Recyclable environment-friendly cleaning agent and preparation method thereof

By using specific combinations of surfactants and other ingredients in the cleaning agent, combined with specific stirring conditions and power circuit design, the problem of insufficient efficiency in the existing cleaning agent preparation process is solved, and the efficient preparation and recycling of environmentally friendly cleaning agents is achieved, which improves the washing performance and environmental protection effect.

CN119709332APending Publication Date: 2025-03-28SHENZHEN JIEWANG FINE CHEM TECH
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Patent Information

Application Number
CN202411926233.4
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-25
Publication Date
2025-03-28

AI Technical Summary

Technical Problem

The existing cleaning agent preparation process has not been considered from the perspective of production efficiency, resulting in insufficient recycling of environmentally friendly cleaning agents.

Method used

The combination of anionic surfactant, cationic surfactant, nonionic surfactant, sodium decahydrate, fatty alcohol polyoxyethylene ether, sodium dodecyl sulfonate, sodium percarbonate, sodium perborate and water composite is used to achieve efficient preparation and recycling of cleaning agents through specific stirring conditions and power circuit design.

Benefits of technology

It improves the washing performance and water solubility of the cleaning agent, meets the recycling needs of the cleaning agent, achieves the goal of energy saving and environmental protection, and enhances the emulsification, foaming, dispersion and other properties of the cleaning agent.

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Abstract

The invention discloses a recyclable environment-friendly cleaning agent which comprises the following components: an anionic surfactant, a cationic surfactant, a nonionic surfactant, sodium sulfate decahydrate and fatty alcohol-polyoxyethylene ether, and a preparation method of the cleaning agent comprises the following steps: S1, raw material distribution, S2, raw material conveying and S3, raw material stirring. The sodium sulfate decahydrate, the fatty alcohol-polyoxyethylene ether and the sodium dodecyl sulfate are adopted, so that the cleaning agent has the characteristic of good washing performance, is general in water solubility, meets the characteristic of cyclic utilization of the cleaning agent, and has the effects of energy conservation and environmental protection; meanwhile, due to the anionic surfactant, the cationic surfactant and the nonionic surfactant, the cleaning agent has good emulsifying, foaming, dispersing, permeating, degreasing, solubilizing, sterilizing, antistatic and dispersing properties; in the raw material conveying step, when one raw material conveying pipe breaks down, the other raw material box conveys raw materials to the two reaction kettles at the same time.
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Description

Technical Field

[0001] The invention relates to the technical field of cleaning agents, and in particular to a recyclable environmentally friendly cleaning agent and a preparation method thereof. Background Art

[0002] With the continuous improvement of modern science and technology, various cleaning agents continue to emerge. However, in order to meet the market's requirements for environmental protection, some cleaning agents are striving to be recyclable.

[0003] In the current preparation process of cleaning agents, such as patent number: CN116286216A, patent name, composition for preparing environmentally friendly cleaning agents, environmentally friendly cleaning agents and preparation methods and applications thereof, it is recorded that "the components in any one of the compositions are mixed" and "under stirring conditions, and the stirring speed is 500-800rpm, the time is 100-120min, and the temperature is 50-80°C". Those skilled in the art can know that it only records how to produce, and does not take into account the production efficiency.

[0004] In summary, a recyclable and environmentally friendly cleaning agent and a preparation method thereof are designed. Summary of the invention

[0005] In order to overcome the above-mentioned shortcomings, the present invention provides a recyclable environmentally friendly cleaning agent and a preparation method thereof.

[0006] The present invention achieves the above-mentioned purpose through the following technical solutions:

[0007] A recyclable environmentally friendly cleaning agent comprises the following components: an anionic surfactant, a cationic surfactant, a nonionic surfactant, sodium sulfate decahydrate, fatty alcohol polyoxyethylene ether, sodium dodecyl sulfonate, sodium percarbonate, sodium perborate and a water complex;

[0008] The detergent comprises 0.05-1% anionic surfactant, 0.05-1% cationic surfactant, 0.05-1% nonionic surfactant, 15% or 20-30% sodium sulfate decahydrate, 0.5-4.5% fatty alcohol polyoxyethylene ether, 0.05-1% sodium dodecyl sulfonate, 0.05-1% sodium percarbonate, 0.05-1% sodium perborate and a water complex.

[0009] Preferably, the water complex comprises propionic acid, propionic acid ester, a co-solvent and water.

