Production device of ultra-fine adipic acid

Abstract

The invention relates to the field of ultra-fine adipic acid production, in particular to an ultra-fine adipic acid production device which comprises a mixing mechanism for processing raw materials, a heating mechanism for heat preservation and a control mechanism for control, the heating mechanism is arranged outside the mixing mechanism in a wrapping mode, and the bottom of the heating mechanism is fixed to a machine base. A control mechanism is installed at the front end of the machine base, a power mechanism for providing power is installed at the top of the mixing mechanism, the stirring and cooling mechanism is used for mixing raw materials, the mixing mechanism is used for providing state adjustment for the stirring and cooling mechanism, and the stirring and cooling mechanism is installed in the mixing mechanism and installed on a main shaft of the power mechanism. The mixing mechanism is installed at the position of a cooling pipe of the stirring and cooling mechanism, and the state matching mechanism is installed at the bottom of the mixing mechanism and used for solving the technical problem that in the stirring production process of ultra-fine adipic acid, crystals separated out are attached to the cooling pipe, so that the production temperature cannot be adjusted in time, and part of raw materials go bad.

Description

Technical Field

[0001] The invention relates to the field of super refined adipic acid production, and in particular to a super refined adipic acid production device. Background Art

[0002] The ultra-fine adipic acid mixing production device is a combination of equipment used to accurately mix adipic acid raw materials with other additives (such as catalysts, stabilizers, other additives, etc.) to produce high-purity ultra-fine adipic acid products. The device needs to meet the production requirements of high precision, high purity, and high stability to ensure that the product quality reaches the ultra-fine standard, and the temperature needs to be accurately controlled to avoid crystallization caused by temperature changes, thereby affecting the local temperature increase and causing some raw materials to deteriorate.

[0003] In the prior art, a Chinese invention with a publication number of CN116371342A discloses a device for preparing adipic acid dihydrazide, in which a structure for scraping off crystals is arranged in the lower chamber, but the volume of the mixing chamber becomes smaller, and stratification occurs at the top and bottom during mixing, making it easier for temperature localization to accumulate. The temperature cannot be diffused in time during the subsequent mixing, causing the raw materials to deteriorate. Summary of the invention

[0004] The invention provides a production device for super refined adipic acid, so as to solve the technical problem that during the stirring production process of super refined adipic acid, precipitated crystals adhere to a cooling pipe, so that the production temperature cannot be adjusted in time, resulting in the deterioration of part of the raw materials.

[0005] The production device of super refined adipic acid of the present invention adopts the following technical scheme: comprising a mixing mechanism for processing raw materials, a heating mechanism for heat preservation and a control mechanism for control, the heating mechanism is wrapped and arranged outside the mixing mechanism, the bottom of the heating mechanism is fixed on the machine base, the front end of the machine base is installed with a control mechanism, the top of the mixing mechanism is installed with a power mechanism for providing power, and also comprises a stirring and cooling mechanism for mixing raw materials and a mixing mechanism for providing state adjustment for the stirring and cooling mechanism, the stirring and cooling mechanism is installed inside the mixing mechanism and installed on the main shaft of the power mechanism, the mixing mechanism is installed at the cooling pipe position of the stirring and cooling mechanism, the state matching mechanism is installed at the bottom of the mixing mechanism, and the top of the mixing mechanism is installed with a state adjustment mechanism for driving the state change of the mixing mechanism;

[0006] The stirring and cooling mechanism includes a stirring frame, and several groups of cross frames are installed horizontally at the upper and lower ends of the stirring frame. The cross frames are arranged in a circular array on the stirring frame. The upper and lower corresponding cross frames form a group, and several cooling pipes are vertically installed on each group of stirring frames. The mixing mechanism includes a spiral blade, and the spiral blade is wrapped on the cooling pipe, and the spiral blade is rotatably connected to the cooling pipe. The upper end of the spiral blade is equipped with a blade power component that drives the spiral blade to rotate, and the bottom of the spiral blade is connected to a bottom matching gear group. The state matching mechanism is used to cooperate with the stirring and cooling mechanism and the bottom matching gear group to change the spiral blade between two states.

