Catalyst unloading device and unloading system for methanol synthesis reactor
By designing a fully automatic catalyst discharge device for methanol synthesis reactor, the safety hazards and problems of missing passivation operations in the prior art are solved, and efficient and safe collection of catalysts are achieved.
Patent Information
- Application Number
- CN202510521914.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-04-24
- Publication Date
- 2025-05-30
- Estimated Expiration
- 2045-04-24
AI Technical Summary
In the prior art, there are safety hazards in the catalyst unloading process of methanol synthesis reactors. A large amount of heat may be generated when the catalyst falls, and there is a lack of passivation operation, which leads to a dangerous catalyst unloading process.
A fully automatic catalyst discharge device is designed, including a vertical box frame, a first horizontal box frame, a second horizontal box frame, a driving mechanism and a catalyst collection mechanism. The second sliding plate is made into an L-shaped operation through the driving mechanism, and the catalyst is dropped into the passivation reaction chamber for passivation reaction, and the catalyst is cooled and dusted through the spray mechanism.
The automatic stable fall and passivation reaction of the catalyst is realized, and the drop rate of the catalyst discharge is controlled to ensure that the catalyst is collected more efficiently and safely, reducing manpower operations and improving safety.
Smart Images

Figure CN120054330A_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of catalyst discharging, and particularly relates to a catalyst discharging device and a discharging system for a methanol synthesis reactor. Background Art
[0002] The catalysts of two series of methanol synthesis reactors are Clariant's copper-based catalysts for methanol synthesis. So far, the service life has reached the end of its useful life, and the reaction activity cannot meet the production requirements. Now, according to the production requirements, new catalysts need to be replaced. Since they are in a reduced state, they are extremely prone to oxidation reactions and combustion when encountering air. Therefore, before discharging the synthesis catalyst, it is necessary to passivate it first, and second, control the flow rate during the catalyst discharging process, and cool and dust-remove the waste catalyst in a timely manner.
[0003] For example, in the prior art, Chinese Patent Application No. 201921159968.3, a structure of a catalyst discharging port of a methanol synthesis tower reactor, does not perform passivation operations, which is very unsafe. Moreover, a large amount of heat may be generated when the catalyst falls, and it is relatively dangerous for personnel to manually open and close the catalyst discharging.
[0004] Therefore, we designed a catalyst discharging device and a discharging system for a methanol synthesis reactor, which can make the catalyst automatically and stably fall into the passivation reaction chamber and carry out the passivation reaction. Then, after the passivation reaction is completed, the falling speed of the catalyst discharging can be controlled to make the catalyst collected more efficiently and safely. Moreover, this device is fully automatic operation, saving manpower and can be operated safely, and can push out the catalyst better. Summary of the Invention
[0005] The technical problem to be solved by the present invention is to overcome the defects existing in the prior art. The present invention provides a catalyst discharging device and a discharging system for a methanol synthesis reactor, which can make the catalyst automatically and stably fall into the passivation reaction chamber and carry out the passivation reaction. Then, after the passivation reaction is completed, the falling speed of the catalyst discharging can be controlled to make the catalyst collected more efficiently and safely. Moreover, this device is fully automatic operation, saving manpower and can be operated safely, and can push out the catalyst better.
