A heat treatment method for improving hydrogen embrittlement resistance of 316L stainless steel

By performing 20% ​​pre-cooling rolling and 1000℃ annealing and water quenching on 316L stainless steel, a high-proportion Σ3 coherent twin boundary network was constructed, which solved the problem of increased hydrogen embrittlement after recrystallization of 316L stainless steel, and achieved excellent resistance to hydrogen embrittlement at high temperature, meeting the service requirements of hydrogen environment.

CN122405937APending Publication Date: 2026-07-17HEFEI UNIV OF TECH
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
HEFEI UNIV OF TECH
Filing Date
2026-04-16
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing heat treatment methods cannot effectively construct hydrogen-resistant twin boundary networks after recrystallization of 316L stainless steel, resulting in increased hydrogen embrittlement sensitivity at high temperatures and failing to meet the requirements for safe service in hydrogen environments.

Method used

By subjecting cold-rolled 316L stainless steel to 20% pre-cooling and short-time annealing at 1000℃ combined with water quenching, a high proportion of Σ3 coherent twin boundaries are induced to form, constructing a hydrogen-resistant twin boundary network and regulating the distribution of grain boundary characteristics to suppress hydrogen embrittlement.

Benefits of technology

The hydrogen embrittlement index was significantly reduced from 43.4% to 7.3%, achieving excellent resistance to hydrogen embrittlement of 316L stainless steel at high temperatures and meeting the safe service requirements of hydrogen environments such as hydrogen energy and nuclear power.

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Abstract

本发明属于金属材料热处理与氢脆防控技术领域,公开了一种提升316L不锈钢抗氢脆效果的热处理方法。该方法通过对冷轧态316L不锈钢进行20%压下量的室温预冷轧,随后在1000℃下保温10min并水淬,诱导生成高比例Σ3共格孪晶界抗氢网络。本发明解决了常规热处理后316L不锈钢再结晶导致氢脆敏感性急剧升高的技术难题,处理后材料氢脆指数降至7.3%,具备优异的抗氢脆性能与工程应用价值,适用于氢能、核电等氢环境装备用材。
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