Supercritical equipment with temperature control system

Abstract

The invention relates to supercritical equipment with a temperature control system, which is applied to the technical field of supercritical extraction and comprises an extraction outer tank, an extraction inner tank, a telescopic unit, a movable plug, an electric heating column unit, a refrigeration unit, a cooling pipeline and a cooling subdivision pipe. The ratio of the extraction material to the extraction medium in the extraction inner tank is circularly adjusted and changed, and when the movable plug ascends, part of the extraction medium in the extraction inner tank is extruded out of the extraction inner tank, so that the total amount of the extraction medium in the extraction inner tank is reduced to the minimum; then the heating module and the cooling module are used for heating and cooling the extraction material and the residual extraction medium in the extraction inner tank, so that the temperature of the extraction material can be adjusted more directly, and the influence of the extraction medium on the temperature adjustment of the extraction material is also reduced due to the reduction of the proportion of the extraction medium; and the temperature control regulation efficiency of the supercritical extraction equipment is effectively improved.

Description

Technical Field

[0001] The invention relates to a supercritical device, in particular to a supercritical device with a temperature control system applied in the technical field of supercritical extraction. Background Art

[0002] Supercritical extraction is a technique that uses supercritical fluid as an extraction medium to separate different components in a mixture. Supercritical fluid refers to a fluid state above its critical temperature and critical pressure. In this state, the fluid has unique solubility and diffusion properties, making it an effective medium in the extraction process. Supercritical extraction is the best way to extract plant active ingredients.

[0003] The specification of Chinese invention patent CN202120302110.9 discloses "An efficient high-pressure foaming device for supercritical fluids". By monitoring the temperature inside the reactor through a temperature monitoring device, when the temperature is lower than the set temperature, the heating plate inside the heating box is turned on, and the electric valve outside the heating box is opened to allow hot air to enter the temperature control box from the air inlet to achieve heating inside the reactor. When the temperature is higher than the set temperature, the refrigeration plate inside the refrigeration box is turned on, and the electric valve outside the refrigeration box is opened to allow cold air to enter the temperature control box from the air inlet to achieve cooling inside the reactor. The specification of Chinese invention patent CN202122720420.5 discloses "A supercritical extraction device for rose essential oil". Through the setting of a guide hood, it can guide fluid of suitable temperature to surround the extraction tank, so that the extraction tank and its internal substances can reach the expected temperature value, and active temperature control operation can be achieved.

[0004] Currently, there are two ways to perform temperature control on supercritical extraction equipment. One is to perform temperature control on the extraction medium input into the extraction tank and then input it into the tank body. The other is to perform temperature control on the inside of the tank body directly. However, both of these temperature control methods directly act on the extraction medium. The extraction medium needs to be temperature controlled first before the temperature control of the extraction material can be indirectly achieved. The entire adjustment process is inefficient, and the activity of the extraction material is affected by temperature. Therefore, accurate temperature control of the extraction material is an important factor in maintaining extraction activity. Summary of the invention

[0005] In view of the above-mentioned prior art, the technical problem to be solved by the present invention is that the existing temperature control and regulation methods all directly act on the extraction medium. The extraction medium needs to be temperature-controlled and regulated first before the temperature control and regulation of the extraction material can be indirectly achieved. The entire regulation process is inefficient.

[0006] In order to solve the above problems, the present invention provides a supercritical device with a temperature control system, comprising an extraction outer tank, an extraction inner tank is sleeved inside the extraction outer tank, an upper opening and a lower opening are respectively opened at the top and the bottom of the extraction inner tank, the upper opening and the lower opening are both communicated with the inside of the extraction outer tank, the top of the extraction inner tank is fixedly connected with a combined sealing cover, the combined sealing cover is plugged with the top of the extraction outer tank, the bottom of the extraction outer tank is fixedly connected with a telescopic unit, the output end of the telescopic unit extends into the inside of the extraction inner tank from the lower opening, and the output end of the telescopic unit is fixedly connected with a movable plug;

[0007] A heating module is fixedly connected to the interior of the extraction outer tank, and the heating module is composed of an electric heating column unit fixed to the top of the movable plug;

[0008] A cooling module is fixedly connected to the outside of the extraction outer tank. The cooling module consists of a refrigeration unit fixed on the outer frame of the extraction outer tank and a cooling pipeline connected to the refrigeration unit. A cooling subdivision pipe is fixedly connected to the top inner wall of the extraction inner tank. The cooling pipeline is fixedly passed through the combined cover and is connected to the cooling subdivision pipe.