[0010] Preferably, the anionic surfactant includes sodium alkylbenzene sulfonate, alkyl sulfonate and alkyl sulfate, the cationic surfactant includes cationic polyacrylamide and alkyl quaternary ammonium salt, and the nonionic surfactant includes alkylphenol polyoxyethylene ether, polyoxyethylene ether, sorbitan ester and sucrose ester. Anionic surfactants, cationic surfactants and nonionic surfactants are used as surfactants so that the obtained cleaning agent has good emulsification, foaming, dispersion, penetration, degreasing, solubilization, sterilization, antistatic and dispersion properties.

[0011] A recyclable environmentally friendly cleaning agent and a preparation method of the cleaning agent are also disclosed, the preparation method comprising the following steps:

[0012] S1. Allocate raw materials, and allocate different raw materials to corresponding raw material boxes;

[0013] S2, conveying raw materials, conveying the raw materials in the raw material box to the mixing box according to the corresponding quantity or proportion;

[0014] S3, stirring the raw materials, stirring the raw materials poured into the reaction kettle, and reacting.

[0015] Preferably, in step S3, there are two reactors, each reactor is equipped with a set of raw material conveying structure, and the same raw material conveying pipes in the two raw material conveying structures are interconnected; when one of the raw material conveying pipes fails, the other raw material box will provide raw materials to the two reactors at the same time.

[0016] Preferably, in the step S3, the reactors are equipped with a power module, the power module includes a power circuit, the power circuit includes a first integrated circuit, a second integrated circuit, a third integrated circuit, a first capacitor, a second capacitor, a third capacitor, a fourth capacitor, a fifth capacitor, a sixth capacitor, a first transistor, a second transistor, a first switch, a second switch, a first diode, a second diode and a third diode, the model of the first integrated circuit is ICL7660, the model of the second integrated circuit and the third integrated circuit are both ICL7664, the eighth end of the first integrated circuit is electrically connected to the seventh end of the first integrated circuit through the first capacitor, the first end of the first integrated circuit is electrically connected to the anode of the first diode, the cathode of the first diode is electrically connected to the input end of the second integrated circuit, the third end of the first integrated circuit is grounded, the second end of the first integrated circuit is electrically connected to the fourth end of the first integrated circuit through the second capacitor, the input end of the second integrated circuit is electrically connected to the base of the first transistor, the input end of the second integrated circuit is electrically connected to the eighth end of the first integrated circuit, the base of the first transistor is electrically connected to the collector of the first transistor through the first switch, and the first transistor The emitter of the transistor is electrically connected to the anode of the second diode, the cathode of the second diode is grounded through the second resistor and the third resistor, the grounding terminal of the second integrated circuit is grounded, the input terminal of the second integrated circuit is grounded through the third capacitor, the feedback terminal of the second integrated circuit is electrically connected to the second resistor and the third resistor respectively, the output terminal of the second integrated circuit is grounded through the first resistor and the fourth capacitor, the output terminal of the second integrated circuit is electrically connected to the cathode of the second diode through the first resistor, the grounding terminal of the third integrated circuit is grounded, the input terminal of the third integrated circuit is grounded through the fifth capacitor, the input terminal of the third integrated circuit is electrically connected to the base of the second transistor, the base of the second transistor is electrically connected to the collector of the second transistor through the second switch, the emitter of the second transistor is electrically connected to the anode of the third diode, the cathode of the third diode is electrically connected to the output terminal of the third integrated circuit through the fourth resistor, the cathode of the third diode is grounded through the fifth resistor and the sixth resistor, the feedback terminal of the third integrated circuit is electrically connected to the fifth resistor and the sixth resistor respectively, the sixth capacitor is connected in parallel with the fifth resistor and the sixth resistor, and the output terminal of the third integrated circuit is electrically connected to the cathode of the third diode through the fourth resistor.

[0017] In the power supply circuit, the first integrated circuit controls the on and off of the second integrated circuit and the third integrated circuit. The second integrated circuit and the third integrated circuit respectively form two voltage output circuits. The feedback end of the second integrated circuit collects the voltage division value of the second resistor and the third resistor. Similarly, the third integrated circuit also samples and feedbacks.

[0018] Preferably, in the preparation method, during the process of step S3, step S2 is carried out synchronously. When step S3 is running, the stirring motor in the reactor works, and step S2 is synchronously executed at this time to start preparing raw materials in the reactor in advance.

[0019] Preferably, in the step S3, the reaction kettle is operated under stirring conditions, the stirring speed of the motor in the reaction kettle is 500-800 rpm, the stirring time is 60-120 min, and the temperature is 55-80°C.

