1-adamantanol preparation device

Abstract

The utility model discloses a 1-adamantanol preparation device, which belongs to the technical field of adamantanol preparation equipment, and comprises a reaction tank, an electric heating plate is fixedly connected to the inner wall of the reaction tank, a sealing cover is arranged at a feed port at the edge of the top end of the reaction tank, a motor is fixedly connected to the center of the top end of the reaction tank, and the motor is connected with the electric heating plate. An output shaft of the motor extends to the inner side of the reaction tank and is fixedly connected with a stirring shaft, and the bottom end of the stirring shaft is fixedly connected with stirring blades; according to the utility model, the reciprocating up-down transmission structure is arranged, the stirring blades connected with the transmission shaft are driven by the motor to rotate, and a plurality of components are matched, so that the cam can eject the condensation box, and the spiral distillation pipe moves up and down along with the movement of the condensation box under the action of the sliding seat and the spring; therefore, a product generated during condensation of the inner wall of the spiral distillation pipe can be shaken, the discharging speed of the bottom end of the spiral distillation pipe is greatly increased, and the distillation efficiency and effect are greatly improved.

Description

Technical Field

[0001] The utility model belongs to the technical field of adamantane alcohol preparation equipment, and specifically relates to a 1-adamantanol preparation device. Background Art

[0002] 1-Adamantane alcohol can be purified through a distillation process. Distillation is a commonly used separation technique that uses the difference in boiling points of different substances to separate and purify the components in a mixture. The distillation process of adamantane alcohol can achieve separation based on the difference in its boiling point with the boiling points of other components, and through proper heating and cooling control, adamantane alcohol can be effectively purified.

[0003] The prior art 1-adamantanol preparation device has the following disadvantages during use:

[0004] On the one hand, during the distillation process, a refrigeration structure is used to cool the distillation tube, so that the inner wall of the distillation tube condenses to form adamantane alcohol product. However, the inner wall of the distillation tube will stick to the adamantane alcohol product, resulting in low efficiency and poor effect of distillation preparation.

[0005] Secondly, the opening size of the air inlet at the bottom of the distillation tube is fixed, resulting in a fixed flow rate of the steam generated by heating in the reaction tank entering the distillation tube, which cannot meet the use requirements of different distillation preparations. For this reason, we proposed a 1-adamantanol preparation device. Utility Model Content

[0006] The purpose of the utility model is to provide a 1-adamantanol preparation device to solve the problems raised in the above background technology.

[0007] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a 1-adamantanol preparation device, comprising a reaction tank, the inner wall of the reaction tank is fixedly connected to an electric heating plate, a sealing cover is installed at the feed port at the top edge of the reaction tank, a motor is fixedly connected to the center of the top of the reaction tank, the output shaft of the motor extends to the inner side of the reaction tank and is fixedly connected to a stirring shaft, a stirring blade is fixedly connected to the bottom end of the stirring shaft, a condensing box with a built-in refrigerant is installed on the outer side wall of the reaction tank, a semiconductor refrigeration component is fixedly installed on the side wall of the condensing box away from the reaction tank, and the condensing box A spiral distillation tube is fixed inside the tank, and the top extension of the spiral distillation tube is movably sleeved on the right end outside of the n-type gas outlet pipe. A sealing ring is fixedly connected in the groove provided in the top extension of the spiral distillation tube, and the sealing ring is movably sleeved on the right end outside of the n-type gas outlet pipe. The bottom end of the spiral distillation tube extends to the bottom of the condenser, and the left end of the n-type gas outlet pipe is fixedly penetrated to the inner side of the reaction tank, and an air intake speed adjustment structure is connected to the reaction tank, and the air intake speed adjustment structure can facilitate the adjustment of the speed at which steam enters the spiral distillation tube according to different preparation requirements;

[0008] It also includes a reciprocating up and down transmission structure, which is installed on the reaction tank and connected to the transmission shaft. The reciprocating up and down transmission structure can realize the up and down vibration of the condensation box, so that the liquid condensed on the inner wall of the spiral distillation tube can be quickly discharged.

[0009] As a preferred embodiment, a discharge pipe is fixed at the discharge port at the center of the bottom end of the reaction tank, and an electric valve is installed on the discharge pipe.

