Reaction kettle for producing adhesive film cross-linking agent

Abstract

The invention provides an adhesive film cross-linking agent production reaction kettle, and relates to the technical field of reaction kettles, the adhesive film cross-linking agent production reaction kettle comprises a bottom plate, the top end of the bottom plate is provided with a kettle body, the top end of the kettle body is fixedly provided with a closing cover through a bolt, the kettle body is internally provided with a cold and hot switching assembly, and the top end of the bottom plate is provided with a circulation assembly. According to the present invention, the bottom plate, the kettle body, the closing cover, the bottom cover and the discharge pipe are arranged, and the vitreous glaze slip is sprayed on the inner wall of the kettle body and is sintered to form the compact vitreous coating, such that the corrosion resistance of the kettle body is substantially improved, the service life of the equipment is prolonged, and the leakage of chemical substances and harmful gas caused by the damage of the inner wall is avoided; potential threats to the production environment and the health of workers are fundamentally eliminated, the angle of the nozzle can be adjusted according to needs, uniform spraying of the inner wall of the kettle body can be achieved in actual production, the kettle body and the stirring rod can be comprehensively washed in the cleaning process, and the cleaning effect is improved.

Description

Technical Field

[0001] The invention relates to the technical field of reactors, in particular to a reactor for producing a film crosslinking agent. Background Art

[0002] Reactors are essential equipment used in a wide range of fields, including chemical, pharmaceutical, coating, and new materials processing. They are typically used for mixing, dissolving, dispersing, and polymerizing materials. They are primarily used for mixing, heating, cooling, reacting, volatilizing, crosslinking, and other chemical reactions. Traditional reaction processes are often complicated. Early reactors typically consisted of a simple metal body, heating and cooling components, a stirring system, and a sealed portion for heating or cooling. Their operating principle primarily relied on the body to maintain an internal temperature, making them suitable for general physical mixing or low-corrosive chemical reactions in enclosed spaces. However, with the development of chemical processes in specific industries, materials are increasingly reacting under increasingly complex conditions. With the increasing use of strong acids, strong bases, or highly corrosive organic solvents in modern chemical processes, reactors have placed higher demands on corrosion resistance, temperature control stability, spray uniformity, and ease of cleaning. Traditional metal bodies are susceptible to corrosion over long periods of use, leading to damage to the inner wall.

[0003] Traditionally, the reactor body is typically constructed of metal, without any effective corrosion protection or coating. Prolonged exposure to inorganic acids or organic solvents can cause the metal surface to corrode, leading to pitting, cracking, and even flaking, severely damaging the inner wall. This not only significantly shortens the equipment's lifespan but can also lead to leaks of chemicals and hazardous gases due to corrosion, perforation, or ruptures in the body. This not only pollutes the production environment but also poses serious safety risks to workers. Summary of the Invention

[0004] The purpose of the present invention is to solve the technical problems raised in the above background technology.

[0005] The present invention adopts the following technical solution: a film cross-linking agent production reactor, comprising a bottom plate, a reactor body is placed on the top of the bottom plate, a closing cover is fixed to the top of the reactor body by bolts, a hot and cold switching component is arranged inside the reactor body, a circulation component is placed on the top of the bottom plate, a spraying and scraping wall component is arranged inside the closing cover, the bottom end of the reactor body is connected to the bottom cover by bolts, a discharge pipe is welded to the surface of the bottom cover, a solenoid valve 1 is arranged on the surface of the discharge pipe, a bracket is fixed to the top of the closing cover by bolts, a feed pipe 1 is arranged at the top of the closing cover, a liquid discharge trough is arranged inside the closing cover, a feed pipe 2 is welded to the two side surfaces of the top of the closing cover, and the feed pipe 2 is connected to the liquid discharge trough.

[0006] Preferably, the hot and cold switching assembly includes a heater, a cavity is opened inside the kettle body, a heat pipe is arranged inside the cavity, a cooler is placed on the top of the bottom plate, the output end of the heater is connected and fixed to one end of the heat pipe, the other end of the cooler is connected and fixed to the other end of the heat pipe, and the heat pipe is close to the outer wall of the operating cavity of the kettle body and wrapped around the outer wall of the operating cavity.