[0006] To solve the above technical problems, the technical solution adopted by the present invention is: a catalyst discharging device for a methanol synthesis reactor, comprising: A vertical box frame, the top of the vertical box frame is installed and communicated with the discharging hole of the methanol synthesis reactor, and a catalyst collection mechanism is installed at the bottom of the vertical box frame; A first horizontal box frame is communicated with the left side of the middle part of the vertical box frame. A first limiting slide plate is fixedly connected inside the first horizontal box frame. A second sliding plate is slidably connected on the first limiting slide plate in a limiting manner. A plug plate for the discharging port of the methanol synthesis reactor is fixedly connected to the top of the second sliding plate close to the right side; A transverse baffle is connected to the inner bottom of the first horizontal box frame in a limited sliding manner. A vertical baffle is fixedly connected to the bottom of the first limiting sliding plate near the right side. The transverse baffle is connected to the bottom of the vertical baffle in a sealed sliding manner. The inner wall of the first horizontal box frame is connected to the transverse baffle through an elastic telescopic member; A water inlet pipe communicates with the middle part of the vertical box frame; A driving mechanism, which enables the second sliding plate to perform an L-shaped movement. When the second sliding plate performs a vertical movement, the plug plate of the methanol synthesis reactor discharge port is removed from the top of the vertical box frame and the discharge hole of the methanol synthesis reactor is blocked; when the second sliding plate moves horizontally to the first preset position, the plug plate of the methanol synthesis reactor discharge port, the second sliding plate, the first limiting sliding plate, the inner wall of the vertical box frame, the vertical baffle, and the transverse baffle form a passivation reaction chamber to perform passivation operation by introducing water through the water inlet pipe. After passivation is completed, the second sliding plate moves horizontally and drives the transverse baffle to move to release the passivation space so that the catalyst can be safely removed.
[0007] Furthermore, a flange is fixedly installed outside the top of the vertical box frame, and a plurality of mounting holes are provided on the flange for detachable installation with the discharge port at the discharge hole of the methanol synthesis reactor.
[0008] Furthermore, the catalyst collection mechanism includes an aggregate conical cylinder. The bottom of the vertical box frame is in an open shape, and an aggregate conical cylinder is fixedly installed at the bottom of the vertical box frame. A discharge pipe is communicated and installed at the bottom of the aggregate conical cylinder, and the discharge pipe is placed inside the barrel for enabling the catalyst to safely enter the barrel; It further includes a spraying mechanism for performing spraying operation on the catalyst in the barrel.
[0009] Furthermore, the spraying mechanism includes a water pump, a water tank, a support rod, and a spray head. An auxiliary pipe is fixedly installed on the support rod, and a spray head is fixedly installed at the bottom of the auxiliary pipe. The spray head faces the inside of the barrel. A first pipe and a second pipe are installed on the water pump. The side of the first pipe away from the water pump is placed inside the water tank, and the side of the second pipe away from the water pump is communicated with the auxiliary pipe.
[0010] Furthermore, a water inlet cover is provided at the water inlet of the top of the water tank.
[0011] Furthermore, the driving mechanism includes a first sliding plate. The first limiting sliding plate is connected to the first sliding plate and the second sliding plate in a limited sliding manner through the first limiting chute on it. An articulated rod is hinged between the first sliding plate and the second sliding plate. An elastic member is connected between the first sliding plate and the second sliding plate, so that when the second sliding plate and the plug plate of the methanol synthesis reactor discharge port are pressed against the right inner wall of the vertical box frame, the plug plate of the methanol synthesis reactor discharge port and the second sliding plate move upward to block the discharge hole of the methanol synthesis reactor; A push plate is fixedly connected to the left bottom of the second sliding plate, and an auxiliary extrusion plate is fixedly connected to the left top of the transverse baffle. When the second sliding plate moves leftward on the first limiting sliding plate, it drives the push plate to move leftward to extrude the auxiliary extrusion plate, causing the transverse baffle to be gradually opened; It further includes a moving mechanism for moving the first sliding plate.
[0012] Furthermore, a guide post is fixedly connected between the first limiting sliding plate and the inner wall of the vertical box frame.
[0013] Furthermore, the moving mechanism includes a second horizontal box frame. The second horizontal box frame is fixedly connected to the bottom of the first horizontal box frame. A threaded rod is rotatably limited between the two side walls of the second horizontal box frame. A second limiting sliding plate is threadedly connected to the outer wall of the threaded rod. The top of the second limiting sliding plate is slidably limited in a second limiting chute opened at the inner bottom of the first horizontal box frame. The top of the second limiting sliding plate is fixedly connected to the first sliding plate for driving the first sliding plate to move. It further includes a small motor, and the power output end of the small motor is connected to the threaded rod.
[0014] Furthermore, the front of the second horizontal box frame is open, which is convenient for determining the positions of the blanking port plug plate and the second sliding plate of the current methanol synthesis reactor.
