Homogeneous casting device based on turbulent melt in-situ reaction and using method of homogeneous casting device

Abstract

The invention discloses a homogeneous casting device based on turbulent melt in-situ reaction and a using method of the homogeneous casting device. Comprising a vacuum cavity, two reactors, a feeder, a revolution centrifugal machine and a vacuum pump, the two reactors, the feeder and the revolution centrifugal machine are all arranged in the vacuum cavity, and the vacuum pump vacuumizes the vacuum cavity; by using the gas / liquid / solid feeder, a high-temperature melt can be subjected to sufficient in-situ reaction, the size uniformity of a reaction product is good, and a composite phase is generated in situ or interface modification of the added composite phase is realized in situ; periodic vibration is introduced to generate a synergistic effect with revolution and rotation, so that aggregate in the melt is crushed, and a more sufficient homogenizing effect is generated; and the uniform state of the melt is locked in combination with rapid directional solidification, degassing is achieved through vacuumizing, wall adhesion can be avoided through periodic vibration, overall demolding of the cast ingot is facilitated, and finally the homogeneous cast ingot is obtained. In addition, the device is high in casting speed and casting efficiency.

Description

Technical Field

[0001] The present invention relates to the technical field of stirring casting, and in particular to a homogenous casting device based on in-situ reaction of turbulent melt and a use method thereof. Background Art

[0002] As the demand for metal materials in application fields continues to increase, high-uniformity metal alloys and high-uniformity metal-based composite materials are highly valued. Powder metallurgy can achieve material uniformity, but its high cost, easy pollution, and molding temperature below the melting point limit its development. Stir casting technology is expected to obtain high-uniformity metal alloys and their composite materials at a low cost.

[0003] Stirring casting is a casting technology designed to increase the fluidity and uniformity of metals. It usually uses a mechanical stirring slurry to accelerate the flow of the melt, thereby achieving mixing and uniformity in casting. This stirring method has high requirements for the material of the stirring paddle. On the one hand, it must be resistant to high temperatures, and on the other hand, it must not react with any components in the melt. In addition, it is difficult to ensure the overall stirring effect during the high viscosity stage of the solidification of the metal melt. When the stirring speed is high, cavitation will be continuously generated in the melt, which is not conducive to improving the metallurgical quality of the ingot. On the other hand, for components with high density differences, although mechanical stirring paddle stirring casting can achieve mixing in the melt state, it is difficult to maintain the mixed state of the melt to a solid through rapid solidification, because once the stirring slurry is separated from the melt, it will cause stratification of the melt. If it is not separated, it will be wrapped in the ingot, affecting the quality and yield of the ingot.

[0004] The inventors of the present invention previously disclosed a dual-axis centrifugal stirring casting device and a mixed metal smelting casting method in CN114749622A, which mainly utilizes revolution combined with rotation to realize centrifugal motion, thereby generating a turbulent structure and realizing micro- and nano-level uniform distribution of the doped phase in the alloy melt. However, the device still has defects, such as being unable to realize orderly in-situ reaction in the turbulent structure, no directional solidification, non-dispersion of agglomerates, serious wall sticking phenomenon, and difficulty in demolding. Summary of the invention

[0005] The object of the present invention is to provide a homogenous casting device based on in-situ reaction of turbulent melt and a method of using the same, so as to solve the technical problem of low-cost and high-efficiency homogenous casting of metal alloys and composite materials thereof.

[0006] To achieve the above object, the present invention provides the following technical solutions:

[0007] A homogenous casting device based on in-situ reaction of turbulent melt, comprising: a vacuum chamber, two reactors, a feeder, an orbital centrifuge and a vacuum pump, wherein the two reactors, the feeder and the orbital centrifuge are all placed in the vacuum chamber, and the vacuum pump evacuates the vacuum chamber; the orbital centrifuge comprises an orbital motor, an orbital shaft 14 and an orbital base 141, wherein the orbital shaft 14 is located at the center of the orbital base 141, and the orbital motor drives the orbital shaft 14 and the orbital base 141 to rotate together through a first transmission mechanism, and the two reactors are respectively located in the The left and right sides of the revolution base 141 are arranged with the revolution axis 14 as the symmetry axis, the two reactors are inclined toward the revolution axis 14, the feeder is located above the revolution axis 14, and the feeder is connected to the two reactors 27; the feeder includes a combination chamber and a combination pipeline, each reactor includes a self-rotating component and a non-rotating component, the self-rotating component includes a turbulent melt reaction casting body 1, a drum cover 2, a self-rotating rotating drum 11, a self-rotating shaft 13 and an amplitude device 23; the non-rotating component includes a vibrator base 24 and a support shaft 2 5; the amplitude device 23 and the vibrator base 24 together constitute a periodic vibrator, the self-rotating component and the non-self-rotating component have relative rotation, the periodic vibrator generates periodic axial vibration as the self-rotating component rotates, the turbulent melt reaction casting body 1 is arranged in the self-rotating rotating cylinder 11, the rotating cylinder cover 2 is snap-fittedly connected to the self-rotating rotating cylinder 11, the bottom of the self-rotating rotating cylinder 11 is fixedly connected to the self-rotating rotating shaft 13, the bottom of the turbulent melt reaction casting body 1 is fixedly connected to the amplitude device 23, and the amplitude device 23 is movably arranged in the Inside the vibrator base 24, the amplitude generator 23 realizes periodic axial vibration simultaneously during the rotation process relative to the vibrator base 24. The vibrator base 24 is also located in the cylinder of the self-rotating rotating cylinder 11. The support shaft 25 is arranged inside the self-rotating shaft 13. The top of the support shaft 25 is fixedly connected to the vibrator base 24, and the bottom of the support shaft 25 is fixedly connected to the revolution base 141. The self-rotating shaft 13 and the revolution base 141 have relative rotation. The left and right self-rotating shafts 13 are connected to the self-rotating motor through the second transmission mechanism.The vibrator base 24 includes a cylindrical box 241 and a plurality of balls 242, and the plurality of balls 242 are evenly distributed on the inner bottom surface of the cylindrical box 241. The amplitude device 23 is placed in the cylindrical box 241 and contacts the plurality of balls 242. The amplitude device 23 is disc-shaped, and the upper surface of the amplitude device 23 is a plane. The lower surface of the amplitude device 23 is provided with a plurality of centrally symmetrical fan-shaped hollow portions 231, and one fan-shaped hollow portion 231 corresponds to one ball 242. The plurality of fan-shaped hollow portions 231 are connected end to end in sequence. The circumferential side surface of the fan-shaped hollow portion 231 is a first right-angled triangle 232, and the radial section of the tail end of the fan-shaped hollow portion 231 is a second right-angled triangle 233. The first right-angled triangle 232 and the second right-angled triangle 233 share the same The fan-shaped surface of the fan-shaped hollowing part 231 is placed on the ball 242. The upper surface of the amplitude 23 is fixedly connected to the bottom surface of the turbulent melt reaction casting body 1. The lower surface of the vibrator base 24 is fixedly connected to the top of the support shaft 25. When the self-rotating shaft 13 rotates, the amplitude 23 is driven to rotate through the self-rotating rotating cylinder 11 and the turbulent melt reaction casting body 1. The amplitude 23 rotates relatively on the vibrator base 24. During the relative rotation process, the fan-shaped surface of the fan-shaped hollowing part 231 slides relatively on the ball 242. Due to the existence of the first right-angled triangle 232 and the second right-angled triangle 233, the amplitude 23 is simultaneously made to vibrate axially on the vibrator base 24, driving the axial periodic vibration of the turbulent melt reaction casting body 1. ;