[0007] Preferably, the circulation component includes a placement box and a water tank, the placement box and the water tank are placed on the top of the bottom plate, the bottom ends of the placement box and the water tank are connected to a discharge pipe by welding, the surface of the discharge pipe is provided with a solenoid valve 2, the bottom end of the discharge pipe is connected to a delivery pipe 1 through a flange, the surface of the delivery pipe 1 is connected to a pump 1 and is fixedly connected to the output end of the pump 1, the bottom end of the discharge pipe is connected to a delivery pipe through a flange, the outside of the delivery pipe is provided with a delivery pipe 2, the outer wall of the delivery pipe is welded with a spiral sheet, the top of the water tank is welded with a return pipe 1 near both ends of the outside, the return pipe The top of tube one is connected to return pipe two through a flange, pump two is provided on the surface of return pipe two, pump three is connected to the surface of delivery pipe, a plate and frame filter is placed on the top of the bottom plate, one end of solenoid valve one is connected to return pipe three, the other end of delivery pipe is fixed to feed pipe two through a flange, the other end of delivery pipe two is connected and fixed to solenoid valve three, one end of solenoid valve three is connected and fixed to return pipe four, the other end of solenoid valve three is connected and fixed to delivery pipe three, and the other end of delivery pipe three is fixed to feed pipe two through a flange, and a flow monitor is provided on the inner wall of the delivery pipe.

[0008] Preferably, the spraying and scraping wall assembly includes a motor, the output end of the motor is provided with a stirring rod, the surface of the stirring rod is provided with a cylinder, a hydraulic cylinder is fixed inside the cylinder, the output end of the hydraulic cylinder is connected to a movable frame, the bottom end of the movable frame is installed with a rack, the inside of the stirring rod is provided with a bidirectional screw rod, the center position of the bidirectional screw rod is welded with a gear, the outer surface of the bidirectional screw rod is threadedly connected to an extension frame, and a scraper is welded on the other side of the extension frame, the bottom end of the closing cover is provided with a conical groove, the inside of the closing cover is provided with a groove, the inside of the groove and the conical groove are provided with a nozzle, the outer wall of the other end of the nozzle is fixed with a cross bar, sliders are provided at both ends of the cross bar, a fixing hoop is welded on the other end of the movable frame, a lower pressure frame is provided inside the fixing hoop, and the top of the lower pressure frame is annular, the bottom end of the lower pressure frame is provided with a connecting rod, a slide rail is provided on the surface of the connecting rod, the slide rail is provided inside the slide rail, a spring is connected to one side of the slide rail, a moving groove is provided on the surface of the stirring rod, and the movable frame is provided inside the moving groove.

[0009] Preferably, the solenoid valve 1 and the solenoid valve 3 are both three-way valves, the heater is fixed on the surface of the kettle body, the cooler is placed on the top surface of the bottom plate, and the operating cavity of the kettle body is in the shape of a cylindrical cone.

[0010] Preferably, one end of the delivery pipe 1 is connected and fixed to the surface of the delivery pipe 2 after it is connected to the pump 3, and the other ends of the return pipe 2 and the return pipe 1 are connected and fixed to the upper and lower ends of the plate and frame filter through flanges.

[0011] Preferably, the motor is fixed to the top of the bracket by bolts, and a limiting rod is provided inside the spring, one end of which is connected to the slider and the other end is connected to the internal limiting structure provided on the connecting rod. The nozzle and the conical groove are movably limited. The number of the nozzles and the connecting rods is multiple groups and is distributed in a circular pattern inside the groove and the conical groove.

[0012] Preferably, the surface of the gear is meshed with the surface of the rack, the other end of the spring is connected and fixed to the other end surface of the slide rail, the number of the bidirectional screw rod and the extension frame is three and they are all sleeved inside the stirring rod and distributed in an array, the scraper fits tightly against the inner wall of the operating chamber of the kettle body, the sliding part of the stirring rod and the extension frame is provided with a heat insulating sealing ring, the rear end of the nozzle is connected to a hose and the other end of the hose is connected and fixed to a position near the bottom of the liquid discharge trough.