[0009] In the above-mentioned supercritical equipment with a temperature control system, the ratio of the extraction material and the extraction medium inside the extraction inner tank is cyclically adjusted and changed through the lifting and lowering movement of the movable plug in the extraction inner tank, thereby effectively improving the mixing effect of the extraction material and the extraction medium. At the same time, when the movable plug rises to the maximum height, the total amount of the extraction medium in the extraction inner tank is reduced to a minimum, which facilitates the heating module and the cooling module to adjust the temperature of the extraction environment more quickly, effectively improving the temperature control efficiency of the supercritical extraction equipment.

[0010] As a further improvement of the present application, an output pipeline and an input pipeline are fixedly connected to the top of the combined cover, the output pipeline is fixedly connected to the middle part of the extraction inner tank, and the input pipeline is connected to the upper half of the upper opening, and the extraction medium enters and is discharged from the extraction inner tank through the output pipeline and the input pipeline. The output pipeline connected to the middle part of the extraction inner tank can better discharge the extraction medium containing the extraction components, and the new medium needs to enter from the upper opening, thereby effectively avoiding the direct circulation of the two media and effectively improving the extraction effect.

[0011] As a further improvement of the present application, an inner tank opening connected to the interior of the extraction inner tank is opened in the middle of the combined cover, and a tank plug is inserted into the interior of the inner tank opening. The extraction material in the extraction inner tank can be directly put in and taken out through the inner tank opening, which effectively improves the replacement efficiency of the extraction material.

[0012] As a further improvement of the present application, a material basket is placed inside the extraction inner tank, and a sling is fixedly connected between the bag mouth of the material basket and the bottom of the tank plug. The sling is spirally arranged and made of spring steel wire. The extraction material is stuffed into the material basket and directly placed into the extraction inner tank, thereby effectively improving the replacement efficiency of the extraction material.

[0013] As another improvement of the present application, a connecting sleeve is fixedly connected to the bottom of the material hanging basket, and the connecting sleeve is sleeved with the electric heating column unit. The connecting sleeve is made of stainless steel wire material. By sleeved with the electric heating column unit, the material hanging basket containing the extraction material can be accurately combined with the electric heating column unit, thereby effectively improving the electric heating column unit for the extraction material.

[0014] As another improvement supplement to the present application, a supporting rod is fixedly connected to the middle part of the top of the connecting sleeve, and the top of the supporting rod corresponds to the top bag opening of the material basket. The supporting rod is utilized to provide support for the upper half of the material basket, thereby effectively improving the stability of the material basket when it rises, and at the same time effectively improving the connection effect between the sling and the material basket.

[0015] As another improved supplement of the present application, the middle and bottom inner walls of the extraction outer tank are fixedly connected with separation rings, and two groups of separation rings are respectively sealed and sleeved with the middle and bottom of the extraction inner tank, and a connecting pipe is fixedly connected between the two groups of separation rings. The middle area of ​​the extraction outer tank is isolated by the two groups of separation rings, and the top and bottom of the extraction outer tank are directly connected through the connecting pipe, thereby effectively reducing the total amount of extraction medium outside the extraction inner tank and effectively reducing the amount of extraction medium used.

[0016] As another improvement of the present application, the connecting tube is distributed in a ring shape with respect to the separating ring, and the connecting tube is movably connected inside with a separating plug, the top and bottom ends of the connecting tube are fixedly connected with limiting rings, the inner diameter of the limiting rings is smaller than the outer diameter of the separating plug, and the separating plug is movable in the connecting tube to separate the top space and the bottom space of the extraction outer tank, so that the bottom of the extraction outer tank can be filled with other medium liquids that are easier to seal, further reducing the amount of extraction medium, while effectively reducing the difficulty of sealing the bottom of the extraction outer tank, thereby effectively improving the sealing effect of the bottom of the extraction outer tank.