[0008] Preferably, the combined chamber includes a gas chamber 3, a liquid chamber 4 and a solid chamber 6, and the gas chamber 3, the liquid chamber 4 and the solid chamber 6 are detachably connected up and down in sequence through a card slot, and the solid chamber 6 is located at the top of the revolution shaft 14, and the combined pipeline includes two left and right gas pipelines 8, two liquid pipelines 9 and two solid pipelines 10, one end of the left and right two gas pipelines 8 is respectively connected to the left and right sides of the gas chamber 3, and the other end of the left and right two gas pipelines 8 is respectively connected to the left and right two turbulent melt reaction casting bodies 1, one end of the left and right two liquid pipelines 9 is respectively connected to the left and right sides of the liquid chamber 4, and the other end of the left and right two liquid pipelines 9 is respectively connected to the left and right The two turbulent melt reaction casting bodies 1 are connected, one end of the two left and right solid pipes 10 are respectively connected to the left and right sides of the solid chamber 6, and the other ends of the two left and right solid pipes 10 are respectively connected to the two left and right turbulent melt reaction casting bodies 1, the liquid chamber 4 has a heat preservation function, and the pre-added liquid 5 is preheated and placed in the liquid chamber 4. The solid chamber 6 also has a heat preservation function, and the pre-added solid 7 is pre-dried and preheated and placed in the solid chamber 6. The gas chamber 3 is filled with gas through the air inlet 26. Control valves are set on the left and right sides of the gas chamber 3 to control the opening and closing of the gas pipe 8, while the liquid chamber 4 and the solid chamber 6 do not need to be set with control valves.

[0009] Preferably, the turbulent melt reaction casting body 1 includes a boss cover 16, a cylinder, a support assembly, an insulating material 18, a graphite crucible 20 and a heat absorber 21, the boss cover 16 is sealed and arranged on the cylinder, the support assembly is arranged in the cylinder, the graphite crucible 20 and the heat absorber 21 are arranged in the support assembly, and the heat absorber 21 is arranged directly below the graphite crucible 20 to absorb heat from the bottom of the graphite crucible 20.

[0010] Preferably, the support assembly includes a bracket group 17, a partition group 19, and a support base 22, the bracket group 17 and the partition group 19 are arranged vertically and crosswise, the partition group 19 includes multiple layers of circular partitions spaced at equal distances, the bracket group 17 includes multiple vertically arranged support rods, the circular partitions are all plate-shaped with an inner square and an outer circle, and the inner square is a hollow structure, the support base 22 is arranged below the partition group 19, the support base 22 includes a support platform 221 and a lower convex portion 222, the lower convex portion 222 is arranged below the support platform 221, the lower convex portion 222 and the support platform 221 are coaxially integrally formed or fixedly connected, the support platform 221 has the same outer diameter as the circular partition, the outer diameter of the lower convex portion 222 is smaller than the outer diameter of the support platform 221, a concave circular groove 223 is provided at the axis of the support base 22, the multiple vertically arranged support rods penetrate the multiple layers of the circular partitions in the middle, and the multiple vertically arranged The upper and lower ends of the support rods are respectively fixedly connected to the circular partition of the top layer and the support platform 221, a part of the support rods are evenly distributed on the outer circular edge of the circular partition, and the other part of the support rods are evenly distributed on the inner square edge of the circular partition; the graphite crucible 20 has an octagonal prism shape and a cylindrical interior, and the graphite crucible 20 is placed in a cubic space formed by the inner square of each layer of the circular partition, and the octagonal prism fits the cubic space just right, and the graphite crucible 2 0 is placed on the supporting platform 221, the octagonal bottom of the graphite crucible 20 covers the concave circular groove 223, and the heat absorber 21 is placed in the concave circular groove 223, the heat absorber 21 is in direct contact with the octagonal bottom of the graphite crucible 20, and is used to cool the octagonal bottom of the graphite crucible 20, and the thermal insulation material 18 is filled in the gap between the bracket group 17 and the partition group 19 to keep the graphite crucible 20 warm.

[0011] Preferably, the boss cover 16 includes a central boss 161 and a circumferential cover 162, the central boss 161 is located at the center top of the circumferential cover 162, the central boss 161 is adapted to the graphite crucible 20, the circumferential cover 162 is used to cap the support assembly, the central boss 161 is provided with a gas outlet 15, a gas pipeline interface 81, a liquid pipeline interface 91 and a solid pipeline interface 101, the gas outlet 15 is used for gas outlet, one end of the gas pipeline 8 is inserted into the gas pipeline interface 81 and can rotate relatively, one end of the liquid pipeline 9 is inserted into the liquid pipeline interface 91 and can rotate relatively, and one end of the solid pipeline 10 is inserted into the solid pipeline interface 101 and can rotate relatively.

[0012] Preferably, a rotating channel is provided inside the solid chamber 6, a slot is provided in the rotating channel, and the pre-added solid 7 is placed in the slot, so that the pre-added solid 7 can enter the solid pipe 10 at a higher critical speed, thereby changing the order in which the pre-added liquid 5 and the pre-added solid 7 enter the turbulent melt reaction casting body 1.

[0013] Preferably, the liquid chamber 4 and the liquid pipeline 9 are both made of high temperature resistant materials to increase the preheating temperature of the pre-added liquid 5 .

[0014] Preferably, the sum of the volumes of the original melt, the pre-added solid 7 and the pre-added liquid 5 in the graphite crucible 20 is less than half of the volume of the graphite crucible 20 .

[0015] Preferably, the pre-added solid 7 is wrapped with metal foil into a spherical shape, so that it can gradually enter the turbulent melt reaction casting body 1 under the action of centrifugal force after the revolution begins.

[0016] Preferably, the heat absorber 21 is made of metal material with large heat capacity, which is convenient for repeated use.

