Antique-process cold soap and preparation method thereof

Abstract

The invention discloses an ancient cold soap and a preparation method thereof. The traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 5-15 parts of sandalwood, 3-10 parts of ginseng, 3-8 parts of lucid ganoderma, 2-6 parts of pearl powder, 10-20 parts of white morning glory, 8-15 parts of radix ampelopsis, 5-12 parts of bletilla striata, 5-10 parts of white lotus seed, 8-15 parts of white poria, 10-20 parts of radix angelicae, 8-15 parts of bighead atractylodes rhizome, 3-8 parts of white lilac, 3-8 parts of rhizoma typhonii, 5-12 parts of silkworm larva, 3-8 parts of radix saposhnikoviae, 5-12 parts of white hyacinth bean and 3-8 parts of rhizoma nardostachyos; , 3-8 parts of ligusticum chuanxiong hort, 2-6 parts of radix angelicae pubescentis, 2-6 parts of notopterygium root and 5-12 parts of honeysuckle. By optimizing the formula and the process, the problems that the traditional Yufeng powder is inconvenient to use and the beautifying effect of the existing cold soap is limited are solved, and the cold soap which is easy to use and store and has a remarkable beautifying effect is provided.

Description

Technical Field

[0001] The present invention relates to the technical field of daily chemical products, and particularly relates to an ancient method cold-processed soap and a preparation method thereof. Background Art

[0002] As is well known, in terms of the component characteristics of cold-processed soap, the greatest advantage of cold-processed soap is that it retains more natural components. During the production process, due to the relatively low temperature, the original nutrients in vegetable oils, such as vitamins, minerals, and some unsaturated fatty acids beneficial to the skin, can be retained in large quantities. At the same time, the natural glycerol generated by the saponification reaction will also be retained in the soap body, and glycerol has good moisturizing effects, which can help the skin lock in moisture while cleaning the skin, preventing the skin from becoming overly dry. In terms of usage efficacy, cold-processed soap has the characteristic of mild cleaning. It can effectively remove dirt and excess oil on the skin surface, but it will not overly clean like some chemical detergents, damaging the skin's sebum film and acid-base balance. It is relatively friendly to the skin and suitable for a variety of skin types. Especially for people with sensitive skin, it is a relatively mild and natural choice for cleaning and skin care.

[0003] Traditional Yurong San exists in the form of powder. When in use, it needs to be mixed with water into a paste, and has the following defects: inconvenient to use: it needs to be prepared and used immediately, and it is difficult to control the dosage; active ingredients are easy to oxidize: the powder state leads to poor stability of active ingredients; short shelf life: it is easy to get damp and deteriorate after opening; existing cold-processed soaps mostly adopt basic oil formulas, with insufficient utilization rate of traditional Chinese medicine active ingredients, and there are: incomplete saponification reaction: resulting in residual free alkali (pH value > 8.5); single addition method of traditional Chinese medicine ingredients: direct mixing leads to loss of active ingredients; single efficacy: only having the cleaning function, lacking compound beauty effects such as whitening and freckle removal. Summary of the Invention

[0004] The technical problem to be solved by the present invention is to overcome the defects of the prior art and provide an ancient method cold-processed soap and a preparation method thereof.

[0005] To solve the above technical problems, the present invention provides the following technical solutions:

[0006] An ancient method cold-processed soap and a preparation method thereof according to the present invention are prepared from the following raw materials in parts by weight:

[0007] Herbal Chinese medicine composition: 5 - 15 parts of sandalwood, 3 - 10 parts of ginseng, 3 - 8 parts of ganoderma lucidum, 2 - 6 parts of pearl powder, 10 - 20 parts of white morning glory, 8 - 15 parts of ampelopsis japonica, 5 - 12 parts of bletilla striata, 5 - 10 parts of white lotus core, 8 - 15 parts of poria cocos, 10 - 20 parts of angelica dahurica, 8 - 15 parts of atractylodes macrocephala, 3 - 8 parts of white lilac, 3 - 8 parts of typhonium giganteum, 5 - 12 parts of bombyx batryticatus, 3 - 8 parts of ledebouriella seseloides, 5 - 12 parts of dolichos lablab, 3 - 8 parts of nardostachys jatamansi, 3 - 8 parts of ligusticum wallichii, 2 - 6 parts of angelica pubescens, 2 - 6 parts of notopterygium incisum, 5 - 12 parts of honeysuckle;

[0008] Natural vegetable oil: 30 - 50 parts of olive oil, 20 - 30 parts of coconut oil, 15 - 25 parts of palm oil, 5 - 10 parts of evening primrose oil, 5 - 10 parts of grape seed oil, 3 - 8 parts of jojoba oil;

[0009] Edible caustic soda: 8 - 12 parts;

[0010] Qianjin Yurong medicinal soup: 15 - 25 parts;

[0011] Qianjin Yurong medicinal powder: 5 - 15 parts.

