Smearing type mask and preparation method thereof

Abstract

The invention discloses a smearing type mask and a preparation method of the smearing type mask, and belongs to the technical field of cosmetics. The mask is prepared from the following components in percentage by weight: 0.1 to 1 percent of mesenchymal stem cell exosome, 1 to 5 percent of hydrolyzed sodium hyaluronate, 0.1 to 2 percent of glabridin, 0.5 to 2 percent of tocopherol, 0.5 to 2 percent of resveratrol, 0.1 to 1 percent of curcumin, 0.1 to 1 percent of luteolin, 0.5 to 3 percent of arbutin, 0.5 to 2 percent of idebene, 0.1 to 1 percent of thymol, 1 to 5 percent of herba centellae extract, 1 to 5 percent of propolis and 0.5 to 3 percent of pomegranate peel polyphenol. The components used in the formula are mostly derived from natural plant extracts, the influence on the environment is reduced, meanwhile, the requirements of consumers for green skin care products are met, and the components comprise mesenchymal stem cell exosome, hydrolyzed sodium hyaluronate, glabridin, tocopherol, resveratrol, curcumin and the like, so that the skin care product has the advantages that the skin care effect is good, and the skin care effect is good. The components respectively have multiple skin care effects of resisting aging, preserving moisture, resisting oxidation and the like, and the skin aging problem can be more effectively improved through the combined action of the components.

Description

Technical Field

[0001] The invention relates to the technical field of cosmetics, in particular to a smearable facial mask and a preparation method thereof. Background Art

[0002] Facial masks are used to cover the facial skin to achieve skin care purposes such as cleansing, moisturizing, whitening, and anti-aging. Facial masks usually contain a variety of ingredients that are beneficial to the skin and can be used according to different skin types and needs. Facial masks are classified into: sheet masks, smear masks, peel-off masks, and sleeping masks. Smear masks are a thick paste or mud-like substance that needs to be applied to the cleansed facial skin and washed off or wiped off with a tissue after a certain period of time.

[0003] Many anti-aging smearable facial masks on the market often contain only one or two main active ingredients, such as common tocopherol or hyaluronic acid. Although these ingredients are beneficial to the skin, their scope of action is limited and they can usually only target specific skin aging problems. Free radicals are one of the main factors leading to skin aging. They can damage the DNA of skin cells and cause damage to collagen and elastin. When existing smearable facial masks contain only a single antioxidant ingredient, they cannot effectively resist multiple free radicals, thereby failing to fully protect the skin from oxidative stress. Therefore, a single ingredient may improve the skin in the short term, but due to the lack of synergistic effects of other auxiliary ingredients, the long-term effect may not be ideal and the skin aging condition cannot be continuously improved. To this end, a smearable facial mask and a preparation method thereof are proposed. Summary of the invention

[0004] The present invention aims to solve at least one of the technical problems existing in the prior art, such as limited types of active ingredients and insufficient ability to resist free radical damage. To this end, one object of the present invention is to provide a smearable facial mask and a preparation method thereof.

[0005] To achieve the above object, the present invention provides the following technical solutions:

[0006] A smearable facial mask, comprising the following ingredients by weight percentage: mesenchymal stem cell exosomes: 0.1-1%, hydrolyzed sodium hyaluronate: 1-5%, glabridin: 0.1-2%, tocopherol: 0.5-2%, resveratrol: 0.5-2%, curcumin: 0.1-1%, luteolin: 0.1-1%, arbutin: 0.5-3%, idebenone: 0.5-2%, thymol: 0.1-1%, Centella asiatica extract: 1-5%, beeswax: 0. Gum: 1-5%, pomegranate peel polyphenols: 0.5-3%, ginseng extract: 0.5-3%, rosemary extract: 0.5-3%, calendula extract: 0.5-3%, cucurbita asiatica extract: 0.5-3%, litsea cubeba extract: 0.5-3%, grape seed extract: 0.5-3%, lavender extract: 0.5-3%, spirulina extract: 0.5-3%, angelica extract: 0.5-3%, aloe extract: 1-5%, matrix: balance.

