A tert-butoxide potassium reactor
By combining storage, mixing, and heating mechanisms, the problems of mixing effect and discharge efficiency in the potassium tert-butoxide reactor were solved, achieving rapid mixing and efficient production.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- CHANGYI RONGXIN CHEM CO LTD
- Filing Date
- 2026-05-13
- Publication Date
- 2026-08-04
AI Technical Summary
The existing potassium tert-butoxide reactors are inadequate in terms of mixing effect and discharge efficiency, resulting in long reaction time and low production efficiency.
The design employs a combination of storage, mixing, and heating mechanisms, using heating, mixing, and pressurization to achieve rapid mixing of raw materials and rapid discharge of viscous potassium tert-butoxide.
It improves the mixing uniformity and reaction rate in the potassium tert-butoxide reaction process, enhances the adaptability of the equipment, and increases production efficiency.
Smart Images
Figure CN122164354B_ABST
Abstract
Description
Technical Field
[0001] This invention relates to the technical field of potassium tert-butoxide preparation, and in particular to a potassium tert-butoxide reaction vessel. Background Technology
[0002] Potassium tert-butoxide is a commonly used strong base in organic chemistry. In the production process of potassium tert-butoxide, it is necessary to use a reaction vessel that is easy to feed materials, as disclosed in the invention patent with publication number CN115193371B, and an energy-saving reaction vessel disclosed in the invention patent with publication number CN118179426B, to mix the raw materials for preparing potassium tert-butoxide and make them react.
[0003] However, during the potassium tert-butoxide reaction, the initial reaction stage is a clear solution, the middle reaction stage is a low-viscosity solution, and the later reaction stage is a viscous solution. The existing reactor structure is relatively simple, and the mixing of materials is achieved by simply driving the stirring blades with a stirring shaft. This results in poor mixing effect and long reaction time. Furthermore, the potassium tert-butoxide that is about to be discharged after the reaction is in a viscous state, and it is difficult to discharge it quickly by simply opening the discharge valve, which affects production efficiency and leads to poor practicality. Therefore, there is an urgent need for a potassium tert-butoxide reactor to improve the above problems. Summary of the Invention
[0004] To solve the above-mentioned technical problems, the present invention provides a potassium tert-butoxide reactor in which potassium tert-butoxide raw material is discharged into a storage mechanism, the storage mechanism is heated by a heating mechanism to reach the required temperature, the potassium tert-butoxide raw material is mixed by a mixing mechanism to prepare potassium tert-butoxide, and after preparation, the storage mechanism pressurizes the interior of the storage mechanism and then rapidly discharges the potassium tert-butoxide through the bottom of the storage mechanism, thereby improving the practicality of the equipment.
[0005] The present invention provides a potassium tert-butoxide reactor, comprising a storage mechanism; further comprising a mixing mechanism and a heating mechanism, both of which are mounted on the storage mechanism; The storage unit stores the raw material of potassium tert-butoxide, the mixing unit mixes the raw material of potassium tert-butoxide, and the heating unit regulates the temperature in the storage unit. Potassium tert-butoxide (PTB) is fed into a storage unit. The storage unit is heated to the required temperature by a heating unit. The PTB raw material is then mixed by a mixing unit to prepare PTB. After preparation, the storage unit is pressurized by the mixing unit and then the PTB is quickly discharged from the bottom of the storage unit, thereby improving the practicality of the equipment.
[0006] Preferably, the storage mechanism includes a reactor, multiple sets of frames, multiple sets of feed inlets, exhaust outlets, and a discharge valve. The multiple sets of frames are all installed on the reactor, the multiple sets of feed inlets and exhaust outlets are all installed on the top of the reactor, and the discharge valve is installed at the bottom of the reactor. Multiple raw materials are discharged into the reactor through the multiple sets of feed inlets, and then the heating mechanism and the mixing mechanism work together to mix and react the multiple raw materials to form potassium tert-butoxide. Then the discharge valve is opened to discharge the potassium tert-butoxide.
