Membrane filtration equipment and method for purifying walnut protein peptide

Abstract

The invention relates to the technical field of purification devices, in particular to membrane filtration equipment and method for purifying walnut protein peptides, a primary filtration bin is formed in a purification box, an inner mounting block is slidably clamped in the purification box, the inner mounting block is slidably clamped in the primary filtration bin, an inner protection ring is fixedly connected to the inner side of the inner mounting block, and an outer protection ring is fixedly connected to the inner side of the inner protection ring. A middle partition plate is fixedly connected to the inner wall of the inner protection ring, a discharging inclined net is fixedly connected to one side of the middle partition plate, a liquid inlet box is fixedly connected to the top of the purification box, a mounting top plate is fixedly connected to the top of the liquid inlet box, and a feeding port is formed in the outer side of the liquid inlet box. The walnut protein peptide purification efficiency is improved, the problems that traditional membrane filtration equipment is prone to blockage, high in cleaning frequency, insufficient in transmembrane pressure difference control precision and the like are effectively solved, and meanwhile the design thought of the equipment and the method can provide reference for purification of other similar substances.

Description

Technical Field

[0001] The invention relates to the technical field of purification devices, in particular to membrane filtration equipment and a method for purifying walnut protein peptides. Background Art

[0002] Walnut protein peptides are generally purified by membrane filtration and ultrafiltration. Walnut protein peptide ultrafiltration is a technology that uses the screening principle of semi-permeable membranes to separate, purify and concentrate walnut protein peptides according to the different sizes and shapes of walnut protein peptide molecules.

[0003] In the prior art, walnut protein peptides need to be filtered in advance when being purified. Since the walnut protein peptides are directly obtained from the last discharged liquid, ultrafiltration purification is also required. However, traditional membrane filtration equipment has problems such as easy clogging of the membrane components, high cleaning frequency, and insufficient transmembrane pressure difference control accuracy. Residual lipids and colloidal substances are easy to contaminate the subsequent ultrafiltration membrane surface, further affecting the purity of the target product. To this end, the present invention provides a membrane filtration device and method for purifying walnut protein peptides. Summary of the Invention

[0004] The object of the present invention is to provide a membrane filtration device and method for purifying walnut protein peptides to solve the problems raised in the above background technology.

[0005] The filtration apparatus of the present invention is a filter element and a filter element according to the present invention; the filtration apparatus may be adapted to filter the filter element by sliding the filter element into engagement with the filter element in a manner which allows the filter element to filter in an orderly manner. The collecting plate is fixedly connected to a side filter plate on one side away from the middle partition plate, and a supporting ring is fixedly connected between the side filter plate and the middle partition plate, and a side sealing plate is fixedly connected to a side sealing plate on one side away from the inner mounting block; and a side pull handle is fixedly connected to the side sealing plate on the other side away from the inner mounting block; when in use, the raw material enters the interior of the primary filter bin through the feed port on the outside of the liquid inlet box, so that the raw material passes through the discharge inclined screen for filtration, the rotary motor is started, and the output roller is driven to rotate, so that the output roller drives the side slide plate and the scraper plate to rotate, so that the raw material is stirred in the primary filter bin, so that the raw material is filtered at a faster rate, and at the same time, when the scraper plate contacts the discharge inclined screen each time, the scraper plate scrapes the top of the discharge inclined screen, scrapes and rotates the material on the surface of the discharge inclined screen, and the scraper plate pushes the inner sliding column to move upward and squeezes the internal pressure spring, so that the scraper plate scrapes the material into the interior of the collecting plate, and when it passes over the side filter plate, it is pushed to reset by the internal pressure spring, and at the same time, the liquid is still filtered and discharged through the side filter plate, and the filtered material can be cleaned and processed by pulling the side pull handle.

[0006] The top of the inner pressure plate is fixedly connected to the protective top ring, and the top of the protective top ring is fixedly connected to the inner discharge cylinder, and the inner discharge cylinder is slidably connected to the inner liquid port. The mounting plate is obliquely snapped into the interior of the ultrafiltration box, and a liquid suction pipe is connected to one side of the ultrafiltration box, which is located at the top of one end of the ultrafiltration mounting plate; when in use: the filtered liquid enters the inner discharge barrel through the liquid hole, passes through the inner pressure plate, and enters the ultrafiltration bin. When the output roller rotates, the limit slider on the ground side rotates, driving the inner pressure plate to rotate, so that the adjustment roller moves along the inner adjustment groove. The shape of the inner adjustment groove is two sets of convex corrugations. Whenever the inner pressure plate rotates one circle, the adjustment roller will complete two upward and two downward movements. At the same time, the inner discharge barrel and the inner pressure plate will be closed through the liquid, so that the inner pressure plate moves up and down twice, each time squeezing the liquid to speed up the purification of the liquid, and then the inner discharge barrel and the inner pressure plate continue to be connected, entering a certain amount of filtered liquid and repeating the previous process. When a certain concentration is reached, it is sucked out through the liquid suction pipe. The inclined setting of the ultrafiltration mounting plate facilitates the discharge of purified liquid.

