Anti-aging essence and preparation device
By using a complex solubilizing system of octyl dodecanol and Transcutol P, along with a precise temperature-controlled emulsification process and a dedicated preparation device, the problem of poor solubility of hydrophobic active ingredients in anti-aging serums has been solved. This has led to the construction of a multi-dimensional efficacy system, which improves stability and gentleness, thus meeting consumers' needs for comprehensive anti-aging.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- LULUS IMPORT & EXPORT CO LTD
- Filing Date
- 2026-04-09
- Publication Date
- 2026-06-05
AI Technical Summary
Existing anti-aging products face challenges in solubilizing hydrophobic active ingredients, making it difficult to build a multi-dimensional synergistic efficacy system. Furthermore, their stability and gentleness are insufficient, failing to meet consumers' demand for comprehensive anti-aging.
It adopts a complex solubilization system of octyl dodecanol and TranscutolP, combined with a 65-70℃ pre-dissolution process, to build a multi-dimensional efficacy system of anti-aging, anti-oxidation, anti-glycation and barrier repair. A stable emulsion is formed through a precise temperature-controlled emulsification process, and skin-friendly oils and moisturizing ingredients are used, along with anti-aging ingredients such as HPR, Pro-Xylane, and oleanolic acid, and are mixed with a dedicated preparation device.
It solves the problem of poor solubility of hydrophobic active ingredients, achieves synergistic effects of multiple dimensions, improves product stability and gentleness, and enhances mixing uniformity and absorption, avoiding the sticky problem of traditional anti-aging serums.
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Figure CN122140583A_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the field of cosmetic technology, and in particular to an anti-aging serum and its preparation apparatus. Background Technology
[0002] With the aging population and rising consumer awareness of skincare, anti-aging has become a core demand in the skincare market, and products with combined effects such as anti-aging, anti-oxidation, anti-glycation, and skin barrier repair are highly sought after. Skin aging is the result of the combined effects of endogenous and exogenous factors, manifesting as multiple problems such as wrinkles, decreased elasticity, dull skin tone, and impaired barrier function. Single-function anti-aging products are no longer sufficient to meet consumers' needs for comprehensive anti-aging solutions.
[0003] Currently, the industry has developed a variety of anti-aging active ingredients and related products. Among them, ingredients such as hydroxypinazone retinyl ester, pro-xylene, peptides, and niacinamide are widely used due to their clear anti-aging mechanisms. Oleanolic acid, a natural plant extract, has also become a potential high-efficiency anti-aging ingredient due to its excellent anti-inflammatory, antioxidant, and anti-aging activities. However, existing anti-aging products still face many technical bottlenecks.
[0004] Therefore, developing an anti-aging serum that can solve the problem of solubilizing hydrophobic active ingredients, build a multi-dimensional synergistic efficacy system, and balance stability and gentleness has become a technological direction that the industry urgently needs to break through. Summary of the Invention
[0005] The purpose of this invention is to solve the problems in the prior art by providing an anti-aging serum and its preparation device.
[0006] To achieve the above objectives, the present invention adopts the following technical solution:
[0007] An anti-aging serum is composed of phases A, B, C, and D, and the components of each phase are as follows by weight percentage:
[0008] Phase A: Deionized water 16.15%, rose hydrosol 18.00%, propylene glycol 5.00%, glycerin 4.00%, xanthan gum 0.15%, carbomer 940 0.10%, panthenol (vitamin B5) 2.00%, bleach (30% aqueous solution) 10.00%, ectoine 2.00%, nicotinamide 2.00%, sodium hyaluronate compound 0.50%;
[0009] Phase B: Polyglycerol-6 distearate 1.20%, Squalane 3.00%, Isononyl isononate 2.00%, Octyldodecyl alcohol 5.00%, Rosehip oil 0.50%, Argan oil 0.50%, Ceramide compound powder 0.50%, Cholesterol 0.30%, Free fatty acids (C18-C22) 0.20%, Transcutol P 4.00%, Oleanolic acid (Ligustrum lucidum extract) 0.50%, Plant extract compound solution 5.00%, Ergothioneine 0.30%;
[0010] Phase C: Carnosine 1.00%, Hydroxypinazone Retinyl Ester (HPR) 12.00%, Resveratrol 2.00%, VPIC (Ascorbate Tetraisopalmitate) 1.00%, Tocopherol (Vitamin E) 0.30%, Palmitoyl Pentapeptide-4 2.00%, Oligopeptide-1 1.00%, Bisabolol 4.00%, Compound Essential Oils 0.20%, Coenzyme Q10 0.30%;
[0011] Phase D: Phenoxyethanol 0.80%, Ethylhexylglycerol 0.10%, Triethanolamine (10% aqueous solution) 0.10%.