[0013] Compared with the prior art, the advantages and positive effects of the present invention are: 1. In the present invention, by arranging a bottom plate, a kettle body, a closing cover, a bottom cover, and a discharge pipe structure, a glassy glaze slurry is sprayed on the inner wall of the kettle body and sintered to form a dense glassy coating. This not only greatly improves the corrosion resistance of the kettle body and extends the service life of the equipment, but also avoids the leakage of chemical substances and harmful gases caused by damage to the inner wall, fundamentally eliminating potential threats to the production environment and the health of workers; The nozzle can adjust the angle according to the needs. In actual production, it can not only achieve uniform spraying on the inner wall of the kettle, but also fully rinse the kettle body and stirring rod during the cleaning process, thereby improving the cleaning effect. During the equipment cleaning process, the impurities in the cleaning fluid can be effectively separated through water circulation and plate-and-frame filters. After the cleaning is completed, the water flow can be recycled to reduce resource waste and emission burden. The stirring rod can be adjusted according to the actual processing conditions during the production process to ensure more complete and uniform stirring, thereby improving the mixing efficiency of the reaction materials and the stability of product quality; Through the hot and cold switching structure, it can be flexibly adjusted according to the characteristics of different anti-corrosion materials, making the equipment adaptable to the production of cross-linking agents of various chemical elements, enhancing the universality and adaptability of the process. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 The present invention provides a schematic diagram of the three-dimensional structure of a film cross-linking agent production reactor; Figure 2 The present invention provides a schematic diagram of the rear end structure of a film crosslinking agent production reactor; Figure 3 The present invention provides a bottom-up structural schematic diagram of a film cross-linking agent production reactor; Figure 4 The present invention provides a cross-sectional structural diagram of a film cross-linking agent production reactor; Figure 5 The present invention provides a schematic diagram of the spiral sheet structure of a film cross-linking agent production reactor; Figure 6 The present invention provides a schematic diagram of the connecting rod structure of a film crosslinking agent production reactor; Figure 7 The present invention proposes a film crosslinking agent production reactor Figure 4 Enlarged view of point A in the middle; Figure 8 The present invention proposes a film crosslinking agent production reactor Figure 4 Enlarged view of point B in the middle.

[0015] Legend: 1. Bottom plate; 2. Kettle body; 3. Closing cover; 4. Bottom cover; 5. Discharge pipe; 6. Solenoid valve 1; 7. Bracket; 8. Feed pipe 1; 9. Drain tank; 10. Feed pipe 2; 21. Heater; 22. Chamber; 23. Heat pipe; 24. Cooler; 31. Storage box; 32. Water tank; 33. Discharge pipe; 34. Solenoid valve 2; 35. Delivery pipe 1; 36. Pump 1; 37. Delivery pipe; 38. Delivery pipe 2; 39. Spiral plate; 310. Return pipe 1; 311. Return pipe 2; 312. Pump 2; 313. Pump 3; 314. Plate and frame filter ; 315. Reflux pipe three; 316. Solenoid valve three; 317. Reflux pipe four; 318. Delivery pipe three; 319. Flow monitor; 41. Motor; 42. Stirring rod; 43. Cylinder; 44. Hydraulic cylinder; 45. Moving frame; 46. Rack; 47. Bidirectional screw rod; 48. Gear; 49. Extension frame; 410. Scraper; 411. Conical groove; 412. Groove; 413. Nozzle; 414. Cross bar; 415. Slider; 416. Fixed hoop; 417. Lower pressure frame; 418. Connecting rod; 419. Slide rail; 420. Spring; 421. Moving groove. DETAILED DESCRIPTION

[0016] In order to more clearly understand the above-mentioned objects, features and advantages of the present invention, the present invention is further described below in conjunction with the accompanying drawings and embodiments. It should be noted that the embodiments of the present application and the features therein can be combined with each other without conflict.

[0017] In the following description, many specific details are set forth to facilitate a full understanding of the present invention. However, the present invention may also be implemented in other ways than those described herein. Therefore, the present invention is not limited to the specific embodiments disclosed below.

[0018] Example 1 See also Figures 1-8The present invention provides a technical solution: a film crosslinking agent production reactor, comprising a bottom plate 1, a reactor body 2 is placed on the top of the bottom plate 1, a closing cover 3 is fixed to the top of the reactor body 2 by bolts, a hot and cold switching component is provided inside the reactor body 2, a circulation component is placed on the top of the bottom plate 1, a spraying and scraping component is provided inside the closing cover 3, the bottom end of the reactor body 2 is connected to a bottom cover 4 by bolts, a discharge pipe 5 is welded to the surface of the bottom cover 4, a solenoid valve 6 is provided on the surface of the discharge pipe 5, and a bracket 7 is fixed to the top of the closing cover 3 by bolts. A feed pipe 8 is provided at the top of the closing cover 3, and a liquid discharge tank 9 is provided inside the closing cover 3. Feed pipes 2 10 are welded to the two side surfaces of the top of the closing cover 3, and the feed pipes 2 10 are connected to the liquid discharge tank 9. Glass glaze slurry is sprayed on the inner wall of the kettle body 2 and sintered to form a dense glass coating, which not only greatly improves the corrosion resistance of the kettle body 2 and extends the service life of the equipment, but also avoids the leakage of chemicals and harmful gases due to damage to the inner wall, fundamentally eliminating the potential threat to the production environment and the health of workers.

