A test device and method for assisting research on a CO2 degassing process

By designing an auxiliary research test device for the CO2 degassing process and utilizing an S-shaped trajectory moving channel and flow monitoring components, the research difficulties of the CO2 degassing process were solved, efficient and accurate CO2 removal and data monitoring were achieved, and the chemical reaction efficiency and product quality were improved.

CN119925996BActive Publication Date: 2025-10-10SHANDONG PROVINCIAL GEOLOGICAL & MINERAL EXPLORATION & DEV BUREAU 801 HYDROGEOLOGY & ENG GEOLOGY BRIGADE (SHANDONG PROVINCIAL GEOLOGICAL & MINERAL ENG EXPLORATION INST) +1
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Patent Information

Application Number
CN202510152649.3
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-02-12
Publication Date
2025-10-10
Estimated Expiration
2045-02-12

AI Technical Summary

Technical Problem

Existing technologies make it difficult to effectively study and optimize the CO2 degassing process, resulting in low chemical reaction efficiency, unstable product quality, large environmental impact, and a lack of accurate research data support.

Method used

A CO2 degassing process auxiliary research test device is designed. Adjacent CO2 removal components are connected end to end by setting up a flow monitoring component to form an S-shaped trajectory moving channel. Combined with membrane technology and clean stirring parts, segmented degassing and monitoring are achieved. The flow channel composed of rotating parts and fixed parts is used to perform segmented CO2 removal and data monitoring.

Benefits of technology

It has achieved rich research data on the CO2 degassing process, improved the operation simplicity and maintainability of the device, ensured the accuracy and efficiency of CO2 removal, and reduced environmental impact.

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Abstract

The present application relates to the field of CO2 degassing research, and more particularly to a CO2 degassing process auxiliary research test device and method, wherein adjacent CO2 removal components are connected end to end by setting a flow monitoring assembly to form a channel for the sample solution to move in an S-shaped track. During the movement, the accelerating gas moves in a single direction and sequentially passes through all the CO2 removal components. The CO2 in the solution inside the CO2 removal component is separated into the degassing cavity by using the membrane technology, and is carried out of the device by the accelerating gas flow to realize CO2 degassing. The CO2 removal component can further accelerate CO2 removal by the synchronous action of the forward and reverse rotation of the removal cylinder and the cleaning of the stirring element, and can also clean the carbon dioxide separation membrane. The flow monitoring assembly can segmentally monitor and adjust the sample solution, and master the carbon dioxide balance and temperature data of the solution at different positions, so as to facilitate the research on the CO2 degassing process of different sample solutions. The research data is rich, the device is easy to operate, and the maintainability and accuracy are good.
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Description

Technical Field

[0001] The present invention relates to the field of CO2 degassing research, and in particular to a CO2 degassing process auxiliary research test device and method. Background Art

[0002] Removing carbon dioxide from liquids has many applications:

[0003] 1. Chemical reaction optimization: In some chemical reactions, the presence of carbon dioxide may interfere with or affect the normal progress of the reaction. By removing carbon dioxide from the liquid, the chemical reaction can be carried out in a purer environment, thereby improving reaction efficiency and product quality.

[0004] 2. Product Quality Improvement: For certain liquid products that require high-precision control, such as pharmaceutical preparations and food additives, the presence of carbon dioxide may affect their stability and safety. Removing carbon dioxide from liquids can ensure product purity and quality, meeting higher production and application requirements.

[0005] 3. Environmental Protection and Emission Reduction: Carbon dioxide is a greenhouse gas whose emissions have a significant impact on global climate change. By removing carbon dioxide from liquids, the amount of carbon dioxide emitted into the atmosphere can be reduced, helping to reduce the impact on the environment and mitigate global climate change.

[0006] 4. Energy Production: In some energy production processes, such as biomass and geothermal energy, the liquid may contain carbon dioxide. Removing this carbon dioxide can improve the efficiency and stability of energy production while reducing the impact on the environment.

