Decompression concentration device for W-oxides

Abstract

The utility model relates to the technical field of concentration devices, and provides a vacuum concentration device for WO-oxides, which comprises a base, the top of the base is fixedly connected with a concentrator shell, the surface of the concentrator shell is fixedly connected with a pressure gauge, and an electric stirring rod is arranged and can slowly rotate in the concentrator shell to stir the WO-oxides. When an electric stirring rod is not needed or the electric stirring rod needs to be detached for cleaning, a control ring can be rotated, the control ring immediately descends along a connecting rod, when the control ring descends, a sliding block is driven to synchronously descend through an embedded rod, when the sliding block descends, thrust is applied to a movable plate, and the movable plate is driven to rotate; when the electric stirring rod is dismounted, the movable plate starts to rotate around the joint of the sliding blocks, and when the movable plate rotates, thrust towards the side face is applied to the clamping plate, so that the clamping plate slides out of the clamping groove, the mounting rod is not clamped any more, and at the moment, the electric stirring rod can be dismounted.

Description

Technical Field

[0001] The utility model relates to the technical field of concentration devices, in particular to a Woshi oxide decompression concentration device. Background Art

[0002] Woss is a chemical intermediate, also known as 16α,17α-epoxyprogesterone. It is a white or off-white crystalline powder, odorless, slightly soluble in ethanol, methanol, toluene, and easily soluble in chloroform and dichloromethane. When Woss is produced, it needs to be placed inside the equipment for processing in order to concentrate it.

[0003] However, many of the current Woshi oxide vacuum concentration devices lack the stirring effect on the materials when in use, which may cause the problem of incomplete concentration of the Woshi oxide during concentration.

[0004] In view of this, the utility model proposes a Woshi oxide decompression concentration device. Utility Model Content

[0005] The utility model provides a Woshi oxide vacuum concentration device, which solves the problem that many Woshi oxide vacuum concentration devices in the related technology are lack of stirring effect on materials when in use, so that the Woshi oxide may not be concentrated thoroughly when being concentrated.

[0006] The technical scheme of the utility model is as follows: a Woshi oxide decompression concentrating device comprises a base, the top of the base is fixedly connected with a concentrator shell, the surface of the concentrator shell is fixedly connected with a pressure gauge, the left side of the concentrator shell is fixedly connected with a feed port, the right side of the concentrator shell is fixedly connected with a pressure relief valve, the inside of the concentrator shell is fixedly connected with a heating plate, the top of the concentrator shell is attached with an upper cover, the bottom of the upper cover is fixedly connected with a connecting rod, the surface of the connecting rod is threadedly connected with a control ring, the bottom of the control ring is fixedly connected with a clamping column, the inside of the control ring is slidably connected with three groups of embedded rods, the tails of the three groups of embedded rods are fixedly connected with sliders, the inner walls of the three groups of sliders are rotatably connected with movable plates, the sides of the three groups of movable plates are rotatably connected with clamping plates slidably connected to the inside of the clamping column, the inner wall of the clamping column is attached with a mounting rod, the surface of the mounting rod is provided with three groups of card grooves, and the bottom of the mounting rod is fixedly connected with an electric stirring rod.

[0007] Preferably, a transmission block is fixedly connected to the surface of the concentrator housing, a connecting plate is fixedly connected to the top of the base, a force-bearing block is slidably connected to the side of the connecting plate, and a spring damper connected to the connecting plate is fixedly connected to the tail of the force-bearing block.

[0008] Preferably, the heating plate is annularly arranged along the interior of the concentrator housing, and the concentrator housing is sealed by an upper cover.

[0009] Preferably, the surface of the control ring is provided with a circular connecting groove whose center is located at the same point as the control ring, and the control ring forms a lifting structure along the surface of the connecting rod.

[0010] Preferably, the embedded rod and the sliding block are designed to be perpendicular to each other, and the embedded rod drives the sliding block to form a lifting structure.

[0011] Preferably, the three groups of movable plates are all arranged obliquely inside the slider, and the three groups of movable plates form a rotating structure through the slider.

[0012] Preferably, the connection points between the three groups of movable plates and the three groups of clamping plates are all located at the end points of their own tail ends, and the three groups of clamping plates form a sliding structure inside the clamping column.