[0007] Preferably, the mixing mechanism includes a pressure regulating mechanism, a jetting mechanism, a support pipe, a rotating shaft, stirring blades, a reducer, and a drive motor. The support pipe is installed on the top of the reactor. The rotating shaft is rotatably installed on the reactor, with one end extending into the reactor. The stirring blades are installed on the rotating shaft, and the other end of the rotating shaft passes through the support pipe and extends to the top of the support pipe. The reducer is installed on the support pipe, and the other end of the rotating shaft is connected to the output end of the reducer. The drive motor is installed on the reducer, and the output shaft of the drive motor is connected to the input end of the reducer. Both the pressure regulating mechanism and the jetting mechanism are installed on the reactor. When the drive motor is turned on, the rotating shaft drives the stirring blades to rotate via the reducer, stirring the various raw materials in the reactor. At the same time, the hydrogen produced in the previous preparation of potassium tert-butoxide is pressurized and discharged into the jetting mechanism through the pressure regulating mechanism. Simultaneously, the jetting mechanism operates, causing the raw materials in the reactor to mix with the hydrogen and be sprayed into the reactor. The opposing impact of the sprayed raw materials with the rising hydrogen improves the mixing effect and mixing speed of the various raw materials.
[0008] Preferably, the jetting mechanism includes a conveying mechanism, a first circulating pump, a circulating pipe, a second circulating pump, a rotary connecting pipe, a first spray pipe, and multiple sets of nozzles. The first circulating pump is installed on the reactor, and its suction port communicates with the interior of the reactor. One end of the circulating pipe is connected to the discharge port of the first circulating pump, and the other end of the circulating pipe extends to the bottom of the reactor. The conveying mechanism is installed on the other end of the circulating pipe. The second circulating pump is fixedly installed at the bottom of the reactor. One end of the rotary connecting pipe is rotatably installed on the discharge port of the second circulating pump. The bottom end of the first spray pipe rotates. Installed on the top of the rotary connecting pipe, the top of the first spray pipe is connected to one end of the rotating shaft, and multiple sets of nozzles are installed on the first spray pipe. Through the operation of the first circulation pump, the various raw materials at the top of the reactor flow sequentially through the first circulation pump, the circulation pipe and the conveying mechanism, and then are discharged into the reactor. At the same time, the second circulation pump operates, causing the various raw materials at the bottom of the reactor to flow sequentially through the second circulation pump, the rotary connecting pipe, the first spray pipe and the first nozzle, and then be discharged into the reactor. The various raw materials sprayed from the first set of nozzles collide with the various raw materials sprayed from the conveying mechanism, causing them to mix.
[0009] Preferably, the conveying mechanism includes a connecting pipe, a second spray pipe, a piston ring, a second nozzle, a tension spring, and a telescopic pipe. One end of the connecting pipe is installed on the other end of the circulation pipe. One end of the second spray pipe is slidably installed in the connecting pipe through the piston ring. The second nozzle is installed on the other end of the second spray pipe. One end of the tension spring is installed on the connecting pipe, and the other end of the tension spring is installed on the second nozzle. One end of the telescopic pipe is connected to the connecting pipe, and the other end of the telescopic pipe is connected to the second nozzle. The telescopic pipe wraps around the connecting pipe, the second spray pipe, and the tension spring. The various raw materials discharged from the circulation pipe flow sequentially through the connecting pipe and the second spray pipe. The second nozzle discharges the various raw materials back into the reactor. When the raw materials have good flowability, the elasticity of the tension spring holds the second nozzle in place, maintaining its position. When the flowability of the raw materials decreases, the discharge performance of the second nozzle deteriorates, causing the raw materials to push the piston ring in the connecting pipe, causing the second spray pipe to extend out of the connecting pipe and move the second nozzle closer to the first nozzle, ensuring the impact effect of the raw materials.