[0007] As a further optimization scheme of the present invention, the matrix components and their weight percentages are: deionized water: 65-75%, glycerol: 5-10%, hydroxyethyl cellulose: 0.5-2%, magnesium aluminum silicate: 2-5%, 1,3-butylene glycol: 2-5%, allantoin: 0.5-1%, carbomer: 0.5-2%, preservatives: 0.1-1%, fragrance: 0.1-1%, disodium EDTA: 0.1-0.5%.

[0008] As a further optimized solution of the present invention, the fragrance is lavender oil and the preservative is phenoxyethanol.

[0009] A method for preparing a smearable facial mask comprises the following steps:

[0010] Step 1, premixing active ingredients: weigh mesenchymal stem cell exosomes, hydrolyzed sodium hyaluronate, glabridin, tocopherol, resveratrol, curcumin, luteolin, arbutin, idebenone, and thymol respectively, put them into a premixing container, stir at a speed of 100-300 rpm, and stir for 5-15 min;

[0011] Step 2, prepare the aqueous phase: in a second container, measure deionized water, add hydroxyethyl cellulose, allantoin, and disodium EDTA, stir until completely dissolved, add magnesium aluminum silicate to the aqueous phase, and continue stirring until evenly dispersed;

[0012] Step 3: Prepare the oil phase: In a third container, measure glycerin, 1,3-butylene glycol, carbomer and lavender oil and stir well;

[0013] Step 4: Slowly add the premixed active ingredients into the water phase, while maintaining a stirring speed of 500-1000 rpm for 10-20 min to ensure that the active ingredients are evenly dispersed, slowly add the oil phase into the water phase, and use a high shear emulsifier for emulsification until a stable emulsified system is formed;

[0014] Step 5, adding plant extracts: add Centella asiatica extract, propolis, pomegranate peel polyphenols, ginseng extract, rosemary extract, calendula extract, cucurbita scoparia extract, litsea cubeba extract, grape seed extract, lavender extract, spirulina extract, angelica extract, and aloe extract to the emulsification system in proportion, and continue stirring to ensure that all plant extracts are evenly distributed;

[0015] Step 6: Add hydroxyethyl cellulose and carbomer to adjust the viscosity of the mask;

[0016] Step 7: Add phenoxyethanol to the mask, stir evenly, and finally sterilize the mask.

[0017] As a further optimization scheme of the present invention, in step 2, the stirring speed is 400-600 rpm, the stirring time is 10-15 min, and magnesium aluminum silicate is added to the aqueous phase with a stirring speed of 600-1000 rpm and a stirring time of 15-20 min.

[0018] As a further optimization scheme of the present invention, in step 4, the specific steps of high shear emulsification treatment are:

[0019] During the initial emulsification, start the high shear emulsifier at a speed of 1000-3000rpm, gradually disperse the oil phase into the water phase, and stir for 5-10 minutes. After the oil phase is initially dispersed, increase the speed of the emulsifier to 5000-10000rpm for high-speed emulsification treatment, and the emulsification time is 10-20 minutes;

[0020] After emulsification is completed, the emulsified system is slowly cooled to room temperature to stabilize the emulsified structure. After cooling, post-treatment is performed at a rotation speed of 100-300 rpm to remove the generated bubbles.