[0010] As a preferred embodiment, the air intake speed adjustment structure includes an air intake cylinder fixedly connected to the outer side of the left end extension of the n-type air outlet pipe, the left end of the air intake cylinder is closed, and an L-shaped baffle is movably fitted at the right end opening of the air intake cylinder, the L-shaped baffle is slidably mounted on the outer side of the L-shaped slide rod, and the L-shaped slide rod is fixed to the inner top wall of the reaction tank.

[0011] As a preferred embodiment, a hand screw is threadedly connected to the L-shaped baffle, the top end of the hand screw is rotatably connected to the inner top wall of the reaction tank, and extends to the top of the reaction tank and is fixedly connected to a handle.

[0012] As a preferred embodiment, the reciprocating up and down transmission structure includes a bevel gear a fixedly connected to the outside of the stirring shaft, a bevel gear b is meshedly connected to the bottom of the bevel gear a, and the bevel gear b is fixedly connected to the left end of the connecting shaft. The connecting shaft is rotatably connected to the reaction tank, and the right end of the connecting shaft extends to the outside of the reaction tank and is fixedly connected to a cam, which is movably overlapped with the bottom of the condensation box.

[0013] As a preferred embodiment, a sliding seat with a convex cross-section is fixedly connected to the left side wall of the condensation box, the sliding seat is slidably connected to a sliding groove provided on the connecting seat, the connecting seat is fixed to the outside of the reaction tank, and the top of the sliding seat is connected to the inner top wall of the sliding groove through a spring.

[0014] Compared with the prior art, the 1-adamantanol preparation device provided by the utility model has at least the following beneficial effects:

[0015] (1) By setting the air intake speed adjustment structure, the hand-tightened screw is rotated through the handle, so that the L-shaped baffle moves up or down on the outside of the L-shaped slide rod, so that the size of the right end opening of the air intake cylinder can be adjusted to meet the entry speed of the steam generated by the reaction heating, so that the speed of the steam entering the spiral distillation tube can be adjusted according to different preparation requirements, thereby greatly improving the application range of the 1-adamantanol preparation device;

[0016] (2) By setting up a reciprocating up and down transmission structure, the stirring blade connected to the transmission shaft driven by the motor rotates, and the action of multiple components is coordinated, so that the cam will push the condensation box, thereby cooperating with the action of the sliding seat and the spring, so that the spiral distillation tube moves up and down with the movement of the condensation box, so that the product condensed on the inner wall of the spiral distillation tube can be shaken, which greatly improves the discharge speed of the bottom end of the spiral distillation tube, thereby greatly improving the efficiency and effect of distillation. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 It is a schematic diagram of the overall three-dimensional front side inclined top view structure of the utility model;

[0018] Figure 2 This is a schematic diagram of the planar structure of the reaction tank of the utility model after being cut open;

[0019] Figure 3 It is a schematic diagram of the enlarged structure of point A of the utility model.

[0020] In the figure: 1. reaction tank; 11. discharge pipe; 12. electric heating plate; 2. sealing cover; 3. motor; 31. stirring shaft; 32. stirring blade; 4. condenser; 41. semiconductor refrigeration component; 42. spiral distillation tube; 421. sealing ring; 43. n-type outlet pipe; 5. air intake speed adjustment structure; 51. air intake cylinder; 52. L-shaped baffle; 53. L-shaped slide rod; 54. hand screw; 6. reciprocating up and down transmission structure; 61. bevel gear a; 62. bevel gear b; 63. connecting shaft; 64. cam; 65. sliding seat; 66. connecting seat; 67. spring. DETAILED DESCRIPTION

[0021] The present invention will be further described below in conjunction with the embodiments.

[0022] In order to make the purpose, technical solution and advantages of the embodiments of the present disclosure clearer, the technical solution of the embodiments of the present disclosure will be clearly and completely described below in conjunction with the drawings of the embodiments of the present disclosure. Obviously, the described embodiments are part of the embodiments of the present disclosure, rather than all the embodiments. Based on the described embodiments of the present disclosure, all other embodiments obtained by ordinary technicians in the field without creative work are within the scope of protection of the present disclosure.