[0013] Preferably, the three groups of clamping plates are respectively embedded in the three groups of clamping slots, and the mounting rods form a fixed structure inside the clamping columns.

[0014] Preferably, the force-bearing block is located on the motion track of the transmission block, and the mutually approaching surfaces of the force-bearing block and the transmission block are both designed as inclined surfaces.

[0015] Preferably, the force-bearing block forms a sliding structure through a transmission block, and the spring damper forms a telescopic state through the force-bearing block.

[0016] The working principle and beneficial effects of the utility model are:

[0017] 1. In the utility model, an electric stirring rod is provided, and the electric stirring rod can be slowly rotated inside the concentrator housing to stir the oxide, so that the oxide concentration can be more uniform. When the electric stirring rod is not needed or needs to be disassembled for cleaning, the control ring can be rotated, and the control ring will then descend along the connecting rod. When the control ring descends, the slider will be driven to descend synchronously through the embedded rod. When the slider descends, a thrust is applied to the movable plate, so that the movable plate starts to rotate around the connecting part of the slider, and when the movable plate rotates, a thrust is applied to the card plate to the side, so that the card plate slides out of the card slot and no longer engages with the mounting rod. At this time, the electric stirring rod can be disassembled;

[0018] 2. In the utility model, a transmission block is arranged. When the concentrator housing shakes left and right, the transmission block will be driven to approach the force-bearing block. When the transmission block moves, it will apply a thrust to the force-bearing block through its own inclined surface, so that the force-bearing block slides along the connecting plate and applies a thrust to the spring damper, so that the spring damper converts the thrust of the force-bearing block into elastic potential energy, thereby reducing the shaking amplitude of the concentrator housing to a certain extent. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] The utility model is further described in detail below in conjunction with the accompanying drawings and specific implementation methods.

[0020] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0021] Figure 2 This is a schematic diagram of the three-dimensional structure of the utility model from another perspective;

[0022] Figure 3 This is a schematic diagram of the internal structure of the concentrator housing of the utility model;

[0023] Figure 4 This is a schematic diagram of the structure of the movable plate of the utility model;

[0024] Figure 5 This is a schematic diagram of the locking column structure of the utility model;

[0025] Figure 6 This is a schematic diagram of the transmission block structure of the utility model.

[0026] In the figure: 1. base; 2. concentrator housing; 3. pressure gauge; 4. feed port; 5. pressure relief valve; 6. heating plate; 7. upper cover; 8. connecting rod; 9. control ring; 10. embedded rod; 11. slider; 12. movable plate; 13. clamping plate; 14. clamping groove; 15. clamping column; 16. mounting rod; 17. electric stirring rod; 18. transmission block; 19. connecting plate; 20. force block; 21. spring damper. DETAILED DESCRIPTION

[0027] The following will be combined with the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0028] Example 1

[0029] The preferred embodiment of the Woshi oxide vacuum concentration device provided by the utility model is as follows Figures 1 to 6As shown: a Woshi oxide decompression concentration device, including a base 1, a concentrator shell 2 is fixedly connected to the top of the base 1, a pressure gauge 3 is fixedly connected to the surface of the concentrator shell 2, a feed port 4 is fixedly connected to the left side of the concentrator shell 2, a pressure relief valve 5 is fixedly connected to the right side of the concentrator shell 2, a heating plate 6 is fixedly connected to the inside of the concentrator shell 2, an upper cover 7 is attached to the top of the concentrator shell 2, a connecting rod 8 is fixedly connected to the bottom of the upper cover 7, a control ring 9 is threadedly connected to the surface of the connecting rod 8, and a control ring 9 is threadedly connected to the control ring 9. A locking column 15 is fixedly connected to the bottom of the ring 9, and three groups of embedded rods 10 are slidably connected inside the control ring 9. The tails of the three groups of embedded rods 10 are fixedly connected to sliders 11, and the inner walls of the three groups of sliders 11 are rotatably connected to movable plates 12. The sides of the three groups of movable plates 12 are rotatably connected to clamping plates 13 that are slidably connected to the inside of the locking column 15. The inner wall of the locking column 15 is attached to a mounting rod 16, and the surface of the mounting rod 16 is provided with three groups of slots 14. The bottom of the mounting rod 16 is fixedly connected to an electric stirring rod 17.