[0017] As another improvement supplement to the present application, a liquid inlet pipe and a liquid discharge pipe are fixedly connected to the top and bottom of one end of the extraction outer tank respectively, and the inner end of the liquid inlet pipe passes through the separation ring and extends to the bottom of the extraction outer tank. The injection and discharge of the filling liquid at the bottom of the extraction outer tank are realized through the liquid inlet pipe and the liquid discharge pipe, thereby effectively improving the control of the filling solution at the bottom of the extraction outer tank.

[0018] As another improvement supplement of the present application, a capacity cylinder is fixedly connected to the bottom of the other end of the extraction outer tank, and a capacity plug is movably connected inside the capacity cylinder. By adjusting the position of the capacity plug inside the capacity cylinder, the purpose of adjusting the volume of the bottom of the extraction outer tank is achieved, thereby effectively increasing the variation range of the volume at the top of the extraction outer tank, and effectively improving the ratio adjustment of the extraction medium at the top of the extraction outer tank and the inside of the extraction inner tank.

[0019] In summary, the present invention cyclically adjusts and changes the ratio of the extraction material and the extraction medium inside the extraction inner tank through the lifting and lowering movement of the movable plug in the extraction inner tank, so as to achieve the effect of repeatedly filling the extraction medium into the extraction inner tank and mixing with the extraction material, thereby effectively improving the mixing effect of the extraction material and the extraction medium and the extraction effect of the material components. When it is necessary to temperature-control the internal environment of the extraction equipment, the movable plug is first raised to squeeze part of the extraction medium in the extraction inner tank out of the extraction inner tank, so that the total amount of the extraction medium in the extraction inner tank is reduced to a minimum, and then the heating module and the cooling module are used to heat and cool the extraction material and the remaining extraction medium in the extraction inner tank. At this time, the proportion of the extraction material in the extraction inner tank is larger, so the temperature of the extraction material can be more directly adjusted, and due to the reduction in the proportion of the extraction medium, the influence of the extraction medium on the temperature regulation of the extraction material is also reduced, thereby effectively improving the temperature control efficiency of the supercritical extraction equipment, and realizing that the temperature of the extraction material quickly returns to a temperature suitable for the activity of the extraction substance. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] Figure 1 This is a three-dimensional structural diagram of the first embodiment of the present application;

[0021] Figure 2 This is a plan view of the first embodiment of the present application;

[0022] Figure 3 This is a plan view of the extraction outer tank according to the first embodiment of the present application;

[0023] Figure 4 This is a three-dimensional structural diagram of the extraction inner tank according to the first embodiment of the present application;

[0024] Figure 5 This is a demonstration diagram of the rising movement of the movable plug in the first embodiment of the present application;

[0025] Figure 6 This is a three-dimensional structural diagram of the combined cover of the first embodiment of the present application;

[0026] Figure 7 This is a three-dimensional structural diagram of a material hanging basket according to the second embodiment of the present application;

[0027] Figure 8 This is a demonstration diagram of the second embodiment of the present application, in which the connecting sleeve is connected to the electric heating column unit;

[0028] Fig. 9 This is a three-dimensional structural diagram of the extraction outer tank according to the third embodiment of the present application.

[0029] Description of the numbers in the figure:

[0030] 1. Extraction outer tank; 101. Extraction inner tank; 102. Upper port; 103. Lower port; 104. Combined cover; 105. Telescopic unit; 106. Movable plug; 107. Output pipeline; 108. Input pipeline; 201. Electric heating column unit; 301. Refrigeration unit; 302. Cooling pipeline; 303. Cooling subdivision pipe; 4. Inner tank mouth; 401. Tank plug; 402. Material hanging basket; 403. Sling; 404. Connecting sleeve; 405. Supporting rod; 5. Separation ring; 501. Connecting pipe; 502. Separation plug; 503. Limiting ring; 504. Liquid inlet pipe; 505. Liquid discharge pipe; 506. Capacity cylinder; 507. Capacity plug. DETAILED DESCRIPTION

[0031] Three implementation modes of the present application are described in detail below with reference to the accompanying drawings.

