Raw material adding device based on lauroyl peroxide solution
By designing an automated raw material addition device for dodecano peroxide solution process, the problem of low automation of existing process methods is solved, the automatic addition and extraction of raw materials is realized, labor costs are reduced, and the equipment usage time is extended through auxiliary cooling measures.
Patent Information
- Application Number
- CN202510347724.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-03-24
- Publication Date
- 2025-06-06
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
The existing process methods have a low degree of automation, and the addition of sodium hydroxide solution, hydrogen peroxide, mixed dispersants and lauryl chloride mainly relies on labor, resulting in an increase in labor costs.
A raw material addition device based on dodecano peroxide solution is designed. The device includes components such as frame, reactor, water tank, electromagnetic slide rail and storage box. Through the cooperation of electromagnetic sliders and driving motors, the automatic addition and extraction of liquids are achieved.
The automatic addition and extraction of raw materials is realized, the cost of manual operation is reduced, and the degree of automation of the process is improved. At the same time, airbags assist in cooling, extending the service life of the equipment.
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Figure CN120094495A_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of raw material addition, and in particular to a raw material adding device based on dodecyl peroxide solution. Background Art
[0002] Dodecyl peroxide, also known as dilauroyl peroxide, is a white crystalline powder under normal conditions. It is flammable and explosive with a melting point of 53-55 degrees Celsius, a boiling point of 467 degrees Celsius (760 mmHg), and a density of 0.91 g / cm3. It is insoluble in water, but easily soluble in organic solvents such as acetone and chloroform, and mineral oils. It is stable at room temperature, but may explode when heated. It will react violently when in contact with reducing agents, accelerators, organic matter, combustibles, etc., and there is a risk of combustion and explosion. It is mainly used as an initiator for free radical polymerization reactions of ethylene, vinyl chloride, vinylidene chloride, (meth)acrylates, etc. It can also be used as a polyester curing agent, rubber crosslinking agent, foaming agent, bleaching agent, desiccant, etc.
[0003] The process flow of the oxidized dodecyl solution is as follows: first add clean water into the reactor, start stirring at this time, then add sodium hydroxide solution, turn on the chilled water during the process to cool the reaction system to less than 15°C, and then add hydrogen peroxide to the reactor. After the addition, add a mixed dispersant, add lauroyl chloride dropwise at 0-15°C, and after the addition is complete, continue to keep warm and stir for 30 minutes (the entire reaction process is carried out under normal pressure). After the reaction is completed, discharge the material into the washing barrel to filter out the mother liquor and remove the lower aqueous phase (salty wastewater). Then wash with deionized water to remove the aqueous phase (washing wastewater). Then use a dryer (using warm water (30-35 degrees Celsius as a heat source and automatic control) to vacuum dry and dehydrate to obtain the product, but the existing process means have a low degree of automation, and the addition of sodium hydroxide solution, hydrogen peroxide, mixed dispersant and lauroyl chloride is mostly done manually, which increases labor costs. Summary of the invention
[0004] The purpose of the present invention is to solve the problem that the existing process means in the background technology have a low degree of automation, and the addition of sodium hydroxide solution, hydrogen peroxide, mixed dispersant and lauroyl chloride is mostly done manually, which increases the labor cost. A raw material adding device based on dodecyl peroxide solution is proposed.
[0005] In order to achieve the above-mentioned purpose, the present invention adopts the following technical scheme: a raw material adding device based on dodecyl peroxide solution, comprising: a frame, a reactor is rotatably connected inside the frame, a adding port is arranged on the top of the reactor, a water tank is arranged on the frame, a water pipe is connected to the bottom of the water tank and the end of the water pipe is connected to the reactor, a water pump is installed at the bottom of the frame, and the water in the water tank is discharged from the water pipe to the reactor after the water pump is turned on, an electromagnetic slide rail is fixed on one side of the top of the frame, an electromagnetic slider is arranged outside the electromagnetic slide rail, a storage box is fixed on the top of the electromagnetic slider, the interior of the storage box is divided into four compartments, and a certain amount of sodium hydroxide solution, hydrogen peroxide, mixed dispersant and lauroyl chloride are respectively placed in the four compartments, an adding mechanism is arranged on the top of the frame, and a cleaning mechanism is arranged inside the reactor.
