High-flux electric heating digestion instrument
By designing a high-throughput electric thermal digester and using multiple digestion units, gas delivery and purification systems, the existing electric thermal digester has solved the problems of incomplete digestion, long time, serious corrosion and pollution, and achieved rapid and accurate digestion effects, which are suitable for high-throughput digestion in multiple fields.
Patent Information
- Application Number
- CN202510600010.7
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-05-12
- Publication Date
- 2025-07-08
AI Technical Summary
The existing electric thermal digestion instruments have problems such as incomplete digestion, long digestion time, serious equipment corrosion, insufficient safety and environmental pollution, especially in the digestion process of high-field strength elements.
A high-throughput electric thermal digester is designed, using multiple digestion units, gas delivery systems, purification systems and cooling systems. The sealing is ensured through the locking mechanism, and combined with the electric heating and refrigeration functions to achieve rapid digestion and gas purification.
It improves digestion efficiency and accuracy, reduces equipment corrosion and environmental pollution, and is suitable for high-throughput rapid digestion in geology, environment, agriculture, food, oil, biology, food and other fields.
Smart Images

Figure CN120275141A_ABST
Abstract
Description
Technical Field
[0001] The present invention belongs to the technical field of element analysis test digestion equipment, and particularly relates to a high-throughput electrothermal digester. Background Art
[0002] An electrothermal digester is an instrument that uses high-temperature and high-pressure steam to convert organic or inorganic substances in a sample into atomic or ionic states for easy analysis and measurement. Its principle is based on the thermal decomposition of the sample and the digestion by steam. In an electrothermal digester, the sample is heated to a specific temperature so that the organic or inorganic substances in the sample can be thermally decomposed and dissolved in the heated water. With the development of testing technologies, the sample pretreatment digestion technology has become particularly important and prominent, which determines the efficiency and accuracy of test data.
[0003] Currently, there are mainly 4 digestion methods: 1. The open digestion method, which uses a large amount of acid, has a high blank value, a very high probability of external contamination, seriously corrodes the laboratory fume hood and hot plate, and there is a phenomenon that the sample is not completely digested; 2. The ordinary closed digestion method, which can withstand low pressure, is not safe enough for the digestion of biological samples, is prone to explosion tank phenomenon, has a long digestion time, is difficult to digest some insoluble samples, and has a low recovery rate for some high-field-strength elements, thus polluting the environment. 3. The microwave digestion method, which cannot effectively digest some high-field-strength elements and the pressure it can withstand is much lower than that of a high-pressure digestion tank. 4. It is the traditional high-pressure closed digestion method, which mainly uses a high-pressure reaction kettle for digestion. The acid is easy to leak, corrodes the stainless steel tank body and the heating oven, affects the service life, the acid is easy to volatilize, the digestion is unstable, the buckling is complex, and it is relatively bulky.
[0004] Therefore, the present invention proposes a high-throughput electrothermal digester. Summary of the Invention
[0005] In view of the above situation, in order to overcome the defects of the prior art, the present invention provides a high-throughput electrothermal digester, which solves the technical problems existing in the prior art.
[0006] To achieve the above object, the present invention provides the following technical solution: a high-throughput electrothermal digestion instrument, including a digestion instrument. A lower chamber door is fixedly connected to the front end of the digestion instrument by bolts. An upper chamber door is provided at the top of the lower chamber door and is rotatably connected to the digestion instrument. A control panel is fixed to the front end of the digestion instrument. A partition plate is fixed inside the digestion instrument. A digestion chamber is fixed to the top of the partition plate. A plurality of digestion units are provided inside the digestion chamber. An air delivery pipe is provided inside the digestion chamber. An intake pipe is fixed to the rear of the air delivery pipe. A heating chamber is fixed to the bottom of the intake pipe. An air valve is connected to the bottom of the heating chamber through a pipe. An air pump is fixed to the bottom of the air valve. An exhaust gas outlet is also fixed to the top of the digestion chamber. A waste gas pipe is fixed to the bottom of the exhaust gas outlet. The bottom of the waste gas pipe passes through the partition plate and is fixed to a purification box. An ultrasonic atomizer is fixed to the right side of the purification box through an atomized liquid pipe. A neutralization liquid box is fixed to the front end of the ultrasonic atomizer through a neutralization liquid pipe. A waste water box is fixed to the front end of the purification box through a waste water pipe. A power supply is also fixed inside the digestion instrument. A power cord is fixed to the right end of the power supply. A dehumidification box is fixed to the rear end of the purification box through a dehumidification pipe. An air outlet box is fixed to the rear end of the dehumidification box through a pipe. A compressor is provided at the rear end of the air outlet box. A cold air pipe is provided at the right end of the compressor. Two locking blocks are also provided at the front end of the digestion instrument.
[0007] Preferably, a plurality of support blocks are fixed to the bottom of the digestion instrument. Two gas filters are fixed to the rear of the digestion instrument. A plurality of groups of digestion unit positioning buckles are fixed inside the digestion chamber. Each group of the digestion unit positioning buckles is slidably connected to the digestion unit inside it. A digestion tank is provided at the top of each digestion unit.
[0008] Preferably, a locking chamber is provided inside the front end of the digestion instrument. A locking rod is fixed inside the locking chamber. A locking plate is fixed to the left side of the locking rod. Two locking sliding rods are slidably connected to the left end of the locking plate. A locking spring is provided outside each locking sliding rod. Each locking sliding rod is fixedly connected to the locking block on its left side. Each locking block can be clamped with the groove on the upper chamber door.
[0009] Preferably, a commutation motor is fixed to the right end of the digestion chamber. The commutation motor is rotatably connected to the air delivery pipe through a rotating shaft. A plurality of air outlet heads are fixed to the front end of the air delivery pipe. A temperature sensor is also fixed to the top end inside the digestion chamber.
