Device for improving separation efficiency and test accuracy of capacitive deionization technology

Abstract

The invention relates to the technical field of extraction agent deionization, and discloses a device for improving the separation efficiency and test accuracy of a capacitive deionization technology, the device comprises a base, the top of the base is provided with four cushion blocks, a washing tank is fixedly connected among the tops of the four cushion blocks, and the front side of the washing tank is provided with a first water outlet pipe; the first water outlet pipe penetrates through and extends to the inner wall of the washing tank, the first water outlet pipe is fixedly connected with the washing tank, and the front end of the first water outlet pipe is fixedly connected with a water phase valve. After a machine phase and a water phase are mixed and stirred for a certain time, standing and layering are carried out, at the moment, part of ions of an extracting agent enter the water phase, then a first water outlet pipe is led out from the bottom of a washing tank, a conductivity tester is arranged in a communicating pipe on the first water outlet pipe, and the conductivity tester and the communicating pipe are in a vertical state; therefore, the conductivity tester is always in the water phase, and the situation that the probe of the conductivity tester is in contact with the oil phase, so that the measurement result is inaccurate is avoided.

Description

Technical Field

[0001] The invention relates to the technical field of extractant deionization, in particular to a device for improving the separation efficiency and test accuracy of capacitive deionization technology. Background Art

[0002] The recycling of the organic phase of the extractant has important economic significance for industrial production. It not only reduces costs, but also reduces the pollution of the environment by organic reagents. The water washing deionization device can elute a certain concentration of ions in the organic phase, and the more washing times, the better the elution effect.

[0003] During the water washing and regeneration process of the used organic extractant, it is necessary to use a conductivity meter to test the ion content. If the organic phase contacts the test probe of the conductivity meter, it will adhere to the probe, reducing the accuracy of the test results. Summary of the invention

[0004] In view of the deficiencies of the prior art, the present invention provides a device for improving the separation efficiency and test accuracy of capacitive deionization technology, thereby solving the problem of reduced accuracy of test results.

[0005] To achieve the above objectives, the present invention is implemented through the following technical solutions: a device for improving the separation efficiency and test accuracy of capacitive deionization technology, comprising a base, four pads are arranged on the top of the base, a washing tank is fixedly connected between the tops of the four pads, a first water outlet pipe is arranged on the front side of the washing tank, the first water outlet pipe penetrates and extends to the inner wall of the washing tank, the first water outlet pipe is fixedly connected to the washing tank, a water phase valve is fixedly connected to the front end of the first water outlet pipe, a connecting pipe is fixedly connected to the top of the first water outlet pipe, the connecting pipe and the first water outlet pipe are mutually connected, a conductivity meter is arranged on the inner diameter of the connecting pipe, a connecting column is fixedly connected at the center position of the bottom of the inner wall of the washing tank, a telescopic conduit is fixedly connected to the top of the connecting column, a float guide ball is fixedly connected to the bottom end of the connecting column, a second water outlet pipe is fixedly connected to the bottom end of the second water outlet pipe, an organic phase valve is fixedly connected to the bottom end of the second water outlet pipe, a support frame is arranged on the left side of the top of the base, and a stirring device is arranged on the top of the support frame.

[0006] Preferably, the stirring device comprises a stirring kettle, which is fixedly connected to a support frame, a fixing frame is fixedly connected to the top of the stirring kettle, a driving motor is fixedly connected to the center position of the top of the fixing frame, and a stirring rod is fixedly connected to the output end of the driving motor.

[0007] Preferably, one end of a liquid outlet pipe is fixedly connected to the center of the bottom of the stirring kettle, and the liquid outlet pipe and the stirring kettle are interconnected.

[0008] Preferably, the conductivity meter is threadedly connected to the connecting pipe.

[0009] Preferably, a guide port is provided at the center of the top of the float guide ball, and the guide port and the top of the telescopic conduit are interconnected.

[0010] Preferably, the bottom end of the second water outlet pipe passes through and extends to the bottom of the outer wall of the washing tank, and the second water outlet pipe is fixedly connected to the washing tank.

[0011] Preferably, the connecting column and the second water outlet pipe are interconnected, and the connecting column and the telescopic guide tube are interconnected.