[0007] Furthermore, chambers for transmitting coolant are formed inside the stirring frame and the cross frame, and the cooling pipe is connected to the chamber. The first state of the spiral blade is that there is a gap between the spiral blade and the cooling pipe and it can rotate without restriction to assist in stirring the raw materials. The second state of the spiral blade is that it is in close contact with the surface of the cooling pipe and scrapes the surface of the cooling pipe when rotating. A cooling pipe connecting seat is slidably fitted on the top of the stirring frame, and a cooling circulation pipe group is installed on the top of the cooling pipe connecting seat, and the cooling pipe connecting seat is fixedly installed on the sealing cover of the mixing mechanism.

[0008] Furthermore, the blade power assembly includes a top mating gear set, a driving gear, and a mating gear ring. The top mating gear set is fixedly connected to the upper end of the spiral blade. The top mating gear set is composed of a number of meshing gears, wherein a driving gear is arranged on the upper side of one of the gears. The driving gear and its corresponding gear are matched through a transmission gear. Tooth blocks that match the transmission gear are formed on the driving gear and the corresponding gear. A mating gear ring is arranged on the outside of the driving gear and on the bottom surface of the sealing cover. A magnetic block of a state adjustment mechanism is installed on the top of the driving gear. A number of electromagnets are installed in a circular array corresponding to the position of the magnetic block on the sealing cover. The top mating gear set and the bottom mating gear set are rotatably connected to the cooling pipe.

[0009] Furthermore, the driving gear and the transmission gear at the lower side thereof are connected to the cross frame through a pin shaft, and the driving gear slides up and down to cooperate with the gear ring.

[0010] Furthermore, the state matching mechanism includes a supporting spring, an adjusting gear, and a resistance block. The main shaft passes through the stirring frame and a bottom stirring blade is arranged at the bottom. The stirring frame is connected to the main shaft through a spline sliding connection. A supporting spring is arranged between the bottom of the stirring frame and the bottom stirring blade. The adjusting gear is rotatably connected to the outside of the stirring frame. Four resistance blocks are arranged in a circular array corresponding to the position of the adjusting gear in the stirring frame, and an extrusion ring is fixedly connected to the lower position of the resistance block on the main shaft.

[0011] Furthermore, the top surface of the extrusion ring and the end surface of the extrusion ring corresponding to the inner side of the resistance block are both formed with chamfers.

[0012] Furthermore, the resistance block is made of rubber.

[0013] Furthermore, the spiral directions of adjacent spiral blades are opposite, and the material of the spiral blades is copper.

[0014] Furthermore, the gap size between the inner side of the spiral blade and the cooling pipe ranges from 0 mm to 10 mm.

[0015] Furthermore, the mixing mechanism also includes a sealed tank, a sealing cover is fixedly connected to the top of the sealed tank, an external feed pipe is arranged on one side of the sealed tank, a discharge pipe is arranged at the bottom of the sealed tank, and the heating mechanism includes an electric heating insulation tank and a temperature controller wrapped around the outside of the sealed tank.

[0016] The beneficial effects of the present invention are as follows: the present invention adjusts the state of the spiral blades by coordinating the blade power mechanism with the spiral blades arranged on the surface of the cooling tube, so that the spiral blades can change randomly under suitable conditions, thereby improving the replacement between the upper and lower layers of the raw materials and improving the stirring efficiency. If crystallization occurs, the state of the spiral blades can be adjusted in time to clean the surface of the cooling tube, thereby avoiding the problem of raw material deterioration caused by the local temperature being too high and unable to be adjusted in time. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative labor.

[0018] Figure 1 It is a structural schematic diagram of an embodiment of a production device of super refined adipic acid of the present invention;

[0019] Figure 2 A schematic diagram of the internal structure of a sealed tank of an embodiment of a production device for super refined adipic acid of the present invention;

[0020] Figure 3 A schematic diagram of the structure of a stirring and cooling mechanism of an embodiment of a production device for super refined adipic acid of the present invention;

[0021] Figure 4 It is a detailed layout diagram of a stirring and cooling mechanism and a state regulating mechanism of an embodiment of a production device for ultra-fine adipic acid of the present invention;

[0022] Figure 5 It is a schematic diagram of the installation structure of the state matching mechanism of an embodiment of a production device of super refined adipic acid of the present invention;