[0010] Preferably, the pressure regulating mechanism includes a pressure regulating cylinder, a piston, a hydraulic cylinder, a first gas supply pipe, a first electrically controlled valve, a second gas supply pipe, and a second electrically controlled valve. The pressure regulating cylinder is mounted on the reactor. The piston is slidably mounted inside the pressure regulating cylinder. The hydraulic cylinder is fixedly mounted on the pressure regulating cylinder, with one end of the hydraulic cylinder connected to the piston. One end of the first gas supply pipe communicates with the interior of the pressure regulating cylinder, and the other end of the first gas supply pipe is connected to the exhaust port via the first electrically controlled valve. One end of the second gas supply pipe is connected to the circulation pipe, and the other end of the second gas supply pipe is connected to the pressure regulating cylinder via the second electrically controlled valve. The internal components of the pressure cylinder are interconnected. When the first electric control valve is opened, the hydraulic cylinder contracts, causing the piston to slide upward and draw the hydrogen produced by the reaction of various raw materials into the pressure regulating cylinder. Then, the first electric control valve is closed, and the second electric control valve is opened. The hydraulic cylinder extends, causing the piston to move downward and discharge the hydrogen into the circulation pipe, where it mixes with the various raw materials in the circulation pipe. Afterward, the mixture of various raw materials and hydrogen is discharged into the reaction vessel through the second nozzle. The hydrogen rises among the various raw materials, thereby improving the mixing effect of the various raw materials.
[0011] Preferably, it also includes a positive pressure pipe and an electrically controlled valve three. One end of the positive pressure pipe is connected to the top of the reactor, and the other end of the positive pressure pipe is connected to the inside of the pressure regulating cylinder through the electrically controlled valve three. When discharging, the discharge valve and the electrically controlled valve three are opened, and the piston slides downward by extending the hydraulic cylinder, so that hydrogen is discharged into the top of the reactor, thereby increasing the pressure in the reactor and causing the discharge valve to quickly discharge potassium tert-butoxide.
[0012] Preferably, the heating mechanism includes a heating element, and a cavity is provided in the side wall of the reactor, in which the heating element is installed; the temperature inside the reactor is adjusted by operating the heating element.
[0013] Preferably, an observation window is provided on the top of the reactor; by opening the observation window, it is convenient for staff to inspect the interior of the reactor.
[0014] Preferably, the surface of the reactor is provided with a heat insulation layer to reduce heat loss inside the reactor.
[0015] Compared with the prior art, the beneficial effects of the present invention are as follows: 1. The raw materials are mixed with hydrogen and then sprayed through the jetting mechanism. Multiple sets of nozzles are used for impact spraying, combined with stirring blades, which greatly improves the mixing uniformity and reaction rate of raw materials at each stage of the potassium tert-butoxide reaction. 2. The conveying mechanism is equipped with a retractable spray pipe and tension spring, which can automatically adjust the distance between the nozzle and the opposite nozzle according to the change of raw material viscosity, ensuring the impact mixing effect at different reaction stages and enhancing the adaptability of the equipment. 3. The hydrogen gas generated by the reaction is pressurized by the pressure regulating mechanism and then introduced into the top of the reactor, which increases the pressure inside the reactor. Combined with the bottom discharge valve, this enables the rapid discharge of the viscous potassium tert-butoxide, thereby improving production efficiency. Attached Figure Description
[0016] Figure 1 This is a schematic diagram of the first isometric structure of the present invention; Figure 2 This is a schematic diagram of the second isometric structure of the present invention; Figure 3 This is a front view structural diagram of the present invention; Figure 4 This is a schematic diagram of the isometric cross-sectional structure of the present invention; Figure 5 This is the present invention. Figure 4 A magnified structural diagram of part A in the diagram; Figure 6 This is a frontal cross-sectional structural diagram of the present invention; Figure 7 This is the present invention. Figure 6 A magnified structural diagram of part B in the diagram; Figure 8 This is a first isometric structural schematic diagram of the conveying mechanism of the present invention; Figure 9 This is a schematic diagram of the second isometric structure of the conveying mechanism of the present invention; Figure 10 This is a front view cross-sectional structural schematic diagram of the conveying mechanism of the present invention.