[0015] A catalyst unloading system for a methanol synthesis reactor applies the above-mentioned catalyst unloading device for a methanol synthesis reactor, and includes: A blanking connection module, which includes a vertical box frame, and the vertical box frame is connected to the blanking hole of the methanol synthesis reactor through a flange at the top; A catalyst collection module, which is communicated with the bottom of the vertical box frame for collecting the catalyst in the vertical box frame; A spraying module, which sprays and cools the catalyst collection module; A plugging module, which is placed in the blanking connection module for plugging or opening the blanking hole of the methanol synthesis reactor; A passivation reaction chamber module, which is placed in the blanking connection module for performing a passivation reaction on the catalyst flowing into the passivation reaction chamber module after the blanking hole of the methanol synthesis reactor is opened; An unloading module, which is placed in the blanking connection module for enabling the catalyst after the passivation reaction to enter the catalyst collection module.
[0016] Compared with the prior art, the beneficial effects of the present invention include: The blanking port plug plate of the methanol synthesis reactor of this device can perform an L-shaped movement to plug the blanking hole of the methanol synthesis reactor, realizing efficient and stable plugging operation; When the catalyst needs to be unloaded, the second sliding plate is placed on top of the first limiting sliding plate, and the blanking port plug of the methanol synthesis reactor, the second sliding plate and the right side of the first horizontal box frame are parallel. The right side of the blanking port plug of the methanol synthesis reactor, the right side of the second sliding plate, the right side of the first limiting sliding plate, the right side of the vertical baffle, the top of the horizontal baffle, the rear inner wall of the vertical box frame, the right inner wall of the vertical box frame, and the front inner wall of the vertical box frame form a passivation reaction chamber, so that the dropped catalyst is placed in the passivation reaction chamber, and water is added through the water inlet pipe to make the catalyst undergo a passivation reaction. And when the blanking port plug of the methanol synthesis reactor moves to the left, the blanking port plug of the methanol synthesis reactor cooperates with the upper inner wall of the first horizontal box frame to make the catalyst fall better into the passivation reaction chamber; After the passivation reaction is completed, continue to move the second sliding plate to the left to make the horizontal baffle move to the left. By adjusting the opening degree of the horizontal baffle, the feeding speed of the catalyst is controlled, so that the catalyst can be better collected, and the horizontal baffle cooperates with the vertical baffle to make the passivated catalyst be well pushed out and enter the barrel body. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] The disclosure of the present invention will be described with reference to the accompanying drawings. It should be understood that the drawings are only for illustrative purposes and are not intended to limit the scope of protection of the present invention. In the drawings, the same reference numerals are used to refer to the same components. Among them: Figure 1 It is a schematic structural diagram of the first perspective of the front view of the first horizontal box frame and the vertical box frame of the present invention; Figure 2 It is a schematic structural diagram of the second perspective of the front view of the first horizontal box frame and the vertical box frame of the present invention; Figure 3 It is a schematic structural diagram of the third perspective of the front view of the first horizontal box frame and the vertical box frame of the present invention; Figure 4 It is a schematic structural diagram of the first perspective of the whole of the present invention; Figure 5 It is a schematic structural diagram of the second perspective of the whole of the present invention; Figure 6 For the present invention Figure 1 Upper enlarged structural diagram; Figure 7 For the present invention Figure 2 Upper enlarged structural diagram; Figure 8 It is a schematic cross-sectional structure diagram of the elastic telescopic member of the present invention Reference numerals in the figure: 1, first horizontal box frame; 2, second horizontal box frame; 3, vertical box frame; 4, aggregate conical cylinder; 5, discharge pipe; 6, flange; 7, barrel body; 8, first limit sliding plate; 9, water tank; 10, water pump; 11, first pipe; 12, second pipe; 13, support rod; 14, auxiliary pipe; 15, small motor; 16, first limit chute; 17, first sliding plate; 18, elastic member; 19, hinged rod; 20, methanol synthesis reactor discharge port plugging plate; 21, guide post; 22, water inlet pipe; 23, vertical baffle; 24, horizontal baffle; 25, auxiliary extrusion plate; 26, push plate; 28, second limit chute; 29, threaded rod; 30, second limit sliding plate; 31, spray head; 32, water inlet tank cover; 33, mounting hole; 34, second sliding plate; 35, elastic telescopic member; 351, telescopic sliding sleeve; 352, spring; 353, telescopic head. Detailed implementation manners