[0023] Unless otherwise defined, the technical or scientific terms used in the present disclosure shall have the usual meanings understood by persons with ordinary skills in the field to which the present disclosure belongs. The words "including" or "comprising" and the like used in the present disclosure mean that the elements or objects appearing before the word include the elements or objects listed after the word and their equivalents, without excluding other elements or objects. The words "connect" or "connected" and the like are not limited to physical or mechanical connections, but may also include electrical connections, whether direct or indirect. "Up", "down", "left", "right", etc. are only used to indicate relative position relationships. When the absolute position of the object being described changes, the relative position relationship may also change accordingly.

[0024] Example

[0025] On the one hand, during the distillation process, a refrigeration structure is used to cool the distillation tube, so that the inner wall of the distillation tube condenses to form adamantane alcohol product. However, the inner wall of the distillation tube will stick to the adamantane alcohol product, resulting in low efficiency and poor effect of distillation preparation.

[0026] Secondly, the opening size of the air inlet at the bottom of the distillation tube is fixed, resulting in a fixed flow rate of the steam generated by heating in the reaction tank entering the distillation tube, which cannot meet the use requirements of different distillation preparations.

[0027] To do this, see Figure 1-3 The utility model provides a 1-adamantanol preparation device, comprising: a reaction tank 1, an electric heating plate 12 is fixedly connected to the inner wall of the reaction tank 1, a sealing cover 2 is installed at the feed port at the top edge of the reaction tank 1, a motor 3 is fixedly connected to the center of the top of the reaction tank 1, the output shaft of the motor 3 extends to the inner side of the reaction tank 1 and is fixedly connected to a stirring shaft 31, a stirring blade 32 is fixedly connected to the bottom end of the stirring shaft 31, a condensation box 4 with built-in refrigerant is installed on the outer side wall of the reaction tank 1, a semiconductor refrigeration element 41 is fixedly provided on one side wall of the condensation box 4 away from the reaction tank 1, and a spiral distillation device 32 is fixedly provided inside the condensation box 4. Tube 42, the top extension of the spiral distillation tube 42 is movably sleeved on the right end outside of the n-type outlet pipe 43, a sealing ring 421 is fixedly connected in the groove provided in the top extension of the spiral distillation tube 42, the sealing ring 421 is movably sleeved on the right end outside of the n-type outlet pipe 43, the bottom end of the spiral distillation tube 42 extends to the bottom of the condenser 4, the left end of the n-type outlet pipe 43 is fixedly penetrated to the inner side of the reaction tank 1, and an air intake speed adjustment structure 5 is connected to the reaction tank 1, and the air intake speed adjustment structure 5 can facilitate the adjustment of the speed of steam entering the spiral distillation tube 42 according to different preparation requirements;

[0028] It also includes a reciprocating up and down transmission structure 6, which is installed on the reaction tank 1 and connected to the transmission shaft. The reciprocating up and down transmission structure 6 can realize the up and down vibration of the condensation box 4, so that the liquid condensed on the inner wall of the spiral distillation tube 42 can be quickly discharged.

[0029] The semiconductor refrigeration element 41 can maintain the refrigerant in the condensation tank 4 at a constant temperature, thereby effectively maintaining the condensation effect.

[0030] Further as Figure 1-3 As shown, it is worth explaining in detail that, in order to enable a discharge pipe 11 to be fixed at the discharge port at the center of the bottom end of the reaction tank 1, an electric valve is installed on the discharge pipe 11.

[0031] The distilled solution in the reaction tank 1 can be discharged by starting the electric valve.

[0032] Further as Figure 1-3 As shown, it is worth specifically explaining that, in order to facilitate the adjustment of the speed of steam entering the spiral distillation tube 42 according to different preparation requirements, an air intake speed adjustment structure 5 is provided, including an air intake cylinder 51 fixed to the outside of the left end extension of the n-type air outlet pipe 43, the left end of the air intake cylinder 51 is closed, and an L-shaped baffle 52 is movably fitted at the right end opening of the air intake cylinder 51, the L-shaped baffle 52 is slidably mounted on the outside of the L-shaped slide rod 53, the L-shaped slide rod 53 is fixed to the inner top wall of the reaction tank 1, and a hand screw 54 is threadedly connected to the L-shaped baffle 52, the top end of the hand screw 54 is rotatably connected to the inner top wall of the reaction tank 1, and extends to the top of the reaction tank 1 and is fixed with a handle.