[0021] Compared with the prior art, the present invention has the following beneficial effects:

[0022] The ingredients used in the formula of the present invention are mostly derived from natural plant extracts, which reduces the impact on the environment and also meets the consumer's demand for green skin care products, including mesenchymal stem cell exosomes, hydrolyzed sodium hyaluronate, glabridin, tocopherol, resveratrol, curcumin, etc. These ingredients have multiple skin care effects such as anti-aging, moisturizing, and anti-oxidation, and their combined effects can more effectively improve skin aging problems. And experimental data show that it has significant effects in improving skin elasticity, increasing skin moisture, and reducing fine lines and wrinkles, which is better than existing products on the market, proving that the present invention can provide more effective anti-aging care in practical applications. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] Figure 1 The present invention is a flow chart of the preparation method of the smearable facial mask. DETAILED DESCRIPTION

[0024] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0025] The present invention provides a technical solution:

[0026] Embodiment 1

[0027] A smearable facial mask comprises the following ingredients by weight percentage: mesenchymal stem cell exosomes: 0.1%, hydrolyzed sodium hyaluronate: 1%, glabridin: 0.1%, tocopherol: 0.5%, resveratrol: 0.5%, curcumin: 0.1%, luteolin: 0.1%, arbutin: 0.5%, idebenone: 0.5%, thymol: 0.1%, Centella asiatica extract: 1%, propolis: 1%, pomegranate peel polyphenols: 0.5%, ginseng extract: 0.5%, rosemary extract: 0.5%, calendula extract: 0.5%, cucurbita scoparia extract: 0.5%, litsea cubeba extract: 0.5%, grape seed extract: 0.5%, lavender extract: 0.5%, spirulina extract: 0.5%, angelica extract: 0.5%, aloe extract: 1%, matrix: balance.

[0028] Matrix components and their weight percentages: deionized water: 65%, glycerol: 5%, hydroxyethyl cellulose: 0.5%, magnesium aluminum silicate: 2%, 1,3-butylene glycol: 2%, allantoin: 0.5%, carbomer: 0.5%, preservative: 0.1%, fragrance: 0.1%, disodium EDTA: 0.1%.

[0029] Embodiment 2

[0030] A smearable facial mask, comprising the following ingredients by weight percentage: mesenchymal stem cell exosomes: 0.6%, hydrolyzed sodium hyaluronate: 3%, glabridin: 1.3%, tocopherol: 1.5%, resveratrol: 1%, curcumin: 0.6%, luteolin: 0.6%, arbutin: 1.8%, idebenone: 1.3%, thymol: 0.7%, Centella asiatica extract: 3%, propolis: 3%, pomegranate peel polyphenols: 1.9%, ginseng extract: 1.8%, rosemary extract: 2%, calendula extract: 1.8%, cucurbita serrata extract: 2%, litsea cubeba extract: 1.8%, grape seed extract: 1.8%, lavender extract: 1.7%, spirulina extract: 2%, angelica extract: 1.7%, aloe extract: 3%, matrix: balance.

[0031] Matrix components and their weight percentages: deionized water: 70%, glycerin: 8%, hydroxyethyl cellulose: 1%, magnesium aluminum silicate: 3.5%, 1,3-butylene glycol: 3%, allantoin: 0.8%, carbomer: 1%, preservative: 0.3%, fragrance: 0.3%, disodium EDTA: 0.3%.

[0032] Embodiment 3

[0033] A smearable facial mask, comprising the following ingredients by weight percentage: mesenchymal stem cell exosomes: 1%, hydrolyzed sodium hyaluronate: 5%, glabridin: 2%, tocopherol: 2%, resveratrol: 2%, curcumin: 1%, luteolin: 1%, arbutin: 3%, idebenone: 2%, thymol: 1%, Centella asiatica extract: 5%, propolis: 5%, pomegranate peel polyphenols: 3%, ginseng extract: 3%, rosemary extract: 3%, calendula extract: 3%, cucurbita asiatica extract: 3%, litsea cubeba extract: 3%, grape seed extract: 3%, lavender extract: 3%, spirulina extract: 3%, angelica extract: 3%, aloe extract: 5%, matrix: balance.

[0034] Matrix components and their weight percentages: deionized water: 75%, glycerol: 10%, hydroxyethyl cellulose: 2%, magnesium aluminum silicate: 5%, 1,3-butylene glycol: 5%, allantoin: 1%, carbomer: 2%, preservative: 1%, fragrance: 1%, disodium EDTA: 0.5%.