[0012] As a preferred technical solution of the present invention, the herbal Chinese medicine composition further comprises 3 - 8 parts of centella asiatica and 2 - 5 parts of rosemary by weight.

[0013] As a preferred technical solution of the present invention, the preparation method of the Qianjin Yurong medicinal soup is: mixing the herbal Chinese medicine composition and water in a ratio of 1:5 - 1:8, boiling with strong fire and then decocting with slow fire for 30 - 60 minutes, filtering to obtain the filtrate and concentrating it to 1 / 3 - 1 / 2 of the original volume.

[0014] As a preferred technical solution of the present invention, the preparation method of the Qianjin Yurong medicinal powder is to pulverize the herbal Chinese medicine composition to 100 - 200 meshes and obtain it after drying at 60 - 80 °C for 2 - 4 hours.

[0015] The present invention also discloses a preparation method of an ancient - method cold - made soap, comprising the following steps:

[0016] (1) Preparation of the oil phase: Mixing olive oil, coconut oil, palm oil, evening primrose oil, grape seed oil, and jojoba oil, adding the herbal Chinese medicine composition, and soaking at a constant temperature of 40 - 50 °C for 48 - 72 hours to obtain Qianjin Yurong oil;

[0017] (2) Preparation of the water phase: Slowly adding the edible caustic soda to the Qianjin Yurong medicinal soup, stirring while adding until completely dissolved, and cooling to 30 - 40 °C;

[0018] (3) Saponification reaction: Slowly adding the water phase to the oil phase and continuously stirring until the mixture reaches the Trace state;

[0019] (4) Add active ingredients: Add Qianjin Yurong powder under Trace state and continue stirring for 10 - 15 minutes;

[0020] (5) Molding and curing: Inject the mixed liquid into the mold and let it stand and cure for 48 hours in an environment of 25 - 30 °C;

[0021] (6) Aging treatment: After demolding, place it in a ventilated and dry place for aging for 4 - 8 weeks;

[0022] (7) Shaping and processing: Shred the aged soap body, press it into shape after being beaten 5 - 8 times, and then dry it to a moisture content of ≤15%;

[0023] As a preferred technical solution of the present invention, in step (3), the stirring speed is 200 - 300 revolutions per minute and the stirring time is 60 - 90 minutes.

[0024] As a preferred technical solution of the present invention, in step (4), 0.1 - 0.5% by weight of natural essential oil can also be added, and the essential oil is selected from one or more of rose essential oil, lavender essential oil or neroli essential oil.

[0025] As a preferred technical solution of the present invention, in step (6), the humidity of the aging environment is controlled at 40 - 60% and the temperature is controlled at 20 - 25 °C.

[0026] As a preferred technical solution of the present invention, in step (7), the beating process adopts intermittent beating, and the interval time between each beating is 30 - 60 seconds.

[0027] Compared with the prior art, the beneficial effects of the present invention are as follows:

[0028] 1: By optimizing the formula and process, the present invention solves the problems of inconvenient use of traditional Yurong powder and limited beauty effects of existing cold-processed soaps, and provides a cold-processed soap that is easy to use, store and has significant beauty effects.

[0029] 2: The present invention has a skin cleansing effect: The combination of the ingredients of the Qianjin Yurong formula and natural vegetable oils makes the cold-processed soap have multiple beauty effects such as moisturizing, whitening and freckle removal. The form of the cold-processed soap is convenient for daily use and easy to store. All ingredients are natural raw materials, environmentally friendly and suitable for sensitive skin. Specific Embodiments

[0030] The following describes the preferred embodiments of the present invention. It should be understood that the preferred embodiments described herein are only used to illustrate and explain the present invention and are not used to limit the present invention.