[0012] Preferably, the other end of the liquid outlet pipe passes through and is fixedly connected to the washing tank, the liquid outlet pipe passes through and extends to the inner wall of the washing tank, and the liquid outlet pipe and the washing tank are interconnected.

[0013] Preferably, a limiting ring is sleeved on the outer diameter of the stirring rod, and limiting columns are fixedly connected to both sides of the outer diameter of the limiting ring, and the limiting columns are fixedly connected to the inner wall of the stirring tank.

[0014] Working principle: Add the used extractant into the stirring tank of the stirring device to make it as the organic phase, and add a certain proportion of water into the stirring tank as the aqueous phase, and start the driving motor to drive the stirring rod to rotate and stir, so that the organic phase and the aqueous phase components in the stirring tank are fully mixed, and the ions in the organic phase enter the water. After stirring for a certain period of time, the driving motor in the stirring device stops working, the stirring rod stops rotating, and the mixture of the organic phase and the aqueous phase components flows into the washing tank through the liquid outlet pipe. The mixture in the washing tank is statically layered. The density of the organic phase is smaller than that of water, so it is in the upper layer, and the density of water is larger than that of the organic phase, so it is in the lower layer. At this time, some ions of the extractant enter the aqueous phase, and the first outlet pipe is led out at the bottom of the washing tank. The middle section of the first outlet pipe is also connected to a connecting pipe, and a conductivity meter is also arranged in the connecting pipe. In this way, the conductivity meter will always be in the aqueous phase to avoid the conductivity meter probe from contacting the oil phase, which will make the measurement result inaccurate. The other side of the aqueous phase valve on the first outlet pipe can be connected to a conventional CD I device carries out the adsorption and desorption process of ions in the water phase. After the desorption, the water phase can be returned to the washing tank for recycling until all the ions in the extractant are transferred to the water phase to complete the washing and regeneration of the extractant. After the washing of the extractant is completed, the ions in the organic phase have completely entered the water phase. At this time, the organic phase valve is opened to discharge the organic phase through the diversion port on the top of the float guide ball. The bottom of the float guide ball is connected to the telescopic catheter to meet the continuous change of the liquid level during the discharge of the organic phase. After the organic phase has completely flowed out, the organic phase to be washed is added again to continue to complete the above steps. The float guide ball has a density between the density of the water phase and the organic phase and can be suspended on the interface between the water phase and the organic phase. A diversion port is set on the side close to the organic phase, that is, the upper part of the float guide. The organic phase valve is opened and the organic phase flows out through the diversion port, and it is always ensured that the discharged liquid is the organic phase.

[0015] The present invention provides a device for improving the separation efficiency and test accuracy of capacitive deionization technology. It has the following beneficial effects:

[0016] The present invention mixes an organic phase with an aqueous phase, stirs it for a certain period of time, and then stands to separate the layers. At this time, part of the ions of the extractant enter the aqueous phase, and then a first water outlet pipe is led out from the bottom of the washing tank. The conductivity meter is arranged in a connecting pipe on the first water outlet pipe, and the conductivity meter and the connecting pipe are in a vertical state. In this way, the conductivity meter will always be in the aqueous phase, so as to avoid the probe of the conductivity tester contacting the oil phase, which will make the measurement result inaccurate. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 A perspective view of the present invention;

[0018] Figure 2 It is a three-dimensional top view schematic diagram of the present invention;

[0019] Figure 3 It is a top view schematic diagram of the present invention;

[0020] Figure 4 It is a rear view schematic diagram of the present invention;

[0021] Figure 5 It is a cross-sectional schematic diagram of the present invention.

[0022] Among them, 1. base; 2. support frame; 3. stirring kettle; 4. washing tank; 5. water phase valve; 6. float guide ball; 7. telescopic catheter; 8. connecting column; 9. organic phase valve; 10. stirring rod; 11. fixing frame; 12. driving motor; 13. diversion port; 14. conductivity meter; 15. first water outlet pipe; 16. second water outlet pipe; 17. cushion block; 18. limiting ring; 19. liquid outlet pipe; 20. connecting pipe; 21. limiting column. DETAILED DESCRIPTION