[0018] It is easy to understand that according to the technical solution of the present invention, without changing the essence of the present invention, those of ordinary skill in the art can propose various structural forms and implementation manners that can be mutually replaced. Therefore, the following detailed implementation manners and the accompanying drawings are only exemplary descriptions of the technical solution of the present invention, and should not be regarded as all of the present invention or as a limitation or restriction on the technical solution of the present invention. Embodiment
[0019] Focus on reference Figure 1 , Figure 2 , Figure 4 , Figure 5 , the vertical box frame 3 is in the shape of a box or a cylinder with an open top. Preferably, it is in the shape of a box with open top and bottom, and the middle part on the left side of the vertical box frame 3 is open. The first horizontal box frame 1 is in the shape of a box with an open right side. The open right side of the first horizontal box frame 1 is communicated with the open left side of the vertical box frame 3. It looks like a T-shaped member from the outside of the device.
[0020] Focus on reference Figure 5 , a flange 6 is fixedly installed on the outer wall of the top of the vertical box frame 3, and a plurality of mounting holes 33 are formed in the flange 6. The plurality of mounting holes 33 are evenly distributed, so that the flange 6 can be detachably installed on the discharge hole of the methanol synthesis reactor, thus facilitating the cleaning or replacement of the device.
[0021] Focus on reference Figure 6 and Figure 7 , a first limit sliding plate 8 is fixedly connected horizontally in the middle of the inner wall of the first horizontal box frame 1. A first limit chute 16 is formed in the first limit sliding plate 8. A first sliding plate 17 and a second sliding plate 34 are slidably connected left and right on the first limit chute 16. It should be noted that the right side of the first limit sliding plate 8 is closed, which is convenient for the subsequent formation of a passivation reaction chamber.
[0022] Focus on referenceFigure 6 and Figure 7 There are four articulated rods 19 hinged between the first sliding plate 17 and the second sliding plate 34, two at the front and two at the back, which are used to stably drive the second sliding plate 34 and the methanol synthesis reactor discharge port plug 20 to perform vertical movements. It should be noted that the right side of the second sliding plate 34 is longer and the left side is shorter, so that it is convenient to construct a passivation reaction chamber on the right side of the second sliding plate 34, and it is convenient to be hinged or connected in other forms on the left side of the second sliding plate 34, as long as the hinge and the construction of the passivation reaction chamber are satisfied.
[0023] For key reference Figure 6 An elastic member 18 is fixedly connected between the first sliding plate 17 and the second sliding plate 34.
[0024] For key reference Figure 6 and Figure 7 The methanol synthesis reactor discharge port plug 20 is fixedly installed at the top right of the second sliding plate 34. The cross-section of the methanol synthesis reactor discharge port plug 20 is the same as the inner cross-section of the vertical box frame 3, so that the methanol synthesis reactor discharge port plug 20 can be sealed and removed from above the vertical box frame 3 and block the methanol synthesis reactor discharge hole.
[0025] For key reference Figure 6 The second limit sliding plate 30 is fixedly installed at the bottom of the first sliding plate 17. The second limit sliding plate 30 penetrates through the first limit sliding groove 16 and the second limit sliding groove 28 opened on the lower inner wall of the first horizontal box frame 1.
[0026] For key reference Figure 6 The second horizontal box frame 2 is fixedly installed at the bottom of the first horizontal box frame 1. The front of the second horizontal box frame 2 is open, which is convenient for determining the positions of the methanol synthesis reactor discharge port plug 20 and the second sliding plate 34.