[0012] Furthermore, octyl dodecanol is a highly polar oil that works synergistically with TranscutolP to solubilize oleanolic acid; the ceramide compound powder, cholesterol, and free fatty acids (C18-C22) constitute a skin barrier repair system.
[0013] Furthermore, in phase C, hydroxypinazone retinate (HPR), boswellic acid, oleanolic acid, palmitoyl pentapeptide-4, and coenzyme Q10 constitute a complex anti-aging system; resveratrol, ergothionein, VPIC, and tocopherol (vitamin E) constitute an antioxidant system; carnosine is an anti-glycation active ingredient; and panthenol, ectoine, oligopeptide-1, and bisabolol constitute a repair and soothing system.
[0014] Furthermore, the sodium hyaluronate compound is a cosmetic-grade moisturizing compound ingredient, the plant extract compound solution is a mixture of natural plant extracts with anti-aging auxiliary effects, and the compound essential oil is a mixture of cosmetic-grade fragrance essential oils.
[0015] This invention also provides a method for preparing an anti-aging serum, comprising the following steps:
[0016] S1. Oleanolic acid pre-dissolution: Oleanolic acid, Transcutol P and octyldodecyl alcohol in phase B are mixed, heated to 65-70℃ and stirred until completely dissolved to form a transparent and homogeneous solution. This solution is added to the remaining components of phase B and stirred evenly through a preparation device to obtain phase B mixture.
[0017] S2, Phase component preparation: Mix all components of phase A, stir to dissolve, heat to 80°C, and keep warm until the system is homogeneous; heat the mixture of phase B obtained in step S1 to 75°C and keep warm until the system is homogeneous;
[0018] S3. Emulsification: Slowly add the B phase mixture to the A phase and homogenize at high speed of 3000-5000 rpm for 3-5 minutes to form a stable emulsion.
[0019] S4. Cooling and feeding: Cool the above emulsion to below 40°C, and add all components of phase C and all components of phase D in sequence. Stir until the system is homogeneous after each addition.
[0020] S5. pH Adjustment: Adjust the pH of the product to 5.5-6.0 using triethanolamine (10% aqueous solution) in phase D, and then stir evenly to obtain a multi-effect anti-aging essence.
[0021] The present invention also provides an apparatus for preparing an anti-aging serum, comprising a base and a cylinder, wherein the base and the cylinder are fixedly connected by bolts, the cylinder is rotatably connected to a turntable via bearings, a servo motor is fixedly connected to the inner bottom wall of the base, a motor shaft is fixedly connected to the output shaft of the servo motor, a second gear is fixedly connected to the motor shaft, multiple sliding sleeves are slidably connected to the turntable, a first gear is fixedly connected to the sliding sleeves, a gear ring is fixedly connected to the inner side wall of the base, the first gear meshes with the gear ring and the second gear, a stirring shaft is slidably connected to the sliding sleeves, and multiple main stirring blades are fixedly connected to the stirring shaft.
[0022] Furthermore, the turntable is fixedly connected to multiple heating rods, a first sliding block and a second sliding block are fixedly connected to the lower surface of the turntable, a first fixing ring is fixedly connected to the side wall of the base, and a second fixing ring is fixedly connected to the side wall of the base through an insulating rod. The first sliding block is slidably connected to the first fixing ring, and the second sliding block is slidably connected to the second fixing ring. The heating rods are electrically connected to the first sliding block and the second sliding block through wires, and the first fixing ring and the second fixing ring are electrically connected to the power supply through wires.