[0019] See also Figure 1-Figure 4 The hot and cold switching assembly includes a heater 21, a cavity 22 is provided inside the kettle body 2, a heat pipe 23 is provided inside the cavity 22, a cooler 24 is placed on the top of the bottom plate 1, the output end of the heater 21 is connected and fixed to one end of the heat pipe 23, and the other end of the cooler 24 is connected and fixed to the other end of the heat pipe 23. The heat pipe 23 is close to the outer wall of the operating cavity of the kettle body 2 and is wrapped around the outer wall of the operating cavity. The hot and cold switching assembly formed by configuring the heater 21, the heat pipe 23 and the cooler 24 enables the reactor to achieve rapid heating and cooling during the processing. This design makes the heating and cooling of the glassy glaze slurry more uniform and rapid, thereby improving production efficiency while ensuring the quality of the coating on the inner wall of the kettle body 2 and the process stability. The synergistic effect of the heat pipe 23 and the cooler 24 improves the heat exchange efficiency of the equipment.

[0020] See also Figure 1-Figure 3 、 Figure 5The circulating assembly comprises a placing box 31 and a water tank 32, both placed at the top end of the bottom plate 1, the bottom end of the placing box 31 and the water tank 32 is connected with a discharge pipe 33 through welding, the surface of the discharge pipe 33 is provided with a solenoid valve two 34, the bottom end of the discharge pipe 33 is connected with a conveying pipe one 35 through flange, the surface of the conveying pipe one 35 is connected with a pump one 36 and fixedly connected with the output end of the pump one 36, the bottom end of the discharge pipe 33 is connected with a conveying pipe 37 through flange, the outer side of the conveying pipe 37 is provided with a conveying pipe two 38, the outer wall of the conveying pipe 37 is welded with a spiral blade 39, the top end of the water tank 32 is welded with a backflow pipe one 310 near the two outer ends, the top end of the backflow pipe one 310 is connected with a backflow pipe two 311 through flange, the surface of the backflow pipe two 311 is provided with a pump two 312, the surface of the conveying pipe 37 is connected with a pump three 313, the top end of the bottom plate 1 is placed with a plate frame filter 314, one end of the solenoid valve one 6 is connected with a backflow pipe three 315, the other end of the conveying pipe 37 is fixedly connected with the feeding pipe two 10 through flange, the other end of the conveying pipe two 38 is fixedly connected with a solenoid valve three 316, one end of the solenoid valve three 316 is fixedly connected with the backflow pipe one 310, one end of the solenoid valve three 316 is fixedly connected with a backflow pipe four 317, the other end of the solenoid valve three 316 is fixedly connected with a conveying pipe three 318, and the other end of the conveying pipe three 318 is fixedly connected with the feeding pipe two 10 through flange, the inner wall of the conveying pipe 37 is provided with a flow monitor 319, the design of the circulating assembly comprises the placing box 31, the water tank 32 and related pumps and pipeline systems, which effectively realizes the recycling of water and solvent and reduces the discharge of wastewater in the production process. By setting the solenoid valve two 34 and the flow monitor 319, the delivery amount of fluid can be accurately controlled to ensure the accuracy and stability of the production process. In addition, the circulating assembly not only supports the spraying and cooling process of glassy glaze slurry, but also can clean the inside of the kettle body 2 after processing, ensuring the cleanliness of the reaction kettle and the operability of the next use.