[0010] Preferably, a positioning rod is fixed to the top of the partition plate. A cleaning motor is fixed to the top of the positioning rod. A cleaning rod is rotatably connected to the left side of the cleaning motor. A plurality of cleaning wires are fixed to the left end of the cleaning rod. A filter plate is provided on the left side of the plurality of cleaning wires and is fixedly connected to the air pump.
[0011] Preferably, a ventilation motor is further fixed to the rear end of the digestion chamber. A ventilation fan is rotatably connected to the rear end of the ventilation motor. An intake air temperature sensor is fixed to the rear end of the heating chamber. A heater is provided at the bottom of the intake air temperature sensor. A heating plate is fixed to the front end of the heater, and the heating plate is fixed inside the heating chamber.
[0012] Preferably, an exhaust gas valve is provided at the right end of the heating chamber and is fixedly connected to the exhaust gas outlet. An exhaust gas pump is provided at the bottom of the exhaust gas valve and is fixedly connected to the partition plate. The exhaust gas pump is fixedly connected to the exhaust gas outlet. An atomized liquid nozzle is provided inside the purification tank. The right end of the atomized liquid nozzle is fixedly connected to the atomized liquid pipe. The atomized liquid pipe is fixedly connected to the upper surface inside the purification tank through the atomized liquid pipe positioning plate.
[0013] Preferably, an atomized liquid valve is fixed to the right end of the atomized liquid pipe. An atomized liquid pump is fixed to the right end of the atomized liquid valve. The right end of the atomized liquid pump is fixedly connected to the ultrasonic atomizer through a pipeline. A neutralizing liquid pump is fixed to the front end of the ultrasonic atomizer through the neutralizing liquid pipe. A neutralizing liquid valve is fixed to the front end of the neutralizing liquid pump through the neutralizing liquid pipe.
[0014] Preferably, a waste water valve is fixed to the front end of the purification tank. A waste water pump is fixed to the front end of the waste water valve through the waste water pipe. An outlet pipe is fixed to the front end of the waste water tank. An outlet valve is fixed to the right end of the outlet pipe.
[0015] Preferably, a dehumidification chamber door is provided at the rear end of the purification tank. The dehumidification chamber door is tightly fastened to the dehumidification chamber by bolts. A drying plate is provided inside the dehumidification chamber. An activated carbon adsorption plate is provided in front of the drying plate. A humidity sensor is fixed inside the air outlet box. An acid-base concentration sensor is fixed to the left side of the humidity sensor. The right end of the compressor is fixedly connected to a cold air pump through a pipeline. The top of the cold air pump is fixedly connected to the cold air pipe. An air cooling valve is fixed to the upper end of the cold air pipe. The left end of the air cooling valve is fixedly connected to the intake pipe at the top of the heating chamber through a pipeline.
[0016] Compared with the prior art, the beneficial effects of the present invention are:
[0017] (1) The present invention can drive the locking plate to move through the locking rod, thereby driving the locking block to move, which facilitates the opening of the upper box door. At the same time, due to the action of the locking spring and the locking slide rod, the locking block can be inserted into the slot of the upper box door, so that the upper box door is closed, the digestion chamber is sealed, gas leakage during digestion is prevented, the accuracy of digestion is ensured, and the digestion effect is guaranteed. At the same time, due to the action of the digestion unit, the entire device can allow multiple digestion tanks to work simultaneously, improving the digestion efficiency. At the same time, it is convenient to remove the digestion tank, improving the lightness of the device and increasing the service life of the device. The present invention also solves the problems of long digestion time, low cooling time efficiency, small number of samples digested by a microwave digester, and incomplete digestion in traditional electric heating ovens. The present invention has functions of sample electrothermal digestion, compression refrigeration, cold storage, gas emission recovery, and gas purification;
[0018] (2) The present invention can transport air to the inside of the heating chamber through an air pump and an air valve, and then the air can be heated by a heating plate, and then transported to the inside of the air delivery pipe through an air inlet pipe, and then transported to the inside of the digestion chamber through an air outlet head, so as to heat the digestion tank, improving the digestion efficiency. At the same time, the temperature inside the digestion chamber can be monitored by a temperature sensor to ensure that the digestion temperature is evenly controllable, the number of digested samples is large, the digestion experiments are uniform, and the samples are ensured to be completely digested, which is suitable for high-throughput rapid digestion in fields such as geology, environment, agriculture, food, petroleum, biology, and food;
[0019] (3) The present invention can reduce the air temperature through a compressor, and at the same time, cold air can be transported to the inside of the air inlet pipe through a cold air pump and a cold air valve, and then transported to the inside of the air delivery pipe, and then transported to the inside of the digestion chamber, so as to reduce the temperature of the digestion chamber, achieving rapid cooling, improving the digestion efficiency, and saving time. At the same time, the present device can ensure the uniformity of digestion by driving the air delivery pipe to rotate through a reversing motor, thus ensuring the digestion effect. The compressor of the present device provides a cold storage function for the digester. When the sample digestion in the digestion chamber is completed, the cold storage chamber releases cold air into the digestion chamber to accelerate the gas circulation and refrigeration in the digestion chamber. By connecting the air delivery pipe to a purification box, rapid refrigeration and gas recovery and purification functions in the digestion chamber are achieved. The present invention is a high-throughput digestion instrument in the field of element analysis and testing digestion technology. By electrically heating the temperature of the sample digestion tank in the digestion chamber, rapid heating is achieved, and after maintaining a constant digestion time, centralized cooling, exhaust, and purification are carried out, so as to quickly heat and digest samples, quickly cool down, and purify gases, achieving an efficient digestion and rapid completion digestion instrument;
[0020] (4) By cooperating with the exhaust gas pump and the exhaust gas valve, the present invention can transport the exhaust gas inside the digestion chamber to the inside of the purification box through the exhaust gas outlet and the exhaust gas pipe. Further, the alkaline solution inside the neutralization liquid tank is sprayed out through the atomization liquid pipe by the ultrasonic atomizer, so that the acidic exhaust gas inside the purification box can be humidified and neutralized. Further, it is transported to the air outlet box through the dehumidification box. At the same time, the humidity sensor and the acid-base concentration sensor can monitor whether the output gas meets the standards, so as to realize the decontamination of the exhaust gas and the conversion of fresh air, and can be directly introduced into the laboratory to achieve green, environmentally friendly, high-throughput and efficient digestion;
[0021] (5) By means of the waste water pump and the waste water valve, the present invention can transport the waste liquid that has been neutralized inside the purification box to the inside of the waste water tank. Further, by opening the water outlet valve, the waste liquid inside the waste water tank can be conveniently collected, so as to ensure the accuracy of waste liquid collection and prevent the waste liquid from polluting the environment, thus ensuring the digestion effect. BRIEF DESCRIPTION OF THE DRAWINGS
[0022] The drawings are used to provide a further understanding of the present invention and constitute a part of the specification. Together with the embodiments of the present invention, they are used to explain the present invention and do not constitute a limitation to the present invention.