[0023] The technical solution of the present invention will be described clearly and completely below in conjunction with the accompanying drawings of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0024] Please refer to the attached Figure 1 -Attached Figure 5 The embodiment of the present invention provides a device for improving the separation efficiency and test accuracy of capacitive deionization technology, including a base 1, four pads 17 are arranged on the top of the base 1, a washing tank 4 is fixedly connected between the tops of the four pads 17, a first water outlet pipe 15 is arranged on the front side of the washing tank 4, the first water outlet pipe 15 penetrates and extends to the inner wall of the washing tank 4, the first water outlet pipe 15 is fixedly connected to the washing tank 4, a water phase valve 5 is fixedly connected to the front end of the first water outlet pipe 15, a connecting pipe 20 is fixedly connected to the top of the first water outlet pipe 15, the connecting pipe 20 and the first water outlet pipe 15 are mutually connected, a conductivity meter 14 is arranged on the inner diameter of the connecting pipe 20, a connecting column 8 is fixedly connected at the center position of the bottom of the inner wall of the washing tank 4, a telescopic conduit 7 is fixedly connected to the top of the connecting column 8, a float guide ball 6 is fixedly connected to the top of the telescopic conduit 7, a second water outlet pipe 16 is fixedly connected to the bottom end of the connecting column 8, and an organic phase valve 9 is fixedly connected to the bottom end of the second water outlet pipe 16, a support frame 2 is arranged on the left side of the top of the base 1, and a stirring device is arranged on the top of the support frame 2.

[0025] There are four pads 17 in total, which are respectively located at the four corners of the washing tank 4, so that the washing tank 4 is lifted so that there is a certain space between its bottom and the base 1. A hole with the same diameter as the first water outlet pipe 15 is opened on the front side of the washing tank 4, so that the first water outlet pipe 15 can be directly inserted into the hole, and the first water outlet pipe 15 is fixed to the washing tank 4 by welding, and a flange connector is fixed by screws at one end in front of the first water outlet pipe 15 to fix the water phase valve 5 on the first water outlet pipe 15. The second water outlet pipe 16 passes through the bottom of the washing tank 4 and is connected to the connecting column 8. Because of the lifting of the four pads 17, the second water outlet pipe 16 can be located at the bottom of the washing tank 4.

[0026] The stirring device includes a stirring kettle 3, which is fixedly connected to the support frame 2. A fixing frame 11 is fixedly connected to the top of the stirring kettle 3, a driving motor 12 is fixedly connected to the top center of the fixing frame 11, and a stirring rod 10 is fixedly connected to the output end of the driving motor 12.

[0027] The driving motor 12 is used to drive the stirring rod 10 to rotate in the stirring tank 3 to mix the organic phase with the aqueous phase.

[0028] One end of a liquid outlet pipe 19 is fixedly connected to the center of the bottom of the stirring tank 3 , and the liquid outlet pipe 19 and the stirring tank 3 are interconnected.

[0029] A valve is also provided at one end of the liquid outlet pipe 19 connected to the washing tank 4. The valve will open to transport the mixture to the washing tank 4 through the liquid outlet pipe 19 when the mixing is completed.

[0030] The conductivity meter 14 and the connecting pipe 20 are threadedly connected.

[0031] By providing a thread on the inner wall of the connecting pipe 20 , the conductivity meter 14 can be installed or removed simply by twisting the conductivity meter 14 .

[0032] A flow guide port 13 is provided at the center of the top of the float guide ball 6 , and the flow guide port 13 and the top of the telescopic conduit 7 are interconnected.

[0033] The density of the organic phase is smaller than that of water, so it is in the upper layer; the density of water is larger than that of the organic phase, so it is in the lower layer; the float guide ball 6 has a density between the density of the water phase and the organic phase, and can be suspended on the interface between the water phase and the organic phase; the organic phase is discharged through the guide port 13 at the top of the float guide ball 6, and the organic phase flows along the telescopic conduit 7.

[0034] The bottom end of the second water outlet pipe 16 penetrates through and extends to the bottom of the outer wall of the washing tub 4 , and the second water outlet pipe 16 is fixedly connected to the washing tub 4 .

[0035] The connecting column 8 and the second water outlet pipe 16 are interconnected, and the connecting column 8 and the telescopic conduit 7 are interconnected.

[0036] Because the connecting column 8 is in communication with the second water outlet pipe 16 , the organic phase flows along the telescopic conduit 7 and then continues to flow through the second water outlet pipe 16 , and is finally discharged through the organic phase valve 9 .