[0017] The attached diagram is labeled as follows: 1. Reactor; 2. Frame; 3. Feed inlet; 4. Exhaust outlet; 5. Discharge valve; 6. Support pipe; 7. Rotary shaft; 8. Stirring blades; 9. Reducer; 10. Drive motor; 11. Circulation pump one; 12. Circulation pipe; 13. Circulation pump two; 14. Rotary connecting pipe; 15. Spray pipe one; 16. Nozzle one; 17. Connecting pipe; 18. Spray pipe two; 19. Piston ring; 20. Nozzle two; 21. Tension spring; 22. Telescopic pipe; 23. Pressure regulating cylinder; 24. Piston; 25. Hydraulic cylinder; 26. Gas supply pipe one; 27. Electrically controlled valve one; 28. Gas supply pipe two; 29. Electrically controlled valve two; 30. Positive pressure pipe; 31. Electrically controlled valve three; 32. Heating element; 33. Observation window. Detailed Implementation
[0018] To facilitate understanding of the present invention, a more complete description will be given below with reference to the accompanying drawings. The present invention can be implemented in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
[0019] Example 1: As Figures 1 to 10 As shown, a potassium tert-butoxide reactor includes a storage mechanism; it also includes a mixing mechanism and a heating mechanism, both of which are mounted on the storage mechanism. The storage unit stores the raw material of potassium tert-butoxide, the mixing unit mixes the raw material of potassium tert-butoxide, and the heating unit regulates the temperature in the storage unit. The storage mechanism includes a reactor 1, multiple sets of frames 2, multiple sets of feed inlets 3, exhaust outlets 4, and discharge valves 5. The multiple sets of frames 2 are all installed on the reactor 1, the multiple sets of feed inlets 3 and exhaust outlets 4 are all installed on the top of the reactor 1, and the discharge valves 5 are installed on the bottom of the reactor 1. The mixing mechanism includes a pressure regulating mechanism, a jetting mechanism, a support tube 6, a rotating shaft 7, stirring blades 8, a reducer 9, and a drive motor 10. The support tube 6 is installed on the top of the reactor 1. The rotating shaft 7 is rotatably installed on the reactor 1, and one end of the rotating shaft 7 extends into the reactor 1. The stirring blades 8 are installed on the rotating shaft 7, and the other end of the rotating shaft 7 passes through the support tube 6 and extends to the top of the support tube 6. The reducer 9 is installed on the support tube 6, and the other end of the rotating shaft 7 is connected to the output end of the reducer 9. The drive motor 10 is installed on the reducer 9, and the output shaft of the drive motor 10 is connected to the input end of the reducer 9. The pressure regulating mechanism and the jetting mechanism are both installed on the reactor 1. The jetting mechanism includes a conveying mechanism, a circulating pump 11, a circulating pipe 12, a circulating pump 2 13, a rotary connecting pipe 14, a spray pipe 15, and multiple sets of nozzles 16. The circulating pump 11 is installed on the reactor 1, and the suction port of the circulating pump 11 is connected to the interior of the reactor 1. One end of the circulating pipe 12 is connected to the discharge port of the circulating pump 11, and the other end of the circulating pipe 12 extends to the bottom of the reactor 1. The conveying mechanism is installed on the other end of the circulating pipe 12. The circulating pump 2 13 is fixedly installed at the bottom of the reactor 1. One end of the rotary connecting pipe 14 is rotatably installed on the discharge port of the circulating pump 2 13. The bottom end of the spray pipe 15 is rotatably installed on the top of the rotary connecting pipe 14, and the top of the spray pipe 15 is connected to one end of the rotating shaft 7. Multiple sets of nozzles 16 are all installed on the spray pipe 15. The conveying mechanism includes a connecting pipe 17, a second spray pipe 18, a piston ring 19, a second nozzle 20, a tension spring 21, and a telescopic pipe 22. One end of the connecting pipe 17 is installed on the other end of the circulation pipe 12. One end of the second spray pipe 18 is slidably installed in the connecting pipe 17 through the piston ring 19. The second nozzle 20 is installed on the other end of the second spray pipe 18. One end of the tension spring 21 is installed on the connecting pipe 17, and the other end of