[0007] The present invention provides a membrane filtration device and method for purifying walnut protein peptides through improvements, which have the following improvements and advantages compared with the prior art:

[0008] First: The membrane filtration equipment and method for purifying walnut protein peptides described in the present invention, the raw material enters the interior of the primary filter bin through the feed port on the outside of the liquid inlet box, so that the raw material is filtered through the discharge inclined screen, the rotary motor is started, and the output roller is driven to rotate, so that the output roller drives the side slide plate and the scraper plate to rotate, so that the raw material is stirred in the primary filter bin, so that the raw material is filtered at a faster rate, and at the same time, every time the scraper plate contacts the discharge inclined screen, the scraper plate will scrape the top of the discharge inclined screen, scrape the material on the surface of the discharge inclined screen and rotate, the scraper plate pushes the inner sliding column to move upward and squeezes the internal pressure spring, so that the scraper plate scrapes the material to the inside of the collecting plate, and when it passes over the side filter plate, it will be pushed to reset by the internal pressure spring, and at the same time, the liquid is still filtered and discharged through the side filter plate, and the filtered material can be cleaned and processed by pulling the side pull handle;

[0009] Second: A membrane filtration device and method for purifying walnut protein peptides described in the present invention, the filtered liquid enters the inner discharge barrel through the liquid hole, passes through the inner pressure plate, and enters the ultrafiltration chamber. When the output roller rotates, the limit slider on the ground side rotates, driving the inner pressure plate to rotate, so that the adjustment roller moves along the inner adjustment groove. The shape of the inner adjustment groove is two sets of convex corrugations. Whenever the inner pressure plate rotates one circle, the adjustment roller will complete two upward and two downward movements, and at the same time, the inner discharge barrel and the inner pressure plate will be sealed through the liquid, so that the inner pressure plate moves up and down twice, each time squeezing the liquid to speed up the purification of the liquid, and then the inner discharge barrel and the inner pressure plate continue to be connected, entering a certain amount of filtered liquid, repeating the previous process, when a certain concentration is reached, it is sucked out through the pipette, and the inclined setting of the ultrafiltration mounting plate facilitates the discharge of the purified liquid;

[0010] Summary: The membrane filtration equipment and method for purifying walnut protein peptides described in the present invention, through a unique structural design, not only improve the purification efficiency of walnut protein peptides, but also effectively solve the problems of easy clogging, high cleaning frequency, and insufficient transmembrane pressure difference control accuracy of traditional membrane filtration equipment. At the same time, the design ideas of the equipment and method can also provide reference and reference for the purification of other similar substances. BRIEF DESCRIPTION OF THE DRAWINGS

[0011] The present invention will be further explained below in conjunction with the accompanying drawings and examples:

[0012] Figure 1 It is a schematic diagram of the three-dimensional structure of the present invention;

[0013] Figure 2 It is a schematic structural diagram of the purification box of the present invention;

[0014] Figure 3 It is a schematic cross-sectional view of a purification box of the present invention;

[0015] Figure 4 It is a schematic structural diagram of the output roller of the present invention;

[0016] Figure 5 It is a schematic diagram of the internal mounting block structure of the present invention;

[0017] Figure 6 It is a schematic structural diagram of the ultrafiltration mounting plate of the present invention;

[0018] Figure 7 It is a schematic diagram of the inner adjustment groove of the present invention.