[0023] Furthermore, a top ring is rotatably connected to the lower surface of the sliding sleeve via a bearing, a rotating seat is rotatably connected to the lower surface of the agitator shaft via a bearing, a spring is fixedly connected between the rotating seat and the top ring, two side plates are fixedly connected to the lower surface of the rotating seat, a rotating rod is fixedly connected between the two side plates, a guide wheel is rotatably connected to the rotating rod via a bearing, a track plate is fixedly connected to the inner bottom wall of the base, the guide wheel is engaged with the track plate, and an auxiliary agitator is fixedly connected to the side wall of the main agitator blade.
[0024] Furthermore, the inner wall of the sliding sleeve is provided with multiple spline grooves, and the side wall of the agitator shaft is fixedly connected with multiple spline blocks, which are slidably connected in the spline grooves.
[0025] Furthermore, the contact points between the first fixing ring and the base, the first sliding block, and the second sliding block and the turntable are all coated with an insulating coating.
[0026] The present invention has the following advantages:
[0027] 1. By adopting a composite solubilization system of octyl dodecanol and Transcutol P, combined with a pre-dissolution process at 65-70℃, the problem of poor solubility and easy precipitation of hydrophobic active ingredients such as oleanolic acid is completely solved, ensuring that each functional ingredient can fully exert its effect and improving the bioavailability of the ingredients.
[0028] 2. Construct a multi-dimensional efficacy system of "anti-aging + anti-oxidation + anti-glycation + barrier repair". Anti-aging ingredients such as HPR, Pro-Xylane, and oleanolic acid work synergistically, combined with anti-oxidation, anti-glycation ingredients and biomimetic lipid repair system to achieve one-stop anti-aging repair, taking into account both high efficiency and gentleness.
[0029] 3. Through precise temperature-controlled emulsification process, a stable emulsion is formed. The product showed no stratification or deterioration in accelerated testing, and its stability was greatly improved. At the same time, the use of skin-friendly oils and moisturizing ingredients makes the essence refreshing and easy to absorb, solving the sticky problem of traditional anti-aging essences.
[0030] 4. The preparation device of the present invention, while the main stirring blade revolves around the motor shaft, also rotates around the stirring shaft, thereby achieving a better stirring effect and making the various components more uniformly mixed;
[0031] 5. While the turntable is rotating to stir, it also drives the heating rod to rotate, which in turn heats the rod. This avoids uneven heating caused by heating in a fixed position, and ensures production results through uniform heating.
[0032] 6. While the sliding sleeve drives the stirring shaft to rotate, the guide wheel, track plate, and spring work together to make the stirring shaft rotate and move up and down. The auxiliary stirring blades also mix in the vertical direction while horizontal stirring is in progress, further improving the mixing effect and efficiency. Attached Figure Description
[0033] Figure 1 This is a schematic diagram of the structure of an anti-aging serum preparation device proposed in this invention;
[0034] Figure 2 This is a schematic diagram of the internal structure of the anti-aging serum preparation device proposed in this invention, taken from a longitudinal section.
[0035] Figure 3 for Figure 2 Enlarged view of point A in the image;
[0036] Figure 4 This is a schematic diagram of the internal structure of the anti-aging serum preparation device proposed in this invention, taken from a longitudinal section.
[0037] Figure 5 This is a schematic diagram of the slide and stirring shaft in the preparation device for an anti-aging serum proposed in this invention;
[0038] Figure 6 This is a schematic diagram of the track plate in the preparation device for an anti-aging essence proposed in this invention.