[0007] 5. Industrial Application: In some industrial processes, such as water treatment and metal smelting, liquids may contain carbon dioxide. Removing this carbon dioxide can optimize the process and improve product quality and production efficiency.

[0008] Therefore, research on CO2 degassing process has become a development need in many industries. Summary of the Invention

[0009] In response to the problems existing in the background technology, a CO2 degassing process auxiliary research test device and method are proposed. By setting up a circulation monitoring component, adjacent CO2 removal components are connected end to end to form a channel for the sample solution to move in an S-shaped trajectory. The sample solution is degassed, monitored and adjusted in sections to facilitate the study of the CO2 degassing process of different sample solutions. The research data is rich, the device is simple to operate, and it has good maintainability and accuracy.

[0010] The present invention provides a CO2 degassing process auxiliary research test device, comprising:

[0011] The test box has two sets of partitions that divide the internal space of the test box into a degassing chamber in the middle and installation chambers on both sides. The test box is provided with an air inlet pipe and an air outlet pipe connected to the end of the degassing chamber, and a liquid inlet pipe and a liquid outlet pipe connected to the installation chamber.

[0012] CO2 removal components are arranged in multiple groups along the gas flow direction in the degassing chamber. Each group of CO2 removal components rotates through the baffles on both sides. During the rotation, the CO2 in the internal solution is separated into the degassing chamber through membrane technology and driven out by the airflow. The head end of the first group of CO2 removal components is connected to the liquid inlet pipe through pipe 1, and the tail end of the last group of CO2 removal components is connected to the liquid inlet pipe through pipe 2.

[0013] And a flow monitoring component connects the head end and tail end of two adjacent groups of CO2 removal components and is located in the installation cavity to monitor the data of the liquid flowing through.

[0014] Preferably, the CO2 removal component includes a removal cylinder with a carbon dioxide separation membrane; a rotating part is provided at one end of the removal cylinder to drive its rotation and supply solution in and out, and a fixed part is provided at the other end to be rotatably connected to it and supply solution in and out; the flow monitoring component is located between two adjacent groups of rotating parts / two groups of fixed parts to form a liquid flow channel.

[0015] Preferably, the rotating part includes a rotating tube that is coaxially connected to the removal cylinder and rotatably arranged on the partition; the rotating tube is connected to the corresponding pipeline one / pipeline two / circulation monitoring component, a gear ring is arranged on the outside of the rotating tube, and a motor and a gear connected to the motor main shaft are arranged on one side; the gear is engaged with the gear ring.

[0016] Preferably, the gear is located between adjacent stripping cylinders and engages with the gear rings on both sides.

[0017] Preferably, the fixing part includes a rotating seat that is detachably connected to the end of the removal cylinder; a sealing seat is rotatably set on one side of the rotating seat, a cleaning stirring member that seals through the rotating seat and extends into the interior of the removal cylinder is set on one side of the sealing seat, and a fixed tube is set on the other side; the rotating seat, the sealing seat and the fixed tube are connected in series in sequence and connected to the corresponding flow monitoring components.

[0018] Preferably, the cleaning stirring member includes a stirring frame that rotates through the rotating seat; the lower end of the stirring frame is provided with a liquid inlet and outlet head connected to the circulation monitoring component, the upper end is provided with a mounting frame with a cleaning brush, and the side wall is provided with a leakage slag cover.

[0019] Preferably, the circulation monitoring component includes a connecting pipe connecting two adjacent groups of rotating tubes / two groups of fixed tubes; a monitoring box located on the connecting pipe; a water pump is provided on the monitoring box, and a monitoring probe for monitoring the solution is also provided.

[0020] Preferably, a circulating member is arranged between the liquid inlet pipe and the liquid outlet pipe; the circulating member comprises a communication pipe two for communicating the liquid inlet pipe and the liquid outlet pipe through a three-way valve; a monitoring box two is arranged on the communication pipe two; a water pump two is arranged on the monitoring box two, and a monitoring probe two for monitoring the solution is further arranged.

[0021] Preferably, the test box is provided with a box cover corresponding to the installation cavities on both sides, so as to facilitate the maintenance of the equipment in the installation cavities.

