A reaction vessel and reaction method for producing desulfurizing agent

Abstract

This invention relates to the field of reactor technology, specifically disclosing a reactor and reaction method for producing desulfurizing agents. The reactor includes a main body with an internal baffle; a rotating liquid inlet assembly mounted on the main body, with a transition shell connected to the rotating liquid inlet assembly. In this invention, the liquid outlet rotates with the rotating liquid inlet assembly, and simultaneously, under the action of a position adjustment assembly, the inner and outer rings move regularly. Combined with the reciprocating oscillation caused by the angle adjustment assembly, the liquid distribution range of the outlet is expanded, allowing for a more comprehensive and uniformly layered distribution of the liquid desulfurizing agent raw materials. This avoids the problem of uneven local concentration caused by a single inlet, ensuring uniform distribution of the active ingredients in the desulfurizing agent. Furthermore, the uniform liquid distribution method reduces the natural diffusion time of the raw materials, shortening the overall desulfurizing agent production cycle and improving production efficiency.

Description

Technical Field

[0001] This invention relates to the field of reaction vessel technology, and specifically to a reaction vessel and reaction method for producing desulfurizing agent. Background Technology

[0002] Desulfurizing agents are key materials in environmental protection fields such as industrial flue gas purification and fuel desulfurization. Their production process places stringent requirements on the mixing uniformity of the reaction system, reaction rate, and product purity. The reactor, as the core equipment for desulfurizing agent synthesis, directly affects the performance indicators of the desulfurizing agent through its structural design. Among these factors, the mixing efficiency and stirring effect of liquid raw materials are the core factors determining production efficiency and product quality.

[0003] There are technical defects in the liquid raw material addition and stirring process of the reactor used for desulfurizing agent production: First, the liquid raw material addition method mostly adopts a single inlet direct injection design, that is, after one liquid is placed in the reactor, another liquid is directly injected into the reactor through a fixed inlet pipe. This addition method results in the two liquids only being able to diffuse naturally under gravity or passively mix by relying on the stirring mechanism, which easily leads to local uneven concentration and incomplete reaction. This not only prolongs the reaction cycle, but may also lead to uneven distribution of the active ingredients of the desulfurizing agent, affecting the desulfurization efficiency of the final product. Second, the stirring mechanism of the reactor is mostly a fixed-direction rotating stirring rod, with a single stirring trajectory, making it difficult to form all-round fluid disturbance. Especially in dead areas such as the bottom and side walls of the reactor, raw material deposition is prone to occur, further aggravating the problem of uneven mixing. Summary of the Invention

[0004] This invention provides a reaction vessel and reaction method for producing desulfurizing agent, aiming to solve the technical problems in related technologies where liquids can only diffuse naturally under gravity or rely on a stirring mechanism for passive mixing, resulting in insufficient reaction and difficulty in forming omnidirectional fluid disturbance, leading to uneven mixing.

[0005] A desulfurizing agent production reactor of the present invention includes:

[0006] The main body of the reactor has internal baffles installed.

[0007] A rotary liquid inlet assembly is installed on the main body of the reactor. A transition shell is connected to the rotary liquid inlet assembly. The rotary liquid inlet assembly is used to drive the transition shell to rotate and transport the liquid desulfurizing agent raw material into the interior of the transition shell. A universal joint is connected to the bottom of the transition shell.

[0008] The liquid outlet assembly is connected to the transition shell and includes a liquid outlet.

[0009] A position adjustment assembly is disposed between the partition and the transition shell. The position adjustment assembly is used to adjust the position of the liquid outlet during the rotation of the transition shell. The position adjustment assembly includes a guide plate connected to the partition and a telescopic member connected to the transition shell. A roller is rotatably connected to the telescopic member. The telescopic member is used to make the roller fit against the inner wall of the guide plate. The guide plate includes two interconnected arc-shaped plates, one end of which is located in the outer edge area of ​​the partition, and the other end of which is located in the proximal area of ​​the partition.

[0010] An angle adjustment assembly is connected to the mounting bracket and the liquid outlet. The angle adjustment assembly is used to make the liquid outlet swing.

[0011] The stirring assembly is connected to a universal joint, and the stirring assembly is also connected to an eccentric adjustment component, which is used to make the stirring assembly swing.

[0012] Preferably, the telescopic component includes a telescopic rod, a return spring, and a connecting mounting bracket. Both the telescopic rod and the return spring are mounted on the outer surface of the transition shell, with the telescopic rod located inside the return spring. The connecting mounting bracket is connected to the output end of the telescopic rod.