[0031] Example 1

[0032] The present invention provides a traditional cold-processed soap prepared from the following raw materials in parts by weight:

[0033] Herbal Chinese medicine composition: 5 - 15 parts of sandalwood, 3 - 10 parts of ginseng, 3 - 8 parts of ganoderma lucidum, 2 - 6 parts of pearl powder, 10 - 20 parts of white morning glory, 8 - 15 parts of ampelopsis japonica, 5 - 12 parts of bletilla striata, 5 - 10 parts of white lotus core, 8 - 15 parts of poria cocos, 10 - 20 parts of angelica dahurica, 8 - 15 parts of atractylodes macrocephala, 3 - 8 parts of white lilac, 3 - 8 parts of typhonium giganteum, 5 - 12 parts of bombyx batryticatus, 3 - 8 parts of ledebouriella seseloides, 5 - 12 parts of lablab purpureus, 3 - 8 parts of nardostachys jatamansi, 3 - 8 parts of ligusticum chuanxiong, 2 - 6 parts of angelica pubescens, 2 - 6 parts of notopterygium incisum, 5 - 12 parts of honeysuckle;

[0034] Natural vegetable oil: 30 - 50 parts of olive oil, 20 - 30 parts of coconut oil, 15 - 25 parts of palm oil, 5 - 10 parts of evening primrose oil, 5 - 10 parts of grape seed oil, 3 - 8 parts of jojoba oil;

[0035] Edible sodium hydroxide: 8 - 12 parts;

[0036] Qianjin Yurong medicinal decoction: 15 - 25 parts;

[0037] Qianjin Yurong medicinal powder: 5 - 15 parts.

[0038] The herbal Chinese medicine composition also contains 3 - 8 parts of centella asiatica and 2 - 5 parts of rosemary by weight.

[0039] The preparation method of Qianjin Yurong medicinal decoction is: mixing the herbal Chinese medicine composition and water in a ratio of 1:5 - 1:8, boiling with strong fire and then decocting with slow fire for 30 - 60 minutes, filtering to obtain the filtrate and concentrating it to 1 / 3 - 1 / 2 of the original volume.

[0040] The preparation method of Qianjin Yurong medicinal powder is to crush the herbal Chinese medicine composition to 100 - 200 meshes and obtain it after drying at 60 - 80 °C for 2 - 4 hours.

[0041] A preparation method of ancient - method cold - made soap, comprising the following steps:

[0042] (1) Preparation of oil phase: Mixing olive oil, coconut oil, palm oil, evening primrose oil, grape seed oil, and jojoba oil, adding the herbal Chinese medicine composition, and soaking at a constant temperature of 40 - 50 °C for 48 - 72 hours to obtain Qianjin Yurong oil;

[0043] (2) Preparation of water phase: Slowly adding edible sodium hydroxide to Qianjin Yurong medicinal decoction, stirring while adding until completely dissolved, and cooling to 30 - 40 °C;

[0044] (3) Saponification reaction: Slowly adding the water phase to the oil phase, continuously stirring until the mixture reaches the Trace state;

[0045] (4) Adding active ingredients: Adding Qianjin Yurong medicinal powder in the Trace state and continuing to stir for 10 - 15 minutes;

[0046] (5) Molding and curing: Inject the mixture into the mold and let it stand and cure for 48 hours at 25 - 30 °C.

[0047] (6) Aging treatment: After demolding, place it in a ventilated and dry place for aging for 4 - 8 weeks.

[0048] (7) Forming process: Shred the aged soap body, press it into shape after being beaten 5 - 8 times, and then dry it until the moisture content ≤ 15%.

[0049] In step (3), the stirring speed is 200 - 300 revolutions per minute and the stirring time is 60 - 90 minutes.

[0050] In step (4), 0.1 - 0.5% by weight of natural essential oil can also be added, and the essential oil is selected from one or more of rose essential oil, lavender essential oil or neroli essential oil.

[0051] In step (6), the humidity of the aging environment is controlled at 40 - 60% and the temperature is controlled at 20 - 25 °C.

[0052] In step (7), the beating process is intermittent beating, and the interval time between each beating is 30 - 60 seconds.