[0035] The fragrance is lavender oil and the preservative is phenoxyethanol.

[0036] Embodiment 4

[0037] See also Figure 1 , a method for preparing a smearable facial mask, comprising the following steps:

[0038] Step 1, premixing active ingredients: weigh mesenchymal stem cell exosomes, hydrolyzed sodium hyaluronate, glabridin, tocopherol, resveratrol, curcumin, luteolin, arbutin, idebenone, and thymol respectively, put them into a premixing container, stir at a speed of 100-300 rpm, and stir for 5-15 min;

[0039] Specifically, after weighing, all powdered active ingredients are placed in the first premixing container, and low-speed stirring is started at a speed of 100-150 rpm. After stirring for 5 minutes, pause and check the uniformity of the mixture. If any lumps or inadequately mixed powders are observed, continue stirring until the total stirring time reaches 10-15 minutes.

[0040] Step 2, prepare the aqueous phase: in a second container, measure deionized water, add hydroxyethyl cellulose, allantoin, and disodium EDTA, stir until completely dissolved, add magnesium aluminum silicate to the aqueous phase, and continue stirring until evenly dispersed;

[0041] The stirring speed is 400-600 rpm, and the stirring time is 10-15 min. Magnesium aluminum silicate is added to the water phase, and the stirring speed is 600-1000 rpm, and the stirring time is 15-20 min.

[0042] Step 3: Prepare the oil phase: In a third container, measure glycerin, 1,3-butylene glycol, carbomer and lavender oil and stir well;

[0043] Step 4: Slowly add the premixed active ingredients into the water phase, while maintaining a stirring speed of 500-1000 rpm for 10-20 min to ensure that the active ingredients are evenly dispersed, slowly add the oil phase into the water phase, and use a high shear emulsifier for emulsification until a stable emulsified system is formed;

[0044] The specific steps of high shear emulsification treatment are:

[0045] During the initial emulsification, start the high shear emulsifier at a speed of 1000-3000rpm, gradually disperse the oil phase into the water phase, and stir for 5-10 minutes. After the oil phase is initially dispersed, increase the speed of the emulsifier to 5000-10000rpm for high-speed emulsification treatment, and the emulsification time is 10-20 minutes.

[0046] After emulsification is completed, the emulsified system is slowly cooled to room temperature to stabilize the emulsified structure. After cooling, post-treatment is performed at a rotation speed of 100-300 rpm to remove the generated bubbles.

[0047] Step 5, adding plant extracts: add Centella asiatica extract, propolis, pomegranate peel polyphenols, ginseng extract, rosemary extract, calendula extract, cucurbita scoparia extract, litsea cubeba extract, grape seed extract, lavender extract, spirulina extract, angelica extract, and aloe extract to the emulsification system in proportion, and continue stirring to ensure that all plant extracts are evenly distributed;

[0048] Specifically, during the initial stirring, preliminary mixing is first performed at 500-1000 rpm for 10 minutes to allow the plant extract to begin to disperse, and then the stirring speed is adjusted to 2000-4000 rpm for 15-20 minutes.

[0049] Step 6: Add hydroxyethyl cellulose and carbomer to adjust the viscosity of the mask;

[0050] Specifically, add deionized water to a container, start the agitator, maintain medium-speed stirring at 500-1000 rpm, weigh hydroxyethyl cellulose and slowly add it to the stirring deionized water, continue to stir at medium speed for 10-15 minutes until the hydroxyethyl cellulose is completely dissolved, stop stirring, take out a small amount of the mixture, evaluate the viscosity, and when the viscosity is lower than expected, gradually increase the hydroxyethyl cellulose, and when the viscosity is higher than expected, gradually reduce the amount of hydroxyethyl cellulose.

[0051] Based on the results of the initial assessment, HEC was gradually added or removed, with each adjustment requiring re-stirring for 5-10 minutes and the viscosity reassessed.