[0013] Preferably, the angle adjustment assembly includes a commutator, a turntable, a connecting rod, a rotating connecting frame, a mounting plate, and a support plate. The commutator is mounted on the connecting mounting frame, the input shaft of the commutator is connected to the roller shaft of the roller, and the output shaft of the commutator is connected to the turntable. The connecting rod is rotatably disposed at one edge of the turntable, and the end of the connecting rod is rotatably connected to the rotating connecting frame. The mounting plate is connected to the outer surface of the delivery pipe, and both the connecting mounting frame and the support plate are connected to the mounting plate. The rotating connecting frame is rotatably connected to the support plate, and the bottom end of the rotating connecting frame is connected to the liquid outlet.

[0014] Preferably, the eccentric adjustment assembly includes a rotating shaft, a transmission assembly, a second turntable, a second connecting rocker arm, and a fine-tuning structure. The rotating shaft is rotatably connected to the partition and is located at the edge of the partition. The transmission assembly is located between the rotating shaft and the rotating liquid inlet assembly, and is used to make the rotating shaft rotate with the rotation of the rotating liquid inlet assembly. The second turntable is connected to the bottom end of the rotating shaft, and the second connecting rocker arm is rotatably located at the edge of one side of the second turntable. The fine-tuning structure is located between the stirring assembly and the second connecting rocker arm, and is used to adjust the position of the stirring assembly.

[0015] Preferably, the fine-tuning structure includes a first fine-tuning connecting plate, a second fine-tuning connecting plate, and a bolt and nut connector. The first fine-tuning connecting plate is rotatably connected to the second connecting rocker arm, and the second fine-tuning connecting plate is rotatably connected to the stirring assembly. Both the first fine-tuning connecting plate and the second fine-tuning connecting plate have multiple fine-tuning through holes on one side. The bolt and nut connector and the fine-tuning through holes are used to connect the first fine-tuning connecting plate and the second fine-tuning connecting plate.

[0016] Preferably, the rotary liquid inlet assembly includes an inlet pipe, a rotary joint, and a delivery pipe. The inlet pipe is rotatably connected to the main body of the reactor, the rotary joint is connected to the bottom end of the inlet pipe, the bottom end of the inlet pipe is connected and communicates with the transition shell, and one end of the delivery pipe is connected to the rotary joint.

[0017] Preferably, the stirring assembly includes a stirring shaft, stirring blades, spiral blades, and stirring paddles. The stirring shaft is connected to a fine-tuning connecting plate via bearings. There are multiple stirring blades. Both the stirring blades and spiral blades are mounted on the outer surface of the stirring shaft. The stirring paddles are connected to the bottom end of the stirring shaft and are located at the bottom of the reactor body.

[0018] Preferably, the liquid dispensing assembly further includes a first delivery hose, a delivery pipe, and a second delivery hose. The first delivery hose is connected to the bottom side of the transition shell. One end of the delivery pipe is connected to the first delivery hose, and the other end of the delivery pipe is connected to the second delivery hose. The end of the second delivery hose away from the delivery pipe is connected to the liquid outlet, and the outer surface of the delivery pipe is connected to the mounting plate.

[0019] Preferably, the rotary liquid inlet assembly further includes a delivery pump and a drive unit. The outlet of the delivery pump is connected to the end of the delivery pipe away from the rotary joint. The drive unit is located on the top of the reactor body and is connected to the liquid inlet pipe. The drive unit is used to drive the liquid inlet pipe to rotate.

[0020] A reaction method for producing a desulfurizing agent includes the following steps:

[0021] S1. Add a liquid desulfurizing agent raw material into the interior of the reactor body;

[0022] S2. A liquid desulfurizing agent raw material is transported into the interior of the transition shell by rotating the liquid inlet assembly, and the transition shell is rotated in the process, which drives the stirring assembly to rotate through the universal joint.

[0023] S3. As the transition shell rotates, the stirring component is oscillated by the universal joint through the eccentric adjustment component. The two liquid desulfurizing agent raw materials are mixed by the rotation and oscillation of the stirring component. During this process, the liquid outlet moves regularly towards and away from the center of the reactor body under the action of the position adjustment component. At the same time, the angle adjustment component makes the liquid outlet oscillate back and forth, uniformly conveying the liquid desulfurizing agent raw materials into the interior of the reactor body for mixing.

[0024] The beneficial effects of this invention are:

[0025] 1. The liquid outlet rotates with the rotating liquid inlet component, and the inner and outer rings move regularly under the action of the position adjustment component. Combined with the reciprocating oscillation brought by the angle adjustment component, the liquid distribution range of the liquid outlet is expanded, so that the liquid desulfurizing agent raw materials are distributed more comprehensively and evenly in layers. This avoids the problem of uneven concentration in some areas caused by a single liquid inlet, ensures that the active ingredients of the desulfurizing agent are evenly distributed, and the uniform liquid distribution method reduces the natural diffusion time of the raw materials, shortens the overall desulfurizing agent production cycle, and improves production efficiency.