[0022] The application further provides a CO2 degassing process auxiliary research test method, which adopts the CO2 degassing process auxiliary research test device.

[0023] S1, the sample solution is pretreated in advance; the accelerating gas is introduced into the degassing cavity;

[0024] S2, the sample solution enters from the liquid inlet pipe, passes through the CO2 removal assembly which rotates and is sequentially communicated;

[0025] S3, the sample solution moves in an S-shaped trajectory, and in the moving process, the CO2 in the solution in the CO2 removal assembly is repeatedly separated into the degassing cavity by the membrane technology, and is carried out of the device by the accelerating airflow;

[0026] S4, the flow monitoring assembly monitors the data of the liquid flowing therethrough; the data acquisition end acquires the sample solution data before and after degassing of each section;

[0027] S5, the mixed gas for capturing CO2 is introduced into the measuring equipment to measure the captured CO2 data;

[0028] S6, the captured CO2 data and the acquired sample solution data before and after degassing of each section are used for the CO2 degassing process auxiliary research of the sample solution.

[0029] Compared with the prior art, the application has the following beneficial technical effects: the flow monitoring assembly connects the adjacent CO2 removal assemblies in a head-to-tail manner to form a channel for the sample solution to move in an S-shaped trajectory. In the moving process, the accelerating gas moves in a single direction, sequentially passes through all the CO2 removal assemblies, and the CO2 in the solution in the CO2 removal assembly is separated into the degassing cavity by the membrane technology, and is carried out of the device by the accelerating airflow, so that the CO2 is removed. Through the segmented degassing, the research route can be prolonged, and the CO2 removal assembly can be further accelerated by the synchronous action of the forward and reverse rotation of the removal cylinder and the cleaning of the stirring member, and the carbon dioxide separation membrane can also be cleaned. The flow monitoring assembly can segmentally monitor and adjust the sample solution, master the carbon dioxide balance and temperature data of the solution at different positions, so as to research the CO2 degassing process of different sample solutions, and the research data is rich, the device is simple to operate, and has good maintainability and precision. BRIEF DESCRIPTION OF DRAWINGS

[0030] Figure 1 Schematic diagram of the structure of the CO2 degassing process auxiliary research test device in the present invention (state 1);

[0031] Figure 2 Schematic diagram of the structure of the CO2 degassing process auxiliary research test device in the present invention (state 2);

[0032] Figure 3 This is a schematic diagram of the structure inside the test box of the present invention;

[0033] Figure 4 Schematic diagram of the combination of CO2 removal components in the present invention;

[0034] Figure 5 Schematic diagram of the disassembly of the CO2 removal component in the present invention;

[0035] Figure 6 Schematic diagram of the structure of the cleaning stirring member of the present invention;

[0036] Figure 7 Schematic diagram of the structure of the circulation monitoring component of the present invention;

[0037] Figure 8 It is a structural schematic diagram of the circulation part in the present invention.

[0038] Reference numerals: 1. test chamber; 101. partition; 102. degassing chamber; 103. mounting chamber; 104. chamber cover; 105. air inlet pipe; 106. air outlet pipe; 107. liquid inlet pipe; 108. liquid outlet pipe; 2. circulation monitoring assembly; 201. connecting pipe 1; 202. monitoring box 1; 203. water pump 1; 3. CO2 removal assembly; 301. removal cylinder; 302. rotating member; 302a. rotating tube; 302b, gear ring; 302c, gear; 303, fixing part; 303a, fixing pipe; 303b, sealing seat; 303c, stirring frame; 303d, leakage slag cover; 303e, mounting frame; 303f, cleaning brush; 303g, liquid inlet and outlet head; 303h, rotating seat; 4, pipeline one; 5, pipeline two; 6, circulation part; 601, connecting pipe two; 602, monitoring box two; 603, water pump two. DETAILED DESCRIPTION