[0032] The first implementation method:

[0033] Figures 1 to 6 FIG. 1 shows a supercritical device with a temperature control system, comprising an extraction outer tank 1, wherein an extraction inner tank 101 is sleeved inside the extraction outer tank 1, an upper opening 102 and a lower opening 103 are respectively opened at the top and bottom of the extraction inner tank 101, and the upper opening 102 and the lower opening 103 are both communicated with the inside of the extraction outer tank 1, a combined sealing cover 104 is fixedly connected to the top of the extraction inner tank 101, and the combined sealing cover 104 is plugged into the top of the extraction outer tank 1, and a telescopic unit 105 is fixedly connected to the bottom of the extraction outer tank 1, and the output end of the telescopic unit 105 extends from the lower opening 103 into the inside of the extraction inner tank 101, and the telescopic unit 105 is The output end is fixedly connected with a movable plug 106, and the top of the combined cover 104 is fixedly connected with an output pipeline 107 and an input pipeline 108. The output pipeline 107 is fixedly connected with the middle of the extraction inner tank 101, and the input pipeline 108 is connected with the upper half of the upper opening 102. The extraction medium enters and is discharged from the extraction inner tank 101 through the output pipeline 107 and the input pipeline 108. The output pipeline 107 connected to the middle of the extraction inner tank 101 can better discharge the extraction medium containing the extraction components, and the new medium needs to enter from the upper opening 102, thereby effectively avoiding the direct circulation of the two media and effectively improving the extraction effect;

[0034] When supercritical extraction is performed, the extraction material is stored in the extraction inner tank 101, and the extraction medium in the extraction outer tank 1 enters the extraction inner tank 101 through the upper port 102 to mix with the extraction material. When the movable plug 106 moves upward in the extraction inner tank 101, the space at the top of the extraction inner tank 101 is reduced. Since the extraction material will not be discharged from the extraction inner tank 101, what is squeezed out from the extraction inner tank 101 is the extraction medium. Then the movable plug 106 moves downward again in the extraction inner tank 101, and the top space of the extraction inner tank 101 is restored. The previously squeezed extraction medium returns to the extraction inner tank 101 to mix with the extraction material, so that the extraction medium is repeatedly filled into the extraction inner tank 101 and mixed with the extraction material. The mixing effect of the extraction materials and the extraction medium is improved, thereby effectively improving the mixing effect of the extraction materials and the extraction medium and the extraction effect of the material components. When the extraction medium needs to be replaced, the movable plug 106 still moves upward, and at this time, the output pipeline 107 connected to the middle of the extraction inner tank 101 is opened, and the input pipeline 108 at the top of the extraction inner tank 101 is also opened. In the process of the extraction medium being squeezed out, part of the extraction medium is discharged from the output pipeline 107, and another part of the new extraction medium is sent in from the input pipeline 108 to make up for it, so as to meet the pressure balance of the extraction medium. When the movable plug 106 is subsequently lowered again, the output pipeline 107 and the input pipeline 108 are both closed, and the extraction medium is repeatedly sucked back into the extraction inner tank 101.

[0035] Figures 2 to 6 As shown, a heating module 2 is fixedly connected to the inside of the extraction outer tank 1, and the heating module 2 is composed of an electric heating column unit 2 fixed to the top of the movable plug 106. A cooling module 3 is fixedly connected to the outside of the extraction outer tank 1, and the cooling module 3 is composed of a refrigeration unit 301 fixed to the outer frame of the extraction outer tank 1 and a cooling pipeline 302 connected to the refrigeration unit 301. A cooling subdivision pipe 303 is fixedly connected to the inner wall of the top of the extraction inner tank 101, and the cooling pipeline 302 is fixedly passed through the combined cover 104 and communicated with the cooling subdivision pipe 303.