[0026] 2. The stirring assembly rotates via a universal joint and oscillates under the influence of the eccentric adjustment component. Combined with the synergistic effect of the stirring blades, spiral blades, and bottom stirring paddles, it can cover traditional dead zones such as the bottom and side walls of the reactor, effectively preventing raw material deposition and further enhancing the mixing effect. Comprehensive stirring improves the reaction rate, avoids reaction delays caused by insufficient mixing, and further shortens the desulfurizer production cycle. Moreover, the improved uniformity of raw material mixing and the sufficiency of reaction result in stable and uniform distribution of active ingredients in the desulfurizer, ensuring the quality of the final product. Attached Figure Description

[0027] Figure 1 This is a schematic diagram of the internal structure of the present invention.

[0028] Figure 2 This is a schematic diagram of the structure of the present invention.

[0029] Figure 3 This is a schematic diagram of the structure of the present invention before the assembly of the reaction vessel body.

[0030] Figure 4 This is a structural schematic diagram of the partition and its connecting components of the present invention.

[0031] Figure 5 This is the present invention. Figure 4 A magnified structural diagram of point A in the middle.

[0032] Figure 6 This is a schematic diagram of the structure of the partition and position adjustment assembly of the present invention.

[0033] Figure 7 This is a schematic diagram of the position adjustment component of the present invention.

[0034] Figure 8 This is a schematic diagram of the stirring assembly of the present invention.

[0035] Figure 9 This is a schematic diagram of the eccentric adjustment component of the present invention.

[0036] Figure label:

[0037] 10. Reactor body; 11. Baffle plate; 12. Guide plate; 20. Rotary liquid inlet assembly; 21. Liquid inlet pipe; 22. Rotary joint; 23. Liquid delivery pipe; 24. Transfer pump; 25. Drive component; 30. Transition shell; 31. Universal joint; 40. Stirring assembly; 41. Stirring shaft; 42. Stirring blades; 43. Spiral blades; 44. Stirring impeller; 50. Liquid outlet assembly; 51. First transfer hose; 52. Transfer pipe; 53. Second transfer hose; 54. Liquid outlet; 60. 61. Position adjustment assembly; 62. Telescopic rod; 63. Return spring; 64. Connecting mounting bracket; 65. Roller; 66. Reversing device; 67. Turntable one; 68. Connecting swing arm one; 69. Rotating connecting bracket; 60. Mounting plate; 610. Support plate; 71. Eccentric adjustment assembly; 72. Rotating shaft; 73. Transmission assembly; 74. Turntable two; 75. Connecting swing arm two; 76. Fine-tuning connecting plate one; 77. Fine-tuning through hole; 78. Bolt and nut connector. Detailed Implementation

[0038] Embodiments of the present invention are described in detail below, examples of which are illustrated in the accompanying drawings. The embodiments described below with reference to the accompanying drawings are exemplary and intended to explain the present invention, and should not be construed as limiting the present invention.

[0039] like Figures 1 to 9As shown, a desulfurizing agent production reactor of the present invention includes a reactor body 10, a rotary liquid inlet assembly 20, a transition shell 30, a universal joint 31, a stirring assembly 40, a liquid outlet assembly 50, and a position adjustment assembly 60. A partition 11 is fixedly installed on the inner wall of the reactor body 10. The rotary liquid inlet assembly 20 is disposed between the partition 11 and the reactor body 10. The outlet of the rotary liquid inlet assembly 20 is connected to the transition shell 30. The rotary liquid inlet assembly 20 is used to drive the transition shell 30 to rotate and transport the liquid desulfurizing agent raw material into the interior of the transition shell 30. The interior of the transition shell 30 is a hollow structure. The liquid outlet assembly 50 is connected to the transition shell 30. The liquid outlet assembly 50 includes a first conveying hose 51 connected to the transition shell 30. A conveying pipe 52 is connected to the end of the first conveying hose 51. A second conveying hose is connected to the end of the conveying pipe 52 away from the first conveying hose 51. 53. The end of the conveying hose 53 away from the conveying pipe 52 is connected to the liquid outlet 54. The position adjustment component 60 is set between the partition plate 11 and the liquid outlet component 50. The position adjustment component 60 is used to adjust the position of the liquid outlet 54 during the rotation of the transition shell 30, so that the liquid outlet 54 is regularly close to and away from the center position of the reactor body 10. An angle adjustment component is connected to the position adjustment component 60 and is connected to the liquid outlet 54. The angle adjustment component is used to swing the liquid outlet 54 to expand the liquid distribution range of the liquid outlet 54. An eccentric adjustment component 70 is set inside the reactor body 10. The eccentric adjustment component 70 is connected to the stirring component 40. The eccentric adjustment component 70 is used to swing the stirring component 40 and stir the liquid desulfurizing agent raw material located inside the reactor body 10 to expand the stirring range of the stirring component 40.