[0006] As a further solution of the present invention, a circle of teeth is provided on the outside of the reactor, a driving motor is fixed to the top of the frame, a first bevel tooth and a gear are fixed to the output end of the driving motor, the gear is meshed with the teeth on the outside of the reactor, and a stirring blade is rotatably connected to the inside of the water tank. The top of the stirring blade extends to the top of the frame and is fixed with a second bevel tooth meshed with the first bevel tooth.
[0007] As a further scheme of the present invention, the adding mechanism includes a support plate fixedly arranged on the top of the frame, the support plate is penetrated by a first vertical groove, a horizontal groove and a second vertical groove, and the first vertical groove, the horizontal groove and the second vertical groove are connected, a sliding bar is fixed on one side of the support plate and the outer side of the sliding bar is slidably connected to a movable block, the inner side of the movable block is slidably connected to a cross bar, a forward and reverse motor is fixed on the front side of the support plate, the output end of the forward and reverse motor penetrates to the back side of the support plate and is fixed with a movable rod, the movable rod is penetrated by a hollow groove, a round rod is fixed inside one end of the cross rod, and the round rod penetrates the hollow groove and the first vertical groove.
[0008] As a further solution of the present invention, a pad and a first spring are slidably connected inside the first vertical groove and the second vertical groove, a vertical rod is fixed to the bottom of the pad, a groove is provided at the bottom of the support plate, a pressure plate is slidably connected to the inner wall of the groove and an airbag is provided, the bottom of the vertical rod penetrates into the groove and is fixedly connected to the top of the pressure plate, a nozzle is connected to the bottom of the airbag, the vertical rod penetrates the first spring, and the nozzle is located at the position of the driving motor.
[0009] As a further solution of the present invention, an extraction unit is provided at one end of the cross bar, and the extraction unit includes a hollow cylinder fixedly provided at one end of the cross bar, a piston is provided inside the hollow cylinder and a piston rod is fixed on the top of the piston, a circular plate is fixed on the top of the piston rod, a cylinder is fixed at the bottom of one end of the cross bar, and the output end of the cylinder passes through the top of the cross bar and is fixedly connected to the circular plate, and scale lines are provided on the outside of the hollow cylinder.
[0010] As a further solution of the present invention, the cleaning mechanism includes a support column at the bottom of the frame, the support column extends to the interior of the reactor, a hollow rod is fixed to the top of the support column, a thin plate is fixed to the bottom of the hollow rod, a support foot and a hook are fixed to the bottom of the reactor, a hollow stirring shaft is fixed to one end of the hollow rod, a rectangular block is slidably connected to the inside of the hollow rod, a second spring and a pull rope are fixed to one end of the rectangular block, and the pull rope passes through the hollow rod and the support column in sequence and is led out from the bottom end of the reactor.
[0011] As a further solution of the present invention, one end of the rectangular block is located inside the stirring shaft and is fixed with a scraper, the stirring shaft is provided with an opening, strip grooves are provided on both sides of the opening, a third spring is fixed inside the strip groove, and a scraper is fixed at one end of the third spring.