[0021] Please refer to Figure 4 , Figure 6-Figure 8The spraying and scraping assembly includes a motor 41, a stirring rod 42 is provided at the output end of the motor 41, a cylinder 43 is provided on the surface of the stirring rod 42, a hydraulic cylinder 44 is fixed inside the cylinder 43, a movable frame 45 is connected to the output end of the hydraulic cylinder 44, a rack 46 is installed at the bottom end of the movable frame 45, a bidirectional screw rod 47 is sleeved inside the stirring rod 42, a gear 48 is welded at the center position of the bidirectional screw rod 47, an extension frame 49 is threadedly connected to the outer surface of the bidirectional screw rod 47, a scraper 410 is welded on the other side of the extension frame 49, a conical groove 411 is provided at the bottom end of the closing cover 3, a groove 412 is provided inside the closing cover 3, a nozzle 413 is sleeved inside the groove 412 and the conical groove 411, and a cross bar 414 is fixed to the outer wall of the other end of the nozzle 413. Both ends of the crossbar 414 are provided with sliders 415. The other end of the movable frame 45 is welded with a fixing hoop 416. A lower pressure frame 417 is sleeved inside the fixing hoop 416. The top of the lower pressure frame 417 is annular. The bottom end of the lower pressure frame 417 is sleeved with a connecting rod 418. The other end of the connecting rod 418 has a slide rail 419. The slider 415 is sleeved inside the slide rail 419. A spring 420 is connected to one side of the slider 415. The surface of the stirring rod 42 has a movable groove 421, and the movable frame 45 is sleeved inside the movable groove 421. The design of the spraying and scraping assembly cleverly combines the motor 41, stirring rod 42, hydraulic cylinder 44 and other structures, so that the inner wall of the kettle body 2 can be evenly sprayed and scraped, ensuring that the glassy glaze slurry coating on the inner wall of the kettle body 2 is uniform and strong. The scraper 410 and the extension frame 49 realize a precise scraping action, reducing waste and improving the quality of the coating.

[0022] See also Figure 1-Figure 4 Both solenoid valve 1 (6) and solenoid valve 3 (316) are three-way valves. Heater 21 is fixed to the surface of kettle body 2, and cooler 24 is placed on the top surface of base plate 1. The operating chamber of kettle body 2 is cylindrical and conical. Both solenoid valve 1 (6) and solenoid valve 3 (316) are three-way valves, enabling more precise control of fluid flow direction and flow rate, avoiding the instability of traditional valves during complex operations. The rational configuration of heater 21 and cooler 24 allows the reactor's operating environment to be rapidly adapted to meet diverse processing requirements.

[0023] See also Figure 1-Figure 3 、 Figure 6 One end of delivery pipe 1 35 is fixedly connected to the surface of delivery pipe 2 38 after it connects to pump 3 313. The other ends of return pipe 3 315 and return pipe 2 311 are both connected and fixed to the upper and lower ends of plate-and-frame filter 314 via flanges. The combination of return pipe 3 315, return pipe 2 311, and plate-and-frame filter 314 effectively separates solids and liquids, ensuring the purity of the reaction liquid. The return pipe design allows for the recycling of wastewater.

[0024] See also Figure 4 、 Figure 6-Figure 7 The motor 41 is fixed to the top of the bracket 7 by bolts. A limiting rod is sleeved inside the spring 420, one end of which is connected to the slider 415 and the other end is connected to the internal limiting structure sleeved on the connecting rod 418. The nozzle 413 is connected to the conical groove 411 in a movable limiting manner. The number of nozzles 413 and connecting rods 418 is multiple groups and is distributed circumferentially inside the groove 412 and the conical groove 411. The limiting rod is set in the spring 420 and cooperates with the limiting structure on the connecting rod 418 to effectively control the range of motion of the nozzle 413 and connecting rod 418, avoiding excessive spraying or offset, and ensuring the accuracy of the spraying angle and position. The nozzle 413 is connected to the conical groove 411 in a movable limiting manner, which improves the flexibility of the nozzle 413 adjustment. Multiple groups of nozzles 413 and connecting rods 418 are distributed circumferentially, so that the inner wall of the kettle body 2 can be covered in an all-round and uniform manner, greatly improving the density and consistency of the coating.

[0025] See also Figure 4 、 Figure 8 The surface of the gear 48 meshes with the surface of the rack 46, and the other end of the spring 420 is connected and fixed to the other end surface of the slide rail 419. There are three sets of bidirectional screw rods 47 and extension racks 49, which are all set inside the stirring rod 42 and distributed in an array. The scraper 410 fits tightly against the inner wall of the operating chamber of the kettle body 2. A heat-insulating sealing ring is provided at the sliding part between the stirring rod 42 and the extension rack 49. The rear end of the nozzle 413 is connected to a hose, and the other end of the hose is connected and fixed to the position near the bottom of the liquid discharge tank 9. The rack 46 meshes with the gear 48 to drive the bidirectional screw rod 47 to rotate, which can achieve precise telescopic control of the scraper 410, making the scraping action more stable and controllable. The bidirectional screw rods 47 and extension racks 49 adopt a three-set array distribution structure, so that the scraper 410 forms multi-point synchronous scraping on the inner wall of the kettle body 2, ensuring a more uniform coating distribution. The scraper 410 fits tightly against the inner wall of the kettle body 2 and can play a dual role in the process of removing the glaze layer and uniformly distributing the glaze slurry. A heat-insulating sealing ring is provided between the stirring rod 42 and the extension frame 49, which can effectively isolate high-temperature conduction and extend the service life of the mechanism.