[0023] Figure 6 It is a schematic diagram of the internal structure of the regulating gear of an embodiment of a production device for super refined adipic acid of the present invention;

[0024] Figure 7 It is a front view of the inside of the regulating gear of an embodiment of a production device of super refined adipic acid of the present invention;

[0025] Figure 8 It is a schematic structural diagram of the first state of the spiral blade when the driving gear is located at a high position in an embodiment of a production device of super refined adipic acid of the present invention;

[0026] Fig. 9 It is a schematic structural diagram of the second state of the spiral blade when the driving gear is located at the lower position in an embodiment of a production device of super refined adipic acid of the present invention;

[0027] Fig.10 The present invention is a schematic diagram of the electromagnet distribution structure of an embodiment of a production device for ultra-fine adipic acid.

[0028] In the figure: 1. mixing mechanism; 2. power mechanism; 3. heating mechanism; 4. control mechanism; 5. stirring and cooling mechanism; 6. mixing mechanism; 7. state matching mechanism; 8. state adjustment mechanism; 11. sealing tank; 12. sealing cover; 13. external feed pipe; 14. discharge pipe; 21. main shaft; 22. bottom stirring blade; 51. stirring frame; 52. cross frame; 53. cooling pipe connecting seat; 54. cooling circulation pipe group; 55. cooling pipe; 61. spiral blade; 62. top matching gear group; 63. driving gear; 64. bottom matching gear group; 65. matching gear ring; 71. support spring; 72. adjusting gear; 73. resistance block; 74. extrusion ring; 81. magnetic block; 82. electromagnet. DETAILED DESCRIPTION

[0029] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0030] An embodiment of a production device for super refined adipic acid of the present invention is as follows Figures 1 to 10As shown, it includes a mixing mechanism 1 for processing raw materials, a heating mechanism 3 for heat preservation, and a control mechanism 4 for control, the heating mechanism 3 is wrapped and arranged outside the mixing mechanism 1, the bottom of the heating mechanism 3 is fixed on the machine base, the control mechanism 4 is installed at the front end of the machine base, the top of the mixing mechanism 1 is installed with a power mechanism 2 for providing power, and also includes a stirring and cooling mechanism 5 for mixing raw materials and a mixing mechanism 6 for providing state adjustment for the stirring and cooling mechanism 5, the stirring and cooling mechanism 5 is installed inside the mixing mechanism 1 and installed on the main shaft 21 of the power mechanism 2, the mixing mechanism 6 is installed at the cooling pipe 55 position of the stirring and cooling mechanism 5, the state matching mechanism 7 is installed at the bottom of the mixing mechanism 6, and the top of the mixing mechanism 6 is installed with a state adjustment mechanism 8 for driving the state change of the mixing mechanism 6;

[0031] The stirring and cooling mechanism 5 includes a stirring frame 51, and three groups of horizontal frames 52 are installed horizontally at the upper and lower ends of the stirring frame 51. The horizontal frames 52 are arranged in a circular array on the stirring frame 51. The upper and lower corresponding horizontal frames 52 form a group, and two cooling pipes 55 are vertically installed on each group of stirring frames 51. The mixing mechanism 6 includes a spiral blade 61, and the spiral blade 61 is wrapped around the cooling pipe 55, and the spiral blade 61 is rotatably connected to the cooling pipe 55. The upper end of the spiral blade 61 is equipped with a blade power component that drives it to rotate. The bottom of the spiral blade 61 is connected to a bottom matching gear set 64. The state matching mechanism 7 is used to cooperate with the stirring and cooling mechanism 5 and the bottom matching gear set 64 to change the spiral blade 61 between two states.

[0032] In this embodiment, chambers for transmitting coolant are formed inside the stirring frame 51 and the cross frame 52, and the cooling pipe 55 is connected to the chamber. The first state of the spiral blade 61 is that there is a gap between it and the cooling pipe 55 and it can rotate without restriction to assist in stirring the raw materials. The second state of the spiral blade 61 is that it is in close contact with the surface of the cooling pipe 55 and scrapes the surface of the cooling pipe 55 when rotating. The top of the stirring frame 51 is slidably matched with a cooling pipe connecting seat 53, and a cooling circulation pipe group 54 is installed on the top of the cooling pipe connecting seat 53. The cooling pipe connecting seat 53 is fixedly installed on the sealing cover 12 of the mixing mechanism 1.