[0036] When the temperature of the internal environment of the extraction equipment is controlled, the specific extraction material is at the edge value of its own active temperature range, and the temperature of the extraction material needs to be restored to the middle value. The main control object is the extraction material. The movable plug 106 still moves upward to squeeze the extraction medium in the extraction inner tank 101 outward to reduce the proportion of the extraction material in the extraction inner tank 101. Then, the heating module and the cooling module are used to heat up and cool the extraction material and the remaining extraction medium in the extraction inner tank 101. That is, the electric heating column unit 2 electrically heats the inside of the extraction inner tank 101, and the cooling pipeline 302 cooperates with the cooling subdivision tube 303 to perform heat transfer cooling on the inside of the extraction inner tank 101, so that the extraction material is restored to a temperature that meets the activity of the extraction substance. At this time, the extraction The material occupies a larger proportion in the extraction inner tank 101, so the extraction material can be heated and cooled more directly, and due to the reduction in the proportion of the extraction medium, the influence of the extraction medium on the temperature regulation of the extraction material is also reduced, which effectively improves the temperature control efficiency of the supercritical extraction equipment, enables the extraction material to quickly recover to the most suitable temperature for its own activity, and better protects the activity of the extraction material itself. Subsequently, the movable plug 106 is slowly lowered and restored, allowing the previously squeezed extraction medium to slowly return to the inside of the extraction inner tank 101, and the temperature of the extraction medium is gradually and steadily regulated. For the subsequent extraction medium to be input, the existing medium temperature control method is used to pre-heat and cool it, thereby reducing the impact of the newly input extraction medium on the rapid temperature control of the extraction material.

[0037] The second implementation method:

[0038] Compared with the first embodiment, the main new addition is a material hanging basket 402, and the specific new structure is as follows: the regional structure is consistent with the first embodiment.

[0039] Figures 3 to 5 and Figures 7 and 8As shown, an inner tank port 4 connected to the interior of the extraction inner tank 101 is opened in the middle of the combined cover 104, and a tank plug 401 is inserted into the inner tank port 4, and the extraction material in the extraction inner tank 101 is directly put in and taken out through the inner tank port 4, which effectively improves the replacement efficiency of the extraction material. A material hanging basket 402 is placed inside the extraction inner tank 101, and a sling 403 is fixedly connected between the bag mouth of the material hanging basket 402 and the bottom of the tank plug 401. The sling 403 is spirally arranged and made of spring steel wire. The extraction material is stuffed into the material hanging basket 402 and directly put into the extraction inner tank 101, thereby effectively improving the replacement efficiency of the extraction material. The bottom of the material hanging basket 402 is fixedly connected A connecting sleeve 404 is connected, and the connecting sleeve 404 is sleeved with the electric heating column unit 2. The connecting sleeve 404 is made of stainless steel wire material. By sleeve-fitting the connecting sleeve 404 with the electric heating column unit 2, the material hanging basket 402 containing the extraction material is accurately combined with the electric heating column unit 2, thereby effectively improving the electric heating column unit 2 for extracting the material. A supporting vertical rod 405 is fixedly connected to the middle of the top of the connecting sleeve 404. The top of the supporting vertical rod 405 is sleeved and corresponds to the top bag opening of the material hanging basket 402. The supporting vertical rod 405 is used to provide support for the upper half of the material hanging basket 402, which effectively improves the stability of the material hanging basket 402 when it rises, and at the same time effectively improves the connection effect between the sling 403 and the material hanging basket 402;

[0040] When the extraction material is stored in the extraction inner tank 101, the extraction material is placed in the material basket 402, and the material basket 402 containing the extraction material is directly placed into the extraction inner tank 101 from the inner tank mouth 4, and then the inner tank mouth 4 is sealed with the tank plug 401. During the process of placing the material basket 402 into the extraction inner tank 101, the connecting sleeve 404 at the bottom of the material basket 402 is connected with the electric heating column unit 2, so that the material basket 402 is accurately placed in the middle of the movable plug 106, and when the extraction material is heated, the electric heating column unit 2 effectively improves the uniform heating effect of the extraction material in the material basket 402, and when the material basket 402 rises with the movable plug 106, the material basket 402 can be located at the center of the cooling subdivision tube 303, thereby effectively improving the uniform cooling effect of the cooling subdivision tube 303 on the extraction material.

[0041] The third implementation method:

[0042] Compared with the first embodiment, a separation ring 5 is mainly added. The specific newly added structure is as follows, and the remaining structures are consistent with the first embodiment.