[0017] Preferably, the length of the same right-angled side in the fan-shaped hollow portion 231 is designed according to the degree of wall adhesion between the original melt and the graphite crucible 20 . The more severe the wall adhesion is, the longer the length is, thereby increasing the vibration amplitude.

[0018] The present invention also provides a method for using a homogenous casting device based on an in-situ reaction of a turbulent melt, comprising the following steps:

[0019] (1) Preparatory work is performed: heating and melting the original melt in the graphite crucible 20, preheating the pre-added liquid 5, and wrapping the pre-added solid 7 to be added to the reaction with a metal foil of the same element as the original melt; assembling the amplitude device 23 and the vibrator base 24 into the periodic vibrator 12, placing it at the bottom of the self-rotating rotating cylinder 11, and assembling the bracket group 17, the heat insulating material 18, the partition group 19, the heat absorber 21 and the supporting base 22 into the turbulent melt reaction casting body 1;

[0020] (2) Loading process: the pre-added solid 7 is placed in the solid chamber 6, the pre-heated pre-added liquid 5 is placed in the liquid chamber 4, the pre-added gas is filled into the gas chamber 3, and the gas chamber 3, the liquid chamber 4 and the solid chamber 6 are assembled in sequence from top to bottom; the graphite crucible 20 is covered with the boss cover 16 and loaded into the turbulent melt reaction casting body 1 together with the melt inside, the turbulent melt reaction casting body 1 is placed in the self-rotating rotating drum 11, and fixed on the top of the periodic vibrator 12, and the drum cover 2 is covered, so that the reactor is assembled; the solid pipeline 10, the liquid pipeline 9 and the gas pipeline 8 are respectively installed in the solid chamber 6, the liquid chamber 4 and the gas chamber 3, and the combined chamber is installed on the revolving shaft 14, and the solid pipeline 10, the liquid pipeline 9 and the gas pipeline 8 are all rotatably connected to the boss cover 16, so that the feeder is assembled;

[0021] (3) Start-up process: start the vacuum pump to pump the air pressure of the vacuum chamber after loading to below 0.1 Pa; turn off the vacuum pump, start the orbital motor and the self-rotating motor synchronously to drive the orbital shaft 14 and the self-rotating shaft 13 to rotate respectively, and as the rotation speed increases, the pre-added liquid 5 and the pre-added solid 7 in the liquid chamber 4 and the solid chamber 6 enter the graphite crucible 20 through the liquid pipeline 9 and the solid pipeline 10 respectively, open the control valve to introduce gas, and introduce the gas from the gas chamber 3 and the gas pipeline 8 into the graphite crucible 20; control the inflow and introduction time of the gas by the control valve, and adjust the addition time of the pre-added solid 7 by the rotating channel and the slot structure inside the solid chamber 6;

[0022] (4) Reaction process: As the rotation speed increases, the mixed melt in the graphite crucible 20 forms a central vortex under the combined action of revolution and rotation. When the revolution and rotation speeds both exceed 300 rpm, the mixed melt gradually enters a turbulent state, that is, small vortices and micro vortices continue to appear in the central vortex, which greatly accelerates the exchange and convection of substances in the mixed melt; at this time, the added solids, liquids and gases will be quickly drawn into the mixed melt by the turbulent vortex, and will be continuously decomposed and split by the vortices at all levels, and multiple in-situ reactions will be rapidly carried out in the mixed melt; as the rotation speed reaches more than 1500 rpm, the in-situ reaction has been fully carried out, and the reaction products are evenly dispersed in the existing melt;

[0023] (5) Solidification process: After the added solids, liquids and gases have completed the in-situ reaction, the vacuum pump is started again. After maintaining a high speed for a period of time, the heat of the existing melt is gradually transferred from the bottom of the graphite crucible 20 to the heat absorber 21. The bottom of the graphite crucible 20 closest to the heat absorber 21 is the first to solidify. The existing melt will solidify from the bottom to the top in sequence. As the vacuum degree increases, the gas dissolved in the existing melt is gradually discharged to obtain a directionally solidified metal ingot. The periodic vibrator 12 generates high-frequency axial vibration as the rotation speed increases, which greatly alleviates the adhesion between the solidified metal and the wall of the graphite crucible 20.

[0024] (6) Material removal process: After complete solidification, the components are unloaded in sequence according to the reverse process of assembly, and the metal ingot and heat absorber 21 in the graphite crucible 20 are taken out and water-cooled to room temperature, while the remaining components can be air-cooled.

[0025] Preferably, according to different in-situ reaction requirements, one, two or three of the gas chamber, solid chamber and liquid chamber are selectively used.

[0026] The working principle of the present invention is: under the combined action of high-speed revolution and rotation, the mixed melt in the reactor appears turbulent state, and the material flow in the mixed melt is greatly improved. At this time, under the action of the centrifugal force of revolution, the gas, solid and liquid in the feeder enter the metal melt in the reactor, and while adding, immediate stirring and mixing and sufficient in-situ reaction are achieved. While the in-situ reaction in the melt, the reaction product is fully dispersed under the action of turbulence, the higher the rotation speed, the better the overall dispersion, and the smaller the scale of dispersion. After the reaction is completed, the melt gradually realizes rapid directional solidification from the bottom to the top, and synchronous periodic vibration and vacuuming can maintain the dispersed state in the melt, which is conducive to the gradual discharge of dissolved gas in the high-temperature melt, improves the metallurgical quality of the ingot, and is also conducive to the smooth demoulding of the metal ingot.

[0027] It needs to be further explained that, regarding the heat absorber, although it is placed in the turbulent melt reaction casting body 1 from the beginning, and the melt is cooled after entering, the melt needs to be put in at a temperature above the melting point. Because of the existence of overheat, it will not cool down immediately even if it is cooled. When the turbulent melt reaction casting body 1 rotates and revolves, the heat exchange of the melt will be accelerated, thereby achieving solidification while rotating.

[0028] Compared with the prior art, the beneficial effects of the present invention are mainly reflected in:

[0029] 1. The in-situ reaction is sufficient and the size uniformity of the reaction products is good. The device is conducive to the solid / liquid, liquid / liquid and gas / liquid reactions and the rapid dispersion of the reaction products in the metal melt, and the in-situ generation of composite phases or the in-situ addition of composite phases. Interface modification. Especially for reactions with strong reaction dynamics, this solution can greatly reduce the problem of excessive local reaction products, thereby improving the size uniformity of the reaction products. Because it is a synchronous reaction and dispersion process, the reaction is usually not limited by the melt viscosity and diffusion rate under the condition that the turbulent effect greatly improves the material exchange, which greatly increases the chance of continuous reaction, thereby achieving full reaction.