[0052] After the hydroxyethyl cellulose is completely dissolved and the viscosity is adjusted, weigh the carbomer and slowly add it to the water phase, increase the stirring speed to 2000-4000 rpm, and stir for 5-10 minutes until the carbomer is completely dispersed.

[0053] The viscosity of the mixture was evaluated again and reduced by adding deionized water. After the viscosity adjustment was completed, the mixture was allowed to stand for a period of time to observe whether there was any separation or precipitation.

[0054] Step 7: Add phenoxyethanol to the mask, stir evenly, and finally sterilize the mask.

[0055] Specifically, the mask is moved to a clean work area for operation, and 0.1-1% of phenoxyethanol is weighed out using sterile weighing paper, and the phenoxyethanol is in liquid form and is directly added to the prepared mask matrix.

[0056] Slowly add phenoxyethanol to the mask matrix while stirring at medium speed (500-1000 rpm) and continue stirring for 5-10 minutes. After stirring, take a small amount of the mask matrix for inspection to ensure that there is no visible precipitation or unmixed areas.

[0057] Experimental example:

[0058] Experimental purpose: To verify the effectiveness of the smearable facial mask of the present invention in improving signs of skin aging.

[0059] Experimental materials: anti-aging facial mask (according to the above formula and preparation method), popular anti-aging facial mask on the market (as a control group), skin elasticity tester, skin moisture tester, digital microscope, volunteers (aged between 35-55 years old, with obvious signs of skin aging such as fine lines, wrinkles and skin sagging)

[0060] Experimental steps:

[0061] Volunteer screening: Select 20 eligible volunteers to ensure that they have no history of allergies and have not used any anti-aging products within one month before the experiment.

[0062] Grouping: The volunteers were randomly divided into two groups. The experimental group used a homemade anti-aging mask, and the control group used a popular anti-aging mask on the market.

[0063] Usage instructions: Volunteers in the experimental and control groups were instructed on how to use the mask correctly and were required to use it three times a week for four weeks.

[0064] Data collection: Before the experiment, the initial status of each volunteer's skin elasticity, skin texture, fine lines and wrinkles was recorded. The skin condition of the volunteers was evaluated and the data was recorded every week.

[0065] Evaluation of experimental results: After four weeks, the skin condition of the volunteers was evaluated again using a skin elasticity tester and a skin moisture tester. Changes in fine lines and wrinkles on the volunteers' skin were observed through a digital microscope, and feedback from the volunteers on their experience using the product was collected.

[0066] The experimental results are shown in the following table:

[0067]

[0068]

[0069] Experimental results:

[0070] Skin elasticity: The skin elasticity of the volunteers in the experimental group increased by an average of 25%, while the control group increased by 15%. The results showed that the anti-aging mask was superior to the control group in improving skin elasticity.

[0071] Skin moisture: The skin moisture of the volunteers in the experimental group increased by an average of 30%, and the control group increased by 20%, indicating that the anti-aging mask is also better than the control group in terms of moisturizing effect.

[0072] Fine lines and wrinkles: Observed through digital microscopy, fine lines and wrinkles in the experimental group volunteers were reduced by 40%, while the control group was reduced by 25%. The anti-aging mask showed significant results in reducing the signs of skin aging.

[0073] User feedback: Volunteers in the experimental group generally said that the mask was comfortable to use, fine in texture, easy to absorb, and non-irritating to the skin. Volunteers in the control group also gave positive feedback on popular masks on the market, but thought that the effect was not as good as that of the experimental group.