[0039] Example 1, as Figure 1-Figure 3As shown, the application provides a CO2 degassing process auxiliary research test device, which comprises a test box 1, a CO2 removal assembly 3 and a flow monitoring assembly 2. Two sets of partitions 101 divide the internal space of the test box 1 into a degassing cavity 102 in the middle and installation cavities 103 on both sides. The test box 1 is provided with a gas inlet pipe 105 and a gas outlet pipe 106 which are in communication with the degassing cavity 102 at the head and tail, a liquid inlet pipe 107 and a liquid outlet pipe 108 which are in communication with the installation cavities 103, and a box cover 104 corresponding to the installation cavities 103 on both sides, which facilitates the maintenance of the equipment in the installation cavities 103. The CO2 removal assembly 3 is provided in multiple sets along the gas flow direction in the degassing cavity 102. Each set of CO2 removal assembly 3 is rotatably penetrated through the two partitions 101. During rotation, CO2 in the internal solution is separated into the degassing cavity 102 by membrane technology and is carried out by the gas flow. The head end of the first set of CO2 removal assembly 3 is connected to the liquid inlet pipe 107 through pipeline one 4, and the tail end of the last set of CO2 removal assembly 3 is connected to the liquid inlet pipe 107 through pipeline two 5. The flow monitoring assembly 2 is connected to the head end and tail end of adjacent two sets of CO2 removal assembly 3 and is located in the installation cavity 103, which monitors the data of the liquid flowing through.

[0040] As shown, Figure 4 The CO2 removal assembly 3 comprises a removal cylinder 301 with a carbon dioxide separation membrane. The working principle of the carbon dioxide separation membrane is mainly based on the adsorption and permeation characteristics of carbon dioxide on the membrane material. Since carbon dioxide is a condensed gas with strong polarization, its solubility coefficient in the membrane material is large, so its permeation coefficient and separation coefficient are also large. By controlling the temperature, pressure and gas composition of the membrane material, effective separation of carbon dioxide and other gases can be achieved. Commonly used membrane materials include polydimethylsiloxane membrane, poly-4-methyl-1-pentene membrane, polyether sulfone membrane and polyimide film, etc. One end of the removal cylinder 301 is provided with a rotating part 302 for driving its rotation and supplying solution, and the other end is provided with a fixed part 303 for rotation connection and supplying solution. The flow monitoring assembly 2 is located between the adjacent two sets of rotating parts 302 / two sets of fixed parts 303, forming an S-shaped liquid flow channel.

[0041] Further, as shown, Figure 5 The rotating part 302 comprises a rotating pipe 302a which is coaxially connected to the removal cylinder 301 and is rotatably arranged on the partition 101. The rotating pipe 302a is connected to the corresponding pipeline one 4 / pipeline two 5 / flow monitoring assembly 2. The outside of the rotating pipe 302a is provided with a gear ring 302b, one side is provided with a motor 302d and a gear 302c connected to the main shaft of the motor 302d. The gear 302c is engaged with the gear ring 302b.

[0042] The motor 302d drives the gear 302c to rotate, and the gear ring 302b drives the removal cylinder 301 to rotate synchronously. The rotation process of the removal cylinder 301 can achieve the purpose of mixing the solution, so that the CO2 in the internal solution has the opportunity to contact with the carbon dioxide separation membrane, which is conducive to the comprehensive removal of CO 2。

[0043] It should be further noted that the gear 302c is located between adjacent removal cylinders 301 and engages the gear rings 302b on both sides. Therefore, the adjacent removal cylinders 301 rotate synchronously in opposite directions, causing the liquid to be repeatedly mixed forward and backward as it moves along the S-shaped trajectory, which is beneficial for comprehensive CO2 removal.

[0044] It needs to be further said that Figure 5 As shown, the fixing member 303 comprises a rotating seat 303h that is detachably connected to the end of the removal cylinder 301. A sealing seat 303b is rotatably mounted on one side of the rotating seat 303h. A cleaning and stirring element, which seals through the rotating seat 303h and extends into the interior of the removal cylinder 301, is mounted on one side of the sealing seat 303b. A fixing tube 303a is mounted on the other side of the sealing seat 303b. The rotating seat 303h, sealing seat 303b, and fixing tube 303a are connected in series and communicate with the corresponding flow monitoring assembly 2.