[0012] The present invention proposes a raw material adding device based on dodecyl peroxide solution, which has the following beneficial effects:
[0013] 1. The positive and negative motors are started to drive the movable rod to rotate. Since the round rod at one end of the cross rod passes through the hollow groove, the hollow groove will move outside the round rod when the movable rod rotates, and will carry the round rod from the bottom of the first vertical groove to the top of the first vertical groove. During this process, the cross rod will rise vertically and the movable block will slide upward on the outside of the slide bar. This operation is to make the bottom of the hollow cylinder higher than the highest point of the storage box. As the movable rod continues to rotate, the round rod at this time moves from the first vertical groove to the cross groove. During this process, the cross rod will slide in the movable block but the movable block will not move. This operation is to move the hollow cylinder to the top of the storage box. Then, as the movable rod rotates, the round rod moves from the cross groove to the bottom of the second vertical groove, and then the movable block and the cross rod will drop vertically. This operation is to make the hollow cylinder enter the interior of the storage box. When the liquid to be extracted is sodium hydroxide solution, the hollow cylinder in the extraction unit will enter the compartment where the sodium hydroxide solution is located under the above operation.
[0014] 2. When the round rod moves in the first vertical groove and the second vertical groove, it will compress the pad, and then the pad will move down with the vertical rod and compress the first spring. When the round rod leaves the top of the pad, the pad will be raised under the reset action of the first spring, and then the pad can be lifted and lowered. When the pad is lifted or lowered, the vertical rod will lift and lower the pressure plate, and when the pressure plate descends, it will compress the airbag and then the air in the airbag will be discharged from the nozzle and sprayed toward the drive motor. This is beneficial to achieve auxiliary cooling of the drive motor on the basis of adding liquid through this operation to increase its service life. BRIEF DESCRIPTION OF THE DRAWINGS
[0015] Figure 1 This is a schematic diagram of the overall appearance structure proposed by the present invention;
[0016] Figure 2 This is a schematic diagram of the front structure of the support plate proposed by the present invention;
[0017] Figure 3 This is a schematic diagram of the back structure of the support plate proposed by the present invention;
[0018] Figure 4 This is a schematic diagram of the structure of the extraction unit proposed by the present invention;
[0019] Figure 5 This is a schematic diagram of the connection structure between the forward and reverse motors and the movable rod proposed by the present invention;
[0020] Figure 6 This is a schematic diagram of the structure of the electromagnetic slide rail and the electromagnetic slider proposed by the present invention;
[0021] Figure 7 The present invention proposes Figure 1 Schematic diagram of local structure;
[0022] Figure 8 This is a schematic diagram of the internal structure of the reactor proposed by the present invention;
[0023] Fig. 9 This is a schematic diagram of the connection structure between the hollow rod and the stirring shaft proposed in the present invention;
[0024] Fig.10 This is a schematic diagram of the scraper structure inside the stirring shaft proposed by the present invention;
[0025] Fig.11 The present invention proposes Fig.10 Schematic diagram of local structure;
[0026] Fig.12 The present invention is a simplified process flow diagram for preparing dilauroyl peroxide.
[0027] In the figure: 1, frame; 2, reactor; 3, addition port; 4, water tank; 5, electromagnetic slide rail; 6, electromagnetic slider; 7, storage box; 8, drive motor; 9, stirring blade; 11, support plate; 12, first vertical slot; 13, horizontal slot; 14, second vertical slot; 15, slide bar; 16, movable block; 17, horizontal bar; 18, forward and reverse motor; 19, movable rod; 20, hollow slot; 21, round rod; 22, first spring; 23, vertical rod; 24, groove; 25, pressure plate; 26, air bag; 27, nozzle; 28, hollow cylinder; 29, piston rod; 31, round plate; 32, cylinder; 33, support column; 34, hollow rod; 35, thin plate; 36, hook; 37, stirring shaft; 38, rectangular block; 39, second spring; 40, pull rope; 41, scraper; 42, opening; 43, strip groove; 44, third spring; 45, scraper; 46, pad. DETAILED DESCRIPTION
[0028] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
[0029] In the description of the present invention, it should be noted that the orientation or positional relationship indicated by the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inside", "outside", etc. is based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as limiting the present invention. In addition, the terms "first", "second", and "third" are only used for descriptive purposes and cannot be understood as indicating or implying relative importance. In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", and "set" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be directly connected, or indirectly connected through an intermediate medium, or it can be the internal connection of two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood according to specific circumstances. The following is an explanation of its embodiments based on the overall structure of the present invention.