[0026] Working Principle: When the kettle 2 needs to process inorganic acids or organic solvents, the container is first filled with a silica-rich glassy glaze slurry. Pump Three 313 is activated, and the glassy glaze slurry is transported to the interior of the drain tank 9 via the feed pipe 37. Simultaneously, Pump One 36 is activated, pumping water from the water tank 32 into the delivery pipe 1 35. The water flows along the delivery pipe 1 35 into the delivery pipe 2 38 and, guided by the spiral blade 39, flows closely against the outer wall of the delivery pipe 2 38, thereby cooling the glassy glaze slurry therein and maintaining a relatively low temperature. At this point, solenoid valve Three 316 opens, and the water flows back to the water tank 32 through the return pipe 4 317, completing the circulation.

[0027] After cooling, the vitreous glaze slurry is pressurized by pump 313 and pumped through a flexible hose to nozzle 413. By adjusting the angle of nozzle 413, the glaze slurry is evenly sprayed onto the inner wall of the operating chamber of kettle 2. Subsequently, heater 21 is activated, rapidly transferring heat to heat pipe 23. Thanks to the excellent thermal conductivity of heat pipe 23, the outer wall of the operating chamber rapidly heats up, transferring the heat to the inner wall of chamber 22.

[0028] Next, the hydraulic cylinder 44 and the motor 41 work in tandem: the hydraulic cylinder 44 pushes the movable frame 45 and the fixed hoop 416 downward, driving the downward pressure frame 417 and the connecting rod 418 to move axially. During this process, the connecting rod 418 first compresses the spring 420, while the nozzle 413 maintains a constant angle, always aiming at the inner wall of the kettle 2, ensuring uniform spraying of the glaze slurry. Simultaneously, the downward pressure of the movable frame 45 causes the rack 46 and gear 48 to engage and rotate, thereby driving the bidirectional screw 47. The bidirectional screw 47 is threadedly connected to the extension frame 49. Its rotation gradually retracts the extension frame 49, which in turn drives the scraper 410 to slowly move away from the inner wall of the operating chamber. At this point, the motor 41 drives the stirring rod 42 and scraper 410 to rotate, while the movable frame 45 and the fixed hoop 416 rotate synchronously, evenly spreading the glaze slurry across the inner wall of the kettle 2. As the heat is conducted by the heat pipe 23, the glassy glaze slurry sinters at high temperatures, forming a dense, smooth, and hard glassy coating that firmly bonds to the metal substrate. At the same time, the flow monitor 319 detects the glaze slurry delivery in real time. When the set threshold is reached, the electromagnetic valve 2 34 is automatically closed. At this time, the inorganic acid or organic solvent can be introduced into the kettle body 2 through the feed pipe 1 8 for processing.

[0029] After processing is complete, solenoid valve 1 (6) is opened, allowing the reaction product to exit the kettle 2 through reflux pipe 3 (315). Pump 2 (312) is then activated again, pumping water from the water tank 32 into delivery pipe 1 (35). The water enters delivery pipe 2 (38) and, under the control of solenoid valve 3 (316), is directed into the drain tank 9. Pump 2 (312) then pressurizes and delivers it to the nozzle 413 for cleaning the inner wall. Hydraulic cylinder 44 presses down on the movable frame 45, causing it to move downward. This downward movement of the movable frame 45 then drives the fixed hoop 416 downward. Simultaneously, the movement of the fixed hoop 416 also drives the lower pressing frame 417, which then moves the connecting rod 418 axially. This movement of the connecting rod 418 changes the spray angle of the nozzle 413, ensuring that the water not only rinses the inner wall of the kettle 2 but also cleans the surface of the stirring rod 42. The residual water and solvent then pass through solenoid valve 2 (34) and enter the plate-and-frame filter 314 for solid-liquid separation. The filtered clean water is sent back to the water tank 32 via the second pump 312 for recycling, and the waste residue can be cleaned by opening the filter when needed.