[0039] In the diagram: 1. Base, 2. Cylinder, 3. Turntable, 4. Sliding sleeve, 5. First gear, 6. Servo motor, 7. Motor shaft, 8. Second gear, 9. Gear ring, 10. Stirring shaft, 11. Main stirring blade, 12. Heating rod, 13. First fixing ring, 14. Insulating rod, 15. Second fixing ring, 16. First sliding block, 17. Second sliding block, 18. Spline groove, 19. Spline block, 20. Top ring, 21. Rotating seat, 22. Spring, 23. Side plate, 24. Rotating rod, 25. Guide wheel, 26. Track plate, 27. Secondary stirring blade. Detailed Implementation
[0040] The technical solutions of the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present invention, and not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of the present invention.
[0041] Example
[0042] An anti-aging serum is composed of phases A, B, C, and D, and the components of each phase are as follows by weight percentage:
[0043] Phase A:
[0044] 16.15% deionized water: as a solvent, it provides a dispersion carrier for each component and ensures the homogeneity of the system;
[0045] Rose hydrosol 18.00%: It has both solvent and soothing functions, and is rich in active substances from rose extract. It gently moisturizes and relieves skin redness.
[0046] Propylene glycol 5.00%: A moisturizer and solubilizer that increases skin hydration and helps dissolve some poorly soluble components;
[0047] Glycerin 4.00%: A classic moisturizer that forms a moisturizing film on the skin surface, reducing moisture loss and enhancing skin hydration;
[0048] Xanthan gum 0.15%: Thickener, adjusts product viscosity, prevents stratification, and improves system stability;
[0049] Carbomer 9400.10%: Thickener and emulsifying aid, enhances the gel texture of the product and works synergistically with emulsifiers to improve emulsion stability;
[0050] Panthenol (Vitamin B5) 2.00%: A repairing ingredient that promotes skin barrier repair, increases skin hydration, and relieves dryness and discomfort;
[0051] Pro-Xylane (30% aqueous solution) 10.00%: The core anti-aging ingredient, which activates the activity of skin fibroblasts, promotes collagen synthesis, and improves skin elasticity;
[0052] Ectoin 2.00%: A repairing and soothing ingredient that protects against external irritants such as UV rays and dryness, and relieves skin inflammation.
[0053] Niacinamide 2.00%: A whitening and anti-aging ingredient that inhibits melanin transport, improves dull skin tone, promotes stratum corneum metabolism, and enhances skin barrier function.
[0054] Sodium hyaluronate compound 0.50%: A moisturizing compound containing hyaluronic acid of different molecular weights to achieve deep hydration and surface moisture retention, improving skin hydration;
[0055] Phase B:
[0056] Polyglycerol-6 distearate 1.20%: Nonionic emulsifier, reduces the interfacial tension between water and oil, allowing the water and oil phases to fully mix and form a stable emulsion;
[0057] Squalane 3.00%: A moisturizing ingredient that is similar to the skin's own oil structure, has strong skin affinity, moisturizes without being sticky, and repairs the skin's lipid barrier;
[0058] Isonononyl isononanoate 2.00%: Emollient and solubilizer, with a refreshing texture, it helps dissolve hydrophobic components and improves product spreadability;
[0059] Octyldodecyl alcohol 5.00%: A highly polar oil and solubilizer that provides a hydrophobic environment for oleanolic acid and works synergistically with other solubilizers to achieve efficient solubilization;
[0060] Rosehip oil 0.50%: A moisturizing and repairing ingredient, rich in unsaturated fatty acids, which nourishes the skin and improves rough skin.