[0030] A raw material adding device based on dodecyl peroxide solution comprises: a frame 1, a reactor 2 is rotatably connected inside the frame 1, a adding port 3 is arranged on the top of the reactor 2, a water tank 4 is arranged on the frame 1, a water pipe is connected to the bottom of the water tank 4 and the end of the water pipe is connected to the reactor 2, a water pump is installed at the bottom of the frame 1, and the water in the water tank 4 is discharged from the water pipe to the reactor 2 after the water pump is turned on, an electromagnetic slide rail 5 is fixed to one side of the top of the frame 1, an electromagnetic slider 6 is arranged on the outside of the electromagnetic slide rail 5, and the electromagnetic slider 6 A storage box 7 is fixed on the top, and the interior of the storage box 7 is divided into four compartments, and a certain amount of sodium hydroxide solution, hydrogen peroxide, mixed dispersant and lauroyl chloride are placed in each of the four compartments. An adding mechanism is provided on the top of the frame 1, and a cleaning mechanism is provided inside the reactor 2. Before the adding mechanism works, the electromagnetic slider 6 moves outside the electromagnetic slide rail 5 and moves with the storage box 7, in order to move the compartment where the extracted solution is located to the position of the hollow cylinder 28, so that the hollow cylinder 28 and the compartment are in a straight line to facilitate the extraction of the liquid.
[0031] Furthermore, a circle of teeth is provided on the outside of the reactor 2, a driving motor 8 is fixed on the top of the frame 1, a first bevel tooth and a gear are fixed on the output end of the driving motor 8, the gear is meshed with the teeth on the outside of the reactor 2, the inside of the water tank 4 is rotatably connected with a stirring blade 9, the top of the stirring blade 9 extends to the top of the frame 1 and is fixed with a second bevel tooth meshed with the first bevel tooth, after the water pump is turned on, the water in the water tank 4 is discharged from the water pipe into the reactor 2, and then the driving motor 8 is started to drive the first bevel tooth and the gear to rotate, when the gear rotates, the reactor 2 is driven to rotate by the action of the teeth, the first bevel tooth rotates and drives the stirring blade 9 to rotate in the water tank 4 through the second bevel tooth, and the rotation of the stirring blade 9 makes the water and alum quickly merge to purify the water quality.
[0032] Furthermore, the adding mechanism includes a support plate 11 fixedly arranged on the top of the frame 1, the support plate 11 is penetrated by a first vertical groove 12, a horizontal groove 13 and a second vertical groove 14, and the first vertical groove 12, the horizontal groove 13 and the second vertical groove 14 are connected, a slide bar 15 is fixed on one side of the support plate 11 and the outside of the slide bar 15 is slidably connected to a movable block 16, the inside of the movable block 16 is slidably connected to a cross bar 17, a forward and reverse motor 18 is fixed on the front of the support plate 11, the output end of the forward and reverse motor 18 penetrates to the back of the support plate 11 and is fixed with a movable rod 19, the movable rod 19 is penetrated by a hollow groove 20, a round rod 21 is fixed inside one end of the cross bar 17, and the round rod 21 penetrates the hollow groove 20 and the first vertical groove 12.
[0033] Next, the first vertical groove 12 and the second vertical groove 14 are slidably connected with a cushion block 46 and a first spring 22, a vertical rod 23 is fixed to the bottom of the cushion block 46, a groove 24 is provided at the bottom of the support plate 11, a pressure plate 25 is slidably connected to the inner wall of the groove 24 and an airbag 26 is provided, the bottom of the vertical rod 23 penetrates into the groove 24 and is fixedly connected to the top of the pressure plate 25, a nozzle 27 is connected to the bottom of the airbag 26, the vertical rod 23 penetrates the first spring 22, and the nozzle 27 is located at the position of the drive motor 8.