[0023] In the drawings:
[0024] Figure 1 is the front view schematic diagram of the present invention;
[0025] Figure 2 is the back view schematic diagram of the present invention;
[0026] Figure 3 is the internal schematic diagram of the digester of the present invention;
[0027] Figure 4 is the internal rear end sectional view schematic diagram of the digester of the present invention;
[0028] Figure 5 is the rear end schematic diagram of the digestion chamber of the present invention;
[0029] Figure 6 is the top schematic diagram of the partition board of the present invention;
[0030] Figure 7 is the internal schematic diagram of the heating chamber of the present invention;
[0031] Figure 8 is the cleaning rod schematic diagram of the present invention;
[0032] Figure 9 is the internal schematic diagram of the digestion chamber of the present invention;
[0033] Figure 10 is the bottom schematic diagram of the partition board of the present invention;
[0034] Figure 11Schematic diagram of the interior of the purification box of the present invention;
[0035] Figure 12 Schematic diagram of the dehumidification box of the present invention;
[0036] Figure 13 Schematic diagram of the interior of the dehumidification box of the present invention;
[0037] Figure 14 Schematic diagram of the locking block of the present invention;
[0038] Figure 15 Schematic diagram of the interior of the locking chamber of the present invention.
[0039] In the figure: 1 - digestion instrument; 2 - gas delivery pipe; 3 - purification box; 4 - neutralizing liquid tank; 5 - ultrasonic atomizer; 6 - compressor; 7 - air pump; 8 - waste water tank; 9 - dehumidification box; 101 - lower box door; 102 - upper box door; 103 - control panel; 104 - power cord; 105 - support block; 106 - gas filter; 107 - power supply; 108 - digestion unit; 109 - digestion unit positioning buckle; 110 - partition board; 111 - digestion chamber; 112 - locking block; 113 - locking rod; 114 - locking chamber; 115 - locking plate; 116 - locking spring; 117 - locking slide bar; 118 - temperature sensor; 119 - digestion tank; 201 - reversing motor; 202 - ventilation fan; 203 - ventilation motor; 204 - air outlet head; 301 - waste gas pipe; 302 - waste gas pump; 303 - waste gas valve; 304 - waste gas outlet; 401 - neutralizing liquid valve; 402 - neutralizing liquid pump; 403 - neutralizing liquid pipe; 501 - atomizing liquid pump; 502 - atomizing liquid valve; 503 - atomizing liquid pipe; 504 - atomizing liquid nozzle; 505 - atomizing liquid pipe positioning plate; 601 - cold air pump; 602 - cold air pipe; 603 - cold air valve; 701 - air valve; 702 - intake pipe; 703 - heating chamber; 704 - intake air temperature sensor; 705 - heater; 706 - heating plate; 707 - filter plate; 708 - cleaning rod; 709 - cleaning wire; 710 - cleaning motor; 711 - positioning rod; 801 - water outlet pipe; 802 - water outlet valve; 803 - waste water pump; 804 - waste water valve; 805 - waste water pipe; 901 - dehumidification box door; 902 - dehumidification pipe; 903 - air outlet box; 904 - humidity sensor; 905 - acid-base concentration sensor; 906 - drying plate; 907 - activated carbon adsorption plate. Detailed implementation manners
[0040] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. All other embodiments obtained by those of ordinary skill in the art based on the embodiments of the present invention without creative efforts belong to the scope of protection of the present invention.
[0041] Embodiment 1 is given by Figures 1-6 and Figure 13 It includes a digestion instrument 1. The digestion instrument 1 is made of alloy material. The front end of the digestion instrument 1 is fixedly connected with a lower box door 101 by bolts. The lower box door 101 is made of alloy material. A top box door 102 is provided at the top of the lower box door 101 and is rotatably connected to the digestion instrument 1. The upper box door 102 is made of alloy material. A control panel 103 is fixed at the front end of the digestion instrument 1. A partition plate 110 is fixed inside the digestion instrument 1. The partition plate 110 is made of alloy material. A digestion chamber 111 is fixed at the top of the partition plate 110. The digestion chamber 111 is made of alloy material. A plurality of digestion units 108 are provided inside the digestion chamber 111. The digestion unit 108 is made of alloy material. An air duct 2 is provided inside the digestion chamber 111. The air duct 2 is made of alloy material. An air inlet pipe 702 is fixed at the rear of the air duct 2.