[0045] The end of the removal cylinder 301 is engaged with the rotating seat 303h, and the rotating seat 303h rotates on the sealing seat 303b. When the removal cylinder 301 rotates, the rotating seat 303h rotates synchronously, and the cleaning stirring member is stationary with the sealing seat 303b and is in motion relative to the removal cylinder 301, so the removal cylinder 301 can be cleaned and the solution inside it can be stirred.

[0046] It needs to be further said that Figure 6 As shown, the cleaning and stirring element includes a stirring frame 303c that rotates and extends through a rotating base 303h. The lower end of the stirring frame 303c is equipped with an inlet and outlet head 303g, which is connected to the flow monitoring assembly 2. The upper end is equipped with a mounting frame 303e with a cleaning brush 303f. A leakage slag cover 303d is installed on the side wall. The solution flows into the rotating tube 302a and flows out of the inlet and outlet head 303g, or flows into the inlet and outlet head 303g and flows out of the rotating tube 302a. During the flow, the removal cylinder 301 rotates, the cleaning brush 303f cleans its inner wall, and the leakage slag cover 303d catches dirt accumulated on the carbon dioxide separation membrane. These structures also have a disturbing effect, further mixing the solution. After degassing is completed, the cleaning and stirring element can be removed for cleaning and maintenance.

[0047] It should be further noted that the leakage slag receiving cover 303d is similar to a boat shape, with the concave side facing downwards, so as to catch dirt and allow the solution to pass through.

[0048] It should be further noted that the liquid inlet and outlet head 303g is close to the rotating seat 303h, and the flow time of the liquid is prolonged by being away from the rotating tube 302a.

[0049] like Figure 7 As shown, the flow monitoring assembly 2 includes a connecting pipe 201 connecting two adjacent groups of rotating pipes 302a / two groups of fixed pipes 303a; a monitoring box 202 located on the connecting pipe 201; a water pump 203 is provided on the monitoring box 202, and a monitoring probe for monitoring the solution is also provided.

[0050] like Figure 8 As shown, a circulation component 6 is provided between the liquid inlet pipe 107 and the liquid outlet pipe 108; the circulation component 6 includes a connecting pipe 2 601 respectively connected to the liquid inlet pipe 107 and the liquid outlet pipe 108 through a three-way valve; a monitoring box 2 602 is located on the connecting pipe 2 601; a water pump 2 603 is provided on the monitoring box 2 602, and a monitoring probe 2 for monitoring the solution is also provided.

[0051] It should be further explained that monitoring probe 1 and monitoring probe 2 can be temperature monitoring probes and CO2 concentration monitoring probes, which are inserted into the corresponding solution segments to obtain relevant data before and after degassing. By collecting data in segments, the test conditions can be accurately grasped, facilitating timely adjustment of parameters.

[0052] In addition, temperature regulating components are provided in the rotating tube 302a and the fixed tube 303a, such as resistance wires for electric heating and semiconductor refrigeration plates for electric cooling. According to the monitoring results of the temperature monitoring probe, the temperature of the solution is adjusted in sections to keep the temperature stable throughout the process, thereby reducing the impact of temperature on CO2 degassing.

[0053] When the data acquisition end detects that the CO2 degassing is not complete, the circulation component 6 can be started to degas the CO2 multiple times by repeatedly passing the solution into the S-shaped liquid flow channel. During the degassing process, the temperature and gas flow rate are adjusted to conduct auxiliary research on the CO2 degassing process until the test goal is achieved.

[0054] Example 2: Based on the CO2 degassing process auxiliary research test device in Example 1, this example proposes a CO2 degassing process auxiliary research test method, and the method steps are as follows:

[0055] S1. Pre-treat the sample solution in advance. The main pre-treatment methods include filtering to remove impurities, temperature adjustment, etc. At the same time, accelerate gas (such as nitrogen) and connect the gas source to the degassing chamber 102.