[0034] It should be noted that the forward and reverse motors 18 are started to drive the movable rod 19 to rotate. Since the round rod 21 at one end of the cross bar 17 penetrates the hollow groove 20, the hollow groove 20 will move outside the round rod 21 when the movable rod 19 rotates, and will carry the round rod 21 from the bottom of the first vertical groove 12 to the top of the first vertical groove 12. During this process, the cross bar 17 will rise vertically and the movable block 16 will slide upward on the outside of the slide bar 15. This operation is to make the bottom of the hollow cylinder 28 higher than the highest point of the storage box 7. As the movable rod 19 continues to rotate, the round rod 21 at this time rises from the bottom of the first vertical groove 12 to the top of the first vertical groove 12. Move to the transverse groove 13. During this process, the cross bar 17 will slide in the movable block 16 but the movable block 16 will not move. This operation is to move the hollow cylinder 28 to the top of the storage box 7. Then with the rotation of the movable rod 19, the round rod 21 moves from the transverse groove 13 to the bottom of the second vertical groove 14, and then the movable block 16 and the cross bar 17 will drop vertically. This operation is to allow the hollow cylinder 28 to enter the interior of the storage box 7. When the liquid to be extracted is sodium hydroxide solution, the hollow cylinder 28 in the extraction unit will enter the compartment where the sodium hydroxide solution is located under the above operation.
[0035] Furthermore, an extraction unit is provided at one end of the cross bar 17, and the extraction unit includes a hollow cylinder 28 fixedly provided at one end of the cross bar 17, a piston is provided inside the hollow cylinder 28, and a piston rod 29 is fixed on the top of the piston, a round plate 31 is fixed on the top of the piston rod 29, a cylinder 32 is fixed at the bottom of one end of the cross bar 17, and the output end of the cylinder 32 passes through the top of the cross bar 17 and is fixedly connected to the round plate 31, and a scale line is provided on the outside of the hollow cylinder 28, and the output end of the cylinder 32 is fixed to the top of the cross bar 17. The end extends out to drive the circular plate 31 and the piston rod 29 to rise, and then the sodium hydroxide solution will be extracted into the hollow cylinder 28, and then the forward and reverse motor 18 rotates in the opposite direction, and then drives the hollow cylinder 28 back to the top of the addition port 3 and descends, and then the solenoid valve in the addition port 3 is started to open the addition port 3, and then the hollow cylinder 28 descends to the inside of the addition port 3, and then the output end of the cylinder 32 retracts to drive the piston rod 29 and the piston to descend in the hollow cylinder 28, and then the sodium hydroxide solution in the hollow cylinder 28 is squeezed out into the reactor.
[0036] Next, the cleaning mechanism includes a support column 33 at the bottom of the frame 1, the support column 33 extends to the interior of the reactor 2, a hollow rod 34 is fixed to the top of the support column 33, a thin plate 35 is fixed to the bottom of the hollow rod 34, a support foot and a hook 36 are fixed to the bottom of the reactor 2, a hollow stirring shaft 37 is fixed to one end of the hollow rod 34, a rectangular block 38 is slidably connected to the inside of the hollow rod 34, a second spring 39 and a pull rope 40 are fixed to one end of the rectangular block 38, the pull rope 40 passes through the hollow rod 34 and the support column 33 in sequence and is led out from the bottom end of the reactor 2, one end of the rectangular block 38 is located inside the stirring shaft 37 and a scraper 41 is fixed thereto, the stirring shaft 37 is provided with an opening 42, strip grooves 43 are provided on both sides of the opening 42, a third spring 44 is fixed to the inside of the strip groove 43, and a scraper 45 is fixed to one end of the third spring 44.