the tension spring 21 is installed on the second nozzle 20. One end of the telescopic pipe 22 is connected to the connecting pipe 17, and the other end of the telescopic pipe 22 is connected to the second nozzle 20. The telescopic pipe 22 also wraps around the connecting pipe 17, the second spray pipe 18, and the tension spring 21. The pressure regulating mechanism includes a pressure regulating cylinder 23, a piston 24, a hydraulic cylinder 25, a gas supply pipe 26, an electric control valve 27, a gas supply pipe 28, and an electric control valve 29. The pressure regulating cylinder 23 is installed on the reactor 1. The piston 24 is slidably installed in the pressure regulating cylinder 23. The hydraulic cylinder 25 is fixedly installed on the pressure regulating cylinder 23, and one end of the hydraulic cylinder 25 is connected to the piston 24. One end of the gas supply pipe 26 is connected to the inside of the pressure regulating cylinder 23, and the other end of the gas supply pipe 26 is connected to the exhaust port 4 through the electric control valve 27. One end of the gas supply pipe 28 is connected to the circulation pipe 12, and the other end of the gas supply pipe 28 is connected to the inside of the pressure regulating cylinder 23 through the electric control valve 29. It also includes a positive pressure pipe 30 and an electric control valve 31. One end of the positive pressure pipe 30 is connected to the top of the reactor 1, and the other end of the positive pressure pipe 30 is connected to the inside of the pressure regulating cylinder 23 through the electric control valve 31. An observation window 33 is provided on the top of the reactor 1; Multiple raw materials are fed into the reactor 1 through multiple feed inlets 3. The drive motor 10 is turned on, and through the reducer 9, the rotating shaft 7 drives the stirring blades 8 to rotate, stirring the various raw materials in the reactor 1. Simultaneously, the circulation pump 11 operates, causing the various raw materials at the top of the reactor 1 to flow sequentially through the circulation pump 11, circulation pipe 12, connecting pipe 17, and spray pipe 18, and then be discharged back into the reactor 1 through the spray nozzle 20. At the same time, the circulation pump 13 operates, causing the raw materials at the bottom of the reactor 1 to flow back into the reactor 1. Multiple raw materials flow sequentially through circulating pump 13, rotary connecting pipe 14, spray pipe 15, and nozzle 16 before being discharged into reactor 1. The various raw materials sprayed from multiple sets of nozzles 16 collide with those sprayed from the conveying mechanism, causing them to mix. When the raw materials have good flowability, the elasticity of tension spring 21 holds nozzle 20 in place. As the flowability of the raw materials decreases, the discharge capability of nozzle 20 deteriorates, causing the raw materials to push piston ring 19 in connecting pipe 17, thus causing the spray... Material pipe 218 extends from connecting pipe 17, thereby bringing nozzle 20 closer to nozzle 16 to ensure the impact effect of the raw materials. During the initial and intermediate reaction stages, electrically controlled valve 27 is opened, and hydraulic cylinder 25 retracts, causing piston 24 to slide upward, drawing hydrogen produced by the reaction of various raw materials into pressure regulating cylinder 23. Then, electrically controlled valve 27 is closed, and electrically controlled valve 29 is opened. Hydraulic cylinder 25 extends, causing piston 24 to move downward, discharging hydrogen into circulation pipe 12, allowing the hydrogen to circulate with the circulating fluid. Multiple raw materials are mixed in the ring pipe 12, and then the mixture of multiple raw materials and hydrogen is discharged into the reactor 1 through the nozzle 20. The hydrogen rises in the multiple raw materials, which further improves the mixing effect of the multiple raw materials. After the reaction is completed, the discharge valve 5 and the electric control valve 31 are opened. The hydraulic cylinder 25 extends, causing the piston 24 to slide downward, and the hydrogen is discharged into the top of the reactor 1, which increases the pressure in the reactor 1. Then the discharge valve 5 quickly discharges potassium tert-butoxide, thereby improving the practicality of the equipment.