[0074] Parts not involved in the present invention are the same as the prior art or can be implemented by the prior art. Although the embodiments of the present invention have been shown and described, it is understood by those skilled in the art that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principles and spirit of the present invention, and the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A smearable facial mask, characterized in that: The mask contains the following ingredients by weight percentage: mesenchymal stem cell exosomes: 0.1-1%, hydrolyzed sodium hyaluronate: 1-5%, glabridin: 0.1-2%, tocopherol: 0.5-2%, resveratrol: 0.5-2%, curcumin: 0.1-1%, luteolin: 0.1-1%, arbutin: 0.5-3%, idebenone: 0.5-2%, thymol: 0.1-1%, Centella asiatica extract: 1-5%, propolis: 1- 5%, pomegranate peel polyphenols: 0.5-3%, ginseng extract: 0.5-3%, rosemary extract: 0.5-3%, calendula extract: 0.5-3%, cucurbita asiatica extract: 0.5-3%, litsea cubeba extract: 0.5-3%, grape seed extract: 0.5-3%, lavender extract: 0.5-3%, spirulina extract: 0.5-3%, angelica extract: 0.5-3%, aloe extract: 1-5%, matrix: balance.

2. A smearable facial mask according to claim 1, characterized in that: Matrix components and their weight percentages: deionized water: 65-75%, glycerol: 5-10%, hydroxyethyl cellulose: 0.5-2%, magnesium aluminum silicate: 2-5%, 1,3-butylene glycol: 2-5%, allantoin: 0.5-1%, carbomer: 0.5-2%, preservatives: 0.1-1%, fragrance: 0.1-1%, disodium EDTA: 0.1-0.5%.

3. A smearable facial mask according to claim 2, characterized in that: The fragrance is lavender oil and the preservative is phenoxyethanol.

4. A method for preparing a smearable facial mask, characterized in that: The following steps are involved: Step 1, premixing active ingredients: weigh mesenchymal stem cell exosomes, hydrolyzed sodium hyaluronate, glabridin, tocopherol, resveratrol, curcumin, luteolin, arbutin, idebenone, and thymol respectively, put them into a premixing container, stir at a speed of 100-300 rpm, and stir for 5-15 min; Step 2, prepare the aqueous phase: in a second container, measure deionized water, add hydroxyethyl cellulose, allantoin, and disodium EDTA, stir until completely dissolved, add magnesium aluminum silicate to the aqueous phase, and continue stirring until evenly dispersed; Step 3: Prepare the oil phase: In a third container, measure glycerin, 1,3-butylene glycol, carbomer and lavender oil and stir well; Step 4: Slowly add the premixed active ingredients into the water phase, while maintaining a stirring speed of 500-1000 rpm for 10-20 min, slowly add the oil phase into the water phase, and emulsify using a high shear emulsifier until a stable emulsified system is formed; Step 5, adding plant extracts: add Centella asiatica extract, propolis, pomegranate peel polyphenols, ginseng extract, rosemary extract, calendula extract, cucurbita scoparia extract, litsea cubeba extract, grape seed extract, lavender extract, spirulina extract, angelica extract, and aloe extract to the emulsification system in proportion, and continue stirring to evenly distribute all the plant extracts; Step 6: Add hydroxyethyl cellulose and carbomer to adjust the viscosity of the mask; Step 7: Add phenoxyethanol to the mask, stir evenly, and finally sterilize the mask.

5. The method for preparing a smearable facial mask according to claim 4, characterized in that: In step 2, the stirring speed is 400-600 rpm, the stirring time is 10-15 min, and magnesium aluminum silicate is added to the aqueous phase at a stirring speed of 600-1000 rpm and a stirring time of 15-20 min.

6. The method for preparing a smearable facial mask according to claim 4, characterized in that: In step 4, the specific steps of using high shear emulsification treatment are: During the initial emulsification, start the high shear emulsifier at a speed of 1000-3000rpm, gradually disperse the oil phase into the water phase, and stir for 5-10 minutes. After the oil phase is initially dispersed, increase the speed of the emulsifier to 5000-10000rpm for high-speed emulsification treatment, and the emulsification time is 10-20 minutes; After emulsification is completed, the emulsified system is slowly cooled to room temperature to stabilize the emulsified structure. After cooling, post-treatment is performed at a rotation speed of 100-300 rpm to remove the generated bubbles.

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