[0020] The beneficial effects of the present invention are as follows: the recyclable environmentally friendly cleaning agent and the preparation method thereof:

[0021] 1. It uses sodium sulfate decahydrate, fatty alcohol polyoxyethylene ether, and sodium dodecyl sulfonate, which have good washing performance and general water solubility, meet the characteristics of detergent recycling, and play a role in energy saving and environmental protection. At the same time, anionic surfactants, cationic surfactants, and nonionic surfactants make the detergent have good emulsification, foaming, dispersion, penetration, degreasing, solubilization, sterilization, antistatic and dispersion properties;

[0022] 2. In the raw material delivery step, when one of the raw material delivery pipes fails, the other raw material box delivers raw materials to the two reactors at the same time, and the raw material delivery power of the raw material box is increased to ensure that the two reactors always maintain efficient operation;

[0023] 3. In the power supply circuit, the first integrated circuit controls two voltage outputs to meet the stirring of two reactors or the transportation of two raw material boxes. When one raw material box is needed to provide raw materials to two reactors at the same time, the power supply circuit increases the output power of the power supply circuit through the first switch or the second switch. BRIEF DESCRIPTION OF THE DRAWINGS

[0024] The present invention will now be described by way of example with reference to the accompanying drawings, in which:

[0025] Figure 1 It is a system step diagram of the present invention;

[0026] Figure 2 It is a circuit principle diagram of the power supply circuit of the present invention. DETAILED DESCRIPTION

[0027] The present invention will now be described in further detail with reference to the accompanying drawings. These drawings are simplified schematic diagrams, which only illustrate the basic structure of the present invention in a schematic manner, and therefore only show the components related to the present invention.

[0028] like Figure 1 and Figure 2 As shown, a recyclable environmentally friendly cleaning agent includes the following components: an anionic surfactant, a cationic surfactant, a nonionic surfactant, sodium sulfate decahydrate, fatty alcohol polyoxyethylene ether, sodium dodecyl sulfonate, sodium percarbonate, sodium perborate and a water complex;

[0029] The detergent comprises 0.05-1% anionic surfactant, 0.05-1% cationic surfactant, 0.05-1% nonionic surfactant, 15% or 20-30% sodium sulfate decahydrate, 0.5-4.5% fatty alcohol polyoxyethylene ether, 0.05-1% sodium dodecyl sulfonate, 0.05-1% sodium percarbonate, 0.05-1% sodium perborate and a water complex.

[0030] Specifically, the water complex comprises propionic acid, propionic ester, cosolvent and water, and the proportion of the water complex is 50-60%.

[0031] Specifically, the anionic surfactant includes sodium alkylbenzene sulfonate, alkyl sulfonate and alkyl sulfate, the cationic surfactant includes cationic polyacrylamide and alkyl quaternary ammonium salt, and the nonionic surfactant includes alkylphenol polyoxyethylene ether, polyoxyethylene ether, sorbitan ester and sucrose ester. Anionic surfactants, cationic surfactants and nonionic surfactants are used as surfactants so that the obtained cleaning agent has good emulsification, foaming, dispersion, penetration, degreasing, solubilization, sterilization, antistatic and dispersion properties.

[0032] A recyclable environmentally friendly cleaning agent and a preparation method of the cleaning agent are also disclosed, the preparation method comprising the following steps:

[0033] S1. Allocate raw materials, and allocate different raw materials to corresponding raw material boxes;

[0034] S2, conveying raw materials, conveying the raw materials in the raw material box to the mixing box according to the corresponding quantity or proportion;

[0035] S3, stirring the raw materials, stirring the raw materials poured into the reaction kettle, and reacting.

[0036] Specifically, in the step S3, there are two reactors, each reactor is equipped with a set of raw material delivery structure, and the same raw material delivery pipes in the two raw material delivery structures are connected to each other. A connecting pipe is provided between the two raw material delivery pipes, and a three-way valve is provided between the connecting pipe and the raw material delivery pipe. When one of the raw material delivery pipes fails, the three-way valve between the raw material delivery pipe and the reactor will be closed, and the three-way valve of the other raw material delivery pipe will be opened, then the other raw material box will provide raw materials to the two reactors at the same time, and the raw material box increases the output power to meet the two reactors to always operate efficiently.