[0020] Example 2: A potassium tert-butoxide reactor, which, based on Example 1, further includes: The heating mechanism includes a heating element 32. A cavity is provided in the side wall of the reactor 1, and the heating element 32 is installed in the side wall of the reactor 1. The surface of reactor 1 is provided with a heat insulation layer; Multiple raw materials are fed into reactor 1 through multiple feed inlets 3. Then, one feed inlet 3 is connected to a vacuum pump to expel air from reactor 1 and introduce a suitable amount of nitrogen. During operation, the drive motor 10 is turned on, and through the reducer 9, the rotating shaft 7 drives the stirring blades 8 to rotate, stirring the various raw materials in reactor 1. Simultaneously, the circulation pump 11 operates, causing the various raw materials at the top of reactor 1 to flow sequentially through the circulation pump 11, circulation pipe 12, connecting pipe 17, and spray pipe 18, and then through nozzle 20 to return the various raw materials to reactor 1. Heating element 32 operates to adjust the temperature inside reactor 1. Simultaneously, circulating pump 2 13 operates, causing various raw materials at the bottom of reactor 1 to flow sequentially through circulating pump 2 13, rotary connecting pipe 14, spray pipe 1 15, and nozzle 1 16 before being discharged into reactor 1. Furthermore, the various raw materials sprayed from multiple sets of nozzles 16 collide with those sprayed from the conveying mechanism, mixing them. During the reaction, a small amount of nitrogen is continuously introduced to maintain a slight positive pressure. Excess gas is discharged into the plant's gas treatment pipeline through the pipe connected to inlet 3. When the raw materials have good flowability, the elasticity of tension spring 21 holds them in place. Nozzle 20 is maintained in its position. After the material flowability decreases, the discharge performance of nozzle 20 deteriorates, causing the material to push piston ring 19 in connecting pipe 17, causing spray pipe 2 18 to extend from connecting pipe 17. This brings nozzle 20 closer to nozzle 1 16, ensuring the impact effect of the material. During the initial and intermediate reaction stages, electronic control valve 1 27 is opened, and hydraulic cylinder 25 contracts, causing piston 24 to slide upward, drawing hydrogen gas produced by the reaction of various materials into pressure regulating cylinder 23. Then, electronic control valve 1 27 is closed, and electronic control valve 2 29 is opened, through hydraulic cylinder 25... Extending the piston 24 downwards, hydrogen is discharged into the circulation pipe 12, where it mixes with various raw materials. The mixture is then discharged into the reactor 1 via nozzle 20. The hydrogen rises among the raw materials, further enhancing the mixing effect. After the reaction, discharge valve 5 and electric control valve 31 are opened. The hydraulic cylinder 25 extends, causing piston 24 to slide downwards, discharging hydrogen to the top of the reactor 1. This increases the pressure inside the reactor 1, allowing discharge valve 5 to quickly discharge potassium tert-butoxide, thus improving the equipment's usability.
[0021] The hydrogen circulation of this invention is an intermittent, quantitative circulation, activated only in the initial stage (clear solution) and the middle stage (low viscosity solution) of the reaction to enhance material mixing; the hydrogen circulation loop is immediately shut off in the later stage of the reaction (concentrated solution), and the remaining hydrogen is safely discharged through the exhaust port, preventing its continuous accumulation in the reactor; the main functions achieved by this invention are: 1. The raw materials are mixed with hydrogen and then sprayed through the jetting mechanism. Multiple sets of nozzles are used for impact spraying, combined with stirring blades, which greatly improves the mixing uniformity and reaction rate of raw materials at each stage of the potassium tert-butoxide reaction. 2. The conveying mechanism is equipped with a retractable spray pipe and tension spring, which can automatically adjust the distance between the nozzle and the opposite nozzle according to the change of raw material viscosity, ensuring the impact mixing effect at different reaction stages and enhancing the adaptability of the equipment. 3. The hydrogen gas generated by the reaction is pressurized by the pressure regulating mechanism and then introduced into the top of the reactor, which increases the pressure inside the reactor. Combined with the bottom discharge valve, this enables the rapid discharge of the viscous potassium tert-butoxide, thereby improving production efficiency.