[0043] Figure 3 and Fig. 9As shown, the middle and bottom inner walls of the extraction outer tank 1 are fixedly connected with a spacer ring 5, and two groups of spacer rings 5 ​​are respectively sealed and sleeved with the middle and bottom of the extraction inner tank 101, and a connecting pipe 501 is fixedly connected between the two groups of spacer rings 5. The middle area of ​​the extraction outer tank 1 is isolated by the two groups of spacer rings 5, and the top and bottom of the extraction outer tank 1 are directly connected through the connecting pipe 501, thereby effectively reducing the total amount of extraction medium outside the extraction inner tank 101 and effectively reducing the amount of extraction medium used;

[0044] When the extraction outer tank 1 and the extraction inner tank 101 are sleeved and assembled, the middle and bottom of the extraction inner tank 101 are sealed with two sets of separation rings 5 ​​respectively, so that the middle area of ​​the extraction outer tank 1 is isolated, and the top and bottom of the extraction outer tank 1 are directly connected through the connecting pipe 501, that is, the middle area of ​​the extraction inner tank 101 does not need to be filled with extraction medium, thereby effectively reducing the total filling amount of the extraction medium, that is, the amount of extraction medium used.

[0045] Figure 3 and Fig. 9 As shown, the connecting tube 501 is distributed in an annular manner with respect to the separation ring 5, and the connecting tube 501 is movably connected with a separation plug 502 inside. The top and bottom ends of the connecting tube 501 are fixedly connected with a limiting ring 503. The inner diameter of the limiting ring 503 is smaller than the outer diameter of the separation plug 502. The separation plug 502 is movable in the connecting tube 501 to separate the top space and the bottom space of the extraction outer tank 1, so that the bottom of the extraction outer tank 1 can be filled with other medium liquids that are easier to seal, further reducing the amount of extraction medium, while effectively reducing the difficulty of sealing the bottom of the extraction outer tank 1, thereby effectively improving the sealing effect of the bottom of the extraction outer tank 1. The top and bottom of one end of the extraction outer tank 1 are respectively fixedly connected with a liquid inlet pipe 504 and a liquid discharge pipe 505. The inner end of the liquid inlet pipe 504 passes through the separation ring 5 and extends to the bottom of the extraction outer tank 1. The filling liquid at the bottom of the extraction outer tank 1 is injected and discharged through the liquid inlet pipe 504 and the liquid discharge pipe 505, effectively improving the control of the filling solution at the bottom of the extraction outer tank 1.

[0046] By moving the partition plug 502 in the connecting tube 501, the top space and the bottom space of the extraction outer tank 1 are separated. The bottom space of the extraction outer tank 1 no longer needs to be filled with the extraction medium, and a medium solution that is easier to seal can be selected. The most common filling liquid is water. The bottom space of the extraction outer tank 1 is filled with water, thereby effectively reducing the use of the extraction medium.

[0047] Figure 1 and Fig. 9As shown, a volume cylinder 506 is fixedly connected to the bottom of the other end of the extraction outer tank 1, and a volume plug 507 is movably connected inside the volume cylinder 506. By adjusting the position of the volume plug 507 in the volume cylinder 506, the purpose of adjusting the volume of the bottom of the extraction outer tank 1 is achieved, thereby effectively increasing the range of the volume change of the top of the extraction outer tank 1, and effectively increasing the ratio adjustment of the extraction medium in the top of the extraction outer tank 1 and the inside of the extraction inner tank 101;

[0048] When adjusting the amount of extraction medium used, that is, when the top of the extraction outer tank 1 requires more extraction medium and the bottom of the extraction outer tank 1 requires less extraction medium, the capacity plug 507 is synchronously controlled to make corresponding position adjustments in the capacity cylinder 506, so as to achieve the effect of indirectly giving up and occupying the space at the top of the extraction outer tank 1 by adjusting the volume at the bottom of the extraction outer tank 1.

[0049] In view of current practical needs, the above-mentioned implementation mode adopted in this application is not limited to the scope of protection. Various changes made within the knowledge scope of technical personnel in this field without departing from the concept of this application still fall within the scope of protection of the present invention.