[0056] S2, the sample solution enters from the liquid inlet pipe 107 and passes through the rotating and sequentially connected CO2 removal components 3;

[0057] S3, the sample solution moves in an S-shaped track, and the rotation of the removal cylinder 301 can mix the solution, so that the CO2 in the solution has the opportunity to contact the carbon dioxide separation membrane, and the membrane technology repeatedly separates the CO2 in the solution into the degassing cavity 102, and is driven out by the accelerated airflow; in addition, when the removal cylinder 301 rotates, the rotating seat 303h rotates synchronously, the cleaning stirring part is stationary with the sealing seat 303b, and the relative removal cylinder 301 is in a moving state, so that the removal cylinder 301 can be cleaned and the solution inside can be stirred;

[0058] S4, the flow monitoring assembly 2 monitors the data of the liquid flowing through: the monitoring probe one and the monitoring probe two can be temperature monitoring probes and CO2 concentration monitoring probes, which extend into the corresponding section of the solution to obtain relevant data before and after degassing; in addition, temperature adjusting parts are arranged in the rotating pipe 302a and the fixed pipe 303a, and the temperature of the solution is adjusted in sections according to the monitoring results of the temperature monitoring probes; when the data acquisition end collects that the CO2 degassing is not complete, the circulating part 6 can be started, the solution is repeatedly introduced into the S-shaped liquid flow channel, and the CO2 degassing is performed multiple times, and in the degassing process, the CO2 degassing process is assisted by temperature adjustment and gas flow rate adjustment, until the test target is reached.

[0059] S5, the mixed gas capturing CO2 is introduced into a measuring device to measure the captured CO2 data, for example, calcium hydroxide solution, because calcium hydroxide reacts with CO2 to produce a precipitate, the amount of precipitate can be calculated by capturing the amount of precipitate, and the green treatment of CO2 is also realized;

[0060] S6, the captured CO2 data and the collected sample solution data before and after each degassing are used for the auxiliary research of the CO2 degassing process of the sample solution.

[0061] The embodiments of the application are described in detail above in combination with the drawings, but the application is not limited thereto, and various changes can be made within the knowledge of those skilled in the art without departing from the purpose of the application.

Claims

1. A CO2 degassing process auxiliary research test device, characterized in that: include: A test box (1), wherein two groups of partitions (101) divide the internal space of the test box (1) into a degassing chamber (102) located in the middle and installation chambers (103) located on both sides. The test box (1) is provided with an air inlet pipe (105) and an air outlet pipe (106) connected to the degassing chamber (102) at the head and tail, and a liquid inlet pipe (107) and a liquid outlet pipe (108) connected to the installation chamber (103); A plurality of CO2 removal components (3) are arranged along the gas flow direction in the degassing chamber (102). Each group of CO2 removal components (3) rotates through the partitions (101) on both sides. During the rotation, the CO2 in the internal solution is separated into the degassing chamber (102) through membrane technology and driven by the air flow to flow out. The head end of the first group of CO2 removal components (3) is connected to the liquid inlet pipe (107) through the pipe 1 (4), and the tail end of the last group of CO2 removal components (3) is connected to the liquid inlet pipe (107) through the pipe 2 (5); And a circulation monitoring component (2) is connected to the head end and the tail end of two adjacent groups of CO2 removal components (3), and is located in the installation cavity (103) to monitor the data of the liquid flowing through.

2. The CO2 degassing process auxiliary research test device according to claim 1, characterized in that: The CO2 removal component (3) includes a removal cartridge (301) with a carbon dioxide separation membrane; A rotating member (302) is provided at one end of the removal cylinder (301) for driving the rotation thereof and for allowing the solution to enter and exit, and a fixing member (303) is provided at the other end for rotationally connecting with the removal cylinder (301) and for allowing the solution to enter and exit; The circulation monitoring assembly (2) is located between two adjacent groups of rotating parts (302) / two adjacent groups of fixed parts (303), forming an S-shaped liquid flow channel.

