface glaze (middle layer) glaze is pushed away to form a network, the base glaze is also relatively sunken without exposing the body to form the networked relief effect, the touch is delicate, the networked relief glaze has warm and moist luster;

[0030] (2) The addition of vanadium pentoxide in the point glaze formula can enhance the transparency and color level of the glaze surface, too little addition is easy to cause the relief effect not obvious, too much addition is easy to cause the relief effect too obvious, even exposing the embryo;

[0031] (3) The addition of zirconium silicate in the surface glaze formula can not only improve the body-glaze separation performance of the ceramic, but also has the effect of whitening, too little addition is easy to cause the surface glaze flow effect not good, leading to the network effect blurred;

[0032] (4) The formula of the three-layer glaze of the present application needs to be added strictly according to the proportion, too much or too little content of a component of the glaze formula will affect the relief effect, glaze luster, texture and other effects of the relief glaze;

[0033] (5) The preparation process of the present application is simple, the lead and cadmium content is low, the thermal stability is high, the networked relief glaze has warm and moist luster, delicate touch, the various indexes meet the relevant standard requirements, has strong universality, is easy to popularize and apply in the industry; the present application can control the color of the base glaze and the network color as needed, can better meet the design requirements and adapt to customer needs. DETAILED DESCRIPTION

[0034] Example 1

[0035] A networked relief glaze formula and preparation method, comprising the following steps:

[0036] (1) A ceramic wet body is made, dried at 110 DEG C for 80 min to form a ceramic dry body. Then glaze is applied on the surface of the ceramic dry body to form a ceramic glaze body; the glaze comprises the following: the base glaze comprises the following components by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou soil 5 parts, zirconium silicate 3 parts, vanadium blue 2 parts, praseodymium yellow 5 parts.

[0037] The components of the surface layer surface glaze by weight: 2# frit 10 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan mud 10 parts, zirconium silicate 20 parts, titanium white 5 parts, calcined bone carbon 2 parts, 1519# wrapped big red 10 parts.

[0038] The composition of the outermost spraying point glaze by weight: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, vanadium pentoxide 8 parts.

[0039] (2) The glaze body is placed at 110°C and dried for 40 minutes, so that the water content of the body is kept below 1%;

[0040] (3) The body after the above processing is put into a kiln at 1200°C for firing, and the firing atmosphere is an oxidizing atmosphere. After firing, the product is a green base white net pattern relief stoneware product.

[0041] Example 2

[0042] A formula and preparation method of a net pattern relief glaze, comprising the following steps:

[0043] (1) A ceramic wet body is made, dried at 100°C for 90 minutes to form a ceramic dry body. Then glaze is applied to the surface of the ceramic dry body to form a ceramic glaze body; the glaze comprises the following: the base glaze comprises the following components by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou clay 5 parts, zirconium silicate 3 parts, vanadium blue 2 parts, praseodymium yellow 5 parts.

[0044] The composition of the surface layer glaze by weight: 2# frit 12 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, zirconium silicate 20 parts, titanium white 5 parts, calcined bone carbon 2 parts.

[0045] The composition of the outermost spraying point glaze by weight: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, vanadium pentoxide 8 parts.

[0046] (2) The glaze body is placed at 100°C and dried for 40 minutes, so that the water content of the body is kept below 1%;

[0047] (3) The body after the above processing is put into a kiln at 1200°C for firing, and the firing atmosphere is an oxidizing atmosphere. After firing, the product is a green base white net pattern relief stoneware product.

[0048] Example 3

[0049] A formula and preparation method of a net pattern relief glaze, comprising the following steps:

[0050] (1) The ceramic wet body is made, dried at 110°C for 80 minutes to form a ceramic dry body. Then the glaze is applied on the surface of the ceramic dry body to form a ceramic glaze body; the glaze comprises the following: the base glaze comprises the following components by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou soil 5 parts, zirconium silicate 3 parts, orange red 6 parts.

[0051] The components of the surface layer glaze by weight are: 2# frit 12 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, zirconium silicate 20 parts, titanium white 5 parts, and calcined bone carbon 2 parts.

[0052] The components of the outermost spraying point glaze by weight are: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, and vanadic oxide 8 parts.

[0053] (2) The glaze body is placed at 110°C and dried for 40 minutes to keep the water content of the body below 1%;

[0054] (3) The body processed above is fired in a kiln at 1200°C, and the firing atmosphere is an oxidizing atmosphere. After firing, the product is a red base white net pattern relief stoneware product.