[0030] 2. Periodic vibration and revolution and rotation produce synergistic effects. Revolution and rotation make the high-temperature melt enter a turbulent state, forming vortices of different sizes. The introduction of periodic vibration further breaks up the agglomerates in the melt. The three work together to produce a more complete homogenization effect.

[0031] 3. The vibration driving force of the periodic vibrator comes from rotation. The support shaft is arranged inside the rotating shaft. The rotating shaft rotates while the support shaft does not rotate, thereby generating relative motion. Combined with the ingenious structural design of the periodic vibrator, periodic vibration is achieved through rotation. Therefore, the turbulent melt reaction casting body not only has revolution and rotation but also periodic vibration. As the rotation speed increases, the frequency of axial vibration increases, which not only achieves the breakage of agglomerates in the melt, but also greatly alleviates the adhesion between the solidified metal and the wall of the graphite crucible, and is also conducive to the smooth demolding of the metal ingot.

[0032] 4. A heat absorber is provided at the bottom of the graphite crucible, which can realize directional solidification from the bottom to the top, obtain directional and single crystal structure, and greatly improve the comprehensive performance of the material.

[0033] 5. Fast casting speed and high casting efficiency. The device can provide very fast reaction speed and melt heat exchange speed. It usually takes only a few minutes from starting rotation to completing solidification and ending rotation. Compared with traditional casting which takes several hours, the efficiency is greatly improved.

[0034] 6. The pre-added solids and liquids are "thrown" out of the pipe by the centrifugal force of revolution and enter the graphite crucible. There is no need to use a control valve, and the addition time and order can be better controlled.

[0035] 7. The graphite crucible is designed to be in an octagonal prism shape and is placed in a cubic space formed by the inner squares of the circular partitions of each layer. The octagonal prism shape just fits the cubic space. The reason why the graphite crucible is not designed to be in a cubic shape is to reduce the weight of the graphite crucible.

[0036] 8. The unique design of the support assembly's bracket group, partition group and support base has stable supporting performance, which can achieve both side insulation and directional solidification. BRIEF DESCRIPTION OF THE DRAWINGS

[0037] Figure 1 It is a schematic diagram of the overall structure of a homogeneous casting device based on in-situ reaction of turbulent melt;

[0038] Figure 2 It is a cross-sectional view of a homogeneous casting device based on an in-situ reaction of a turbulent melt;

[0039] Figure 3 It is a schematic diagram of the structure of the feeder;

[0040] Figure 4 It is a schematic diagram of the structure of a turbulent melt reaction casting body;

[0041] Figure 5 is a schematic diagram of the structure of the support assembly;

[0042] Figure 6 is a schematic diagram of a graphite crucible and its installation;

[0043] Figure 7 It is a structural diagram of a periodic oscillator.

[0044] In the figure: turbulent melt reaction casting body 1, drum cover 2, gas chamber 3, liquid chamber 4, pre-added liquid 5, solid chamber 6, pre-added solid 7, gas pipeline 8, gas pipeline interface 81, liquid pipeline 9, liquid pipeline interface 91, solid pipeline 10, solid pipeline interface 101, self-rotating rotating drum 11, periodic vibrator 12, self-rotating shaft 13, revolving shaft 14, gas outlet 15, boss cover 16, central boss 161, circumferential cover 162, bracket group 17, thermal insulation material 18, partition group 19, graphite crucible 20, heat absorber 21, support base 22, support platform 221, lower convex portion 222, concave circular groove 223, amplitude device 23, fan-shaped hollow portion 231, first right-angled triangle 232, second right-angled triangle 233, vibrator base 24, cylindrical box 241, ball 242, support shaft 25, gas inlet 26. DETAILED DESCRIPTION

[0045] The technical scheme in the embodiment of the present invention will be clearly and completely described below in conjunction with the drawings in the embodiment of the present invention. Obviously, the described embodiment is only a part of the embodiment of the present invention, not all of the embodiments. Based on the embodiment of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the present invention.

[0046] See also Figure 1-7, provides the following implementation scheme: a homogeneous casting device based on turbulent melt in-situ reaction, comprising: a vacuum chamber, two reactors, a feeder, an orbital centrifuge and a vacuum pump, the two reactors, the feeder and the orbital centrifuge are all placed in the vacuum chamber, and the vacuum pump evacuates the vacuum chamber; the orbital centrifuge comprises an orbital motor, an orbital shaft 14 and an orbital base 141, the orbital shaft 14 is located at the center of the orbital base 141, the orbital motor drives the orbital shaft 14 and the orbital base 141 to rotate together through a first transmission mechanism, and ... The reactors are respectively located on the left and right sides of the revolution base 141, and are arranged with the revolution axis 14 as the symmetry axis. The two reactors are inclined toward the revolution axis 14. The feeder is located above the revolution axis 14, and the feeder is connected to both reactors. The feeder includes a combination chamber and a combination pipeline. Each reactor includes a self-rotating component and a non-rotating component. The self-rotating component includes a turbulent melt reaction casting body 1, a drum cover 2, a self-rotating rotating drum 11, a self-rotating shaft 13 and an amplitude device 23. The non-rotating component includes a vibrator base 24 and The support shaft 25; the amplitude device 23 and the vibrator base 24 together constitute a periodic vibrator, the self-rotating component and the non-rotating component have relative rotation, and the periodic vibrator generates periodic axial vibration as the self-rotating component rotates, the turbulent melt reaction casting body 1 is arranged in the self-rotating rotating cylinder 11, the rotating cylinder cover 2 is snap-fittedly connected to the self-rotating rotating cylinder 11, the bottom of the self-rotating rotating cylinder 11 is fixedly connected to the self-rotating rotating shaft 13, the bottom of the turbulent melt reaction casting body 1 is fixedly connected to the amplitude device 23, and the amplitude device 23 is movably arranged on Inside the vibrator base 24, the amplitude generator 23 realizes periodic axial vibration simultaneously during the rotation process relative to the vibrator base 24. The vibrator base 24 is also located inside the self-rotating rotating cylinder 11. The support shaft 25 is arranged inside the self-rotating shaft 13. The top of the support shaft 25 is fixedly connected to the vibrator base 24, and the bottom of the support shaft 25 is fixedly connected to the revolution base 141. The self-rotating shaft 13 and the revolution base 141 can rotate relative to each other. The left and right self-rotating shafts 13 are connected to the self-rotating motor through the second transmission mechanism.The vibrator base 24 includes a cylindrical box 241 and a plurality of balls 242, and the plurality of balls 242 are evenly distributed on the inner bottom surface of the cylindrical box 241. The amplitude device 23 is placed in the cylindrical box 241 and contacts the plurality of balls 242. The amplitude device 23 is disc-shaped, and the upper surface of the amplitude device 23 is a plane. The lower surface of the amplitude device 23 is provided with a plurality of centrally symmetrical fan-shaped hollow portions 231, and one fan-shaped hollow portion 231 corresponds to one ball 242. The plurality of fan-shaped hollow portions 231 are connected end to end in sequence. The circumferential side surface of the fan-shaped hollow portion 231 is a first right-angled triangle 232, and the radial section of the tail end of the fan-shaped hollow portion 231 is a second right-angled triangle 233. The first right-angled triangle 232 and the second right-angled triangle 233 share the same The fan-shaped surface of the fan-shaped hollowing part 231 is placed on the ball 242. The upper surface of the amplitude 23 is fixedly connected to the bottom surface of the turbulent melt reaction casting body 1. The lower surface of the vibrator base 24 is fixedly connected to the top of the support shaft 25. When the self-rotating shaft 13 rotates, the amplitude 23 is driven to rotate through the self-rotating rotating cylinder 11 and the turbulent melt reaction casting body 1. The amplitude 23 rotates relatively on the vibrator base 24. During the relative rotation process, the fan-shaped surface of the fan-shaped hollowing part 231 slides relatively on the ball 242. Due to the existence of the first right-angled triangle 232 and the second right-angled triangle 233, the amplitude 23 is simultaneously made to vibrate axially on the vibrator base 24, driving the axial periodic vibration of the turbulent melt reaction casting body 1. ;