[0061] Argan oil 0.50%: A moisturizing ingredient containing nutrients such as vitamin E and sterols, which enhances skin hydration and aids in barrier repair;
[0062] Ceramide compound powder 0.50%: The core ingredient for barrier repair, replenishing ceramides in the stratum corneum of the skin, repairing the damaged barrier, and reducing moisture loss;
[0063] Cholesterol 0.30%: A barrier repair ingredient that works synergistically with ceramides and free fatty acids to maintain the stability of the skin's lipid bilayer;
[0064] Free fatty acids (C18-C22) 0.20%: Barrier repair ingredient, mimicking the lipid composition of the skin's stratum corneum to enhance barrier integrity and water retention capacity;
[0065] Transcutol P4.00%: A highly efficient cosolvent that reduces the interfacial tension of hydrophobic components such as oleanolic acid, achieving complete dissolution and improving bioavailability;
[0066] Oleanolic acid (privet fruit extract) 0.50%: a core anti-aging ingredient that inhibits matrix metalloproteinase activity, reduces collagen degradation, and also has anti-inflammatory and antioxidant effects;
[0067] Plant extract compound solution 5.00%: auxiliary anti-aging ingredients, containing a variety of natural plant active substances, which synergistically enhance antioxidant and soothing effects;
[0068] Ergothioneine 0.30%: A cell-level antioxidant that scavenge free radicals, protects cellular DNA from damage, and delays skin aging;
[0069] Phase C:
[0070] Carnosine 1.00%: An anti-glycation ingredient that inhibits the formation of advanced glycation end products (AGEs) and improves dull skin tone and sagging skin;
[0071] Hydroxypinazone Retinyl Ester (HPR) 12.00%: A powerful anti-aging ingredient, a retinol derivative that acts directly on the skin without conversion, promoting collagen regeneration and improving wrinkles and enlarged pores;
[0072] Resveratrol 2.00%: An antioxidant that scavenge free radicals, inhibits lipid peroxidation, and works synergistically with other ingredients to enhance anti-aging effects;
[0073] VPIC (Tetraisopalmitate Ascorbate) 1.00%: An antioxidant and whitening ingredient, a vitamin C derivative, fat-soluble and easily absorbed, it scavenge free radicals and inhibits melanin production;
[0074] Tocopherol (Vitamin E) 0.30%: A fat-soluble antioxidant that protects skin cell membranes from free radical damage while enhancing product stability;
[0075] Palmitoyl pentapeptide - 42.00%: A signal peptide anti-aging ingredient that mimics skin growth factor to promote collagen and elastin synthesis and firm the skin;
[0076] Oligopeptide - 11.00%: A repairing ingredient that promotes skin cell proliferation and repair, improves damaged skin condition, and enhances skin resistance;
[0077] Bisabolol 4.00%: A soothing ingredient with significant anti-inflammatory activity, it relieves skin irritation that may be caused by highly active ingredients and reduces the risk of redness;
[0078] 0.20% blended essential oil: Fragrance ingredient that gives the product a gentle aroma, enhances the user experience, and has a mild soothing effect;
[0079] Coenzyme Q100 30%: An anti-aging and antioxidant ingredient that enhances mitochondrial activity, delays cell aging, and improves dull skin.
[0080] Phase D:
[0081] Phenoxyethanol 0.80%: The main preservative, which inhibits the growth of bacteria and fungi and extends the shelf life of the product;
[0082] Ethylhexylglycerin 0.10%: an auxiliary preservative and solubilizer, enhancing the preservative effect of phenoxyethanol, and also helping to dissolve some hydrophobic components;
[0083] Triethanolamine (10% aqueous solution) 0.10%: pH adjuster, neutralizes acidic components such as carbomer, adjusts the product pH to 5.5-6.0, matches the skin's physiological environment, and ensures the stability of active ingredients.
[0084] This invention also provides a method for preparing an anti-aging serum, comprising the following steps:
[0085] S1. Oleanolic acid pre-dissolution: Oleanolic acid, Transcutol P and octyldodecyl alcohol in phase B are mixed, heated to 65-70℃ and stirred until completely dissolved to form a transparent and homogeneous solution. This solution is added to the remaining components of phase B and stirred evenly through a preparation device to obtain phase B mixture.
[0086] S2, Phase component preparation: Mix all components of phase A, stir to dissolve, heat to 80°C, and keep warm until the system is homogeneous; heat the mixture of phase B obtained in step S1 to 75°C and keep warm until the system is homogeneous;
[0087] S3. Emulsification: Slowly add the B phase mixture to the A phase and homogenize at high speed of 3000-5000 rpm for 3-5 minutes to form a stable emulsion.
[0088] S4. Cooling and feeding: Cool the above emulsion to below 40°C, and add all components of phase C and all components of phase D in sequence. Stir until the system is homogeneous after each addition.