[0040] During the desulfurizing agent production process, after one type of liquid desulfurizing agent raw material is added to the interior of the reactor body 10, another type of liquid desulfurizing agent raw material is transported to the interior of the transition shell 30 via the rotary liquid inlet assembly 20. During this process, the transition shell 30 rotates, driving the stirring assembly 40 to rotate via the universal joint 31. Simultaneously, the stirring assembly 40 is made to oscillate under the action of the universal joint 31 via the eccentric adjustment assembly 70. The rotation and oscillation of the stirring assembly 40 expand the stirring range of the liquid desulfurizing agent raw material inside the reactor body 10, thus disturbing the liquid desulfurizing agent raw material located inside the reactor body 10. This greatly avoids the deposition of raw materials at the bottom and side walls of the reactor body 10. During the rotation of the transition shell 30, the position adjustment component 60 causes the liquid outlet 54 to move regularly toward and away from the center of the reactor body 10, uniformly conveying the liquid desulfurizing agent raw material into the interior of the reactor body 10. At the same time, the angle adjustment component causes the liquid outlet 54 to swing back and forth, thereby expanding the liquid outlet range of the liquid outlet 54 and more uniformly conveying the liquid desulfurizing agent raw material into the interior of the reactor body 10, so that the stirring component can quickly and evenly mix the liquid desulfurizing agent raw material.

[0041] It should be noted that a feed pipe is connected to the reactor body 10, and a through hole corresponding to the feed pipe is opened on the partition plate 11. The feed pipe passes through the through hole and extends to the bottom of the partition plate 11, so that the feed pipe can directly transport the liquid desulfurizing agent raw material to the position below the partition plate 11 (i.e., the reaction working area of ​​the reactor body 10).

[0042] like Figures 3-7 The position adjustment assembly 60 includes a telescopic component, which includes a telescopic rod 61 and a return spring 62 mounted on the outer surface of the transition shell 30. The telescopic rod 61 is located inside the return spring 62. A connecting mounting bracket 63 is connected to the end of the telescopic rod 61 and the return spring 62 away from the transition shell 30. The connecting mounting bracket 63 is in the shape of an inverted L. The connecting mounting bracket 63 is connected to the conveying pipe 52. A guide plate 12 is installed at the bottom of the partition 11. The guide plate 12 is composed of two arc-shaped plates connected together. The two arc-shaped plates are distributed in an eccentric arc with the center of the partition 11 as the reference. One end of the arc-shaped plate is located in the outer edge area of ​​the partition 11, and the other end of the arc-shaped plate is located in the proximal area of ​​the partition 11. A roller 64 is rolled on the inner wall of the guide plate 12. A roller shaft is connected to the roller 64. The roller shaft is rotatably connected to the top of the connecting mounting bracket 63, and the roller shaft passes through the top of the connecting mounting bracket 63.

[0043] As the transition shell 30 rotates, the telescopic rod 61, the connecting mounting bracket 63, and the roller 64 rotate accordingly. When the roller 64 moves from the outer edge of the guide plate 12 towards the proximal end of the partition 11, it gradually moves towards the center of the partition 11. At this time, the telescopic rod 61 retracts, and the return spring 62 is compressed. The reaction force of the return spring 62 makes the roller 64 fit tightly against the inner wall of the guide plate 12. As the connecting mounting bracket 63 moves, the conveying pipe 52 drives the conveying hose 2 53 and the liquid outlet 54 to gradually move towards the center of the partition 11. Through the gradual movement of the liquid outlet 54, from the top view of the reactor body 10, the liquid outlet 54 gradually delivers the liquid desulfurizing agent raw material from the outer ring. Similarly, as the roller 64 moves from the proximal end of the guide plate 12 to the outer edge of the partition 11, it gradually moves away from the center of the partition 11. At this time, as the connecting mounting bracket 63 moves, the conveying pipe 52 drives the conveying hose 53 and the outlet 54 to gradually move away from the center of the partition 11. Through the gradual movement of the outlet 54, from the top view of the reactor body 10, the outlet 54 distributes the liquid desulfurizing agent raw material in layers from the inner circle to the outer circle, thereby uniformly conveying the liquid desulfurizing agent raw material to the interior of the reactor body 10, avoiding the uneven concentration distribution caused by adding the liquid desulfurizing agent raw material from a single inlet to the interior of the reactor body 10.