[0022] The top of the reactor 1 is equipped with a hydrogen concentration sensor and a pressure sensor. After the reactor 1 is installed, the entire equipment is connected to the ground wire in the explosion-proof plant and is equipped with an electrostatic eliminator. During the use of the equipment, regular inspections are carried out to ensure the safety and stability of the equipment. The piston 24 in the pressure regulating cylinder 23 is coated with an antistatic polytetrafluoroethylene coating, and the piston rod of the hydraulic cylinder 25 is treated with hard chrome plating. The installation, connection, or setting method of the potassium tert-butoxide reactor of the present invention are all common mechanical methods, and any method that can achieve its beneficial effects can be implemented. The reactor 1, reducer 9, drive motor 10, circulating pump 11, circulating pump 13, hydraulic cylinder 25, electric control valve 27, electric control valve 29, electric control valve 31, and heating element 32 of the potassium tert-butoxide reactor of the present invention are commercially available. Technical personnel in this industry only need to install and operate them according to the accompanying instruction manual, without requiring any creative work from those skilled in the art.
[0023] The above description is only a preferred embodiment of the present invention. It should be noted that for those skilled in the art, several improvements and modifications can be made without departing from the technical principles of the present invention, and these improvements and modifications should also be considered within the scope of protection of the present invention.
Claims
1. A potassium tert-butoxide reactor, comprising a storage mechanism; characterized in that, It also includes a mixing mechanism and a heating mechanism, both of which are mounted on the storage mechanism; The storage unit stores the raw material of potassium tert-butoxide, the mixing unit mixes the raw material of potassium tert-butoxide, and the heating unit regulates the temperature in the storage unit. The storage mechanism includes a reactor (1), multiple sets of frames (2), multiple sets of feed inlets (3), exhaust outlets (4) and discharge valves (5). The multiple sets of frames (2) are all installed on the reactor (1), the multiple sets of feed inlets (3) and exhaust outlets (4) are all installed on the top of the reactor (1), and the discharge valves (5) are installed on the bottom of the reactor (1). The mixing mechanism includes a pressure regulating mechanism, a jetting mechanism, a support tube (6), a rotating shaft (7), stirring blades (8), a reducer (9), and a drive motor (10). The support tube (6) is installed on the top of the reactor (1). The rotating shaft (7) is rotatably installed on the reactor (1), and one end of the rotating shaft (7) extends into the reactor (1). The stirring blades (8) are installed on the rotating shaft (7), and the other end of the rotating shaft (7) passes through the support tube (6) and extends to the top of the support tube (6). The reducer (9) is installed on the support tube (6), and the other end of the rotating shaft (7) is connected to the output end of the reducer (9). The drive motor (10) is installed on the reducer (9), and the output shaft of the drive motor (10) is connected to the input end of the reducer (9). The pressure regulating mechanism and the jetting mechanism are both installed on the reactor (1). The jetting mechanism includes a conveying mechanism, a first circulating pump (11), a circulating pipe (12), a second circulating pump (13), a rotary connecting pipe (14), a first spray pipe (15), and multiple sets of nozzles (16). The first circulating pump (11) is installed on the reactor (1), and the suction port of the first circulating pump (11) is connected to the interior of the reactor (1). One end of the circulating pipe (12) is connected to the discharge port of the first circulating pump (11), and the other end of the circulating pipe (12) extends to the reactor (16). 