[0027] For key reference Figure 7 A threaded rod 29 is rotatably connected between the two inner walls of the second horizontal box frame 2 with limited movement. The second limit sliding plate 30 is threadedly connected to the outer wall of the threaded rod 29. Since the second limit sliding plate 30 is slidably connected to the second limit sliding groove 28 with limited movement, the rotating threaded rod 29 can drive the second limit sliding plate 30 to move left and right.
[0028] For key reference Figure 7 A small motor 15 is fixedly installed on the outer wall of the second horizontal box frame 2. The power output end of the small motor 15 is connected to the threaded rod 29, so that starting the small motor 15 drives the second limit sliding plate 30 and the first sliding plate 17 to move left and right, thereby driving the second sliding plate 34 and the methanol synthesis reactor discharge port plug 20 to perform an L-shaped movement.
[0029] It should be noted that the right side position of the first limit slide plate 8 is horizontal with the right side position of the first horizontal box frame 1. A guide post 21 is fixedly connected between the right side of the first limit slide plate 8 and the vertical box frame 3, which plays a role in guiding the second slide plate 34 and maintaining the stability of the device.
[0030] Key reference Figure 7 , a vertical baffle 23 is fixedly connected to the bottom of the right side of the first limit slide plate 8, and a heat-resistant and sealable elastic pad is arranged at the bottom of the vertical baffle 23.
[0031] Key reference Figure 7 and Figure 8 , a horizontal baffle 24 is connected to the inner bottom of the first horizontal box frame 1 in a limited sliding manner. The horizontal baffle 24 can be slidably connected to the bottom of the vertical baffle 23 left and right, and the vertical baffle 23 can seal the top of the horizontal baffle 24 through the elastic pad. An elastic telescopic member 35 is fixedly connected to the left inner wall of the first horizontal box frame 1. The elastic telescopic member 35 in the contracted state is a telescopic rod with a spring 352 inside. The elastic telescopic member 35 includes a telescopic sleeve 351. A telescopic head 353 is connected to the telescopic sleeve 351 in a limited sliding manner, and a spring 352 is fixedly connected between the telescopic head 353 and the inner bottom of the telescopic sleeve 351. That is, it normally maintains an extended action under the action of the spring 352 and is in a contracted state when the telescopic head 353 is squeezed and the spring 352 is squeezed. The telescopic head 353 on the right side of the elastic telescopic member 35 is connected to the horizontal baffle 24, so that the right side of the horizontal baffle 24 normally presses against the right inner wall of the vertical box frame 3. That is, when the rightmost sides of the second slide plate 34 and the methanol synthesis reactor discharge port plug 20 are parallel to the rightmost side of the first horizontal box frame 1, the right side of the methanol synthesis reactor discharge port plug 20, the right side of the second slide plate 34, the right side of the first limit slide plate 8, the right side of the vertical baffle 23, the top of the horizontal baffle 24, the rear inner wall of the vertical box frame 3, the right inner wall of the vertical box frame 3, and the front inner wall of the vertical box frame 3 form a passivation reaction chamber.
[0032] A water inlet pipe 22 is connected to the middle of the vertical box frame 3. The horizontal height of the water inlet pipe 22 is higher than that of the horizontal baffle 24. After the passivation reaction chamber is formed, water is introduced through the water inlet pipe 22 for catalyst passivation reaction.
[0033] Embodiment 2: On the basis of Embodiment 1, a technical means for automatically removing the horizontal baffle 24 from the passivation reaction chamber is added.
[0034] Key reference Figure 6 and Figure 7 , an auxiliary extrusion plate 25 is fixedly connected to the top of the left side of the horizontal baffle 24, and the telescopic head 353 of the elastic telescopic member 35 is fixedly connected to the auxiliary extrusion plate 25. A push plate 26 is fixedly connected to the bottom of the left side of the second slide plate 34. The push plate 26 penetrates through the first limit chute 16, and the push plate 26 is placed on the right side of the auxiliary extrusion plate 25.
[0035] It should be noted that when the push plate 26 moves upward following the second sliding plate 34, the push plate 26 will not be squeezed against the vertical baffle 23, because the left side of the second sliding plate 34 is longer, and when the plug plate 20 at the discharge port of the methanol synthesis reactor moves upward within the vertical box frame 3, the left side of the second sliding plate 34 remains within the first horizontal box frame 1.