Claims

1. A supercritical device with a temperature control system, characterized in that: The invention comprises an extraction outer tank (1), wherein an extraction inner tank (101) is sleeved inside the extraction outer tank (1), an upper opening (102) and a lower opening (103) are respectively provided at the top and the bottom of the extraction inner tank (101), wherein the upper opening (102) and the lower opening (103) are both communicated with the interior of the extraction outer tank (1), a combined sealing cover (104) is fixedly connected to the top of the extraction inner tank (101), and the combined sealing cover (104) is plugged into the top of the extraction outer tank (1), and a telescopic unit (105) is fixedly connected to the bottom of the extraction outer tank (1), wherein the output end of the telescopic unit (105) extends from the lower opening (103) into the interior of the extraction inner tank (101), and a movable plug (106) is fixedly connected to the output end of the telescopic unit (105); A heating module is fixedly connected to the interior of the extraction outer tank (1), and the heating module is composed of an electric heating column unit (201) fixed to the top of the movable plug (106); The outside of the extraction outer tank (1) is fixedly connected to a cooling module, and the cooling module is composed of a refrigeration unit (301) fixed to the outer frame of the extraction outer tank (1) and a cooling pipeline (302) connected to the refrigeration unit (301). The top inner wall of the extraction inner tank (101) is fixedly connected to a cooling subdivision pipe (303), and the cooling pipeline (302) is fixedly passed through the combined cover (104) and is connected to the cooling subdivision pipe (303).

2. The supercritical equipment with a temperature control system according to claim 1, characterized in that: An output pipeline (107) and an input pipeline (108) are fixedly connected to the top of the combined cover (104); the output pipeline (107) is fixedly connected to the middle of the extraction inner tank (101); and the input pipeline (108) is connected to the upper half of the upper opening (102).

3. The supercritical equipment with a temperature control system according to claim 1, characterized in that: An inner tank opening (4) communicating with the interior of the extraction inner tank (101) is provided in the middle of the combined sealing cover (104), and a tank plug (401) is inserted into the interior of the inner tank opening (4).

4. The supercritical equipment with a temperature control system according to claim 3, characterized in that: A material hanging basket (402) is placed inside the extraction inner tank (101), and a sling (403) is fixedly connected between the bag mouth of the material hanging basket (402) and the bottom of the tank plug (401). The sling (403) is arranged in a spiral shape and is made of spring steel wire.

5. The supercritical equipment with a temperature control system according to claim 4, characterized in that: The bottom of the material hanging basket (402) is fixedly connected with a connecting sleeve (404), the connecting sleeve (404) is sleeved with the electric heating column unit (2), and the connecting sleeve (404) is made of stainless steel wire material.

6. The supercritical equipment with a temperature control system according to claim 5, characterized in that: A supporting rod (405) is fixedly connected to the middle of the top end of the connecting sleeve (404), and the top end of the supporting rod (405) is sleeved and corresponds to the top bag opening of the material hanging basket (402).

7. The supercritical equipment with a temperature control system according to claim 1, characterized in that: The middle and bottom inner walls of the extraction outer tank (1) are fixedly connected with a separation ring (5), two groups of the separation rings (5) are respectively sealed and sleeved with the middle and bottom of the extraction inner tank (101), and a connecting pipe (501) is fixedly connected between the two groups of separation rings (5).

8. The supercritical equipment with a temperature control system according to claim 7, characterized in that: The connecting tube (501) is distributed in an annular shape with respect to the separation ring (5), and a separation plug (502) is movably connected inside the connecting tube (501), and the top and bottom ends of the connecting tube (501) are fixedly connected to a limiting ring (503), and the inner ring diameter of the limiting ring (503) is smaller than the outer ring diameter of the separation plug (502).

9. The supercritical equipment with a temperature control system according to claim 1, characterized in that: A liquid inlet pipe (504) and a liquid outlet pipe (505) are respectively fixedly connected to the top and bottom of one end of the extraction outer tank (1); the inner end of the liquid inlet pipe (504) passes through the separation ring (5) and extends to the bottom of the extraction outer tank (1).

10. The supercritical equipment with a temperature control system according to claim 1, characterized in that: The bottom of the other end of the extraction outer tank (1) is fixedly connected to a capacity cylinder (506), and the interior of the capacity cylinder (506) is movably connected to a capacity plug (507).

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