[0030] When producing different cross-linking agents, they may react with the glass glaze slurry due to different chemical elements, which may cause the cross-linking agent produced to be substandard. Therefore, different materials need to be replaced for corrosion protection. At the same time, in order to avoid interference with the chemical reaction caused by the residual glassy glaze slurry, the glaze layer needs to be removed. At this time, the heater 21 is started first, and the inner wall of the kettle body 2 is quickly heated through the heat pipe 23. Then, the cooler 24 is immediately started and rapid cooling is achieved through the heat pipe 23. The alternating action of hot and cold separates the glassy glaze slurry from the kettle body 2. Subsequently, the stirring rod 42 and the scraper 410 rotate to scrape off the detached glaze layer and push it to the bottom. At this time, water is delivered to the nozzle 413 by the pump 36 for secondary flushing. The flushing liquid is discharged into the plate and frame filter 314 together with the glaze slurry debris. After filtration, the clean water flows back to the water tank 32 for recycling. This not only prevents the performance of the cross-linking agent from being damaged, but also greatly improves the applicability and maintenance convenience of the kettle body 2. In addition, the nozzle 413 is made of corrosion-resistant material to adapt to the spraying environment of highly corrosive media such as inorganic acids and organic solvents. The inorganic acid and organic solvent are both in a viscous state during the processing process. When sprayed, they can stably adhere to the inner wall of the kettle body 2 without splashing onto the bottom end of the closing cover 3 of the kettle body 2 and the surface of the nozzle 413. By connecting and fixing multiple modular structures through this equipment, the equipment can be flexibly maintained and quickly replaced, which not only ensures the safety and efficiency of the production process, but also improves the adaptability under different process conditions.

[0031] The above description is merely a preferred embodiment of the present invention and does not constitute any other form of limitation to the present invention. Any person skilled in the art may utilize the technical contents disclosed above to change or modify them into equivalent embodiments with equivalent changes for application in other fields. However, any simple modification, equivalent change, and modification of the above embodiments made in accordance with the technical essence of the present invention without departing from the technical solution of the present invention shall still fall within the scope of protection of the technical solution of the present invention.

Claims

1. A film crosslinking agent production reactor, comprising a bottom plate (1), characterized in that: A kettle body (2) is placed on the top of the bottom plate (1), a closing cover (3) is fixed to the top of the kettle body (2) by bolts, a hot and cold switching component is arranged inside the kettle body (2), a circulation component is placed on the top of the bottom plate (1), a spraying and scraping component is arranged inside the closing cover (3), the bottom end of the kettle body (2) is connected to a bottom cover (4) by bolts, a discharge pipe (5) is welded to the surface of the bottom cover (4), a solenoid valve (6) is arranged on the surface of the discharge pipe (5), a bracket (7) is fixed to the top of the closing cover (3) by bolts, a feed pipe (8) is arranged on the top of the closing cover (3), a liquid discharge trough (9) is arranged inside the closing cover (3), a feed pipe (10) is welded to both sides of the top of the closing cover (3), and the feed pipe (10) is connected to the liquid discharge trough (9).

2. The film crosslinking agent production reactor according to claim 1, characterized in that: The hot and cold switching assembly comprises a heater (21), a cavity (22) is provided inside the kettle body (2), a heat pipe (23) is provided inside the cavity (22), a cooler (24) is placed on the top of the bottom plate (1), an output end of the heater (21) is connected and fixed to one end of the heat pipe (23), and the other end of the cooler (24) is connected and fixed to the other end of the heat pipe (23), and the heat pipe (23) is closely attached to and wrapped around the outer wall of the operating cavity of the kettle body (2).

3. The film crosslinking agent production reactor according to claim 1, characterized in that: The circulation component includes a placement box (31) and a water tank (32), the placement box (31) and the water tank (32) are both placed on the top of the bottom plate (1), the bottom ends of the placement box (31) and the water tank (32) are both connected to a discharge pipe (33) by welding, the surface of the discharge pipe (33) is provided with a second solenoid valve (34), the bottom end of the discharge pipe (33) is connected to a delivery pipe (35) by a flange, the surface of the delivery pipe (35) is connected to a pump (36) and is fixedly connected to the output end of the pump (36), the bottom end of the discharge pipe (33) is connected to a delivery pipe (37) by a flange, the outer side of the delivery pipe (37) is provided with a delivery pipe (38), the outer wall of the delivery pipe (37) is welded with a spiral sheet (39), the top of the water tank (32) is welded with a return pipe (310) near both ends of the outer side, the return pipe (310) ) is connected to a return pipe 2 (311) at the top through a flange, a pump 2 (312) is provided on the surface of the return pipe 2 (311), a pump 3 (313) is connected to the surface of the delivery pipe (37), a plate-and-frame filter (314) is placed on the top of the bottom plate (1), one end of the solenoid valve 1 (6) is connected to a return pipe 3 (315), the other end of the delivery pipe (37) is fixedly connected to the feed pipe 2 (10) through a flange, the other end of the delivery pipe 2 (38) is connectedly fixedly connected to a solenoid valve 3 (316), one end of the solenoid valve 3 (316) is connectedly fixedly connected to a return pipe 4 (317), the other end of the solenoid valve 3 (316) is connectedly fixedly connected to a delivery pipe 3 (318), and the other end of the delivery pipe 3 (318) is fixedly connected to the feed pipe 2 (10) through a flange, and a flow monitor (319) is provided on the inner wall of the delivery pipe (37).