[0019] Description of reference numerals:

[0020] 1. Purification box; 2. Ultrafiltration box; 3. Drain box; 4. Liquid inlet box; 5. Mounting top plate; 6. Rotating motor; 7. Suction pipe; 8. Output roller; 9. Inner adjustment groove; 10. Internal pressure spring; 11. Inner slide column; 12. Side slide plate; 13. Scraper plate; 14. Side sealing plate; 15. Side pull handle; 16. Inner mounting block; 17. Inner protective ring; 18. Middle partition; 19. Discharge inclined screen; 20. Collecting plate; 21. Side filter plate; 22. Support ring; 23. Side limit slide bar; 24. Inner pressure plate; 25. Protective top ring; 26. Inner discharge barrel; 27. Adjustment roller; 28. Ultrafiltration mounting plate; 29. Ultrafiltration screen. DETAILED DESCRIPTION

[0021] The present invention is described in detail below, clearly and completely describing the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only some embodiments of the present invention, not all embodiments. All other embodiments obtained by ordinary technicians in this field based on the embodiments of the present invention without making any creative efforts shall fall within the scope of protection of the present invention.

[0022] The present invention provides a membrane filtration device and method for purifying walnut protein peptides through improvement. The technical solution of the present invention is:

[0023] like Figure 1-Figure 7As shown, a membrane filtration device and method for purifying walnut protein peptides include a purification box 1, a primary filtration bin is opened inside the purification box 1, an inner mounting block 16 is slidably connected to the interior of the purification box 1, the inner mounting block 16 is slidably connected to the primary filtration bin, an inner side of the inner mounting block 16 is fixedly connected to an inner protective ring 17, an inner wall of the inner protective ring 17 is fixedly connected to a middle partition 18, one side of the middle partition 18 is fixedly connected to a discharge inclined net 19, the top of the purification box 1 is fixedly connected to a liquid inlet box 4, the top of the liquid inlet box 4 is fixedly connected to a mounting top plate 5, the liquid inlet box 4 A feed port is provided on the outside of the filter bin, a rotating motor 6 is fixedly connected to the top of the mounting top plate 5, an output roller 8 is fixedly connected to the output end of the rotating motor 6, an inner sliding column 11 is slidably connected to the inner side of the output roller 8, a side slide 12 is fixedly connected to the outer side of the inner slide 11, a scraper plate 13 is fixedly connected to the other side of the side slide 12, the scraper plate 13 is slidably connected between the output roller 8 and the inner wall of the primary filter bin, a collecting plate 20 is fixedly connected to the side of the middle partition 18 away from the discharging inclined net 19, and a side filter plate is fixedly connected to the side of the collecting plate 20 away from the middle partition 18 21, a support ring 22 is fixedly connected between the side filter plate 21 and the middle partition plate 18, a side sealing plate 14 is fixedly connected to the side of the inner mounting block 16 away from the inner protective ring 17, and a side pull handle 15 is fixedly connected to the side sealing plate 14 away from the inner mounting block 16; when in use: the raw material enters the interior of the primary filter bin through the feed port on the outside of the liquid inlet box 4, and the raw material is filtered through the discharge inclined screen 19, the rotary motor 6 is started, and drives the output roller 8 to rotate, so that the output roller 8 drives the side slide plate 12 and the scraper plate 13 to rotate, so that the raw material is stirred in the primary filter bin, The raw materials are filtered at a faster rate. At the same time, every time the scraper plate 13 contacts the discharge inclined screen 19, the scraper plate 13 will scrape the top of the discharge inclined screen 19, scraping the material on the surface of the discharge inclined screen 19 and rotating it. The scraper plate 13 pushes the inner slide column 11 to move upward and squeezes the internal pressure spring 10, so that the scraper plate 13 scrapes the material to the inside of the collecting plate 20. When it passes the side filter plate 21, it will be pushed to reset by the internal pressure spring 10. At the same time, the liquid is still filtered and discharged through the side filter plate 21. The filtered material can be cleaned and processed by pulling the side pull handle 15.

[0024] Furthermore, an ultrafiltration tank is provided inside the purification box 1, a liquid port is provided between the primary filtration tank and the ultrafiltration tank, the bottom of the purification box 1 is fixedly connected to the ultrafiltration tank 2, the bottom of the ultrafiltration tank 2 is fixedly connected to the drainage tank 3, the interior of the ultrafiltration tank 2 is slidably connected to the ultrafiltration mounting plate 28, the interior of the ultrafiltration mounting plate 28 is fixedly connected to the ultrafiltration screen 29, the inner wall of the ultrafiltration tank of the purification box 1 is provided with an inner adjustment groove 9, the interior of the ultrafiltration tank is slidably connected to the inner pressure plate 24, the inner pressure plate 24 is There are two adjustment rollers 27 fixedly connected to the outside, and the adjustment rollers 27 are slidably connected to the inside of the inner adjustment groove 9. The outside of the output roller 8 is fixedly connected with a side limit slide 23. The output roller 8 and the side limit slide 23 are slidably connected to the inside of the inner pressure plate 24. The top of the inner pressure plate 24 is rotatably connected to the protective top ring 25. The top of the protective top ring 25 is fixedly connected with the inner discharge cylinder 26. The inner discharge cylinder 26 is slidably connected to the inside of the liquid port. The ultrafiltration mounting plate 28 is tilted. When the filter element 24 is in the working state, the filter element 26 is sucked out through the pipette 7 and the filter element 27 is rotated.