[0037] It can be concluded that, in the initial state, the pull rope 40 is in a tensioned state and the bottom of the pull rope 40 is wound around the hook 36. When the pull rope 40 is in a tensioned state, the rectangular block 38 will retreat and compress the second spring 39, and then the scraper 41 will enter the inside of the stirring shaft 37 from the position of the opening 42. Therefore, in the initial state, the scraper 41 is located inside the stirring shaft 37. When the reactor 2 rotates, the liquid inside will hit the thin plate 35 and the stirring shaft 37. When the collision occurs, water waves are formed to enter and stir the liquid in the reactor 2. However, after a certain period of use, impurities will adhere to the inner wall of the reactor 2. At this time, the pull rope 40 needs to be loosened from the hook 36, and then the second spring 39 resets the rectangular block 38 to move the scraper 41 from the stirring shaft 37, and then the blade of the scraper 41 contacts the inner wall of the reactor 2. When the reactor 2 rotates, the scraper 41 scrapes off the impurities inside it. When scraping, the water in the water tank 4 will enter the reactor 2, and then the water and impurities will be discharged from the discharge port at the bottom of the reactor 2, thereby realizing the two functions of stirring and cleaning.
[0038] Working principle: A filling port is provided on the back of the water tank 4, through which water and alum can be injected into the water tank 4. A certain amount of sodium hydroxide solution, hydrogen peroxide, mixed dispersant and lauroyl chloride are placed in the four compartments inside the storage box 7 respectively. After the water pump is turned on, the water in the water tank 4 is discharged from the water pipe to the reactor 2, and then the driving motor 8 is started to drive the first bevel gear and the gear to rotate. When the gear rotates, the reactor 2 is driven to rotate through the action of the teeth. The rotation of the first bevel gear drives the stirring blade 9 to rotate in the water tank 4 through the second bevel gear. The rotation of the stirring blade 9 makes the water and alum merge quickly to purify the water quality. The rotation of the reactor 2 can achieve the stirring of the internal liquid. After the stirring is turned on, sodium hydroxide solution needs to be added to the inside of the reactor 2. During this process, the chilled water is turned on to cool the reaction system to less than 15°C, and then hydrogen peroxide is added to the reactor. After the addition is completed, add the mixed dispersant, add lauroyl chloride dropwise at 0-15°C, and continue to keep warm and stir for 30 minutes (the entire reaction process is carried out under normal pressure). After the reaction is completed, discharge the material into the washing bucket to filter out the mother liquor and remove the lower aqueous phase (salt-containing wastewater). Then wash with deionized water to remove the aqueous phase (washing wastewater). Then use a dryer (using warm water (30-35°C) as a heat source and automatic control) to vacuum dry and dehydrate to obtain the product. The addition process is as follows:
[0039] The forward and reverse motor 18 is started to drive the movable rod 19 to rotate. Since the round rod 21 at one end of the cross bar 17 penetrates the hollow groove 20, the hollow groove 20 will move outside the round rod 21 when the movable rod 19 rotates, and will bring the round rod 21 from the bottom of the first vertical groove 12 to the top of the first vertical groove 12. In this process, the cross bar 17 will rise vertically and the movable block 16 will slide upward outside the slide bar 15. This operation is to make the bottom of the hollow cylinder 28 higher than the highest point of the storage box 7. As the movable rod 19 continues to rotate At this time, the round rod 21 moves from the first vertical groove 12 to the horizontal groove 13. During this process, the horizontal rod 17 will slide in the movable block 16, but the movable block 16 will not move. This operation is to move the hollow cylinder 28 to the top of the storage box 7. Then, with the rotation of the movable rod 19, the round rod 21 moves from the horizontal groove 13 to the bottom of the second vertical groove 14, and then the movable block 16 and the horizontal rod 17 will drop vertically. This operation is to make the hollow cylinder 28 enter the interior of the storage box 7. Before the adding mechanism works, the electromagnetic slider 6 is The outside of the electromagnetic slide rail 5 moves and moves the storage box 7 with it, the purpose is to move the compartment where the extracted solution is located to the position of the hollow cylinder 28, so that the hollow cylinder 28 and the compartment are in a straight line to facilitate the extraction of liquid. When the liquid to be extracted is sodium hydroxide solution, the hollow cylinder 28 in the extraction unit will enter the compartment where the sodium hydroxide solution is located under the above operation, and then the output end of the cylinder 32 will extend to drive the circular plate 31 and the piston rod 29 to rise, and then the sodium hydroxide solution will be extracted into the hollow cylinder 28, and then The counter motor 18 rotates in the reverse direction, and then brings the hollow cylinder 28 back to the top of the addition port 3 and descends. Then the solenoid valve in the addition port 3 is started to open the addition port 3. Then the hollow cylinder 28 descends to the inside of the addition port 3. Then the output end of the cylinder 32 retracts and brings the piston rod 29 and the piston down in the hollow cylinder 28. Then the sodium hydroxide solution in the hollow cylinder 28 is squeezed out into the reactor. The same operation is performed when extracting hydrogen peroxide, mixed dispersant, and lauroyl chloride. The labor cost is reduced by automatic addition.