[0044] It should be noted that anti-slip textures are provided on the inner wall of the guide plate 12, and the roller 64 can be made of a material with high friction, such as rubber, so that the roller 64 can rotate close to the center during the rotation along the guide plate 12.

[0045] like Figures 4-7 The angle adjustment assembly includes a commutator 65 mounted on a connecting mounting bracket 63 (the commutator is prior art, so its specific structure is not described). The input shaft of the commutator 65 is connected to the roller shaft, and the output shaft of the commutator 65 is connected to a turntable 66. The input shaft and output shaft of the commutator 65 are perpendicular. A connecting rocker arm 67 is rotatably connected to one edge of the turntable 66. A rotating connecting bracket 68 is rotatably connected to one end of the connecting rocker arm 67 away from the turntable 66. A mounting plate 69 connected to the connecting mounting bracket 63 is connected to the outer surface of the delivery pipe 52. A support plate 610 is fixedly connected to one side of the mounting plate 69. The rotating connecting bracket 68 is rotatably connected to the support plate 610, and the bottom end of the rotating connecting bracket 68 is connected to the liquid outlet 54.

[0046] During the rotation of roller 64, the roller shaft rotates accordingly. At this time, the output shaft of the commutator 65 drives the turntable 66 to rotate. Because the connecting rocker arm 67 and the turntable 66 are eccentrically and rotatingly positioned, and because the rotating connecting frame 68 is rotatably connected to the support plate 610, during the adjustment of the outlet 54 position, the rotation of the turntable 66 causes the connecting rocker arm 67 to drive the rotating connecting frame 68 to rotate. The center of rotation is the rotatable connection between the rotating connecting frame 68 and the support plate 610, thus causing the outlet 54 to be in a reciprocating oscillating state. Based on the radial movement of the outlet 54 driven by the position adjustment component 60... The oscillating motion causes the liquid desulfurizing agent raw material to form a composite motion trajectory of "radial movement + circumferential oscillation". When the liquid outlet 54 moves closer to the center of the baffle 11, the oscillation will spread the raw material to both sides, avoiding liquid accumulation in the inner circle area. When the liquid outlet moves to the outer edge area, the oscillation can cover the "blind area" between the radial movement trajectories, so that the raw material forms a relatively comprehensive mesh-like liquid distribution pattern inside the reactor body 10. This composite motion completely eliminates the problems of "strip-like liquid accumulation" and "local excessive concentration" that may be caused by single-direction spraying, allowing the liquid desulfurizing agent raw material to form a uniform concentration field in the liquid medium, ensuring the consistency of the reaction from the source.

[0047] like Figure 3 , Figure 8 and Figure 9The eccentric adjustment component 70 includes a rotating shaft 71 rotatably connected to the partition 11. The rotating shaft 71 is located at the edge of the partition 11. A transmission component 72 is provided between the rotating shaft 71 and the rotating liquid inlet component 20. The transmission component 72 is used to make the rotating shaft 71 rotate with the rotating liquid inlet component 20. A turntable 73 is connected to the bottom end of the rotating shaft 71. A connecting rocker arm 74 is rotatably connected to one edge of the turntable 73. A fine-tuning structure is rotatably provided at the end of the connecting rocker arm 74 away from the turntable 73. The stirring component 40 is rotatably connected to the fine-tuning structure. The fine-tuning structure is used to adjust the position of the stirring component 40 to adjust the swing range of the subsequent stirring component 40.

[0048] During the process of the rotating liquid inlet assembly 20 driving the transition shell 30 to rotate and conveying liquid desulfurizing agent raw materials, the rotating shaft 71 will drive the turntable 73 to rotate under the transmission action of the transmission assembly 72. At this time, under the action of the connecting swing rod 74, the fine adjustment structure and the universal joint 31, the stirring assembly 40 will swing. During this process, the stirring assembly 40 itself rotates. The rotation and swing of the stirring assembly 40 itself expands the stirring range and speed, thereby shortening the time required to stir and mix the liquid desulfurizing agent raw materials and improving the mixing efficiency.