[0036] In summary, when the second sliding plate 34 moves leftward to drive the push plate 26 to move leftward, the push plate 26 pushes the auxiliary extrusion plate 25, causing the horizontal baffle 24 to be gradually opened, and the opening degree of the horizontal baffle 24 is adjustable, thus facilitating the adjustment of the discharge speed of the catalyst.
[0037] Other structures are the same as those in the first embodiment.
[0038] Embodiment 3: On the basis of Embodiment 2, technical means for better collecting the catalyst are added.
[0039] Focus on referring to Figure 3 , a collecting conical cylinder 4 is fixedly installed at the bottom of the vertical box frame 3, and a discharge pipe 5 is connected and installed at the bottom of the collecting conical cylinder 4. The discharge pipe 5 is placed inside the barrel 7, and is used to enable the catalyst to safely enter the barrel 7.
[0040] An auxiliary pipe 14 is fixedly installed on the support rod 13. A spray head 31 is fixedly installed at the bottom of the auxiliary pipe 14, and the spray head 31 faces the inside of the barrel 7. A first pipe 11 and a second pipe 12 are installed on the water pump 10. The side of the first pipe 11 away from the water pump 10 is placed inside the water tank 9, and the side of the second pipe 12 away from the water pump 10 is communicated with the auxiliary pipe 14.
[0041] Other structures are the same as those in Embodiment 2.
[0042] In this embodiment, first, the device is fixedly installed with the discharge hole of the methanol synthesis reactor through the flange 6. Then, the small motor 15 is started to make the second limit sliding plate 30 and the first sliding plate 17 move rightward. At this time, under the action of the elastic member 18 and the hinge rod 19, the first sliding plate 17 drives the second sliding plate 34 and the plug plate 20 at the discharge port of the methanol synthesis reactor to move rightward. After the plug plate 20 at the discharge port of the methanol synthesis reactor contacts the inner wall of the vertical box frame 3, at this time, under the action of multiple hinge rods 19 and elastic members 18, the plug plate 20 at the discharge port of the methanol synthesis reactor moves upward and moves to the discharge hole of the methanol synthesis reactor to block it.
[0043] It should be noted that the top of the plug plate 20 at the discharge port of the methanol synthesis reactor is preferably horizontal.
[0044] When the catalyst in the methanol synthesis reactor needs to be unloaded, the small motor 15 is started in reverse at this time. Under the action of the elastic member 18, the plug plate 20 at the discharge port of the methanol synthesis reactor and the second sliding plate 34 move vertically downward and move to the left when the second sliding plate 34 moves to the top of the first limit sliding plate 8. The cooperation between the plug plate 20 at the discharge port of the methanol synthesis reactor and the inner wall of the first horizontal box frame 1 enables the catalyst to fall onto the top of the horizontal baffle 24, thus achieving better material discharge.
[0045] At this time, under the action of the elastic telescopic member 35, the horizontal baffle 24 has sufficient supporting force.
[0046] At this time, the right side of the plug plate 20 at the discharge port of the methanol synthesis reactor, the right side of the second sliding plate 34, the right side of the first limit sliding plate 8, the right side of the vertical baffle 23, the top of the horizontal baffle 24, the rear inner wall of the vertical box frame 3, the right inner wall of the vertical box frame 3, and the front inner wall of the vertical box frame 3 form a passivation reaction chamber. By adding water to the water inlet pipe 22, the catalyst in the passivation reaction chamber undergoes a passivation reaction.
[0047] After the reaction ends, the small motor 15 is continuously started in reverse to make the second sliding plate 34 move to the left. The second sliding plate 34 drives the push plate 26 and the auxiliary extrusion plate 25 to move to the left, so that the horizontal baffle 24 moves to the left. By adjusting the opening degree of the horizontal baffle 24, the falling speed of the catalyst is adjusted. The catalyst enters the barrel 7 from the discharge pipe 5. According to the temperature state of the barrel 7, water is sprayed through the spray head 31 for cooling.