[0037] The other end of the liquid outlet pipe 19 penetrates and is fixedly connected to the washing tank 4 . The liquid outlet pipe 19 penetrates and extends to the inner wall of the washing tank 4 . The liquid outlet pipe 19 and the washing tank 4 are interconnected.

[0038] A limiting ring 18 is sleeved on the outer diameter of the stirring rod 10 , and limiting columns 21 are fixedly connected to both sides of the outer diameter of the limiting ring 18 . The limiting columns 21 are fixedly connected to the inner wall of the stirring tank 3 .

[0039] When the stirring device is in use, as the stirring rod 10 rotates, the stirring rod 10 is subjected to resistance from the liquid, and the limiting ring 18 is sleeved on the stirring rod 10 and supported by the limiting column 21 to prevent the stirring rod 10 from being offset and deformed due to the resistance.

[0040] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A device for improving the separation efficiency and test accuracy of capacitive deionization technology, comprising a base (1), characterized in that: Four cushion blocks (17) are arranged on the top of the base (1), a washing tank (4) is fixedly connected between the tops of the four cushion blocks (17), a first water outlet pipe (15) is arranged on the front side of the washing tank (4), the first water outlet pipe (15) penetrates and extends to the inner wall of the washing tank (4), the first water outlet pipe (15) is fixedly connected to the washing tank (4), a water valve (5) is fixedly connected to the front end of the first water outlet pipe (15), a connecting pipe (20) is fixedly connected to the top of the first water outlet pipe (15), and the connecting pipe (20) and the first water outlet pipe (15) are connected to each other. The two connecting pipes (20) are interconnected, the inner diameter of which is provided with a conductivity meter (14), a connecting column (8) is fixedly connected to the center position of the bottom of the inner wall of the washing tank (4), the top of the connecting column (8) is fixedly connected to a telescopic guide tube (7), the top of the telescopic guide tube (7) is fixedly connected to a float guide ball (6), the bottom end of the connecting column (8) is fixedly connected to a second water outlet pipe (16), the bottom end of the second water outlet pipe (16) is fixedly connected to an organic phase valve (9), a support frame (2) is provided on the left side of the top of the base (1), and a stirring device is provided on the top of the support frame (2).

2. A device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 1, characterized in that: The stirring device comprises a stirring kettle (3), wherein the stirring kettle (3) is fixedly connected to a support frame (2), a fixing frame (11) is fixedly connected to the top of the stirring kettle (3), a driving motor (12) is fixedly connected at the center position of the top of the fixing frame (11), and a stirring rod (10) is fixedly connected to the output end of the driving motor (12).

3. A device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 2, characterized in that: One end of a liquid outlet pipe (19) is fixedly connected to the center of the bottom of the stirring kettle (3), and the liquid outlet pipe (19) and the stirring kettle (3) are interconnected.

4. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 1, characterized in that: The conductivity meter (14) and the connecting pipe (20) are threadedly connected.

5. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 1, characterized in that: A flow guide port (13) is provided at the center of the top of the float flow guide ball (6), and the flow guide port (13) and the top of the telescopic conduit (7) are interconnected.

6. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 1, characterized in that: The bottom end of the second water outlet pipe (16) penetrates through and extends to the bottom of the outer wall of the washing tank (4), and the second water outlet pipe (16) is fixedly connected to the washing tank (4).

7. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 1, characterized in that: The connecting column (8) and the second water outlet pipe (16) are interconnected, and the connecting column (8) and the telescopic guide tube (7) are interconnected.

8. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 3, characterized in that: The other end of the liquid outlet pipe (19) passes through and is fixedly connected to the washing tank (4); the liquid outlet pipe (19) passes through and extends to the inner wall of the washing tank (4); and the liquid outlet pipe (19) and the washing tank (4) are interconnected.

9. The device for improving separation efficiency and test accuracy of capacitive deionization technology according to claim 2, characterized in that: The outer diameter of the stirring rod (10) is sleeved with a limiting ring (18), and both sides of the outer diameter of the limiting ring (18) are fixedly connected to limiting columns (21), and the limiting columns (21) are fixedly connected to the inner wall of the stirring tank (3).

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