[0089] S5. pH Adjustment: Adjust the pH of the product to 5.5-6.0 using triethanolamine (10% aqueous solution) in phase D, and then stir evenly to obtain a multi-effect anti-aging essence.
[0090] Reference Figure 1-6 The present invention also provides an apparatus for preparing an anti-aging essence, including a base 1 and a cylinder 2. The base 1 and the cylinder 2 are fixedly connected by bolts. The cylinder 2 is rotatably connected to a turntable 3 via a bearing. A servo motor 6 is fixedly connected to the inner bottom wall of the base 1. The output shaft of the servo motor 6 is fixedly connected to a motor shaft 7. A second gear 8 is fixedly connected to the motor shaft 7. Multiple sliding sleeves 4 are slidably connected to the turntable 3. A first gear 5 is fixedly connected to the sliding sleeves 4. A gear ring 9 is fixedly connected to the inner side wall of the base 1. The first gear 5 meshes with the gear ring 9 and the second gear 8. A stirring shaft 10 is slidably connected to the sliding sleeves 4. A hole (not shown in the figure) is opened at the bottom of the sliding sleeves 4 to ensure the free sliding of the stirring shaft 10. Multiple main stirring blades 11 are fixedly connected to the stirring shaft 10.
[0091] Multiple heating rods 12 are fixedly connected to the turntable 3. A first sliding block 16 and a second sliding block 17 are fixedly connected to the lower surface of the turntable 3. A first fixing ring 13 is fixedly connected to the side wall of the base 1. A second fixing ring 15 is fixedly connected to the side wall of the base 1 through an insulating rod 14. The first sliding block 16 is slidably connected to the first fixing ring 13, and the second sliding block 17 is slidably connected to the second fixing ring 15. The heating rods 12 are electrically connected to the first sliding block 16 and the second sliding block 17 through wires. The first fixing ring 13 and the second fixing ring 15 are electrically connected to the power source through wires.
[0092] A top ring 20 is rotatably connected to the lower surface of the sliding sleeve 4 via a bearing. A rotating seat 21 is rotatably connected to the lower surface of the stirring shaft 10 via a bearing. A spring 22 is fixedly connected between the rotating seat 21 and the top ring 20. Two side plates 23 are fixedly connected to the lower surface of the rotating seat 21. A rotating rod 24 is fixedly connected between the two side plates 23. A guide wheel 25 is rotatably connected to the rotating rod 24 via a bearing. A track plate 26 is fixedly connected to the inner bottom wall of the base 1. The guide wheel 25 is snapped onto the track plate 26. A secondary stirring blade 27 is fixedly connected to the side wall of the main stirring blade 11.
[0093] The inner sidewall of the sliding sleeve 4 is provided with multiple spline grooves 18, and the sidewall of the agitator shaft 10 is fixedly connected with multiple spline blocks 19. The spline blocks 19 are slidably connected in the spline grooves 18. Through the arrangement of the spline grooves 18 and the spline blocks 19, the designed agitator shaft 10 can slide up and down in the sliding sleeve 4, and can also rotate with the sliding sleeve 4.
[0094] Insulating coatings are applied to the contact points between the first fixing ring 13 and the base 1, the first sliding block 16, the second sliding block 17 and the turntable 3. The insulating coatings ensure the insulation of the contact points between the first fixing ring 13 and the base 1, the first sliding block 16, the second sliding block 17 and the turntable 3, and prevent power leakage.
[0095] The sliding connections of the preparation equipment of the present invention are all provided with sealing gaskets to ensure its sealing performance.
[0096] In this invention, the raw materials to be mixed are placed inside the cylinder 2, and the servo motor 6 is turned on. The servo motor 6 drives the second gear 8 to rotate through the motor shaft 7. The second gear 8, through its cooperation with the gear ring 9, causes the first gear 5 to rotate around the second gear 8 while also rotating itself. This causes the first gear 5 to drive the stirring shaft 10 to rotate around the second gear 8 while also rotating itself. Consequently, the stirring shaft 10 drives the main stirring blade 11 to rotate on its own axis while also revolving around the central axis, thus stirring the internal raw materials.