[0048] Finally, the horizontal baffle 24, in cooperation with the vertical baffle 23, pushes all the catalysts on it into the barrel 7, completing the collection operation after the catalyst passivation.
[0049] The technical scope of the present invention is not limited to the content described above. Those skilled in the art can make various deformations and modifications to the above embodiments without departing from the technical idea of the present invention, and these deformations and modifications should all fall within the protection scope of the present invention.
Claims
1. A catalyst unloading device for a methanol synthesis reactor, characterized in that: include: A vertical box frame (3), the top of the vertical box frame (3) being connected to a discharge hole of a methanol synthesis reactor, and a catalyst collecting mechanism being installed at the bottom of the vertical box frame (3); The left side of the middle of the vertical box frame (3) is connected to the first horizontal box frame (1), a first limit slide plate (8) is fixedly connected inside the first horizontal box frame (1), a second slide plate (34) is slidably connected to the upper limit position of the first limit slide plate (8), and a methanol synthesis reactor discharge port plugging plate (20) is fixedly connected to the top of the second slide plate (34) near the right side; The inner bottom of the first horizontal box frame (1) is limitedly slidably connected to a transverse baffle (24); the bottom of the first limit slide plate (8) close to the right side is fixedly connected to a vertical baffle (23); the transverse baffle (24) is sealingly slidably connected to the bottom of the vertical baffle (23); the inner wall of the first horizontal box frame (1) is connected to the transverse baffle (24) via an elastic telescopic member (35); The middle part of the vertical box frame (3) is connected to a water inlet pipe (22); A driving mechanism, wherein the driving mechanism causes the second sliding plate (34) to perform an L-shaped movement. When the second sliding plate (34) performs a vertical movement, the methanol synthesis reactor discharge port plugging plate (20) is moved out from the top of the vertical box frame (3) and the methanol synthesis reactor discharge hole is blocked; when the second sliding plate (34) performs a horizontal movement to a first preset position, the methanol synthesis reactor discharge port plugging plate (20), the second sliding plate (34), the first limiting slide plate (8), the inner wall of the vertical box frame (3), the vertical baffle plate (23), and the horizontal baffle plate (24) form a passivation reaction chamber, and a passivation operation is performed by introducing water from the water inlet pipe (22). After the passivation is completed, the second sliding plate (34) performs a horizontal movement and drives the horizontal baffle plate (24) to move to release the passivation space so that the catalyst can be safely removed.
2. A methanol synthesis reactor catalyst unloading device according to claim 1, characterized in that: A flange (6) is fixedly mounted on the top outer wall of the vertical box frame (3), and a plurality of mounting holes (33) are provided on the flange (6) for detachable mounting with a discharge port at a discharge hole of a methanol synthesis reactor.
3. A methanol synthesis reactor catalyst unloading device according to claim 1, characterized in that: The catalyst collecting mechanism comprises a material collecting conical cylinder (4), the bottom of the vertical box frame (3) is open, and the material collecting conical cylinder (4) is fixedly installed at the bottom of the vertical box frame (3), and the bottom of the material collecting conical cylinder (4) is connected to a discharge pipe (5) installed, and the discharge pipe (5) is placed in the barrel body (7) to allow the catalyst to enter the barrel body (7) safely; It also includes a spraying mechanism for spraying the catalyst in the barrel (7).
4. A methanol synthesis reactor catalyst unloading device according to claim 3, characterized in that: The spray mechanism comprises a water pump (10), a water tank (9), a support rod (13), and a spray head (31); an auxiliary pipe (14) is fixedly mounted on the support rod (13); a spray head (31) is fixedly mounted on the bottom of the auxiliary pipe (14); the spray head (31) faces the interior of the barrel (7); a first pipe (11) and a second pipe (12) are mounted on the water pump (10); a side of the first pipe (11) away from the water pump (10) is placed in the water tank (9); a side of the second pipe (12) away from the water pump (10) is connected to the auxiliary pipe (14).