[0049] It should be noted that the transmission assembly 72 is a synchronous belt drive or gear drive structure, and when the liquid outlet 54 swings to its maximum angle towards the inner wall of the reactor body 10, the maximum distance between the center of the baffle 11 and the liquid outlet 54 is less than the minimum distance between the center of the baffle 11 and the rotating shaft 71. This ensures that the liquid outlet 54 will not interfere with the rotating shaft 71 during rotation, thus ensuring that the liquid outlet 54 swings smoothly. In addition, a support seat is installed on the inner wall of the reactor body 10, and the rotating shaft 71 is rotatably connected to the support seat through a bearing to ensure the stability of the rotating shaft 71 during rotation.

[0050] like Figure 8 and Figure 9 The fine-tuning structure includes a fine-tuning connecting plate 75 rotatably connected to the connecting rocker arm 74 and a fine-tuning connecting plate 76 rotatably connected to the rotating liquid inlet assembly 20. Both the fine-tuning connecting plate 75 and the fine-tuning connecting plate 76 have multiple fine-tuning through holes 77 on one side. A bolt and nut connector 78 is provided between the fine-tuning connecting plate 75 and the fine-tuning connecting plate 76. The bolt and nut connector 78 and the fine-tuning through holes 77 are used to adjust the position of the fine-tuning connecting plate 75 and the fine-tuning connecting plate 76.

[0051] By cooperating with the fine-tuning through holes 77 at different positions on the fine-tuning connecting plate 75 and the fine-tuning connecting plate 76, and by fixing the fine-tuning connecting plate 75 and the fine-tuning connecting plate 76 with the bolt and nut connectors 78 and the fine-tuning through holes 77, the distance between the turntable 73 and the center of the stirring assembly 40 can be adjusted, thereby adjusting the angle range of the stirring assembly 40 during the swing process, so that the mixing effect of the stirring assembly 40 on the liquid desulfurizing agent raw material inside the reactor body 10 is better.

[0052] like Figures 1-3 The rotary liquid inlet assembly 20 includes a liquid inlet pipe 21 rotatably connected to the reactor body 10. The bottom end of the liquid inlet pipe 21 is connected to the transition shell 30. The top end of the liquid inlet pipe 21 is connected to a rotary joint 22. The liquid inlet pipe 21 passes through the partition plate 11 and is rotatably connected to the partition plate 11 through a bearing. The end of the rotary joint 22 away from the liquid inlet pipe 21 is connected to a delivery pipe 23. The end of the delivery pipe 23 away from the rotary joint 22 is connected to a delivery pump 24. The top of the reactor body 10 is connected to a drive component 25, which is used to drive the liquid inlet pipe 21 to rotate.

[0053] During the process of conveying a liquid desulfurizing agent raw material, the liquid desulfurizing agent raw material is conveyed to the inside of the rotary joint 22 by the conveying pump 24 and the liquid delivery pipe 23. At this time, the inlet pipe 21 is rotated by the driving component 25. During this process, the rotary joint 22 conveys the liquid desulfurizing agent raw material to the inside of the inlet pipe 21 and then conveys the liquid desulfurizing agent raw material to the inside of the transition shell 30 through the inlet pipe 21. This ensures the smooth conveying of the liquid desulfurizing agent raw material while allowing the inlet pipe 21 and the transition shell 30 to rotate.

[0054] like Figure 1 , Figure 3 , Figure 4 and Figure 8 The stirring assembly 40 includes a stirring shaft 41, which is connected to a fine-tuning connecting plate 76 via a bearing. Multiple stirring blades 42 and spiral blades 43 are connected to the outer surface of the stirring shaft 41, and a stirring paddle 44 is connected to the bottom end of the stirring shaft 41.

[0055] During the stirring process, the universal joint 31 causes the stirring shaft 41 to rotate with the rotation of the transition shell 30. During this process, the eccentric adjustment component 70 drives the stirring shaft 41 to swing. At this time, the stirring blade 42, the spiral blade 43 and the stirring paddle 44 will rotate and swing to stir and mix the liquid desulfurizing agent raw material located inside the reactor body 10. The stirring paddle 44 will also stir the bottom of the reactor body 10 more thoroughly, preventing the liquid desulfurizing agent raw material from settling to the bottom of the reactor body 10. The spiral surface of the spiral blade 43 will generate an axial force on the liquid desulfurizing agent raw material, and through its interaction with the stirring blade 42, the stirring and mixing effect of the liquid desulfurizing agent raw material will be ensured.

[0056] A reaction method for producing a desulfurizing agent includes the following steps:

[0057] S1. A liquid desulfurizing agent raw material is added to the interior of the reactor body 10;

[0058] S2. A liquid desulfurizing agent raw material is transported into the interior of the transition shell 30 by rotating the liquid inlet assembly 20, and the transition shell 30 is rotated in the process, which drives the stirring assembly 40 to rotate through the universal joint 31.