3. The CO2 degassing process auxiliary research test device according to claim 2, characterized in that: The rotating member (302) comprises a rotating tube (302a) coaxially connected to the removal cylinder (301) and rotatably arranged on the partition (101); the rotating tube (302a) is connected to the corresponding pipeline 1 (4) / pipeline 2 (5) / circulation monitoring component (2); a gear ring (302b) is arranged on the outside of the rotating tube (302a), and a motor (302d) and a gear (302c) connected to the main shaft of the motor (302d) are arranged on one side; the gear (302c) is meshed with the gear ring (302b).

4. The CO2 degassing process auxiliary research test device according to claim 3, characterized in that: The gear (302c) is located between adjacent stripping cylinders (301) and simultaneously engages with the gear rings (302b) on both sides.

5. The CO2 degassing process auxiliary research test device according to claim 3, characterized in that: The fixing member (303) comprises a rotating seat (303h) detachably connected to the end of the removal cylinder (301); a sealing seat (303b) is rotatably provided on one side of the rotating seat (303h); a cleaning stirring member is provided on one side of the sealing seat (303b) that seals and penetrates the rotating seat (303h) and extends into the interior of the removal cylinder (301); and a fixing tube (303a) is provided on the other side. The rotating seat (303h), the sealing seat (303b) and the fixed tube (303a) are connected in series in sequence and communicate with the corresponding flow monitoring components (2).

6. The CO2 degassing process auxiliary research test device according to claim 5, characterized in that: The cleaning stirring member comprises a stirring frame (303c) that rotates and penetrates a rotating seat (303h); a liquid inlet and outlet head (303g) that is connected to a circulation monitoring component (2) is provided at the lower end of the stirring frame (303c); a mounting frame (303e) with a cleaning brush (303f) is provided at the upper end; and a liquid leakage slag receiving cover (303d) is provided on the side wall.

7. The CO2 degassing process auxiliary research test device according to claim 6, characterized in that: The circulation monitoring assembly (2) comprises a connecting pipe (201) connecting two adjacent groups of rotating pipes (302a) / two groups of fixed pipes (303a); a monitoring box (202) located on the connecting pipe (201); a water pump (203) and a monitoring probe for monitoring the solution are provided on the monitoring box (202).

8. The CO2 degassing process auxiliary research test device according to claim 1, characterized in that: A circulation component (6) is provided between the liquid inlet pipe (107) and the liquid outlet pipe (108); the circulation component (6) comprises a second connecting pipe (601) respectively connected to the liquid inlet pipe (107) and the liquid outlet pipe (108) via a three-way valve; a second monitoring box (602) is located on the second connecting pipe (601); a second water pump (603) is provided on the second monitoring box (602), and a second monitoring probe for monitoring the solution is also provided.

9. The CO2 degassing process auxiliary research test device according to claim 1, characterized in that: The test box (1) is provided with box covers (104) corresponding to the installation cavities (103) on both sides, so as to facilitate maintenance of the equipment in the installation cavities (103).

10. A CO2 degassing process auxiliary research test method, characterized in that: The CO2 degassing process auxiliary research test device according to claim 1 is used, and the method steps are as follows: S1, pre-treating the sample solution in advance; passing the accelerating gas into the degassing chamber (102); S2, the sample solution enters from the liquid inlet pipe (107), passes through the rotating and sequentially connected CO2 removal components (3); S3, the sample solution moves in an S-shaped trajectory, and during the movement, the CO2 in the solution inside the CO2 removal component (3) is repeatedly separated into the degassing chamber (102) through membrane technology, and is driven out by the accelerated airflow; S4, the circulation monitoring component (2) performs data monitoring on the liquid flowing through; The data acquisition end collects the sample solution data before and after each degassing; S5, passing the mixed gas of captured CO2 into the measuring equipment to measure the captured CO2 data; S6. The captured CO2 data and the sample solution data collected before and after each degassing stage are used to assist in the study of the CO2 degassing process of the sample solution.

Citation Information

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