[0055] Example 4

[0056] A net pattern relief glaze formula and preparation method, comprising the following steps:

[0057] (1) The ceramic wet body is made, dried at 120°C for 70 minutes to form a ceramic dry body. Then the glaze is applied on the surface of the ceramic dry body to form a ceramic glaze body; the glaze comprises the following: the base glaze comprises the following components by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou soil 5 parts, zirconium silicate 3 parts, deep blue 5 parts, and bright black 0.5 parts.

[0058] The components of the surface layer glaze by weight are: 2# frit 12 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, zirconium silicate 20 parts, titanium white 5 parts, and calcined bone carbon 2 parts.

[0059] The components of the outermost spraying point glaze by weight are: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, and vanadic oxide 8 parts.

[0060] (2) Put the glaze body at 120℃, dry for 30min, keep the water content of the body below 1% ;

[0061] (3) Put the body finished above into the kiln, fire at 1180℃, the firing atmosphere is oxidation atmosphere, after firing, the product is a blue base white net pattern relief stoneware product.

[0062] Example 5

[0063] A formula and preparation method of a net pattern relief glaze, comprising the following steps:

[0064] (1) Make a ceramic wet body, dry at 110℃ for 80min to form a ceramic dry body. Then apply glaze on the surface of the ceramic dry body to form a ceramic glaze body; the glaze comprises the following components by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou clay 5 parts, zirconium silicate 3 parts, deep blue 5 parts, and bright black 0.5 parts.

[0065] The components of the surface layer glaze by weight are: 2# frit 12 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, zirconium silicate 20 parts, titanium white 5 parts, and calcined bone carbon 2 parts. 1519# package big red 10 parts.

[0066] The components of the outermost spray point glaze by weight are: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan clay 10 parts, and vanadium pentoxide 8 parts.

[0067] (2) Put the glaze body at 110℃, dry for 40min, keep the water content of the body below 1% ;

[0068] (3) Put the body finished above into the kiln, fire at 1200℃, the firing atmosphere is oxidation atmosphere, after firing, the product is a blue base red net pattern relief stoneware product, with a purple tone overall.

[0069] Example 6

[0070] The components of the spray point glaze by weight are: 3# frit 18 parts, potassium feldspar 38 parts, quartz 12 parts, calcite 12 parts, barium carbonate 7 parts, calcined talc 2 parts, zinc 3 parts, Longyan clay 12 parts, and vanadium pentoxide 6 parts.

[0071] The others are the same as Example 1.

[0072] Example 7

[0073] The components of the surface layer of the surface glaze by weight parts: 2# frit 15 parts, potassium feldspar 38 parts, quartz 14 parts, calcite 13 parts, barium carbonate 5 parts, calcined talc 3 parts, burned zinc 5 parts, Longyan clay 12 parts, zirconium silicate 18 parts, titanium white 5 parts, calcined bone carbon 2 parts, synthetic colorant 5010# wrapped yellow 8 parts.

[0074] The other is the same as Example 1.

[0075] Example 8

[0076] The formula of the base glaze is 3# frit 13 parts, potassium feldspar 42 parts, quartz 14 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 7 parts, burned zinc 3 parts, Guizhou soil 4 parts, zirconium silicate 5 parts, synthetic colorant 5010# wrapped yellow 7 parts.

[0077] The other is the same as Example 1.

[0078] Comparative Example 1

[0079] The vanadium pentoxide in the formula of the spot glaze is reduced to 3 parts, and the other is the same as Example 1.

[0080] Comparative Example 2

[0081] The vanadium pentoxide in the formula of the spot glaze is increased to 18 parts, and the other is the same as Example 1.

[0082] Comparative Example 3

[0083] The zirconium silicate in the surface glaze layer is reduced to 5 parts, and the burned zinc is increased to 10 parts, and the other is the same as Example 1.

[0084] Comparative Example 4

[0085] Compared with Example 1, no surface glaze is used, and the spot is directly sprayed on the base glaze, that is, the intermediate glaze layer is reduced, and the other is the same as Example 1.

[0086] Comparative Example 5

[0087] The components of the surface layer of the surface glaze by weight parts: 2# frit 15 parts, potassium feldspar 38 parts, quartz 14 parts, calcite 13 parts, barium carbonate 5 parts, calcined talc 3 parts, burned zinc 5 parts, Longyan clay 12 parts, zirconium silicate 18 parts, titanium white 5 parts, calcined bone carbon 2 parts, synthetic colorant 5010# wrapped yellow 8 parts.

[0088] The other base glaze and spot glaze components are the same as Example 1, and the preparation method is the same as Example 1.

[0089] Comparative Example 6

[0090] The components of the spot glaze by weight parts: 3# frit 8 parts, potassium feldspar 45 parts, quartz 6 parts, calcite 16 parts, barium carbonate 10 parts, calcined talc 5 parts, burned zinc 2 parts, Longyan clay 6 parts, vanadium pentoxide 10 parts.