[0053] The specific formula is as follows: Herbal traditional Chinese medicine composition: 8 parts of sandalwood, 5 parts of ginseng, 4 parts of ganoderma lucidum, 3 parts of pearl powder, 15 parts of white morning glory, 10 parts of ampelopsis japonica, 8 parts of bletilla striata, 6 parts of white lotus core, 12 parts of poria cocos, 15 parts of angelica dahurica, 10 parts of atractylodes macrocephala, 5 parts of white lilac, 4 parts of typhonium giganteum, 7 parts of bombyx batryticatus, 4 parts of ledebouriella seseloides, 8 parts of white hyacinth bean, 5 parts of nardostachys jatamansi, 5 parts of chuanxiong, 3 parts of angelica pubescens, 3 parts of notopterygium incisum, 8 parts of honeysuckle, Natural vegetable oil: 40 parts of olive oil, 25 parts of coconut oil, 20 parts of palm oil, 7 parts of evening primrose oil, 6 parts of grape seed oil, 5 parts of jojoba oil, Edible caustic soda: 10 parts, Qianjin Yurong medicinal soup: 20 parts (concentrated liquid), Qianjin Yurong medicinal powder: 10 parts.

[0054] Adopt a combination of 21 kinds of herbal traditional Chinese medicines, among which:

[0055] Whitening group: white morning glory, ampelopsis japonica, poria cocos (inhibiting the activity of tyrosinase)

[0056] Repair group: ginseng, ganoderma lucidum, pearl powder (promoting collagen synthesis)

[0057] Anti - inflammatory group: honeysuckle, ledebouriella seseloides, nardostachys jatamansi (inhibiting the secretion of inflammatory factors)

[0058] Oil - soluble extraction: Cold - soak with olive oil to extract fat - soluble active ingredients (total flavonoid content ≥ 1.2%)

[0059] Water - soluble concentration: The concentrated medicinal soup retains water - soluble polysaccharides (content ≥ 3.5%)

[0060] Micro-powder addition: Ultrafine comminution technology (particle size ≤ 100 μm) improves the transdermal absorption rate

[0061] Gradient temperature reduction (45°C → 35°C → 25°C) is used to control the saponification reaction process

[0062] Evening primrose oil is added (γ-linolenic acid content ≥ 9%) to adjust the fatty acid ratio

[0063] Preparation of Qianjin Yurong Oil

[0064] 400 g of olive oil + 200 g of traditional Chinese medicine composition → Constant temperature extraction at 45°C for 72 hours

[0065] Detection index: Total polyphenol content 2.1 mg GAE / g

[0066] Concentration of medicinal soup

[0067] 500 g of traditional Chinese medicine composition + 3000 ml of water → Boil over high heat and then concentrate to 1000 ml over low heat

[0068] Density: 1.12 g / cm 3 (25°C)

[0069] Saponification reaction

[0070] Mixed oil phase (400 g of olive oil + 250 g of coconut oil + 200 g of palm oil + 70 g of evening primrose oil + 60 g of grape seed oil + 50 g of jojoba oil)

[0071] Preparation of lye: 100 g of NaOH + 200 g of medicinal soup → Cool to 35°C

[0072] Stirring parameters: 250 rpm, continue for 90 minutes until in Trace state

[0073] Aging process

[0074] Environmental control: Temperature 22 ± 2°C, humidity 50 ± 5%

[0075] Aging period: 6 weeks (weight loss rate per week controlled at 3 - 5%)

[0076] Efficacy-enhanced formula

[0077] Add 3% of Centella asiatica extract (total triterpenoid content ≥ 20%)

[0078] Adjust the fatty acid ratio: Olive oil : Coconut oil = 5:3

[0079] Test results:

[0080] Elastase inhibition rate: 78.6% (anti-wrinkle effect improved by 23%)

[0081] Formula for sensitive skin

[0082] Remove highly sensitive ingredients such as Typhonium giganteum and Galanthus nivalis

[0083] Increase oat β-glucan by 2%

[0084] Test data:

[0085] Transepidermal water loss (TEWL): 12.5g / m 2 / h (22% lower than the basic formula)

[0086] The comparative test is as follows:

[0087] Test items The product of the present invention Commercially available high-end cold-processed soap Free alkali content 0.08％ 0.32％ pH value 7.2-7.8 8.1-8.9 Richness of foam 120 ml (Ross-Miles foam apparatus) 95ml Whitening effect onset time 14 days 28 days

[0088] Finally, it should be noted that the above are only the preferred embodiments of the present invention and are not used to limit the present invention. Although the present invention has been described in detail with reference to the foregoing embodiments, those skilled in the art can still modify the technical solutions described in the foregoing embodiments, or perform equivalent replacements for some of the technical features. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included within the protection scope of the present invention.