[0042] Advantageously, the digestion instrument 1 is used to support the entire device. The lower box door 101 can ensure the sealing of the lower end of the digestion instrument 1. The upper box door 102 can ensure the sealing of the digestion chamber 111. The control panel 103 is used to control the entire device. The partition plate 110 is used to partition the digestion instrument 1. The digestion chamber 111 is used for digestion. The digestion unit 108 is used to hold the digestion tank 119. The air duct 2 is used to supply the required gas to the digestion chamber 111. The air inlet pipe 702 is made of flexible material, so as to facilitate the rotation of the air duct 2.
[0043] At the bottom of the intake pipe 702, a heating chamber 703 is fixed. The heating chamber 703 is made of alloy material. At the bottom of the heating chamber 703, an air valve 701 is connected through a pipe. At the bottom of the air valve 701, an air pump 7 is fixed. At the top of the digestion chamber 111, an exhaust gas outlet 304 is also fixed. The exhaust gas outlet 304 is made of alloy material. At the bottom of the exhaust gas outlet 304, an exhaust gas pipe 301 is fixed. The exhaust gas pipe 301 is made of alloy material. The bottom of the exhaust gas pipe 301 passes through the partition plate 110 and a purification box 3 is fixed. The purification box 3 is made of alloy material. On the right side of the purification box 3, an ultrasonic atomizer 5 is fixed through an atomized liquid pipe 503. The atomized liquid pipe 503 is made of alloy material. At the front end of the ultrasonic atomizer 5, a neutralizing liquid box 4 is fixed through a neutralizing liquid pipe 403. At the front end of the purification box 3, a waste water tank 8 is fixed through a waste water pipe 805. Inside the digester 1, a power supply 107 is also fixed. At the right end of the power supply 107, a power cord 104 is fixed. At the rear end of the purification box 3, a dehumidifying box 9 is fixed through a dehumidifying pipe 902. The dehumidifying pipe 902 is made of alloy material. The dehumidifying box 9 is made of alloy material. At the rear end of the dehumidifying box 9, an air outlet box 903 is fixed through a pipe. The air outlet box 903 is made of alloy material. At the rear end of the air outlet box 903, a compressor 6 is provided. At the right end of the compressor 6, a cold air pipe 602 is provided. At the front end of the digester 1, two locking blocks 112 are also provided. The locking blocks 112 are made of alloy material. The locking blocks 112 are used to lock the upper box door 102.
[0044] Advantageously, the external air can be transported into the heating chamber 703 through the cooperation of the air pump 7 and the air valve 701, and further the heating chamber 703 is used to heat the air; the exhaust gas can be output through the exhaust gas outlet 304, and further the exhaust gas can be transported into the purification box 3 through the exhaust gas pipe 301, so that the exhaust gas can be purified through the purification box 3; the alkaline solution can be atomized through the ultrasonic atomizer 5, and further the atomized liquid nozzle 504 can be positioned through the atomized liquid pipe 503; the alkaline solution can be contained in the neutralizing liquid box 4, the completely neutralized waste liquid can be contained in the waste water tank 8, and the power supply 107 provides the energy required for the whole device; the drying plate 906 can be positioned through the dehumidifying box 9, the humidity sensor 904 and the acid-base concentration sensor 905 can be fixed through the air outlet box 903; the air can be cooled through the compressor 6, and the compressor 6 provides a cold storage function for the digester 1.
[0045] Beneficially, when the sample digestion in the digestion tank 111 is completed, the cold storage cavity releases cold to the digestion tank 111, accelerating the gas circulation refrigeration in the digestion tank 111. Connected to the purification box 3 through the gas transmission pipe 2, it achieves rapid refrigeration and the function of gas recovery and purification in the digestion tank 111. The present invention is a high-throughput digestion instrument in the field of element analysis and testing digestion technology. By heating the temperature of the sample digestion tank in the digestion tank 111 in an electric heating manner, it rapidly raises the temperature. After maintaining a constant digestion time, it centrally cools, exhausts, and purifies, so as to rapidly heat and digest the sample, rapidly cool down, and purify the gas, achieving an efficient digestion and a rapidly completed digestion instrument.
[0046] Embodiment 2, based on Embodiment 1, is given by Figures 7-10 Multiple support blocks 105 are fixed at the bottom of the digestion instrument 1. The support blocks 105 are made of alloy materials. Two gas filter meshes 106 are fixed at the rear of the digestion instrument 1. Multiple groups of digestion unit positioning buckles 109 are fixed inside the digestion tank 111. The digestion unit positioning buckles 109 are made of alloy materials. Each group of digestion unit positioning buckles 109 is slidably connected to the digestion unit 108 inside it. A digestion tank 119 is provided at the top of each digestion unit 108. A locking chamber 114 is provided inside the front end of the digestion instrument 1. A locking rod 113 is fixed inside the locking chamber 114. A locking plate 115 is fixed on the left side of the locking rod 113. The locking plate 115 is made of alloy materials. Two locking slide rods 117 are slidably connected to the left end of the locking plate 115. The locking slide rods 117 are made of alloy materials. A locking spring 116 is provided outside each locking slide rod 117. Each locking slide rod 117 is fixedly connected to the locking block 112 on its left side. Each locking block 112 can be snap-fitted with the groove on the upper box door 102.
[0047] Beneficially, the support blocks 105 are used to support the entire device. The gas filter meshes 106 facilitate the entry of air into the digestion instrument 1. The digestion unit positioning buckles 109 are used to position the digestion unit 108. The locking chamber 114 is used to fix the locking rod 113. The locking rod 113 is telescopic, so as to drive the movement of the locking plate 115. The locking plate 115 is used to position the locking slide rods 117. The locking slide rods 117 are used to position the locking blocks 112. The locking springs 116 are elastic, so as to drive the movement of the locking blocks 112.