[0040] When the round rod 21 moves in the first vertical groove 12 and the second vertical groove 14, it will compress the pad 46, and then the pad 46 will move down with the vertical rod 23 and compress the first spring 22. When the round rod 21 leaves the top of the pad 46, the pad 46 is lifted under the reset action of the first spring 22, and then the pad 46 can be lifted and lowered. When the pad 46 is lifted and lowered, the vertical rod 23 will lift and lower the pressure plate 25. When the pressure plate 25 descends, it compresses the airbag 26 and then the air in the airbag 26 is discharged from the nozzle 27 and sprayed toward the drive motor 8. This is beneficial to achieve auxiliary cooling of the drive motor 8 on the basis of adding liquid through this operation to increase its service life.
[0041] In the initial state, the pull rope 40 is in a tensioned state and the bottom of the pull rope 40 is wrapped around the hook 36. When the pull rope 40 is in a tensioned state, the rectangular block 38 will retreat and compress the second spring 39, and then the scraper 41 will enter the inside of the stirring shaft 37 from the position of the opening 42. Therefore, in the initial state, the scraper 41 is located inside the stirring shaft 37. When the reactor 2 rotates, the liquid inside will hit the thin plate 35 and the stirring shaft 37. When the collision occurs, water waves are formed to enter and stir the liquid in the reactor 2. However, after a certain period of use, impurities will adhere to the inner wall of the reactor 2. At this time, the pull rope 40 needs to be loosened from the hook 36, and then the second spring 39 resets the rectangular block 38 resets and moves the scraper 41 out of the stirring shaft 37 , and then the blade of the scraper 41 contacts the inner wall of the reactor 2. When the reactor 2 rotates, the scraper 41 scrapes off the impurities inside it. When scraping, the water in the water tank 4 will enter the reactor 2, and then the water and impurities will be discharged from the discharge port at the bottom of the reactor 2, thereby realizing the two functions of stirring and cleaning. After cleaning, it is necessary to tighten the pull rope 40 again, and then the scraper 41 returns to the stirring shaft 37. When returning, the scraper 45 contacts the side wall of the scraper 41, so that the impurities on the side wall of the scraper 41 can be removed by the scraper 45 to prevent the impurities from being brought into the stirring shaft 37. The scraper 41 will push against the scraper 45 during the process of going in and out, so that the scraper 45 can expand and contract in the strip groove 43 under the action of the third spring 44.
[0042] The above are only preferred specific implementation modes of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical solutions and inventive concepts of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A raw material adding device based on lauroyl peroxide solution, comprising: The frame (1) is characterized in that: a reaction kettle (2) is rotatably connected inside the frame (1), a feeding port (3) is arranged on the top of the reaction kettle (2), a water tank (4) is arranged on the frame (1), an electromagnetic slide rail (5) is fixed on one side of the top of the frame (1), an electromagnetic slider (6) is arranged on the outside of the electromagnetic slide rail (5), a storage box (7) is fixed on the top of the electromagnetic slider (6), an adding mechanism is arranged on the top of the frame (1), and a cleaning mechanism is arranged inside the reaction kettle (2).