[0030] In this embodiment, the heating plate 6 is arranged in a ring shape along the interior of the concentrator housing 2. The concentrator housing 2 forms a sealed structure through the upper cover 7. The heating plate 6 heats the interior of the concentrator housing 2 to increase the concentration efficiency of the oxide.

[0031] In this embodiment, the surface of the control ring 9 is provided with a circular connection groove whose center is located at the same point as the control ring 9, and the control ring 9 forms a lifting structure along the surface of the connection rod 8.

[0032] In this embodiment, the embedded rod 10 and the slider 11 are designed to be perpendicular to each other. The embedded rod 10 drives the slider 11 to form a lifting structure. The control ring 9 is rotated, and the control ring 9 then descends along the connecting rod 8. When it descends, it will drive the slider 11 to descend synchronously through the embedded rod 10.

[0033] In this embodiment, the three groups of movable plates 12 are all inclined inside the slider 11. The three groups of movable plates 12 form a rotating structure through the slider 11. When the slider 11 descends, a thrust is applied to the movable plates 12, causing the movable plates 12 to start rotating around the connection point of the slider 11.

[0034] In this embodiment, the connection points between the three groups of movable plates 12 and the three groups of clamping plates 13 are all located at the tail end points of themselves. The three groups of clamping plates 13 form a sliding structure inside the locking column 15. When the movable plates 12 rotate, a lateral thrust is applied to the clamping plates 13, causing the clamping plates 13 to slide out of the inside of the clamping slots 14.

[0035] In this embodiment, the three groups of clamping plates 13 are respectively embedded in the three groups of clamping slots 14, and the mounting rod 16 forms a fixed structure inside the clamping column 15. When the clamping plate 13 no longer clamps the mounting rod 16, the electric stirring rod 17 can be disassembled.

[0036] Example 2

[0037] On the basis of Example 1, a preferred embodiment of the Woshi oxide decompression concentration device provided by the utility model is as follows Figures 1 to 6 As shown: a transmission block 18 is fixedly connected to the surface of the concentrator housing 2, a connecting plate 19 is fixedly connected to the top of the base 1, a force block 20 is slidably connected to the side of the connecting plate 19, and a spring damper 21 connected to the connecting plate 19 is fixedly connected to the tail of the force block 20.

[0038] In this embodiment, the force-bearing block 20 is located on the movement trajectory of the transmission block 18, and the mutually approaching surfaces of the force-bearing block 20 and the transmission block 18 are both designed as inclined surfaces. By setting the transmission block 18, when the concentrator housing 2 shakes left and right, it will drive the transmission block 18 to approach the force-bearing block 20. When the transmission block 18 moves, it will apply thrust to the force-bearing block 20 through its own inclined surface.

[0039] In this embodiment, the force block 20 forms a sliding structure through the transmission block 18, and the spring damper 21 forms a telescopic state through the force block 20. The force block 20 slides along the connecting plate 19 and applies thrust to the spring damper 21, so that the spring damper 21 converts the thrust of the force block 20 into elastic potential energy, thereby reducing the shaking amplitude of the concentrator housing 2 to a certain extent.

[0040] The working principle and use process of the utility model are as follows: first, the oxide is discharged into the interior of the concentrator housing 2 through the feed port 4, and then the interior of the concentrator housing 2 is heated by the heating plate 6 to increase the concentration efficiency of the oxide. The user can observe the pressure value in the device through the pressure gauge 3. When the pressure inside the device is too high, the pressure relief valve 5 can be used to reduce the pressure inside the device. In order to make the oxide concentrate evenly, the electric stirring rod 17 can be used to slowly rotate inside the concentrator housing 2 to stir the oxide;

[0041] Since the electric stirring rod 17 is connected to the engaging column 15 through the clamping plate 13, when the electric stirring rod 17 is not needed or needs to be disassembled for cleaning, the control ring 9 can be rotated, and the control ring 9 will then descend along the connecting rod 8. When it descends, it will drive the slider 11 to descend synchronously through the embedded rod 10. When the slider 11 descends, it will apply a thrust to the movable plate 12, so that the movable plate 12 starts to rotate around the connecting part of the slider 11, and when the movable plate 12 rotates, it will apply a side thrust to the clamping plate 13, so that the clamping plate 13 slides out of the inside of the clamping groove 14 and no longer engages with the mounting rod 16. At this time, the electric stirring rod 17 can be disassembled;

[0042] When the equipment is working, shaking is inevitable. By setting the transmission block 18, when the concentrator housing 2 shakes left and right, it will drive the transmission block 18 to approach the force-bearing block 20. When the transmission block 18 moves, it will apply a thrust to the force-bearing block 20 through its own inclined surface, so that the force-bearing block 20 slides along the connecting plate 19 and applies a thrust to the spring damper 21, so that the spring damper 21 converts the thrust of the force-bearing block 20 into elastic potential energy, thereby reducing the shaking amplitude of the concentrator housing 2 to a certain extent.