5. A methanol synthesis reactor catalyst unloading device according to claim 4, characterized in that: The water inlet at the top of the water tank (9) is provided with a water inlet tank cover (32).
6. A methanol synthesis reactor catalyst unloading device according to claim 5, characterized in that: The driving mechanism comprises a first sliding plate (17), the first limiting sliding plate (8) is slidingly connected to the first sliding plate (17) and the second sliding plate (34) via a first limiting sliding groove (16) thereon, a hinge rod (19) is hinged between the first sliding plate (17) and the second sliding plate (34), and an elastic member (18) is connected between the first sliding plate (17) and the second sliding plate (34), so that when the second sliding plate (34) and the methanol synthesis reactor discharge port plugging plate (20) are pressed against the right inner wall of the vertical box frame (3), the methanol synthesis reactor discharge port plugging plate (20) and the second sliding plate (34) move upward to block the methanol synthesis reactor discharge hole; The left bottom of the second sliding plate (34) is fixedly connected to a push plate (26), and the left top of the transverse baffle (24) is fixedly connected to an auxiliary extrusion plate (25); when the second sliding plate (34) is placed on the first limiting slide plate (8) and moves to the left, it drives the push plate (26) to move to the left to squeeze the auxiliary extrusion plate (25), so that the transverse baffle (24) is gradually opened; It also includes a moving mechanism for moving the first sliding plate (17).
7. A methanol synthesis reactor catalyst unloading device according to claim 6, characterized in that: A guide column (21) is fixedly connected between the first limiting slide plate (8) and the inner wall of the vertical box frame (3).
8. A methanol synthesis reactor catalyst unloading device according to claim 7, characterized in that: The moving mechanism comprises a second horizontal box frame (2), the bottom of the first horizontal box frame (1) is fixedly connected to the second horizontal box frame (2), a threaded rod (29) is connected between the two side walls of the second horizontal box frame (2) in a limited rotation manner, the outer wall of the threaded rod (29) is threadedly connected to a second limiting slide plate (30), the top of the second limiting slide plate (30) is limitedly slidably connected to a second limiting slide groove (28) provided at the inner bottom of the first horizontal box frame (1), the top of the second limiting slide plate (30) is fixedly connected to the first sliding plate (17) for driving the first sliding plate (17) to move, It also includes a small motor (15), wherein a power output end of the small motor (15) is connected to a threaded rod (29).
9. A methanol synthesis reactor catalyst unloading device according to claim 8, characterized in that: The front side of the second transverse box frame (2) is open, which facilitates the determination of the positions of the blocking plate (20) and the second sliding plate (34) of the discharge port of the current methanol synthesis reactor.
10. A methanol synthesis reactor catalyst unloading system, using the methanol synthesis reactor catalyst unloading device according to claim 9, characterized in that: include: A discharge connection module, the discharge connection module comprising a vertical box frame (3), the vertical box frame (3) being connected to a discharge hole of a methanol synthesis reactor via a flange (6) at the top; A catalyst collection module, the catalyst collection module being in communication with the bottom of the vertical box frame (3) and being used to collect the catalyst in the vertical box frame (3); A spray module, wherein the spray module sprays and cools the catalyst collection module; The plugging module is placed in the discharge connection module and is used to plug or open the discharge hole of the methanol synthesis reactor; The passivation reaction chamber module is placed in the discharge connection module and is used for allowing the catalyst to flow into the passivation reaction chamber module for passivation reaction after the discharge hole of the methanol synthesis reactor is opened; The discharge module is placed in the discharge connection module and is used to allow the catalyst at the end of the passivation reaction to enter the catalyst collection module.
Citation Information
Patent Citations
Catalyst discharge port structure of methanol synthesis tower reactor
CN210815132U
Initial hydrothermal deactivation method for selective hydrogenation nickel catalyst
CN104226375A
Passivating device for high-temperature Fischer-Tropsch synthesis of waste catalyst
CN108940382A
Device and method for unloading coal ethylene glycol hydrogenation catalyst
CN115715959A
Catalyst surface film-forming passivator as well as use method and application thereof
CN117138844A