[0097] At the same time, the sliding sleeve 4 will also drive the turntable 3 to rotate, and the rotation of the turntable 3 will drive the heating rod 12 to rotate, so that the heating rod 12 heats the raw material during the rotation process, which makes the heating more uniform compared to a fixed heating position.
[0098] While the sliding sleeve 4 rotates, it also drives the guide wheel 25 to move through the rotating seat 21. The guide wheel 25 then moves on the track plate 26. Through the shape design of the track plate 26, in conjunction with the spring 22, the guide wheel 25 moves up and down repeatedly during rotation, thereby causing the stirring shaft 10 to move up and down repeatedly. This, in conjunction with the auxiliary stirring blade 27, stirs the raw materials vertically, thus combining horizontal and vertical directions to continuously stir the raw materials, significantly improving the mixing effect and mixing efficiency.
[0099] The above description is only a preferred embodiment of the present invention, but the scope of protection of the present invention is not limited thereto. Any equivalent substitutions or modifications made by those skilled in the art within the scope of the technology disclosed in the present invention, based on the technical solution and inventive concept of the present invention, should be covered within the scope of protection of the present invention.
Claims
1. An anti-aging serum, characterized in that, It consists of phases A, B, C, and D, and the composition of each phase by weight percentage is as follows: Phase A: Deionized water 16.15%, rose hydrosol 18.00%, propylene glycol 5.00%, glycerin 4.00%, xanthan gum 0.15%, carbomer 940 0.10%, panthenol (vitamin B5) 2.00%, bleach (30% aqueous solution) 10.00%, ectoine 2.00%, nicotinamide 2.00%, sodium hyaluronate compound 0.50%; Phase B: Polyglycerol-6 distearate 1.20%, Squalane 3.00%, Isononyl isononate 2.00%, Octyldodecyl alcohol 5.00%, Rosehip oil 0.50%, Argan oil 0.50%, Ceramide compound powder 0.50%, Cholesterol 0.30%, Free fatty acids (C18-C22) 0.20%, Transcutol P 4.00%, Oleanolic acid (Ligustrum lucidum extract) 0.50%, Plant extract compound solution 5.00%, Ergothioneine 0.30%; Phase C: Carnosine 1.00%, Hydroxypinazone Retinyl Ester (HPR) 12.00%, Resveratrol 2.00%, VPIC (Ascorbate Tetraisopalmitate) 1.00%, Tocopherol (Vitamin E) 0.30%, Palmitoyl Pentapeptide-4 2.00%, Oligopeptide-1 1.00%, Bisabolol 4.00%, Compound Essential Oils 0.20%, Coenzyme Q10 0.30%; Phase D: Phenoxyethanol 0.80%, Ethylhexylglycerol 0.10%, Triethanolamine (10% aqueous solution) 0.10%.
2. The anti-aging serum according to claim 1, characterized in that, In phase B, octyl dodecanol is a highly polar oil that works synergistically with TranscutolP to solubilize oleanolic acid; the ceramide compound powder, cholesterol, and free fatty acids (C18-C22) constitute a skin barrier repair system.
3. The anti-aging serum according to claim 1, characterized in that, In phase C, hydroxypinazone retinate (HPR), boswellic acid, oleanolic acid, palmitoyl pentapeptide-4, and coenzyme Q10 constitute a complex anti-aging system; resveratrol, ergothionein, VPIC, and tocopherol (vitamin E) constitute an antioxidant system; carnosine is an anti-glycation active ingredient; and panthenol, ectoine, oligopeptide-1, and bisabolol constitute a repair and soothing system.
4. The anti-aging serum according to claim 1, characterized in that, The sodium hyaluronate compound is a cosmetic-grade moisturizing compound ingredient, the plant extract compound solution is a mixture of natural plant extracts with anti-aging auxiliary effects, and the compound essential oil is a mixture of essential oils for cosmetic fragrance.