[0048] A reversing motor 201 is fixed to the right end of the digestion chamber 111. The reversing motor 201 is rotationally connected to the air delivery pipe 2 through a rotating shaft. A plurality of air outlet heads 204 are fixed to the front end of the air delivery pipe 2. A temperature sensor 118 is also fixed to the top inside the digestion chamber 111. A positioning rod 711 is fixed to the top of the partition plate 110. The positioning rod 711 is made of an alloy material. A cleaning motor 710 is fixed to the top of the positioning rod 711. A cleaning rod 708 is rotationally connected to the left side of the cleaning motor 710. The cleaning rod 708 is made of an alloy material. A plurality of cleaning wires 709 are fixed to the left end of the cleaning rod 708. A filter plate 707 is provided on the left side of the plurality of cleaning wires 709 and is fixedly connected to the air pump 7. A ventilation motor 203 is also fixed to the rear end of the digestion chamber 111. A ventilation fan 202 is rotationally connected to the rear end of the ventilation motor 203.
[0049] Advantageously, the ventilation motor 203 can drive the ventilation fan 202 to rotate, and the ventilation fan 202 can increase the air flow rate, thereby ensuring the ventilation effect. The reversing motor 201 can drive the air delivery pipe 2 to rotate, and the air outlet head 204 facilitates air outlet. The temperature sensor 118 is used to monitor the temperature inside the digestion chamber 111. The positioning rod 711 is used to fix the cleaning motor 710. The cleaning motor 710 can drive the cleaning rod 708 to rotate. The cleaning rod 708 is used to fix the cleaning wires 709. The cleaning wires 709 are made of a flexible material. The cleaning wires 709 are used to clean the impurities on the surface of the filter plate 707.
[0050] An intake air temperature sensor 704 is fixed to the rear end of the heating chamber 703. A heater 705 is provided at the bottom of the intake air temperature sensor 704. A heating plate 706 is fixed to the front end of the heater 705. The heating plate 706 is fixed inside the heating chamber 703. The right end of the compressor 6 is fixedly connected to a cold air pump 601 through a pipeline. The top of the cold air pump 601 is fixedly connected to a cold air pipe 602. A cold air valve 603 is fixed to the upper end of the cold air pipe 602. The left end of the cold air valve 603 is fixedly connected to the intake pipe 702 at the top of the heating chamber 703 through a pipeline.
[0051] Advantageously, the intake air temperature sensor 704 is used to monitor the gas temperature inside the heating chamber 703. The heater 705 is used to control the operation of the heating plate 706. The heating plate 706 is made of a semiconductor material. The heating plate 706 is used to heat the air inside the heating chamber 703. The cold air pump 601 and the cold air valve 603 can transport cold air through the cold air pipe 602 into the intake pipe 702.
[0052] Before using this device, the staff place the digestion instrument 1 in the required position. Further, the staff electrically connect the digestion instrument 1 to an external power supply through the power cord 104. Further, the staff open the control panel 103 to control the contraction of the locking rod 113, thereby driving the locking plate 115 to move to the right, thereby driving the locking block 112 to move to the right, so that the upper box door 102 is disengaged.
[0053] Further, the staff open the upper box door 102. At this time, the staff place a plurality of digestion tanks 119 filled with acid solution inside onto the digestion unit 108. Further, the staff close the upper box door 102. Further, the control panel 103 controls the reset of the locking rod 113. At this time, due to the action of the locking spring 116 and the locking slide rod 117, the locking block 112 is clamped into the right end slot of the upper box door 102, thereby preventing the upper box door 102 from opening and ensuring the airtightness of the device. At this time, the control panel 103 controls the air pump 7 and the air valve 701 to work, so that external air enters the digestion instrument 1 through the gas filter net 106 at the top. At this time, the control panel 103 controls the ventilation motor 203 to work, so that the ventilation fan 202 rotates, thereby accelerating air circulation and then entering the air inlet pipe 702 through the filter plate 707. At this time, the control panel 103 controls the cleaning motor 710 to work, thereby driving the cleaning rod 708 to rotate, thereby driving the cleaning wire 709 to rotate, so as to prevent the filter plate 707 from being blocked. At this time, air is conveyed to the heating chamber 703 through the air inlet pipe 702.
[0054] Further, the control panel 103 controls the heater 705 and the heating plate 706 to work, thereby heating the air inside the heating chamber 703, and then delivering it to the inside of the air delivery pipe 2 through the air inlet pipe 702, and then outputting it to the inside of the digestion chamber 111 through the air outlet head 204, so as to heat the digestion chamber 111, thereby accelerating digestion. At this time, the temperature sensor 118 transmits the temperature information inside the digestion chamber 111 to the control panel 103. At the same time, the control panel 103 controls the reversing motor 201 to work, thereby driving the air delivery pipe 2 to rotate, so as to ensure the uniformity of heating, thus ensuring the heating effect, and further ensuring the stability of the accuracy of digestion. When digestion is carried out for a certain period of time, the control panel 103 controls the heater 705 to stop working, and at the same time controls the air pump 7 and the air valve 701 to stop working. Further, the control panel 103 controls the compressor 6 to work, thereby cooling the external air, and then delivering the cold air to the inside of the air inlet pipe 702 through the cold air pump 601 and the cold air valve 603, and then outputting it through the air outlet head 204, so as to reduce the temperature inside the digestion chamber 111. At the same time, the control panel 103 controls the reversing motor 201 to work again, so that the digestion chamber 111 cools down evenly. When the temperature of the digestion chamber 111 drops to room temperature, the control panel 103 controls the compressor 6 to stop working. Further, the control panel 103 controls the upper box door 102 to open, so as to take out the digestion tank 119 that has completed digestion.
[0055] Embodiment 3, on the basis of Embodiment 1, is given by Figures 11-12 The right end of the heating chamber 703 is provided with an exhaust gas valve 303 fixedly connected to the exhaust gas outlet 304, and the bottom of the exhaust gas valve 303 is provided with an exhaust gas pump 302 fixedly connected to the partition plate 110.