[0047] The combined chamber includes a gas chamber 3, a liquid chamber 4 and a solid chamber 6, and the gas chamber 3, the liquid chamber 4 and the solid chamber 6 are detachably connected up and down in sequence through a card slot. The solid chamber 6 is located at the top of the revolution shaft 14. The combined pipeline includes two left and right gas pipelines 8, two liquid pipelines 9 and two solid pipelines 10. One end of the left and right gas pipelines 8 is respectively connected to the left and right sides of the gas chamber 3, and the other end of the left and right gas pipelines 8 is respectively connected to the left and right turbulent melt reaction casting bodies 1, one end of the left and right liquid pipelines 9 is respectively connected to the left and right sides of the liquid chamber 4, and the other end of the left and right liquid pipelines 9 is respectively connected to the left and right The turbulent melt reaction casting body 1 is connected, one end of the left and right two solid pipes 10 are respectively connected to the left and right sides of the solid chamber 6, and the other ends of the left and right two solid pipes 10 are respectively connected to the left and right two turbulent melt reaction casting bodies 1, the liquid chamber 4 has a heat preservation function, and the pre-added liquid 5 is preheated and placed in the liquid chamber 4. The solid chamber 6 also has a heat preservation function, and the pre-added solid 7 is pre-dried and preheated and placed in the solid chamber 6. The gas chamber 3 is filled with gas through the air inlet 26. Control valves are set on the left and right sides of the gas chamber 3 to control the opening and closing of the gas pipe 8, while the liquid chamber 4 and the solid chamber 6 do not need to be set with control valves.

[0048] The turbulent melt reaction casting body 1 includes a boss cover 16, a cylinder, a support assembly, an insulating material 18, a graphite crucible 20 and a heat absorber 21. The boss cover 16 is sealed and arranged on the cylinder. The support assembly is arranged in the cylinder. The graphite crucible 20 and the heat absorber 21 are arranged in the support assembly. The heat absorber 21 is arranged directly below the graphite crucible 20 to absorb heat from the bottom of the graphite crucible 20.

[0049] The support assembly includes a bracket group 17, a partition group 19, and a support base 22. The bracket group 17 is vertically crossed with the partition group 19. The partition group 19 includes multiple layers of circular partitions with equal spacing. The bracket group 17 includes multiple vertically arranged support rods. The circular partitions are all plate-shaped with an inner square and an outer circle, and the inner square is a hollow structure. The support base 22 is arranged below the partition group 19. The support base 22 includes a support platform 221 and a lower convex portion 222. The lower convex portion 222 is arranged below the support platform 221. The lower convex portion 222 and the support platform 221 are coaxially integrally formed or fixedly connected. The support platform 221 has the same outer diameter as the circular partition, and the outer diameter of the lower convex portion 222 is smaller than the outer diameter of the support platform 221. A concave circular groove 223 is provided at the axis of the support base 22. The multiple vertically arranged support rods penetrate the multiple layers of the circular partitions in the middle. The multiple vertically arranged support rods The upper and lower ends of the rods are respectively fixedly connected to the circular partition of the top layer and the support platform 221, a part of the support rods are evenly distributed on the outer circular edge of the circular partition, and the other part of the support rods are evenly distributed on the inner square edge of the circular partition; the graphite crucible 20 has an octagonal prism shape and a cylindrical interior, and the graphite crucible 20 is placed in a cubic space formed by the inner square of each layer of the circular partition, and the octagonal prism fits the cubic space just right, and the graphite crucible 20 The octagonal bottom of the graphite crucible 20 is placed on the supporting platform 221, the octagonal bottom of the graphite crucible 20 covers the concave circular groove 223, and the heat absorber 21 is placed in the concave circular groove 223, the heat absorber 21 is in direct contact with the octagonal bottom of the graphite crucible 20, and is used to cool the octagonal bottom of the graphite crucible 20, and the thermal insulation material 18 is filled in the gap between the bracket group 17 and the partition group 19 to keep the graphite crucible 20 warm.

[0050] The boss cover 16 includes a central boss 161 and a circumferential cover 162. The central boss 161 is located at the center top of the circumferential cover 162. The central boss 161 is compatible with the graphite crucible 20. The circumferential cover 162 is used to cap the support assembly. The central boss 161 is provided with a gas outlet 15, a gas pipeline interface 81, a liquid pipeline interface 91 and a solid pipeline interface 101. The gas outlet 15 is used for gas outlet. One end of the gas pipeline 8 is inserted into the gas pipeline interface 81 and can rotate relatively. One end of the liquid pipeline 9 is inserted into the liquid pipeline interface 91 and can rotate relatively. One end of the solid pipeline 10 is inserted into the solid pipeline interface 101 and can rotate relatively.

[0051] Specifically, a rotating channel is provided inside the solid chamber 6, and a slot is provided in the rotating channel. The pre-added solid 7 is placed in the slot, so that the pre-added solid 7 can enter the solid pipeline 10 at a higher critical speed, thereby changing the order in which the pre-added liquid 5 and the pre-added solid 7 enter the turbulent melt reaction casting body 1.

[0052] Specifically, the liquid chamber 4 and the liquid pipeline 9 are both made of high temperature resistant materials to increase the preheating temperature of the pre-added liquid 5 .