[0091] Other underglaze, overglaze components are as in Example 1, and the preparation method is as in Example 1.

[0092] The test results are shown in the following table.

[0093] Table 1 Product quality test results

[0094]

[0095]

[0096] It should be understood by those of ordinary skill in the art that the above discussion of any of the embodiments is merely exemplary and is not intended to be limiting of the scope of protection of the present application; the above embodiments or technical features among different embodiments can also be combined, the steps can be implemented in any order, and there are many other changes of different aspects of one or more embodiments of the present application as described above, which are not provided in detail for the sake of brevity.

[0097] One or more embodiments of the present application are intended to cover all such alternatives, modifications, and variations as fall within the broad scope of the present application. Accordingly, any omission, modification, equivalent replacement, improvement, etc. made within the spirit and principles of one or more embodiments of the present application should be included in the scope of protection of the present application.

Claims

1. A netted relief glaze, characterized by, The bottom glaze, the surface glaze and the spray point glaze, the bottom glaze comprises the following raw materials by weight: 3# frit 13-17 parts, potassium feldspar 38-42 parts, quartz 14-20 parts, calcite 10-15 parts, barium carbonate 2-6 parts, calcined talc 3-7 parts, zinc 3-7 parts, Guizhou soil 3-7 parts, zirconium silicate 1-5 parts, synthetic colorant 0.1-10 parts; The surface glaze comprises the following raw materials by weight: 2# frit 8-15 parts, potassium feldspar 38-42 parts, quartz 14-20 parts, calcite 13-17 parts, barium carbonate 3-7 parts, calcined talc 1-3 parts, zinc 3-7 parts, Longyan mud 8-12 parts, zirconium silicate 15-22 parts, titanium white 3-7 parts, calcined bone carbon 1-3 parts, synthetic colorant 0-10 parts; The spray point glaze comprises the following raw materials by weight: 3# frit 14-18 parts, potassium feldspar 38-42 parts, quartz 8-12 parts, calcite 10-14 parts, barium carbonate 3-7 parts, calcined talc 1-3 parts, zinc 3-7 parts, Longyan mud 8-12 parts, vanadium pentoxide 6-10 parts.

2. The networked relief glaze of claim 1, wherein The bottom glaze comprises the following raw materials by weight: 3# frit 15 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 12 parts, barium carbonate 4 parts, calcined talc 5 parts, zinc 5 parts, Guizhou soil 5 parts, zirconium silicate 3 parts, synthetic colorant 7 parts; The surface glaze comprises the following raw materials by weight: 2# frit 10 parts, potassium feldspar 40 parts, quartz 16 parts, calcite 15 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan mud 10 parts, zirconium silicate 20 parts, titanium white 5 parts, calcined bone carbon 2 parts, synthetic colorant 10 parts; The spray point glaze comprises the following raw materials by weight: 3# frit 16 parts, potassium feldspar 40 parts, quartz 10 parts, calcite 12 parts, barium carbonate 5 parts, calcined talc 2 parts, zinc 5 parts, Longyan mud 10 parts, vanadium pentoxide 8 parts.

3. A method of preparing a netted relief glaze as claimed in claim 1 or 2, characterized in that, It comprises the following steps: (1) making ceramic wet body, drying, forming ceramic dry body; (2) applying bottom glaze on the surface of the ceramic dry body, then spraying surface glaze, finally spraying appropriate size spray point glaze, forming ceramic glaze body; (3) drying the ceramic glaze body, so that the water content of the body is less than 1%; (4) putting the dried body into the kiln for firing, obtaining net-shaped relief glaze product.

4. The method of claim 3, wherein the netted relief glaze is prepared by the steps of: The thickness of the bottom glaze in step (2) is 0.10-0.25mm.

5. The method for preparing the reticulated relief glaze as described in claim 3, characterized in that, The thickness of the surface glaze in step (2) is 0.10-0.15mm.

6. The method of claim 3, wherein the netted relief glaze is prepared by the steps of: The average particle size of the slurry of the bottom glaze and the surface glaze in step (2) is 40-60μm.

7. The method for preparing the reticulated relief glaze as described in claim 3, characterized in that, The drying temperature of the ceramic wet body in step (1) is 100-120℃, and the drying time is 70-90min.

8. The method for preparing the reticulated relief glaze as described in claim 3, characterized in that, The drying temperature of the ceramic glaze body in step (3) is 100-120℃, and the drying time is 30-50min.

9. The method for preparing the reticulated relief glaze as described in claim 3, characterized in that, The firing atmosphere in step (4) is oxidation atmosphere.

10. The method of claim 3 to 9, wherein the method is characterized by, The firing temperature in step (4) is 1170-1210℃.

Citation Information

Patent Citations

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