[0043] The above are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A Woshi oxide vacuum concentration device, comprising a base (1), characterized in that: The top of the base (1) is fixedly connected to a concentrator housing (2), the surface of the concentrator housing (2) is fixedly connected to a pressure gauge (3), the left side of the concentrator housing (2) is fixedly connected to a feed port (4), the right side of the concentrator housing (2) is fixedly connected to a pressure relief valve (5), the interior of the concentrator housing (2) is fixedly connected to a heating plate (6), the top of the concentrator housing (2) is fitted with an upper cover (7), the bottom of the upper cover (7) is fixedly connected to a connecting rod (8), the surface of the connecting rod (8) is threadedly connected to a control ring (9), the bottom of the control ring (9) is fixedly connected to A locking column (15) is connected, and three groups of embedded rods (10) are slidably connected inside the control ring (9), and the tails of the three groups of embedded rods (10) are fixedly connected to sliders (11), and the inner walls of the three groups of sliders (11) are rotatably connected to movable plates (12), and the sides of the three groups of movable plates (12) are rotatably connected to clamping plates (13) slidably connected to the inside of the locking column (15), and the inner wall of the locking column (15) is fitted with a mounting rod (16), and the surface of the mounting rod (16) is provided with three groups of slots (14), and the bottom of the mounting rod (16) is fixedly connected to an electric stirring rod (17).

2. A Woshi oxide vacuum concentration device according to claim 1, characterized in that: A transmission block (18) is fixedly connected to the surface of the concentrator housing (2), a connecting plate (19) is fixedly connected to the top of the base (1), a force-bearing block (20) is slidably connected to the side of the connecting plate (19), and a spring damper (21) connected to the connecting plate (19) is fixedly connected to the tail of the force-bearing block (20).

3. A Woshi oxide vacuum concentration device according to claim 1, characterized in that: The heating plate (6) is arranged in a ring shape along the interior of the concentrator housing (2), and the concentrator housing (2) forms a sealed structure through an upper cover (7).

4. A Woshi oxide vacuum concentration device according to claim 1, characterized in that: The surface of the control ring (9) is provided with a circular connecting groove whose center is located at the same point as the control ring (9), and the control ring (9) forms a lifting structure along the surface of the connecting rod (8).

5. The Woshi oxide vacuum concentration device according to claim 1, characterized in that: The embedded rod (10) and the sliding block (11) are designed to be perpendicular to each other, and the embedded rod (10) drives the sliding block (11) to form a lifting structure.

6. The Woshi oxide decompression concentration device according to claim 1, characterized in that: The three groups of movable plates (12) are all arranged in an inclined manner inside the slider (11), and the three groups of movable plates (12) form a rotating structure through the slider (11).

7. The Woshi oxide decompression concentration device according to claim 1, characterized in that: The connection points between the three groups of movable plates (12) and the three groups of clamping plates (13) are all located at the end points of their own tails, and the three groups of clamping plates (13) form a sliding structure inside the clamping column (15).

8. The Woshi oxide vacuum concentration device according to claim 1, characterized in that: The three groups of clamping plates (13) are respectively embedded in the interior of the three groups of clamping slots (14), and the mounting rod (16) forms a fixed structure inside the clamping column (15).

9. The Woshi oxide decompression concentration device according to claim 2, characterized in that: The force-bearing block (20) is located on the motion track of the transmission block (18), and the mutually approaching surfaces of the force-bearing block (20) and the transmission block (18) are both designed as inclined surfaces.

10. The Woshi oxide decompression concentration device according to claim 2, characterized in that: The force-bearing block (20) forms a sliding structure through the transmission block (18), and the spring damper (21) forms a telescopic state through the force-bearing block (20).

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