[0053] Specifically, the sum of the volumes of the original melt, the pre-added solid 7 and the pre-added liquid 5 in the graphite crucible 20 is less than half of the volume of the graphite crucible 20 .

[0054] Specifically, the pre-added solid 7 is wrapped with metal foil into a spherical shape, so that it can gradually enter the turbulent melt reaction casting body 1 under the action of centrifugal force after the revolution begins.

[0055] Specifically, the heat absorber 21 is made of metal material with large heat capacity, which is convenient for repeated use.

[0056] Specifically, the length of the same right-angled side in the fan-shaped hollow portion 231 is designed according to the degree of wall adhesion between the original melt and the graphite crucible 20. The more severe the wall adhesion is, the longer the length is, thereby increasing the vibration amplitude.

[0057] The present invention also provides a method for using a homogenous casting device based on an in-situ reaction of a turbulent melt, comprising the following steps:

[0058] (1) Preparatory work is performed: heating and melting the original melt in the graphite crucible 20, preheating the pre-added liquid 5, and wrapping the pre-added solid 7 to be added to the reaction with a metal foil of the same element as the original melt; assembling the amplitude device 23 and the vibrator base 24 into the periodic vibrator 12, placing it at the bottom of the self-rotating rotating cylinder 11, and assembling the bracket group 17, the heat insulating material 18, the partition group 19, the heat absorber 21 and the supporting base 22 into the turbulent melt reaction casting body 1;

[0059] (2) Loading process: the pre-added solid 7 is placed in the solid chamber 6, the pre-heated pre-added liquid 5 is placed in the liquid chamber 4, the pre-added gas is filled into the gas chamber 3, and the gas chamber 3, the liquid chamber 4 and the solid chamber 6 are assembled in sequence from top to bottom; the graphite crucible 20 is covered with the boss cover 16 and loaded into the turbulent melt reaction casting body 1 together with the melt inside, the turbulent melt reaction casting body 1 is placed in the self-rotating rotating drum 11, and fixed on the top of the periodic vibrator 12, and the drum cover 2 is covered, so that the reactor is assembled; the solid pipeline 10, the liquid pipeline 9 and the gas pipeline 8 are respectively installed in the solid chamber 6, the liquid chamber 4 and the gas chamber 3, and the combined chamber is installed on the revolving shaft 14, and the solid pipeline 10, the liquid pipeline 9 and the gas pipeline 8 are all rotatably connected to the boss cover 16, so that the feeder is assembled;

[0060] (3) Start-up process: start the vacuum pump to pump the air pressure of the vacuum chamber after loading to below 0.1 Pa; turn off the vacuum pump, start the orbital motor and the self-rotating motor synchronously to drive the orbital shaft 14 and the self-rotating shaft 13 to rotate respectively, and as the rotation speed increases, the pre-added liquid 5 and the pre-added solid 7 in the liquid chamber 4 and the solid chamber 6 enter the graphite crucible 20 through the liquid pipeline 9 and the solid pipeline 10 respectively, open the control valve to introduce gas, and introduce the gas from the gas chamber 3 and the gas pipeline 8 into the graphite crucible 20; control the inflow and introduction time of the gas by the control valve, and adjust the addition time of the pre-added solid 7 by the rotating channel and the slot structure inside the solid chamber 6;

[0061] (4) Reaction process: As the rotation speed increases, the mixed melt in the graphite crucible 20 forms a central vortex under the combined action of revolution and rotation. When the revolution and rotation speeds both exceed 300 rpm, the mixed melt gradually enters a turbulent state, that is, small vortices and micro vortices continue to appear in the central vortex, which greatly accelerates the exchange and convection of substances in the mixed melt; at this time, the added solids, liquids and gases will be quickly drawn into the mixed melt by the turbulent vortex, and will be continuously decomposed and split by the vortices at all levels, and multiple in-situ reactions will be rapidly carried out in the mixed melt; as the rotation speed reaches more than 1500 rpm, the in-situ reaction has been fully carried out, and the reaction products are evenly dispersed in the existing melt;

[0062] (5) Solidification process: After the added solids, liquids and gases have completed the in-situ reaction, the vacuum pump is started again. After maintaining a high speed for a period of time, the heat of the existing melt is gradually transferred from the bottom of the graphite crucible 20 to the heat absorber 21. The bottom of the graphite crucible 20 closest to the heat absorber 21 is the first to solidify. The existing melt will solidify from the bottom to the top in sequence. As the vacuum degree increases, the gas dissolved in the existing melt is gradually discharged, and a directionally solidified metal ingot is obtained; the periodic vibrator 12 generates high-frequency axial vibration as the rotation speed increases, which greatly alleviates the adhesion between the solidified metal and the wall of the graphite crucible 20;

[0063] (6) Material removal process: After complete solidification, the components are unloaded in sequence according to the reverse process of assembly, and the metal ingot and heat absorber 21 in the graphite crucible 20 are taken out and water-cooled to room temperature, while the remaining components can be air-cooled.

[0064] Specifically, according to different in-situ reaction requirements, one, two or three of the gas chamber, the solid chamber and the liquid chamber are selectively used.

[0065] The above description is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and modifications can be made without departing from the principle of the present invention. These improvements and modifications should also be regarded as the scope of protection of the present invention.