[0059] S3. As the transition shell 30 rotates, the stirring assembly 40 is oscillated by the universal joint 31 through the eccentric adjustment assembly 70. The two liquid desulfurizing agent raw materials are mixed by the rotation and oscillation of the stirring assembly 40. During this process, the liquid outlet 54 is moved regularly towards and away from the center of the reactor body 10 by the position adjustment assembly 60. At the same time, the angle adjustment assembly makes the liquid outlet 54 oscillate back and forth, uniformly conveying the liquid desulfurizing agent raw materials into the interior of the reactor body 10 for mixing.

[0060] In the description of this invention, it should be understood that the terms "center," "longitudinal," "lateral," "length," "width," "thickness," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," "clockwise," "counterclockwise," "axial," "radial," and "circumferential" indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings. They are used only for the convenience of describing this invention and simplifying the description, and are not intended to indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limitations on this invention.

[0061] Furthermore, the terms "first" and "second" are used for descriptive purposes only and should not be construed as indicating or implying relative importance or implicitly specifying the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include at least one of that feature. In the description of this invention, "a plurality of" means at least two, such as two, three, etc., unless otherwise explicitly specified.

[0062] Although embodiments of the present invention have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention. Those skilled in the art can make changes, modifications, substitutions and variations to the above embodiments within the scope of the present invention.

Claims

1. A reaction vessel for producing a desulfurizing agent, characterized in that, The utility model relates to a liquid desulfurization reaction kettle, which comprises the following: a reaction kettle body (10) internally provided with a partition plate (11); a rotating liquid inlet assembly (20) arranged on the reaction kettle body (10), the rotating liquid inlet assembly (20) being connected with a transition shell (30), the rotating liquid inlet assembly (20) being used to drive the transition shell (30) to rotate and to deliver liquid desulfurizer raw materials to the inside of the transition shell (30), the bottom of the transition shell (30) being connected with a universal joint (31); a liquid outlet assembly (50) connected with the transition shell (30), the liquid outlet assembly (50) comprising a liquid outlet (54); a position adjusting assembly (60) arranged between the partition plate (11) and the transition shell (30), the position adjusting assembly (60) being used to adjust the position of the liquid outlet (54) in the process of rotation of the transition shell (30), the position adjusting assembly (60) comprising a guide plate (12) connected with the partition plate (11) and an extension piece connected with the transition shell (30), the extension piece being rotatably connected with a roller (64), the extension piece being used to make the roller (64) fit the inner wall of the guide plate (12), the guide plate (12) comprising two arc-shaped plates connected with each other, one end of the arc-shaped plates being located at the outer edge region of the partition plate (11), the other end of the arc-shaped plates being located at the near-center region of the partition plate (11); an angle adjusting assembly connected with the connecting mounting bracket (63) and the liquid outlet (54), the angle adjusting assembly being used to swing the liquid outlet (54), the angle adjusting assembly comprising a reverser (65), a rotating disc I (66), a connecting swing rod I (67), a rotating connecting bracket (68), a mounting disc (69) and a supporting plate (610), the reverser (65) being mounted on the connecting mounting bracket (63), the input shaft of the reverser (65) being connected with the roller shaft of the roller (64), the output shaft of the reverser (65) being connected with the rotating disc I (66), the connecting swing rod I (67) being rotatably arranged at the edge of one side of the rotating disc I (66), the end of the connecting swing rod I (67) being rotatably connected with the rotating connecting bracket (68), the mounting disc (69) being connected with the liquid outlet assembly (50), the connecting mounting bracket (63) and the supporting plate (610) both being connected with the mounting disc (69), the rotating connecting bracket (68) being rotatably connected with the supporting plate (610), and the bottom end of the rotating connecting bracket (68) being connected with the liquid outlet (54); a stirring assembly (40) connected with the universal joint (31), and the stirring assembly (40) being connected with an eccentric adjusting assembly (70), the eccentric adjusting assembly (70) being used to swing the stirring assembly (40).

2. The reactor for desulfurizer production according to claim 1, characterized in that, The extension piece comprises an extension rod (61), a return spring (62) and a connecting mounting bracket (63), the extension rod (61) and the return spring (62) both being mounted on the outer surface of the transition shell (30), the extension rod (61) being located inside the return spring (62), and the connecting mounting bracket (63) being connected with the output end of the extension rod (61).