5. A method for preparing an anti-aging serum as described in any one of claims 1-4, characterized in that, Includes the following steps: S1. Oleanolic acid pre-dissolution: Oleanolic acid, Transcutol P and octyldodecyl alcohol in phase B are mixed, heated to 65-70℃ and stirred until completely dissolved to form a transparent and homogeneous solution. This solution is added to the remaining components of phase B and stirred evenly through a preparation device to obtain phase B mixture. S2, Phase component preparation: Mix all components of phase A, stir to dissolve, heat to 80°C, and keep warm until the system is homogeneous; heat the mixture of phase B obtained in step S1 to 75°C and keep warm until the system is homogeneous; S3. Emulsification: Slowly add the B phase mixture to the A phase and homogenize at high speed of 3000-5000 rpm for 3-5 minutes to form a stable emulsion. S4. Cooling and feeding: Cool the above emulsion to below 40°C, and add all components of phase C and all components of phase D in sequence. Stir until the system is homogeneous after each addition. S5. pH Adjustment: Adjust the pH of the product to 5.5-6.0 using triethanolamine (10% aqueous solution) in phase D, and then stir evenly to obtain a multi-effect anti-aging essence.
6. An apparatus for preparing an anti-aging serum as described in claim 5, characterized in that, The device includes a base (1) and a cylinder (2). The base (1) and the cylinder (2) are fixedly connected by bolts. The cylinder (2) is rotatably connected to a turntable (3) via a bearing. A servo motor (6) is fixedly connected to the inner bottom wall of the base (1). A motor shaft (7) is fixedly connected to the output shaft of the servo motor (6). A second gear (8) is fixedly connected to the motor shaft (7). Multiple sliding sleeves (4) are slidably connected through the turntable (3). A first gear (5) is fixedly connected to the sliding sleeve (4). A gear ring (9) is fixedly connected to the inner side wall of the base (1). The first gear (5) meshes with the gear ring (9) and the second gear (8). A stirring shaft (10) is slidably connected to the sliding sleeve (4). Multiple main stirring blades (11) are fixedly connected to the stirring shaft (10).
7. The anti-aging serum preparation apparatus according to claim 6, characterized in that, The turntable (3) is fixedly connected to multiple heating rods (12). The lower surface of the turntable (3) is fixedly connected to a first sliding block (16) and a second sliding block (17). The side wall of the base (1) is fixedly connected to a first fixing ring (13). The side wall of the base (1) is fixedly connected to a second fixing ring (15) via an insulating rod (14). The first sliding block (16) is slidably connected to the first fixing ring (13). The second sliding block (17) is slidably connected to the second fixing ring (15). The heating rods (12) are electrically connected to the first sliding block (16) and the second sliding block (17) via wires. The first fixing ring (13) and the second fixing ring (15) are electrically connected to the power source via wires.
8. The anti-aging serum preparation apparatus according to claim 6, characterized in that, The lower surface of the sliding sleeve (4) is rotatably connected to a top ring (20) via a bearing. The lower surface of the stirring shaft (10) is rotatably connected to a rotating seat (21) via a bearing. A spring (22) is fixedly connected between the rotating seat (21) and the top ring (20). Two side plates (23) are fixedly connected to the lower surface of the rotating seat (21). A rotating rod (24) is fixedly connected between the two side plates (23). A guide wheel (25) is rotatably connected to the rotating rod (24) via a bearing. A track plate (26) is fixedly connected to the inner bottom wall of the base (1). The guide wheel (25) is engaged on the track plate (26). A secondary stirring blade (27) is fixedly connected to the side wall of the main stirring blade (11).
9. The anti-aging serum preparation apparatus according to claim 6, characterized in that, The inner wall of the sliding sleeve (4) is provided with multiple spline grooves (18), and the side wall of the stirring shaft (10) is fixedly connected with multiple spline blocks (19), which are slidably connected in the spline grooves (18).
10. The anti-aging serum preparation apparatus according to claim 7, characterized in that, An insulating coating is applied to the contact points between the first fixing ring (13) and the base (1), the first sliding block (16), and the second sliding block (17) and the turntable (3).