[0037] Specifically, in the step S3, the reactors are all equipped with a power module, the power module includes a power circuit, the power circuit includes a first integrated circuit, a second integrated circuit, a third integrated circuit, a first capacitor, a second capacitor, a third capacitor, a fourth capacitor, a fifth capacitor, a sixth capacitor, a first transistor, a second transistor, a first switch, a second switch, a first diode, a second diode and a third diode, the model of the first integrated circuit is ICL7660, the model of the second integrated circuit and the third integrated circuit are both ICL7664, the eighth end of the first integrated circuit is electrically connected to the seventh end of the first integrated circuit through the first capacitor, the first end of the first integrated circuit is electrically connected to the anode of the first diode, the cathode of the first diode is electrically connected to the input end of the second integrated circuit, the third end of the first integrated circuit is grounded, the second end of the first integrated circuit is electrically connected to the fourth end of the first integrated circuit through the second capacitor, the input end of the second integrated circuit is electrically connected to the base of the first transistor, the input end of the second integrated circuit is electrically connected to the eighth end of the first integrated circuit, the base of the first transistor is electrically connected to the collector of the first transistor through the first switch, and the first transistor The emitter of the transistor is electrically connected to the anode of the second diode, the cathode of the second diode is grounded through the second resistor and the third resistor, the grounding terminal of the second integrated circuit is grounded, the input terminal of the second integrated circuit is grounded through the third capacitor, the feedback terminal of the second integrated circuit is electrically connected to the second resistor and the third resistor respectively, the output terminal of the second integrated circuit is grounded through the first resistor and the fourth capacitor, the output terminal of the second integrated circuit is electrically connected to the cathode of the second diode through the first resistor, the grounding terminal of the third integrated circuit is grounded, the input terminal of the third integrated circuit is grounded through the fifth capacitor, the input terminal of the third integrated circuit is electrically connected to the base of the second triode, the base of the second triode is electrically connected to the collector of the second triode through the second switch, the emitter of the second triode is electrically connected to the anode of the third diode, the cathode of the third diode is electrically connected to the output terminal of the third integrated circuit through the fourth resistor, the cathode of the third diode is grounded through the fifth resistor and the sixth resistor, the feedback terminal of the third integrated circuit is electrically connected to the fifth resistor and the sixth resistor respectively, the sixth capacitor is connected in parallel with the fifth resistor and the sixth resistor, and the output terminal of the third integrated circuit is electrically connected to the cathode of the third diode through the fourth resistor.

[0038] In the power supply circuit, the first integrated circuit controls the on and off of the second integrated circuit and the third integrated circuit. The second integrated circuit as the main component and the third integrated circuit as the main component respectively form two voltage output circuits. The feedback end of the second integrated circuit collects the voltage division value of the second resistor and the third resistor. Similarly, the third integrated circuit also samples and feedbacks. The first switch and the second switch control the on and off of the corresponding first transistor and the second transistor to increase the output power of the second integrated circuit or the third integrated circuit.

[0039] Specifically, in the preparation method, during the process of step S3, step S2 will be carried out synchronously. When step S3 is running, the stirring motor in the reactor works, and step S2 is synchronously executed at this time to start preparing raw materials in the reactor in advance.

[0040] Specifically, in the step S3, the reaction kettle is operated under stirring conditions, the stirring speed of the motor in the reaction kettle is 500-800 rpm, the stirring time is 60-120 min, and the temperature is 55-80°C.

[0041] The above is based on the present invention as an inspiration. Through the above description, relevant staff can make various changes and modifications without departing from the technical idea of ​​this invention. The technical scope of this invention is not limited to the content in the specification, and its technical scope must be determined according to the scope of the claims.

Claims

1. A recyclable environmentally friendly cleaning agent, characterized in that: The invention comprises the following components: anionic surfactant, cationic surfactant, nonionic surfactant, sodium sulfate decahydrate, fatty alcohol polyoxyethylene ether, sodium dodecyl sulfonate, sodium percarbonate, sodium perborate and water complex; The detergent comprises 0.05-1% anionic surfactant, 0.05-1% cationic surfactant, 0.05-1% nonionic surfactant, 15% or 20-30% sodium sulfate decahydrate, 0.5-4.5% fatty alcohol polyoxyethylene ether, 0.05-1% sodium dodecyl sulfonate, 0.05-1% sodium percarbonate, 0.05-1% sodium perborate and a water complex.

2. The recyclable environmentally friendly cleaning agent according to claim 1, characterized in that: The water complex comprises propionic acid, propionic acid ester, a co-solvent and water.