[0025] Working principle: When in use: the raw material enters the interior of the primary filter bin through the feed port on the outside of the liquid inlet box 4, and the raw material is filtered through the discharge inclined screen 19. The rotary motor 6 is started, driving the output roller 8 to rotate, so that the output roller 8 drives the side slide plate 12 and the scraper plate 13 to rotate, so that the raw material is stirred in the primary filter bin, and the raw material is filtered at a faster rate. At the same time, every time the scraper plate 13 contacts the discharge inclined screen 19, the scraper plate 13 will scrape the top of the discharge inclined screen 19, scraping and rotating the material on the surface of the discharge inclined screen 19, and the scraper plate 13 pushes the inner slide column 11 to move upward and squeeze the internal pressure spring 10, so that the scraper plate 13 scrapes the material to the inside of the collecting plate 20. When it passes the side filter plate 21, it will be pushed to reset by the internal pressure spring 10. At the same time, the liquid is still filtered and discharged through the side filter plate 21, and can be pulled out by pulling the side handle 15 In order to clean and process the filtrate, the filtered liquid enters the inner discharge barrel 26 through the liquid hole, passes through the inner pressure plate 24, and enters the ultrafiltration chamber. When the output roller 8 rotates, the ground-side limit slide 23 rotates, driving the inner pressure plate 24 to rotate, so that the adjustment roller 27 moves along the inner adjustment groove 9. The shape of the inner adjustment groove 9 is two sets of convex corrugations. Whenever the inner pressure plate 24 rotates one circle, the adjustment roller 27 will complete two upward and two downward movements. At the same time, the inner discharge barrel 26 and the inner pressure plate 24 will be closed through the liquid, so that the inner pressure plate 24 moves up and down twice, each time squeezing the liquid to speed up the purification of the liquid. After that, the inner discharge barrel 26 and the inner pressure plate 24 continue to be connected, entering a certain amount of filtered liquid, repeating the previous process. When a certain concentration is reached, it is sucked out through the pipette 7. The inclined setting of the ultrafiltration mounting plate 28 facilitates the discharge of the purified liquid.

[0026] The above description is intended to enable one skilled in the art to implement or use the present invention. Various modifications to these embodiments will be readily apparent to one skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the present invention. Therefore, the present invention is not limited to the embodiments shown herein but is intended to conform to the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. A membrane filtration device for purifying walnut protein peptides, comprising a purification box (1), characterized in that: The interior of the purification box (1) is provided with a primary filter bin, the interior of the purification box (1) is slidably connected to an inner mounting block (16), the inner mounting block (16) is slidably connected to the primary filter bin, the inner side of the inner mounting block (16) is fixedly connected to an inner protective ring (17), the inner wall of the inner protective ring (17) is fixedly connected to a middle partition (18), one side of the middle partition (18) is fixedly connected to a discharge inclined net (19), the top of the purification box (1) is fixedly connected to a liquid inlet box (4), the top of the liquid inlet box (4) is fixedly connected to a mounting top plate (5), and a feed port is provided on the outer side of the liquid inlet box (4).

2. A membrane filtration device for purifying walnut protein peptide according to claim 1, characterized in that: The top of the mounting top plate (5) is fixedly connected to a rotating motor (6), the output end of the rotating motor (6) is fixedly connected to an output roller (8), the inner side of the output roller (8) is slidably engaged with an inner sliding column (11), the outer side of the inner sliding column (11) is fixedly connected to a side slide plate (12), the other side of the side slide plate (12) is fixedly connected to a scraper plate (13), and the scraper plate (13) is slidably engaged between the output roller (8) and the inner wall of the primary filter bin.