[0056] Advantageously, the exhaust gas pump 302 and the exhaust gas valve 303 cooperate to deliver the exhaust gas inside the digestion chamber 111 to the inside of the exhaust gas pipe 301.
[0057] The exhaust gas pump 302 is fixedly connected to the exhaust gas outlet 304. Inside the purification box 3, there is an atomized liquid spray head 504. The right end of the atomized liquid spray head 504 is fixedly connected to the atomized liquid pipe 503. The atomized liquid pipe 503 is fixedly connected to the upper surface inside the purification box 3 through the atomized liquid pipe positioning plate 505. The atomized liquid pipe positioning plate 505 is made of alloy material. The right end of the atomized liquid pipe 503 is fixed with an atomized liquid valve 502. The right end of the atomized liquid valve 502 is fixed with an atomized liquid pump 501. The right end of the atomized liquid pump 501 is connected to the ultrasonic atomizer 5 through a pipe. The front end of the ultrasonic atomizer 5 is fixed with a neutralizing liquid pump 402 through the neutralizing liquid pipe 403. The front end of the neutralizing liquid pump 402 is fixed with a neutralizing liquid valve 401 through the neutralizing liquid pipe 403.
[0058] Advantageously, the neutralizing liquid valve 401 and the neutralizing liquid pump 402 can transport the alkaline solution inside the neutralizing liquid tank 4 to the ultrasonic atomizer 5. The atomized liquid valve 502 and the atomized liquid pump 501 cooperate to transport the alkaline solution atomized by the ultrasonic atomizer 5 to the atomized liquid spray head 504 through the atomized liquid pipe 503. The atomized liquid spray head 504 is used to spray the alkaline solution, and the atomized liquid pipe positioning plate 505 is used to position the atomized liquid pipe 503.
[0059] The front end of the purification box 3 is fixed with a waste water valve 804. The front end of the waste water valve 804 is fixed with a waste water pump 803 through the waste water pipe 805. The front end of the waste water tank 8 is fixed with a water outlet pipe 801. The water outlet pipe 801 is made of flexible material. The right end of the water outlet pipe 801 is fixed with a water outlet valve 802.
[0060] Advantageously, the waste water valve 804 and the waste water pump 803 cooperate to transport the waste liquid inside the purification box 3 to the waste water tank 8. The water outlet pipe 801 facilitates the output of the waste liquid inside the waste water tank 8, and the water outlet valve 802 can control the output of the waste liquid inside the waste water tank 8.
[0061] The back end of the purification box 3 is provided with a dehumidification box door 901. The dehumidification box door 901 is fixedly connected to the dehumidification box 9 through bolts. Inside the dehumidification box 9, there is a drying plate 906. In front of the drying plate 906, there is an activated carbon adsorption plate 907. Inside the air outlet box 903, there is a humidity sensor 904 fixed. On the left side of the humidity sensor 904, there is an acid-base concentration sensor 905 fixed.
[0062] Beneficially, the dehumidification chamber door 901 can ensure the sealing of the dehumidification chamber 9. The drying plate 906 is used to dry the air inside the purification chamber 3. The activated carbon adsorption plate 907 is used to adsorb the unreacted acid and alkali solutions in the gas inside the dehumidification chamber 9. The humidity sensor 904 is used to monitor the dryness and humidity of the gas output from the dehumidification chamber 9. The acid-base concentration sensor 905 is used to monitor the pH value of the gas output from the dehumidification chamber 9.
[0063] When reducing the temperature inside the digestion chamber 111, the control panel 103 controls the exhaust gas pump 302 and the exhaust gas valve 303 to work simultaneously. As a result, while cold air enters the digestion chamber 111, the acidic gas leaked from the digestion chamber 111 due to digestion is transported through the exhaust gas outlet 304 to the exhaust gas pipe 301, and then to the inside of the purification chamber 3. At this time, the control panel 103 controls the neutralizing liquid valve 401 and the neutralizing liquid pump 402 to work, so as to transport the alkaline solution to the ultrasonic atomizer 5. Then, the ultrasonic atomizer 5 atomizes the alkaline solution. Further, the control panel 103 controls the atomized liquid pump 501 and the atomized liquid valve 502 to work, so as to transport the atomized alkaline liquid through the atomized liquid pipe 503 to the atomized liquid nozzle 504, so as to humidify and neutralize the acidic gas transported from the exhaust gas pipe 301 to the inside of the purification chamber 3. At this time, the control panel 103 controls the waste water pump 803 and the waste water valve 804 to work, so as to pump the neutralized waste liquid inside the purification chamber 3 to the waste water tank 8.
[0064] Furthermore, the gas neutralized inside the purification chamber 3 is transported to the inside of the dehumidification chamber 9 through the dehumidification pipe 902. At this time, due to the action of the drying plate 906 and the activated carbon adsorption plate 907, the unreacted acid and alkali solutions in the air inside the dehumidification chamber 9 can be adsorbed while the gas is dried, and then further transported to the inside of the air outlet chamber 903. At this time, the control panel 103 can monitor the humidity and pH value of the purified gas inside the air outlet chamber 903 through the humidity sensor 904 and the acid-base concentration sensor 905. If the purified gas meets the emission standards, the purified gas is directly discharged into the environment, thus realizing green, environmentally friendly, high-throughput and efficient digestion. If the pH value and humidity are unqualified, the control panel 103 will alarm. Further, the staff replaces the drying plate 906 and the activated carbon adsorption plate 907, and at the same time adjusts the atomized liquid valve 502 to control the neutralization accuracy. When the temperature reduction is completed, the staff opens the lower chamber door 101, and further opens the water outlet valve 802 to collect the waste liquid, so as to prevent the waste liquid from polluting the environment.