1) The bottom of the reactor (1) is connected to the bottom of the reactor (1). The conveying mechanism is installed on the other end of the circulation pipe (12). The second circulation pump (13) is fixedly installed on the bottom of the reactor (1). One end of the rotary connecting pipe (14) is rotatably installed on the discharge port of the second circulation pump (13). The bottom end of the first spray pipe (15) is rotatably installed on the top of the rotary connecting pipe (14). The top of the first spray pipe (15) is connected to one end of the rotating shaft (7). Multiple sets of nozzles (16) are installed on the first spray pipe (15). The conveying mechanism includes a connecting pipe (17), a second spray pipe (18), a piston ring (19), a second nozzle (20), a tension spring (21), and a telescopic pipe (22). One end of the connecting pipe (17) is installed on the other end of the circulation pipe (12). One end of the second spray pipe (18) is slidably installed in the connecting pipe (17) through the piston ring (19). The second nozzle (20) is installed on the other end of the second spray pipe (18). One end of the tension spring (21) is installed on the connecting pipe (17), and the other end of the tension spring (21) is installed on the second nozzle (20). One end of the telescopic pipe (22) is connected to the connecting pipe (17), and the other end of the telescopic pipe (22) is connected to the second nozzle (20). The telescopic pipe (22) wraps around the connecting pipe (17), the second spray pipe (18), and the tension spring (21). The pressure regulating mechanism includes a pressure regulating cylinder (23), a piston (24), a hydraulic cylinder (25), a gas supply pipe (26), an electric control valve (27), a gas supply pipe (28), and an electric control valve (29). The pressure regulating cylinder (23) is installed on the reactor (1), the piston (24) is slidably installed in the pressure regulating cylinder (23), the hydraulic cylinder (25) is fixedly installed on the pressure regulating cylinder (23), and one end of the hydraulic cylinder (25) is connected to the piston (24). One end of the gas supply pipe (26) is connected to the inside of the pressure regulating cylinder (23), and the other end of the gas supply pipe (26) is connected to the exhaust port (4) through the electric control valve (27). One end of the gas supply pipe (28) is connected to the circulation pipe (12), and the other end of the gas supply pipe (28) is connected to the inside of the pressure regulating cylinder (23) through the electric control valve (29). It also includes a positive pressure pipe (30) and an electric control valve three (31). One end of the positive pressure pipe (30) is connected to the top of the reactor (1), and the other end of the positive pressure pipe (30) is connected to the inside of the pressure regulating cylinder (23) through the electric control valve three (31). In the initial and intermediate reaction stages, the first electric control valve (27) is opened, and the hydraulic cylinder (25) contracts, causing the piston (24) to slide upward, drawing the hydrogen generated by the reaction of various raw materials into the pressure regulating cylinder (23). Then, the first electric control valve (27) is closed, and the second electric control valve (29) is opened. The piston (24) is moved downward by the extension of the hydraulic cylinder (25), discharging the hydrogen into the circulation pipe (12), mixing the hydrogen with the various raw materials in the circulation pipe (12). Then, the mixture of various raw materials and hydrogen is discharged into the reactor (1) through the nozzle (20). After the reaction is completed, the discharge valve (5) and the third electric control valve (31) are opened. The piston (24) is moved downward by the extension of the hydraulic cylinder (25), discharging the hydrogen into the top of the reactor (1), increasing the pressure inside the reactor (1), and then the discharge valve (5) quickly discharges potassium tert-butoxide.
2. The potassium tert-butoxide reactor as described in claim 1, characterized in that, The heating mechanism includes a heating element (32), and a cavity is provided in the side wall of the reactor (1). The heating element (32) is installed in the side wall of the reactor (1).
3. The potassium tert-butoxide reactor as described in claim 1, characterized in that, An observation window (33) is provided on the top of the reactor (1).
4. The potassium tert-butoxide reactor as described in claim 1, characterized in that, The surface of the reactor (1) is provided with a heat insulation layer.