[0033] In this embodiment, the blade power assembly includes a top matching gear set 62, a driving gear 63, and a matching gear ring 65. The top matching gear set 62 is fixedly connected to the upper end of the spiral blade 61. The top matching gear set 62 is composed of two meshing gears, one of which is provided with a driving gear 63 on the upper side. The driving gear 63 and its corresponding gear are matched through a transmission gear. The driving gear 63 and the corresponding gear are formed with tooth blocks that match the transmission gear. A matching gear ring 65 is provided on the outer side of the driving gear 63 and on the bottom surface of the sealing cover 12. A magnetic block 81 of the state adjustment mechanism 8 is installed on the top of the gear 63, and a plurality of electromagnets 82 are installed in a circular array corresponding to the position of the magnetic block 81 on the sealing cover 12. The top matching gear set 62 and the bottom matching gear set 64 are rotatably connected to the cooling pipe 55. When the stirring frame 51 and the cross frame 52 drive the top matching gear set 62 and the driving gear 63 to rotate, the driving gear 63 cooperates with the matching gear ring 65, so that the rotating power of the driving gear 63 drives the top matching gear set 62 to rotate through the transmission gear, so that the spiral blade 61 rotates and stirs the raw materials.

[0034] In this embodiment, the driving gear 63 and the transmission gear below it are connected to the cross frame 52 via a pin shaft, and the driving gear 63 slides up and down to cooperate with the gear ring 65.

[0035] In this embodiment, the state matching mechanism 7 includes a supporting spring 71, an adjusting gear 72, and a resistance block 73. The main shaft 21 passes through the stirring frame 51 and is provided with a bottom stirring blade 22 at the bottom. The stirring frame 51 is slidably connected to the main shaft 21 through a spline. A supporting spring 71 is provided between the bottom of the stirring frame 51 and the bottom stirring blade 22. The adjusting gear 72 is rotatably connected to the outside of the stirring frame 51. Four resistance blocks 73 are provided in a circular array corresponding to the position of the adjusting gear 72 in the stirring frame 51. An extrusion ring 74 is fixedly connected to the lower position of the main shaft 21 corresponding to the resistance block 73. When the stirring frame 51 descends, the stirring frame 51 is The resistance block 73 at the bottom is squeezed by the extrusion ring 74. At this time, the resistance block 73 expands outward and frictionally cooperates with the support spring 71. After the support spring 71 obtains the friction force, the rotation speed slows down, and the same resistance is transmitted to the bottom matching gear set 64. Then, the bottom of the spiral blade 61 obtains resistance, and the top of the spiral blade 61 obtains the power of the top matching gear set 62 to continue to rotate. Due to the spring characteristics, when the spring transitions to the spiral direction and twists, the inner diameter of the spiral blade 61 will shrink inward. At this time, the inner side of the spiral blade 61 is in close contact with the cooling tube 55 and rotates at the same time, so that the crystals adhered to the surface of the cooling tube 55 are scraped off.

[0036] In this embodiment, the top surface of the extrusion ring 74 and the end surface of the extrusion ring 74 corresponding to the inner side of the resistance block 73 are both formed with chamfers to facilitate the cooperation with the resistance block 73 when the resistance block 73 descends.

[0037] In this embodiment, the resistance block 73 is made of rubber.

[0038] In this embodiment, the spiral directions of adjacent spiral blades 61 are opposite. The spiral blades 61 are made of copper. Copper can conduct temperature better and has toughness and is easy to deform.

[0039] In this embodiment, the gap size between the inner side of the spiral blade 61 and the cooling pipe 55 ranges from 0 mm to 10 mm.

[0040] In this embodiment, the mixing mechanism 1 also includes a sealed tank 11, a sealing cover 12 is fixedly connected to the top of the sealed tank 11, an external feed pipe 13 is arranged on one side of the sealed tank 11, and a discharge pipe 14 is arranged at the bottom of the sealed tank 11. The heating mechanism 3 includes an electric heating insulation tank and a temperature controller wrapped around the outside of the sealed tank 11.