[0065] The working process of the present invention is as follows: Before using this device, the staff places the digestion instrument 1 in the required position. Further, the staff electrically connects the power cord 104 to an external power source. Further, the staff opens the control panel 103 to control the contraction of the locking rod 113, thereby driving the locking plate 115 to move to the right, thereby driving the locking block 112 to move to the right, so that the upper box door 102 is disengaged. Further, the staff opens the upper box door 102. At this time, the staff places a plurality of digestion tanks 119 filled with acid solution inside into the digestion unit 108. Further, the staff closes the upper box door 102. Further, the control panel 103 controls the reset of the locking rod 113. At this time, due to the action of the locking spring 116 and the locking slide rod 117, the locking block 112 is snapped into the right end slot of the upper box door 102, thereby preventing the upper box door 102 from opening, thus ensuring the sealing performance of the device. At this time, the control panel 103 controls the air pump 7 and the air valve 701 to work, so that external air enters the digestion instrument 1 through the gas filter screen 106 at the top. At this time, the control panel 103 controls the ventilation motor 203 to work, so that the ventilation fan 202 rotates, thereby accelerating air circulation, and then enters the air inlet pipe 702 through the filter plate 707. At this time, the control panel 103 controls the cleaning motor 710 to work, thereby driving the cleaning rod 708 to rotate, thereby driving the cleaning wire 709 to rotate, so as to prevent the filter plate 707 from being blocked. At this time, the air is transported to the heating chamber 703 through the air inlet pipe 702. Further, the control panel 103 controls the heater 705 and the heating plate 706 to work, so as to heat the air inside the heating chamber 703, and then transport it to the air delivery pipe 2 through the air inlet pipe 702, and then output it to the digestion chamber 111 through the air outlet head 204, so as to heat the digestion chamber 111, thereby accelerating digestion. At this time, the temperature sensor 118 transmits the temperature information inside the digestion chamber 111 to the control panel 103. At the same time, the control panel 103 controls the reversing motor 201 to work, thereby driving the air delivery pipe 2 to rotate, so as to ensure the uniformity of heating, thus ensuring the heating effect, and thus ensuring the accuracy and stability of digestion. When digestion is carried out for a certain period of time, the control panel 103 controls the heater 705 to stop working, and at the same time controls the air pump 7 and the air valve 701 to stop working. Further, the control panel 103 controls the compressor 6 to work, so as to cool the external air, and then transport the cold air to the air inlet pipe 702 through the cold air pump 601 and the cold air valve 603, and then output it through the air outlet head 204, so as to reduce the temperature inside the digestion chamber 111. At the same time, the control panel 103 controls the reversing motor 201 to work again,Thus, the digestion chamber 111 is cooled evenly. At the same time, the control panel 103 controls the waste gas pump 302 and the waste gas valve 303 to work simultaneously, so that cold air enters the interior of the digestion chamber 111 while the acidic gas leaked due to digestion in the interior of the digestion chamber 111 is transported to the waste gas pipe 301 through the waste gas outlet 304, and then transported to the interior of the purification tank 3. At this time, the control panel 103 controls the neutralizing liquid valve 401 and the neutralizing liquid pump 402 to work, so as to transport the alkaline solution to the ultrasonic atomizer 5. Then, the ultrasonic atomizer 5 atomizes the alkaline solution. Further, the control panel 103 controls the atomized liquid pump 501 and the atomized liquid valve 502 to work, so as to transport the atomized alkaline liquid through the atomized liquid pipe 503 to the atomized liquid nozzle 504, so as to humidify and neutralize the acidic gas transported from the waste gas pipe 301 to the interior of the purification tank 3. At this time, the control panel 103 controls the waste water pump 803 and the waste water valve 804 to work, so as to pump the neutralized waste liquid in the interior of the purification tank 3 to the waste water tank 8. Further, the gas neutralized in the interior of the purification tank 3 is transported to the interior of the dehumidification tank 9 through the dehumidification pipe 902. At this time, due to the action of the drying plate 906 and the activated carbon adsorption plate 907, the unreacted acid-base solution in the air in the interior of the dehumidification tank 9 can be adsorbed while the gas is dried, and then transported to the interior of the air outlet tank 903. At this time, the control panel 103 can monitor the humidity and pH value of the purified gas in the interior of the air outlet tank 903 through the humidity sensor 904 and the acid-base concentration sensor 905. If the purified gas meets the emission standard, the purified gas is directly discharged into the environment, thus realizing green, environmentally friendly, high-throughput and efficient digestion. If the pH value and humidity are unqualified, the control panel 103 gives an alarm. Further, the staff replaces the drying plate 906 and the activated carbon adsorption plate 907, and at the same time adjusts the atomized liquid valve 502 to control the neutralization accuracy. When the digestion chamber 111 cools down to room temperature, the control panel 103 controls the compressor 6 to stop working. Further, the control panel 103 controls the upper box door 102 to open, so that the digested digestion tank 119 can be taken out. Further, the staff opens the lower box door 101, and further opens the water outlet valve 802, so as to collect the waste liquid, thus preventing the waste liquid from polluting the environment.,
[0066] It should be noted that in this text, relational terms such as first and second are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any actual relationship or order between these entities or operations. Moreover, the terms "comprising", "including" or any other variant thereof are intended to cover non-exclusive inclusion, such that a process, method, article or device comprising a series of elements not only includes those elements but also includes other elements not expressly listed, or further includes elements inherent to such process, method, article or device.
[0067] Although the embodiments of the present invention have been shown and described, those of ordinary skill in the art can understand that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principles and spirit of the present invention. The scope of the present invention is defined by the appended claims and their equivalents.