Claims

1. A homogeneous casting device based on turbulent melt in-situ reaction, comprising: A vacuum chamber, two reactors, a feeder, an orbital centrifuge and a vacuum pump, wherein the two reactors, the feeder and the orbital centrifuge are all placed in the vacuum chamber, and the vacuum pump evacuates the vacuum chamber; the orbital centrifuge comprises an orbital motor, an orbital shaft (14) and an orbital base (141), wherein the orbital shaft (14) is located at the center of the orbital base (141), and the orbital motor drives the orbital shaft (14) and the orbital base (141) to rotate together through a first transmission mechanism, and the two reactors are respectively located on the left and right sides of the orbital base (141), and the orbital shaft (14) is used to rotate the two reactors. ) is arranged as a symmetric axis, the two reactors are inclined toward the revolution axis (14), the feeder is located above the revolution axis (14), and the feeder is connected to the two reactors; the feeder includes a combination chamber and a combination pipeline, each of the reactors includes a self-rotating component and a non-self-rotating component, the self-rotating component includes a turbulent melt reaction casting body (1), a drum cover (2), a self-rotating rotating drum (11), a self-rotating shaft (13) and an amplitude device (23); the non-self-rotating component includes a vibrator base (24) and a support shaft (25); the amplitude device (23) and the vibrator base (24) Together they constitute a periodic vibrator, wherein the self-rotating component and the non-self-rotating component have relative rotation, and the periodic vibrator generates periodic axial vibration as the self-rotating component rotates, and is characterized in that: the turbulent melt reaction casting body (1) is arranged inside the self-rotating rotating cylinder (11), the rotating cylinder cover (2) is snap-fittedly connected to the self-rotating rotating cylinder (11), the bottom of the self-rotating rotating cylinder (11) is fixedly connected to the self-rotating rotating shaft (13), the bottom of the turbulent melt reaction casting body (1) is fixedly connected to the amplitude device (23), and the amplitude device (23) is movably arranged inside the vibrator base (24), The amplitude device (23) realizes periodic axial vibration simultaneously during the rotation process relative to the vibrator base (24); the vibrator base (24) is also located in the cylinder of the self-rotating rotating cylinder (11); the support shaft (25) is arranged inside the self-rotating shaft (13); the top of the support shaft (25) is fixedly connected to the vibrator base (24); the bottom of the support shaft (25) is fixedly connected to the revolution base (141); the self-rotating shaft (13) and the revolution base (141) can rotate relative to each other; the left and right self-rotating shafts (13) are connected to the self-rotating motor via a second transmission mechanism;The vibrator base (24) comprises a cylindrical box (241) and a plurality of balls (242), wherein the plurality of balls (242) are evenly distributed on the inner bottom surface of the cylindrical box (241), the vibrator (23) is placed in the cylindrical box (241) and is in contact with the plurality of balls (242), the vibrator (23) is disc-shaped, the upper surface of the vibrator (23) is a plane, and the lower surface of the vibrator (23) is provided with a plurality of centrosymmetric The fan-shaped hollowed-out portion (231) corresponds to one of the ball bearings (242), and the plurality of fan-shaped hollowed-out portions (231) are connected end to end in sequence. The circumferential side surface of the fan-shaped hollowed-out portion (231) is a first right-angled triangle (232), and the radial cross section of the tail end of the fan-shaped hollowed-out portion (231) is a second right-angled triangle (233). The first right-angled triangle (232) and the second right-angled triangle (233) share On the same right angle side, the fan-shaped surface of the fan-shaped hollowing part (231) is placed on the ball (242), the upper surface of the amplitude device (23) is fixedly connected to the bottom surface of the turbulent melt reaction casting body (1), and the lower surface of the vibrator base (24) is fixedly connected to the top of the support shaft (25). When the self-rotating shaft (13) rotates, the amplitude device (23) is driven to rotate through the self-rotating rotating cylinder (11) and the turbulent melt reaction casting body (1), and the amplitude device (23) rotates relatively on the vibrator base (24). During the relative rotation process, the fan-shaped surface of the fan-shaped hollowing part (231) slides relatively on the ball (242), and due to the existence of the first right-angled triangle (232) and the second right-angled triangle (233), the amplitude device (23) is simultaneously caused to axially periodically vibrate on the vibrator base (24), thereby driving the axially periodic vibration of the turbulent melt reaction casting body (1).

2. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 1, characterized in that: The combined chamber comprises a gas chamber (3), a liquid chamber (4) and a solid chamber (6); the gas chamber (3), the liquid chamber (4) and the solid chamber (6) are detachably connected in sequence up and down through a slot; the solid chamber (6) is located at the top of the revolution shaft (14); the combined pipe comprises two left and right gas pipes (8), two liquid pipes (9) and two solid pipes (10); one end of the left and right gas pipes (8) are respectively connected to the left and right sides of the gas chamber (3); the other end of the left and right gas pipes (8) are respectively connected to the left and right turbulent melt reaction casting bodies (1); one end of the left and right liquid pipes (9) are respectively connected to the left and right sides of the liquid chamber (4); the other end of the left and right liquid pipes (9) are respectively connected to the left and right turbulent melt reaction casting bodies (1); one end of the left and right solid pipes (10) are respectively connected to the left and right sides of the solid chamber (6); the other end of the left and right solid pipes (10) are respectively connected to the left and right sides of the solid chamber (6); The two turbulent melt reaction casting bodies (1) are connected, one end of the two left and right liquid pipelines (9) are respectively connected to the left and right sides of the liquid chamber (4), and the other end of the two left and right liquid pipelines (9) are respectively connected to the two left and right turbulent melt reaction casting bodies (1). One end of the two left and right solid pipelines (10) are respectively connected to the left and right sides of the solid chamber (6), and the other end of the two left and right solid pipelines (10) are respectively connected to the two left and right turbulent melt reaction casting bodies (1). The liquid chamber (4) has a heat preservation function, and the pre-added liquid (5) is preheated and placed in the liquid chamber (4). The solid chamber (6) also has a heat preservation function, and the pre-added solid (7) is pre-dried and preheated and placed in the solid chamber (6). The gas chamber (3) is filled with gas through the air inlet (26). Control valves are set on the left and right sides of the gas chamber (3) to control the opening and closing of the gas pipeline (8), while the liquid chamber (4) and the solid chamber (6) do not need to be set with control valves.

3. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 2, characterized in that: The turbulent melt reaction casting body (1) comprises a boss cover (16), a cylinder, a support assembly, a heat insulating material (18), a graphite crucible (20) and a heat absorber (21); the boss cover (16) is sealed and arranged on the cylinder; the support assembly is arranged in the cylinder; the graphite crucible (20) and the heat absorber (21) are arranged in the support assembly; the heat absorber (21) is arranged directly below the graphite crucible (20) to absorb heat from the bottom of the graphite crucible (20).

4. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 3, characterized in that: The support assembly comprises a bracket group (17), a partition group (19), and a support base (22); the bracket group (17) and the partition group (19) are arranged vertically and crosswise; the partition group (19) comprises multiple layers of circular partitions spaced at equal distances; the bracket group (17) comprises a plurality of vertically arranged support rods; the circular partitions are all in the shape of plates with a square inside and a round outside, and the square inside is a hollow structure; the support base (22) is arranged below the partition group (19); the support base (22) comprises a support platform (221) and a lower convex portion ( 222), the lower convex part (222) is arranged below the support platform (221), the lower convex part (222) and the support platform (221) are coaxially integrally formed or fixedly connected, the outer diameter of the support platform (221) is the same as that of the circular partition, the outer diameter of the lower convex part (222) is smaller than the outer diameter of the support platform (221), a concave circular groove (223) is provided at the axis of the support base (22), the multiple vertically arranged support rods penetrate the multiple layers of the circular partition in the middle, and the multiple vertically arranged support rods are connected to the support platform (221) and the support platform (221) and the circular partition are connected to the support platform (221). The upper and lower ends of the vertically arranged support rods are respectively fixedly connected to the circular partition of the top layer and the support platform (221); a portion of the support rods are evenly distributed on the outer circular edge of the circular partition, and another portion of the support rods are evenly distributed on the inner square edge of the circular partition; the graphite crucible (20) is octagonal in shape and cylindrical in interior; the graphite crucible (20) is placed in a cubic space formed by the inner squares of the circular partitions of each layer; the octagonal shape fits the cubic space exactly; the octagonal shape of the graphite crucible (20) The bottom is placed on the supporting platform (221), the octagonal bottom of the graphite crucible (20) covers the concave circular groove (223), and the heat absorber (21) is placed in the concave circular groove (223), the heat absorber (21) is in direct contact with the octagonal bottom of the graphite crucible (20), and is used to cool the octagonal bottom of the graphite crucible (20), and the heat insulation material (18) is filled in the gap between the bracket group (17) and the partition group (19), so as to keep the graphite crucible (20) warm.

5. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 4, characterized in that: The boss cover (16) comprises a central boss (161) and a circumferential cover (162); the central boss (161) is located at the center top of the circumferential cover (162); the central boss (161) is compatible with the graphite crucible (20); the circumferential cover (162) is used to cap the support assembly; the central boss (161) is provided with a gas outlet (15), a gas pipeline interface (81), a liquid pipeline interface (91) and a solid pipeline interface (101); the gas outlet (15) is used for gas outlet; one end of the gas pipeline (8) is inserted into the gas pipeline interface (81) and can rotate relative to each other; one end of the liquid pipeline (9) is inserted into the liquid pipeline interface (91) and can rotate relative to each other; one end of the solid pipeline (10) is inserted into the solid pipeline interface (101) and can rotate relative to each other.

6. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 2, characterized in that: The solid chamber (6) is provided with a rotating channel inside, and a slot is provided inside the rotating channel. The pre-added solid (7) is placed in the slot, so that the pre-added solid (7) can enter the solid pipeline (10) at a higher critical speed, thereby changing the order in which the pre-added liquid (5) and the pre-added solid (7) enter the turbulent melt reaction casting body (1).

7. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 3, characterized in that: The sum of the volumes of the original melt, the pre-added solid (7) and the pre-added liquid (5) in the graphite crucible (20) is less than half the volume of the graphite crucible (20).

8. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 3, characterized in that: According to different in-situ reaction requirements, one, two or three of the gas chamber, solid chamber and liquid chamber are selectively used.

9. A homogeneous casting device based on turbulent melt in-situ reaction according to claim 3, characterized in that: The length of the same right-angled side in the fan-shaped hollow portion (231) is designed according to the degree of wall adhesion between the original melt and the graphite crucible (20). The more severe the wall adhesion, the longer the length, thereby increasing the vibration amplitude.

10. A method for using a homogenous casting device based on turbulent melt in-situ reaction according to any one of claims 1 to 9, comprising the following steps: (1) performing preparatory work: heating and melting the original melt in the graphite crucible (20), preheating the pre-added liquid (5), and wrapping the pre-added solid (7) required to be added to the reaction with a metal foil of the same element as the original melt; assembling the amplitude device (23) and the vibrator base (24) into the periodic vibrator (12), placing it at the bottom of the self-rotating rotating cylinder (11), and assembling the bracket group (17), the heat insulating material (18), the partition group (19), the heat absorber (21) and the supporting base (22) into the turbulent melt reaction casting body (1); (2) Loading process: placing the pre-added solid (7) into the solid chamber (6), placing the pre-heated pre-added liquid (5) into the liquid chamber (4), filling the pre-added gas into the gas chamber (3), and assembling the gas chamber (3), liquid chamber (4) and solid chamber (6) in sequence from top to bottom; placing the graphite crucible (20) with the boss cover (16) and the melt inside into the turbulent melt reaction casting body (1), and placing the turbulent melt reaction casting body (1) into the rotating The drum (11) is rotated and fixed above the periodic vibrator (12), and the drum cover (2) is covered, thereby realizing the assembly of the reactor; the solid pipeline (10), the liquid pipeline (9) and the gas pipeline (8) are respectively installed in the solid chamber (6), the liquid chamber (4) and the gas chamber (3), and the combined chamber is installed on the revolution shaft (14), and the solid pipeline (10), the liquid pipeline (9) and the gas pipeline (8) are all rotatably connected to the boss cover (16), thereby realizing the assembly of the feeder; (3) Start-up process: start the vacuum pump to pump the air pressure of the vacuum chamber after loading to below 0.1 Pa; turn off the vacuum pump, start the orbital motor and the self-rotating motor synchronously to drive the orbital shaft (14) and the self-rotating shaft (13) to rotate respectively, and as the rotation speed increases, the pre-added liquid (5) and the pre-added solid (7) in the liquid chamber (4) and the solid chamber (6) enter the graphite crucible (20) through the liquid pipeline (9) and the solid pipeline (10) respectively, open the control valve to introduce gas, and let the gas pass from the gas chamber (3) through the gas pipeline (8) into the graphite crucible (20); control the inflow and introduction time of the gas by the control valve, and adjust the addition time of the pre-added solid (7) by the rotating channel and the slot structure inside the solid chamber (6); (4) Reaction process: As the rotation speed increases, the mixed melt in the graphite crucible (20) forms a central vortex under the combined action of revolution and rotation. When the revolution and rotation speeds both exceed 300 rpm, the mixed melt gradually enters a turbulent state, that is, small vortices and micro vortices continuously appear in the central vortex, which greatly accelerates the exchange and convection of substances in the mixed melt. At this time, the added solids, liquids and gases will be quickly drawn into the mixed melt by the turbulent vortex and continuously decomposed and split by the vortices at various levels, and multiple in-situ reactions will be rapidly carried out in the mixed melt. As the rotation speed reaches more than 1500 rpm, the in-situ reaction has been fully carried out, and the reaction products are evenly dispersed in the existing melt. (5) Solidification process: After the added solid, liquid and gas have completed the in-situ reaction, the vacuum pump is started again. After maintaining a high rotation speed for a period of time, the heat of the existing melt is gradually transferred from the bottom of the graphite crucible (20) to the heat absorber (21). The bottom of the graphite crucible (20) closest to the heat absorber (21) is the first to solidify. The existing melt will solidify from the bottom to the top in sequence. As the vacuum degree increases, the gas dissolved in the existing melt is gradually discharged, and a directionally solidified metal ingot is obtained; the periodic vibrator (12) generates high-frequency axial vibration as the rotation speed increases, which greatly alleviates the adhesion between the solidified metal and the wall of the graphite crucible (20); (6) Material removal process: After complete solidification, the components are unloaded in sequence according to the reverse process of assembly, and the metal ingot and the heat absorber (21) in the graphite crucible (20) are taken out and water-cooled to room temperature, and the remaining components can be air-cooled.

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