[0041] The working principle is as follows: after the raw materials are poured into the sealed tank 11, the motor of the power mechanism 2 is started, and the stirring frame 51 is driven to rotate as a whole through the main shaft 21. At this time, the driving gear 63 cooperates with the matching gear ring 65, so that the rotating power of the driving gear 63 drives the top matching gear set 62 to rotate through the transmission gear, so that the spiral blade 61 rotates and stirs the raw materials. At this time, the spiral blade 61 is in the first state, and there is a gap between the spiral blade 61 and the cooling tube 55 and it rotates without restriction, thereby assisting the stirring of the raw materials;

[0042] At the same time, the power-on state of the electromagnet 82 is controlled by detecting the internal raw material temperature. For example, by controlling the electromagnet 82 to generate the same magnetic pole as the magnetic block 81, the top matching gear set 62 is made to descend, and the entire stirring and cooling mechanism 5 is descended. When descending, the resistance block 73 inside the stirring frame 51 is squeezed by the extrusion ring 74. At this time, the resistance block 73 expands outward and rubs with the support spring 71. After the support spring 71 obtains the friction force, the rotation speed slows down, and the same resistance is transmitted to the bottom matching gear set 64. Then, the bottom of the spiral blade 61 obtains resistance, and the top of the spiral blade 61 obtains the power of the top matching gear set 62 to continue to rotate. Due to the spring characteristics, when the spring is twisted in the spiral direction, the inner diameter of the spiral blade 61 will shrink inward. At this time, the inner side of the spiral blade 61 is tightly attached to the cooling tube 55 and rotates at the same time, so that the crystals attached to the surface of the cooling tube 55 are scraped off.

[0043] Alternatively, the circular array of electromagnets 82 can be controlled to intermittently change the magnetic poles, so that the stirring frame 51 floats up and down during rotation, thereby randomly changing the state of the spiral blade 61, and also improving the stirring power. The cooling tube 55 does not pass through the cooling chamber under normal conditions, and the sealed tank 11 only ensures the mixing processing of the super-fine adipic acid through the heating of the heating mechanism 3. If a sudden temperature rise occurs, the cooling tube 55 is used to mix with cooling water. During mixing, due to the sudden drop in temperature, the raw materials may crystallize rapidly, resulting in instantaneous crystallization on the surface of the cooling tube 55. At this time, the weight caused by the instantaneous crystallization on the surface of the cooling tube 55 increases, and the stirring frame 51 sinks, so that the spiral blade 61 also enters the second state.

[0044] The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims

1. A production device for ultra-fine adipic acid, comprising a mixing mechanism (1) for processing raw materials, a heating mechanism (3) for heat preservation, and a control mechanism (4) for control, wherein the heating mechanism (3) is wrapped and arranged outside the mixing mechanism (1), the bottom of the heating mechanism (3) is fixed on a machine base, the front end of the machine base is equipped with a control mechanism (4), and the top of the mixing mechanism (1) is equipped with a power mechanism (2) for providing power, characterized in that: It also includes a stirring and cooling mechanism (5) for mixing raw materials and a mixing mechanism (6) for providing state adjustment for the stirring and cooling mechanism (5), wherein the stirring and cooling mechanism (5) is installed inside the mixing mechanism (1) and on the main shaft (21) of the power mechanism (2), the mixing mechanism (6) is installed at the cooling pipe (55) position of the stirring and cooling mechanism (5), the state matching mechanism (7) is installed at the bottom of the mixing mechanism (6), and a state adjustment mechanism (8) for driving the mixing mechanism (6) to change its state is installed at the top of the mixing mechanism (6); The stirring and cooling mechanism (5) comprises a stirring frame (51), wherein a plurality of groups of horizontal frames (52) are transversely mounted at the upper and lower ends of the stirring frame (51), wherein the horizontal frames (52) are arranged in a circular array on the stirring frame (51), wherein the horizontal frames (52) corresponding to the upper and lower ends form a group, and wherein a plurality of cooling pipes (55) are vertically mounted on each group of stirring frames (51); the mixing mechanism (6) comprises a spiral blade (61), wherein the spiral blade (61) is wrapped around the cooling pipe (55), and the spiral blade (61) is rotatably connected to the cooling pipe (55), wherein a blade power assembly driving the spiral blade (61) is mounted on the upper end of the spiral blade (61) and driven to rotate, and a bottom matching gear set (64) is connected to the bottom of the spiral blade (61); and a state matching mechanism (7) is used to match the stirring and cooling mechanism (5) and the bottom matching gear set (64) to change the spiral blade (61) between two states.