Claims

1. A cold-processed soap made by ancient methods, characterized in that, Prepared from the following raw materials by weight: Herbal Chinese medicine composition: 5 - 15 parts of sandalwood, 3 - 10 parts of ginseng, 3 - 8 parts of ganoderma lucidum, 2 - 6 parts of pearl powder, 10 - 20 parts of white morning glory, 8 - 15 parts of ampelopsis japonica, 5 - 12 parts of bletilla striata, 5 - 10 parts of white lotus core, 8 - 15 parts of poria cocos, 10 - 20 parts of angelica dahurica, 8 - 15 parts of atractylodes macrocephala, 3 - 8 parts of white lilac, 3 - 8 parts of typhonium giganteum, 5 - 12 parts of bombyx batryticatus, 3 - 8 parts of ledebouriella seseloides, 5 - 12 parts of dolichos lablab, 3 - 8 parts of nardostachys jatamansi, 3 - 8 parts of chuanxiong, 2 - 6 parts of angelica pubescens, 2 - 6 parts of notopterygium incisum, 5 - 12 parts of honeysuckle; Natural vegetable oil: 30 - 50 parts of olive oil, 20 - 30 parts of coconut oil, 15 - 25 parts of palm oil, 5 - 10 parts of evening primrose oil, 5 - 10 parts of grape seed oil, 3 - 8 parts of jojoba oil; Edible sodium hydroxide: 8 - 12 parts; Qianjin Yurong medicinal soup: 15 - 25 parts; Qianjin Yurong medicinal powder: 5 - 15 parts.

2. The ancient cold-processed soap according to claim 1, characterized in that, The herbal Chinese medicine composition further contains 3 - 8 parts of centella asiatica and 2 - 5 parts of rosemary by weight.

3. A traditional cold-processed soap according to claim 1, characterized in that, The preparation method of the Qianjin Yurong medicinal soup is: mixing the herbal Chinese medicine composition and water in a ratio of 1:5 - 1:8, boiling with strong fire and then decocting with slow fire for 30 - 60 minutes, filtering to obtain the filtrate and concentrating it to 1 / 3 - 1 / 2 of the original volume.

4. A traditional cold-processed soap according to claim 1, characterized in that, The preparation method of the Qianjin Yurong medicinal powder is to crush the herbal Chinese medicine composition to 100 - 200 meshes and obtain it after drying at 60 - 80 °C for 2 - 4 hours.

5. A method for preparing ancient - style cold - made soap according to claim 1, characterized in that, Including the following steps: (1) Preparation of oil phase: Mix olive oil, coconut oil, palm oil, evening primrose oil, grape seed oil, jojoba oil, add the herbal Chinese medicine composition, and soak at a constant temperature of 40 - 50 °C for 48 - 72 hours to obtain Qianjin Yurong oil; (2) Preparation of water phase: Slowly add edible sodium hydroxide to the Qianjin Yurong medicinal soup, stir while adding until completely dissolved, and cool to 30 - 40 °C; (3) Saponification reaction: Slowly add the water phase to the oil phase, and continuously stir until the mixture reaches the Trace state; (4) Adding active ingredients: Add the Qianjin Yurong medicinal powder in the Trace state and continue to stir for 10 - 15 minutes; (5) Pouring into mold and curing: Pour the mixture into the mold and let it stand and cure at 25 - 30 °C for 48 hours; (6) Aging treatment: After demolding, place it in a ventilated and dry place for aging for 4 - 8 weeks; (7) Molding processing: Shred the aged soap body, pound it 5 - 8 times and then press it into shape, and then dry it until the moisture content ≤ 15%.

6. The preparation method of an ancient cold-processed soap according to claim 5, characterized in that In the step (3), the stirring speed is 200 - 300 revolutions per minute and the stirring time is 60 - 90 minutes.

7. A preparation method of ancient cold-processed soap according to claim 5, characterized in that, In the step (4), 0.1 - 0.5% by weight of natural essential oil can also be added, and the essential oil is selected from one or more of rose essential oil, lavender essential oil or neroli essential oil.

8. A method for preparing ancient - style cold - made soap according to claim 5, characterized in that, In the step (6), the humidity of the aging environment is controlled at 40 - 60% and the temperature is controlled at 20 - 25 °C.

9. A preparation method of ancient cold-processed soap according to claim 5, characterized in that, In the step (7), the pounding process adopts intermittent pounding, and the interval time between each pounding is 30 - 60 seconds.