4. The film crosslinking agent production reactor according to claim 1, characterized in that: The spraying and scraping assembly comprises a motor (41), an output end of the motor (41) is provided with a stirring rod (42), a surface of the stirring rod (42) is provided with a cylinder (43), a hydraulic cylinder (44) is fixed inside the cylinder (43), an output end of the hydraulic cylinder (44) is connected to a movable frame (45), a rack (46) is installed at the bottom end of the movable frame (45), a bidirectional screw rod (47) is sleeved inside the stirring rod (42), a gear (48) is welded at the center position of the bidirectional screw rod (47), an extension frame (49) is threadedly connected to the outer surface of the bidirectional screw rod (47), a scraper (410) is welded on the other side of the extension frame (49), a conical groove (411) is provided at the bottom end of the closing cover (3), a groove (412) is provided inside the closing cover (3), and the groove (412) ) and the conical groove (411) are provided with a nozzle (413), the outer wall of the other end of the nozzle (413) is fixed with a cross bar (414), both ends of the cross bar (414) are provided with sliders (415), the other end of the movable frame (45) is welded with a fixing hoop (416), the interior of the fixing hoop (416) is provided with a lower pressing frame (417), and the top of the lower pressing frame (417) is annular, the bottom end of the lower pressing frame (417) is provided with a connecting rod (418), the other end surface of the connecting rod (418) is provided with a slide rail (419), the slider (415) is provided inside the slide rail (419), one side of the slider (415) is connected to a spring (420), the surface of the stirring rod (42) is provided with a moving groove (421), and the movable frame (45) is provided inside the moving groove (421).

5. The film crosslinking agent production reactor according to claim 2, characterized in that: The solenoid valve 1 (6) and the solenoid valve 3 (316) are both three-way valves. The heater (21) is fixed on the surface of the kettle body (2). The cooler (24) is placed on the top surface of the bottom plate (1). The operating cavity of the kettle body (2) is in the shape of a cylindrical cone.

6. The film crosslinking agent production reactor according to claim 3, characterized in that: One end of the delivery pipe 1 (35) is connected and fixed to the surface of the delivery pipe 2 (38) after it is connected to the pump 3 (313), the other ends of the return pipe 3 (315) and the return pipe 2 (311) are connected and fixed to the upper and lower ends of the plate and frame filter (314) through flanges, and the other end of the return pipe 4 (317) is connected and fixed to the return pipe 1 (310) through a flange.

7. The film crosslinking agent production reactor according to claim 4, characterized in that: The motor (41) is fixed to the top of the bracket (7) by bolts. A limiting rod is sleeved inside the spring (420), one end of which is connected to the slider (415) and the other end is connected to the internal limiting structure sleeved on the connecting rod (418). The nozzle (413) and the conical groove (411) are connected in a movable limiting manner. The nozzles (413) and the connecting rod (418) are in multiple groups and are distributed in a circular pattern inside the groove (412) and the conical groove (411).

8. The film crosslinking agent production reactor according to claim 4, characterized in that: The surface of the gear (48) is meshed with the surface of the rack (46), the other end of the spring (420) is connected and fixed to the other end surface of the slide rail (419), the number of the bidirectional screw rod (47) and the extension frame (49) is three, and they are all set inside the stirring rod (42) and distributed in an array, the scraper (410) is tightly fitted with the inner wall of the operating chamber of the kettle body (2), and the sliding part of the stirring rod (42) and the extension frame (49) is provided with a heat-insulating sealing ring, and the rear end of the nozzle (413) is connected to a hose and the other end of the hose is connected and fixed to a position near the bottom of the liquid discharge tank (9).

Images