3. A membrane filtration device for purifying walnut protein peptide according to claim 2, characterized in that: The side of the middle partition (18) away from the discharging inclined net (19) is fixedly connected to a collecting plate (20), the side of the collecting plate (20) away from the middle partition (18) is fixedly connected to a side filter plate (21), a support ring (22) is fixedly connected between the side filter plate (21) and the middle partition (18), the side of the inner mounting block (16) away from the inner protective ring (17) is fixedly connected to a side sealing plate (14), and the side of the side sealing plate (14) away from the inner mounting block (16) is fixedly connected to a side pull handle (15).

4. A membrane filtration device for purifying walnut protein peptide according to claim 3, characterized in that: An ultrafiltration chamber is provided inside the purification box (1), a liquid outlet is connected between the primary filtration chamber and the ultrafiltration chamber, the bottom of the purification box (1) is fixedly connected to the ultrafiltration box (2), the bottom of the ultrafiltration box (2) is fixedly connected to the drainage box (3), the interior of the ultrafiltration box (2) is slidably connected to an ultrafiltration mounting plate (28), and the interior of the ultrafiltration mounting plate (28) is fixedly connected to an ultrafiltration screen (29).

5. The membrane filtration device for purifying walnut protein peptide according to claim 4, characterized in that: An inner adjustment groove (9) is provided on the inner wall of the ultrafiltration chamber of the purification box (1), and an inner pressure plate (24) is slidably engaged inside the ultrafiltration chamber. Two adjustment rollers (27) are fixedly connected to the outer side of the inner pressure plate (24), and the adjustment rollers (27) are slidably engaged inside the inner adjustment groove (9). A side limit slide (23) is fixedly connected to the outer side of the output roller (8), and the output roller (8) and the side limit slide (23) are slidably engaged on the inner side of the inner pressure plate (24).

6. The membrane filtration device for purifying walnut protein peptide according to claim 5, characterized in that: The top of the inner pressure plate (24) is rotatably engaged with the protective top ring (25), the top of the protective top ring (25) is fixedly connected with an inner discharge cylinder (26), and the inner discharge cylinder (26) is slidably engaged with the inside of the liquid passage.

7. The membrane filtration device for purifying walnut protein peptide according to claim 6, characterized in that: The ultrafiltration mounting plate (28) is obliquely clamped to the interior of the ultrafiltration box (2); one side of the ultrafiltration box (2) is connected to a liquid suction pipe (7), which is located at the top of one end of the ultrafiltration mounting plate (28).

8. A method for using a membrane filtration device for purifying walnut protein peptide according to any one of claims 1 to 7, characterized in that: The raw materials enter the interior of the primary filter bin through the feed port on the outside of the liquid inlet box (4), and are filtered through the discharge inclined screen (19). The rotary motor (6) is started, driving the output roller (8) to rotate, so that the output roller (8) drives the side slide plate (12) and the scraper plate (13) to rotate, so that the raw materials are stirred in the primary filter bin, so that the raw materials are filtered at a faster rate. At the same time, when the scraper plate (13) contacts the discharge inclined screen (19) each time, the scraper plate (13) scrapes the discharge material. The top of the inclined screen (19) scrapes the material on the surface of the discharge inclined screen (19) and rotates it. The scraper plate (13) pushes the inner slide column (11) to move upward and squeezes the inner pressure spring (10), so that the scraper plate (13) scrapes the material to the inside of the collecting plate (20). When it passes over the side filter plate (21), it will be pushed to reset by the inner pressure spring (10). At the same time, the liquid is still filtered and discharged through the side filter plate (21). The filtered material can be cleaned and processed by pulling the side pull handle (15); The filtered liquid enters the inner discharge barrel (26) through the liquid hole, passes through the inner pressure plate (24), and enters the ultrafiltration chamber. When the output roller (8) rotates, the ground-side limit slide (23) rotates, driving the inner pressure plate (24) to rotate, so that the adjustment roller (27) moves along the inner adjustment groove (9). The shape of the inner adjustment groove (9) is two groups of convex corrugations. Whenever the inner pressure plate (24) rotates one circle, the adjustment roller (27) will complete two upward and two downward movements, and at the same time, the inner discharge barrel (26) and the inner pressure plate (24) will be closed by liquid communication, so that the inner pressure plate (24) moves up and down twice, each time squeezing the liquid and accelerating the purification of the liquid. After that, the inner discharge barrel (26) and the inner pressure plate (24) continue to be connected, and a certain amount of filtered liquid enters. The previous process is repeated. When a certain concentration is reached, it is sucked out through the pipette (7). The inclined setting of the ultrafiltration mounting plate (28) facilitates the discharge of the purified liquid.

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