3. The recyclable environmentally friendly cleaning agent according to claim 1, characterized in that: The anionic surfactants include sodium alkylbenzene sulfonate, alkyl sulfonate and alkyl sulfate, the cationic surfactants include cationic polyacrylamide and alkyl quaternary ammonium salts, and the nonionic surfactants include alkylphenol polyoxyethylene ether, polyoxyethylene ether, sorbitan ester and sucrose ester.

4. According to the recyclable environmentally friendly cleaning agent of claim, a preparation method of the cleaning agent is also disclosed, characterized in that: The preparation method comprises the following steps: S1. Allocate raw materials, and allocate different raw materials to corresponding raw material boxes; S2, conveying raw materials, conveying the raw materials in the raw material box to the mixing box according to the corresponding quantity or proportion; S3, stirring the raw materials, stirring the raw materials poured into the reaction kettle, and reacting.

5. The method for preparing a recyclable environmentally friendly cleaning agent according to claim 4, characterized in that: In the step S3, there are two reactors, each reactor is equipped with a set of raw material conveying structure, and the same raw material conveying pipes in the two raw material conveying structures are interconnected; when one of the raw material conveying pipes fails, the other raw material box will provide raw materials to the two reactors at the same time.

6. The method for preparing a recyclable environmentally friendly cleaning agent according to claim 1, characterized in that: In the step S3, the reactors are all equipped with a power module, the power module includes a power circuit, the power circuit includes a first integrated circuit, a second integrated circuit, a third integrated circuit, a first capacitor, a second capacitor, a third capacitor, a fourth capacitor, a fifth capacitor, a sixth capacitor, a first transistor, a second transistor, a first switch, a second switch, a first diode, a second diode and a third diode, the model of the first integrated circuit is ICL7660, the model of the second integrated circuit and the third integrated circuit are both ICL7664, the eighth end of the first integrated circuit is electrically connected to the seventh end of the first integrated circuit through the first capacitor, the first end of the first integrated circuit is electrically connected to the anode of the first diode, the cathode of the first diode is electrically connected to the input end of the second integrated circuit, the third end of the first integrated circuit is grounded, the second end of the first integrated circuit is electrically connected to the fourth end of the first integrated circuit through the second capacitor, the input end of the second integrated circuit is electrically connected to the base of the first transistor, the input end of the second integrated circuit is electrically connected to the eighth end of the first integrated circuit, the base of the first transistor is electrically connected to the collector of the first transistor through the first switch, and the cathode of the first diode is electrically connected to the input end of the second integrated circuit. The emitter is electrically connected to the anode of the second diode, the cathode of the second diode is grounded through the second resistor and the third resistor, the grounding terminal of the second integrated circuit is grounded, the input terminal of the second integrated circuit is grounded through the third capacitor, the feedback terminal of the second integrated circuit is electrically connected to the second resistor and the third resistor respectively, the output terminal of the second integrated circuit is grounded through the first resistor and the fourth capacitor, the output terminal of the second integrated circuit is electrically connected to the cathode of the second diode through the first resistor, the grounding terminal of the third integrated circuit is grounded, the input terminal of the third integrated circuit is grounded through the fifth capacitor, the input terminal of the third integrated circuit is electrically connected to the base of the second triode, the base of the second triode is electrically connected to the collector of the second triode through the second switch, the emitter of the second triode is electrically connected to the anode of the third diode, the cathode of the third diode is electrically connected to the output terminal of the third integrated circuit through the fourth resistor, the cathode of the third diode is grounded through the fifth resistor and the sixth resistor, the feedback terminal of the third integrated circuit is electrically connected to the fifth resistor and the sixth resistor respectively, the sixth capacitor is connected in parallel with the fifth resistor and the sixth resistor, and the output terminal of the third integrated circuit is electrically connected to the cathode of the third diode through the fourth resistor.

7. The recyclable environmentally friendly cleaning agent and preparation method thereof according to claim 1, characterized in that: In the preparation method, during the process of step S3, step S2 is carried out simultaneously.

8. The recyclable environmentally friendly cleaning agent and preparation method thereof according to claim 1, characterized in that: In the step S3, the reaction kettle is operated under stirring conditions, the stirring speed of the motor in the reaction kettle is 500-800 rpm, the stirring time is 60-120 min, and the temperature is 55-80°C.

Citation Information

Patent Citations

  • Composition for preparing environment-friendly cleaning agent, environment-friendly cleaning agent as well as preparation method and application of environment-friendly cleaning agent

    CN116286216A