2. A raw material adding device based on dodecyl peroxide solution according to claim 1, characterized in that: The adding mechanism comprises a support plate (11) fixedly arranged on the top of the frame (1); the support plate (11) is penetrated by a first vertical groove (12), a horizontal groove (13) and a second vertical groove (14); the first vertical groove (12), the horizontal groove (13) and the second vertical groove (14) are communicated; a slide bar (15) is fixed on one side of the support plate (11); the outside of the slide bar (15) is slidably connected to a movable block (16); the inside of the movable block (16) is slidably connected to a cross bar (17).
3. A raw material adding device based on dodecyl peroxide solution according to claim 2, characterized in that: A forward and reverse motor (18) is fixed on the front side of the support plate (11); the output end of the forward and reverse motor (18) passes through the back side of the support plate (11) and is fixed with a movable rod (19); a hollow groove (20) is penetrated by the movable rod (19); a round rod (21) is fixed inside one end of the cross rod (17); the round rod (21) passes through the hollow groove (20) and the first vertical groove (12).
4. A raw material adding device based on dodecyl peroxide solution according to claim 3, characterized in that: A cushion block (46) and a first spring (22) are slidably connected inside the first vertical groove (12) and the second vertical groove (14); a vertical rod (23) is fixed to the bottom of the cushion block (46); a groove (24) is provided at the bottom of the support plate (11); a pressure plate (25) is slidably connected to the inner wall of the groove (24) and is provided with an air bag (26); the bottom of the vertical rod (23) passes through the groove (24) and is fixedly connected to the top of the pressure plate (25); and a nozzle (27) is connected to the bottom of the air bag (26).
5. A raw material adding device based on dodecyl peroxide solution according to claim 2, characterized in that: An extraction unit is provided at one end of the cross bar (17), and the extraction unit comprises a hollow cylinder (28) fixedly provided at one end of the cross bar (17), a piston is provided inside the hollow cylinder (28), a piston rod (29) is fixed at the top of the piston, a round plate (31) is fixed at the top of the piston rod (29), a cylinder (32) is fixed at the bottom of one end of the cross bar (17), and an output end of the cylinder (32) passes through the top of the cross bar (17) and is fixedly connected to the round plate (31).
6. A raw material adding device based on dodecyl peroxide solution according to claim 1, characterized in that: The cleaning mechanism comprises a support column (33) at the bottom of the frame (1), the support column (33) extending into the interior of the reaction kettle (2), a hollow rod (34) fixed to the top of the support column (33), a thin plate (35) fixed to the bottom of the hollow rod (34), and a support foot and a hook (36) fixed to the bottom of the reaction kettle (2).
7. A raw material adding device based on dodecyl peroxide solution according to claim 6, characterized in that: A hollow stirring shaft (37) is fixed to one end of the hollow rod (34), and a rectangular block (38) is slidably connected to the inside of the hollow rod (34). A second spring (39) and a pull rope (40) are fixed to one end of the rectangular block (38). The pull rope (40) passes through the hollow rod (34) and the support column (33) in sequence and is led out from the bottom end of the reactor (2).
8. A raw material adding device based on dodecyl peroxide solution according to claim 7, characterized in that: One end of the rectangular block (38) is located inside the stirring shaft (37) and is fixed with a scraper (41); the stirring shaft (37) is provided with an opening (42); strip grooves (43) are provided on both sides of the opening (42); a third spring (44) is fixed inside the strip groove (43); and a scraper (45) is fixed to one end of the third spring (44).
9. The raw material adding device based on dodecyl peroxide solution according to claim 1, characterized in that: The interior of the storage box (7) is divided into four compartments, and a certain amount of sodium hydroxide solution, hydrogen peroxide, mixed dispersant, and lauroyl chloride are respectively placed in the four compartments.