Claims
1. A high-throughput electrothermal digestion instrument, characterized in that: It includes a digestion instrument. The front end of the digestion instrument is fixedly connected with a lower box door through bolts. There is an upper box door on the top of the lower box door, which is rotatably connected to the digestion instrument. A control panel is fixed at the front end of the digestion instrument. A partition board is fixed inside the digestion instrument. A digestion chamber is fixed on the top of the partition board. There are multiple digestion units inside the digestion chamber. An air delivery pipe is arranged inside the digestion chamber. An intake pipe is fixed at the rear of the air delivery pipe. A heating chamber is fixed at the bottom of the intake pipe. An air valve is connected to the bottom of the heating chamber through a pipeline. An air pump is fixed at the bottom of the air valve. An exhaust gas outlet is also fixed at the top of the digestion chamber. A waste gas pipe is fixed at the bottom of the exhaust gas outlet. The bottom of the waste gas pipe passes through the partition board and is fixed with a purification box. An ultrasonic atomizer is fixed to the right side of the purification box through an atomized liquid pipe. A neutralizing liquid box is fixed to the front end of the ultrasonic atomizer through a neutralizing liquid pipe. A waste water box is fixed to the front end of the purification box through a waste water pipe. A power supply is also fixed inside the digestion instrument. A power cord is fixed to the right end of the power supply. A dehumidifying box is fixed to the rear end of the purification box through a dehumidifying pipe. An air outlet box is fixed to the rear end of the dehumidifying box through a pipeline. A compressor is arranged at the rear end of the air outlet box. A cold air pipe is arranged at the right end of the compressor. There are also two locking blocks at the front end of the digestion instrument.
2. The high-throughput electrothermal digestion instrument according to claim 1, wherein: Multiple support blocks are fixed at the bottom of the digestion instrument. Two gas filters are fixed at the rear of the digestion instrument. Multiple groups of digestion unit positioning buckles are fixed inside the digestion chamber. Each group of digestion unit positioning buckles is slidably connected with the digestion unit inside it. A digestion tank is arranged at the top of each digestion unit.
3. The high-throughput electrothermal digestion instrument according to claim 2, characterized in that: A locking chamber is arranged inside the front end of the digestion instrument. A locking rod is fixed inside the locking chamber. A locking plate is fixed on the left side of the locking rod. Two locking sliding rods are slidably connected to the left end of the locking plate. A locking spring is arranged outside each locking sliding rod. Each locking sliding rod is fixedly connected with the locking block on its left side. Each locking block can be clamped with the groove on the upper box door.
4. The high-throughput electrothermal digestion instrument according to claim 2, wherein: A reversing motor is fixed at the right end of the digestion chamber. The reversing motor is rotatably connected with the air delivery pipe through a rotating shaft. Multiple air outlet heads are fixed at the front end of the air delivery pipe. A temperature sensor is also fixed at the top end inside the digestion chamber.
5. The high-throughput electrothermal digestion instrument according to claim 1, wherein: A positioning rod is fixed on the top of the partition board. A cleaning motor is fixed on the top of the positioning rod. A cleaning rod is rotatably connected to the left side of the cleaning motor. Multiple cleaning wires are fixed to the left end of the cleaning rod. A filter plate is arranged on the left side of the multiple cleaning wires and is fixedly connected with the air pump.
6. The high-throughput electrothermal digestion instrument according to claim 5, wherein: A ventilation motor is also fixed at the rear end of the digestion chamber. A ventilation fan is rotatably connected to the rear end of the ventilation motor. An intake air temperature sensor is fixed at the rear end of the heating chamber. A heater is arranged at the bottom of the intake air temperature sensor. A heating plate is fixed to the front end of the heater and is fixed inside the heating chamber.
7. The high-throughput electrothermal digestion instrument according to claim 6, characterized in that: A waste gas valve is provided at the right end of the heating chamber and is fixedly connected to the waste gas outlet. A waste gas pump is provided at the bottom of the waste gas valve and is fixedly connected to the partition plate. The waste gas pump is fixedly connected to the waste gas outlet. An atomized liquid nozzle is provided inside the purification box. The right end of the atomized liquid nozzle is fixedly connected to the atomized liquid pipe. The atomized liquid pipe is fixedly connected to the upper surface inside the purification box through the atomized liquid pipe positioning plate.
8. The high-throughput electrothermal digestion instrument according to claim 7, wherein: An atomized liquid valve is fixed at the right end of the atomized liquid pipe. An atomized liquid pump is fixed at the right end of the atomized liquid valve. The right end of the atomized liquid pump is fixedly connected to the ultrasonic atomizer through a pipe. A neutralizing liquid pump is fixed at the front end of the ultrasonic atomizer through the neutralizing liquid pipe. A neutralizing liquid valve is fixed at the front end of the neutralizing liquid pump through the neutralizing liquid pipe.
9. The high-throughput electrothermal digestion instrument according to claim 7, characterized in that: A waste water valve is fixed at the front end of the purification box. A waste water pump is fixed at the front end of the waste water valve through the waste water pipe. An outlet pipe is fixed at the front end of the waste water tank. An outlet valve is fixed at the right end of the outlet pipe.
10. The high-throughput electrothermal digestion instrument according to claim 9, wherein: A dehumidification box door is provided at the rear end of the purification box. The dehumidification box door is tightly connected to the dehumidification box through bolts. A drying plate is provided inside the dehumidification box. An activated carbon adsorption plate is provided in front of the drying plate. A humidity sensor is fixed inside the air outlet box. An acid-base concentration sensor is fixed on the left side of the humidity sensor. The right end of the compressor is fixedly connected to a cold air pump through a pipe. The top of the cold air pump is fixedly connected to the cold air pipe. A cold air valve is fixed at the upper end of the cold air pipe. The left end of the cold air valve is fixedly connected to the intake pipe at the top of the heating chamber through a pipe.