3. The reactor for desulfurizer production according to claim 2, characterized in that, The eccentric adjusting assembly (70) comprises a rotating shaft (71), a transmission assembly (72), a rotating disc two (73), a connecting swing lever two (74) and a fine adjustment structure, the rotating shaft (71) is rotatably connected with the partition plate (11) and is arranged at the edge of the partition plate (11), the transmission assembly (72) is arranged between the rotating shaft (71) and the rotating liquid inlet assembly (20), the transmission assembly (72) is used for rotating the rotating shaft (71) with the rotation of the rotating liquid inlet assembly (20), the rotating disc two (73) is connected with the bottom end of the rotating shaft (71), and the connecting swing lever two (74) is rotatably arranged at the edge of one side of the rotating disc two (73), the fine adjustment structure is arranged between the stirring assembly (40) and the connecting swing lever two (74), and the fine adjustment structure is used for adjusting the position of the stirring assembly (40).

4. The reactor for desulfurizer production according to claim 3, characterized in that, The fine adjustment structure comprises a fine adjustment connecting plate one (75), a fine adjustment connecting plate two (76) and a bolt and nut connecting piece (78), the fine adjustment connecting plate one (75) is rotatably connected with the connecting swing lever two (74), the fine adjustment connecting plate two (76) is rotatably connected with the stirring assembly (40), and a plurality of fine adjustment through holes (77) are formed in one side of each of the fine adjustment connecting plate one (75) and the fine adjustment connecting plate two (76), and the bolt and nut connecting piece (78) and the fine adjustment through holes (77) are used for connecting the fine adjustment connecting plate one (75) and the fine adjustment connecting plate two (76).

5. The reactor for desulfurizer production according to claim 4, characterized in that, The rotating liquid inlet assembly comprises a liquid inlet pipe (21), a rotating joint (22) and a liquid delivery pipe (23), the liquid inlet pipe (21) is rotatably connected with the reaction kettle body (10), the rotating joint (22) is connected with the bottom end of the liquid inlet pipe (21), the bottom end of the liquid inlet pipe (21) is connected with and communicates with the transition shell (30), and one end of the liquid delivery pipe (23) is connected with the rotating joint (22).

6. The reactor for desulfurizer production according to claim 5, characterized in that, The stirring assembly comprises a stirring shaft (41), a plurality of stirring blades (42), a helical blade (43) and a stirring paddle (44), the stirring shaft (41) is connected with the fine adjustment connecting plate two (76) through a bearing, the plurality of stirring blades (42) are arranged on the outer surface of the stirring shaft (41), the helical blade (43) is arranged on the outer surface of the stirring shaft (41), and the stirring paddle (44) is connected with the bottom end of the stirring shaft (41) and is located at the bottom position in the reaction kettle body (10).

7. The reactor for desulfurizer production according to claim 6, characterized in that, The liquid outlet assembly (50) further comprises a conveying hose one (51), a conveying pipe (52) and a conveying hose two (53), the conveying hose one (51) is connected with the bottom side of the transition shell (30), one end of the conveying pipe (52) is connected with the conveying hose one (51), the other end of the conveying pipe (52) is connected with the conveying hose two (53), one end of the conveying hose two (53) away from the conveying pipe (52) is connected with the liquid outlet (54), and the outer surface of the conveying pipe (52) is connected with the mounting disc (69).

8. The reactor for desulfurizer production according to claim 7, characterized in that, The rotating liquid inlet assembly further comprises a delivery pump (24) and a driving member (25), the delivery pump (24) is connected with the liquid outlet of the infusion tube (23) far away from the rotary joint (22), the driving member (25) is arranged on the top of the reaction kettle body (10), the driving member (25) is connected with the liquid inlet tube (21), and the driving member (25) is used for driving the liquid inlet tube (21) to rotate.

9. A reaction method for desulfurizer production, applied to the desulfurizer production reactor in claim 8, characterized in that, The method comprises the following steps: S1, adding a liquid desulfurizer raw material into the inside of the reaction kettle body (10); S2, conveying the liquid desulfurizer raw material into the inside of the transition shell (30) through the rotating liquid inlet assembly (20), and rotating the transition shell (30) in the process, and rotating the stirring assembly (40) through the universal joint (31); S3, with the rotation of the transition shell (30), swinging the stirring assembly (40) under the action of the universal joint (31) through the eccentricity adjusting assembly (70), mixing the two liquid desulfurizer raw materials through the rotation and swinging of the stirring assembly (40), and in the process, moving the liquid outlet (54) regularly to the direction close to and far away from the center of the reaction kettle body (10) under the action of the position adjusting assembly (60), and at the same time, reciprocating the liquid outlet (54) to swing through the angle adjusting assembly, uniformly conveying the liquid desulfurizer raw material into the inside of the reaction kettle body (10) and mixing the liquid desulfurizer raw material.

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