2. The production device of super refined adipic acid according to claim 1, characterized in that: The stirring frame (51) and the cross frame (52) are both internally formed with a chamber for transmitting cooling liquid, and the cooling pipe (55) is connected to the chamber. The first state of the spiral blade (61) is that there is a gap between the spiral blade (61) and the cooling pipe (55) and the spiral blade (61) can rotate without restriction to assist in stirring the raw materials. The second state of the spiral blade (61) is that it is in close contact with the surface of the cooling pipe (55) and scrapes the surface of the cooling pipe (55) when rotating. The top of the stirring frame (51) is slidably matched with a cooling pipe connecting seat (53), and a cooling circulation pipe group (54) is installed on the top of the cooling pipe connecting seat (53). The cooling pipe connecting seat (53) is fixedly installed on the sealing cover (12) of the mixing mechanism (1).

3. A production device for super refined adipic acid according to claim 2, characterized in that: The blade power assembly comprises a top matching gear set (62), a driving gear (63), and a matching gear ring (65). The top matching gear set (62) is fixedly connected to the upper end of the spiral blade (61). The top matching gear set (62) is composed of a plurality of meshing gears, wherein a driving gear (63) is arranged on the upper side of one of the gears. The driving gear (63) and its corresponding gear are matched through a transmission gear. The driving gear (63) and the corresponding gear are formed with tooth blocks matching the transmission gear. A matching gear ring (65) is arranged outside the driving gear (63) and on the bottom surface of the sealing cover (12). A magnetic block (81) of a state adjustment mechanism (8) is installed on the top of the driving gear (63). A plurality of electromagnets (82) are installed in a circumferential array corresponding to the position of the magnetic block (81) on the sealing cover (12). The top matching gear set (62) and the bottom matching gear set (64) are rotatably connected to the cooling pipe (55).

4. The production device of super refined adipic acid according to claim 3, characterized in that: The driving gear (63) and the transmission gear on the lower side thereof are connected to the cross frame (52) via a pin shaft, and the driving gear (63) slides up and down to cooperate with the gear ring (65).

5. The production device of super refined adipic acid according to claim 4, characterized in that: The state matching mechanism (7) comprises a supporting spring (71), an adjusting gear (72), and a resistance block (73); the main shaft (21) penetrates the stirring frame (51) and is provided with a bottom stirring blade (22) at the bottom; the stirring frame (51) is slidably connected to the main shaft (21) via a spline; a supporting spring (71) is provided between the bottom of the stirring frame (51) and the bottom stirring blade (22); the adjusting gear (72) is rotatably connected to the outside of the stirring frame (51); four resistance blocks (73) are provided in a circular array in the stirring frame (51) corresponding to the position of the adjusting gear (72); and an extrusion ring (74) is fixedly connected to the main shaft (21) at a position below the resistance block (73).

6. The production device of super refined adipic acid according to claim 5, characterized in that: The top surface of the extrusion ring (74) and the inner side of the resistance block (73) corresponding to the end surface of the extrusion ring (74) are both formed with chamfers.

7. The production device of super refined adipic acid according to claim 6, characterized in that: The material of the resistance block (73) is rubber.

8. The production device of super refined adipic acid according to claim 3, characterized in that: The spiral directions of adjacent spiral blades (61) are opposite, and the material of the spiral blades (61) is copper.

9. The production device of super refined adipic acid according to claim 8, characterized in that: The size of the gap between the inner side of the spiral blade (61) and the cooling tube (55) ranges from 0 mm to 10 mm.

10. The production device of super refined adipic acid according to claim 2, characterized in that: The mixing mechanism (1) also includes a sealed tank (11), a sealed cover (12) fixedly connected to the top of the sealed tank (11), an external feed pipe (13) provided on one side of the sealed tank (11), and a discharge pipe (14) provided at the bottom of the sealed tank (11), and the heating mechanism (3) includes an electric heating insulation tank and a temperature controller wrapped around the outside of the sealed tank (11).

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