[0033] Among them, after the L-shaped baffle 52 moves down to be blocked by the bottom of the L-shaped sliding rod 53, the right end opening of the air inlet cylinder 51 is expanded to the maximum limit, so that the heated steam can enter the spiral distillation tube 42 at the maximum speed. Conversely, after the top end of the L-shaped baffle 52 is pressed against the top wall of the reaction tank 1, the right end opening of the air inlet cylinder 51 can be closed.

[0034] Further as Figure 1-3As shown, it is worth specifically explaining that in order to enable the condensed product on the inner wall of the spiral distillation tube 42 to be quickly discharged, a reciprocating up and down transmission structure 6 is provided, including a bevel gear a61 fixedly connected to the outside of the stirring shaft 31, and a bevel gear b62 is meshed and connected below the bevel gear a61, and the bevel gear b62 is fixedly connected to the left end outer side of the connecting shaft 63, and the connecting shaft 63 is rotatably connected to the reaction tank 1, and the right end of the connecting shaft 63 extends to the outside of the reaction tank 1 and is fixedly connected to a cam 64, and the cam 64 is movably overlapped on the bottom of the condensation box 4, and a sliding seat 65 with a convex cross-section is fixedly connected to the left side wall of the condensation box 4, and the sliding seat 65 is slidably connected to the sliding groove provided on the connecting seat 66, and the connecting seat 66 is fixed to the outside of the reaction tank 1, and the top of the sliding seat 65 is connected to the inner top wall of the sliding groove through a spring 67.

[0035] Among them, the setting of spring 67 allows the condensing box 4 to rebound better after moving up, so that the condensing box 4 can drive the spiral distillation tube 42 to move up and down. In addition, it can also drive the refrigerant in the condensing box 4 to shake, so that the semiconductor refrigeration component 41 can further maintain the temperature of the refrigerant.

[0036] In summary: when using the 1-adamantanol preparation device, first, open the sealing cover 2, and pour the solution to be distilled into the reaction tank 1, and start the motor 3 and turn on the electric heating plate 12 for heating. In addition, the stirring shaft 31 drives the stirring blade 32 to stir the solution, so that the solution is evenly heated to the specified temperature, and the generated steam enters through the right end opening of the air inlet cylinder 51, and flows into the spiral distillation tube 42, and is condensed by the refrigerant in the condensation box 4, so that the steam condenses on the inner wall of the spiral distillation tube 42 to become liquid and flows to the external receiving container. In addition, the bevel gear a61 drives the bevel gear b62, so that the cam 64 connected to the connecting shaft 63 will push the condensation box 4, so that the spiral distillation tube 42 moves up and down with the movement of the condensation box 4 in cooperation with the sliding seat 65 and the spring 67, so that the product when the inner wall of the spiral distillation tube 42 is condensed can be shaken, which greatly improves the bottom end discharge speed of the spiral distillation tube 42, thereby greatly improving the efficiency and effect of distillation.

Claims

1. A 1-adamantanol preparation device, comprising a reaction tank (1), characterized in that: The inner wall of the reaction tank (1) is fixedly connected to an electric heating plate (12); a sealing cover (2) is installed at the feed port at the top edge of the reaction tank (1); a motor (3) is fixedly connected to the center of the top of the reaction tank (1); an output shaft of the motor (3) extends to the inner side of the reaction tank (1) and is fixedly connected to a stirring shaft (31); a stirring blade (32) is fixedly connected to the bottom end of the stirring shaft (31); a condensing box (4) with built-in refrigerant is installed on the outer wall of the reaction tank (1); a semiconductor refrigeration element (41) is fixedly installed on the side wall of the condensing box (4) away from the reaction tank (1); a spiral distillation tube (42) is fixed inside the condensing box (4); and the spiral distillation tube (42) is fixedly connected to the inner side of the condensing box (4). The top extension of the spiral distillation tube (42) is movably sleeved on the right outer side of the n-type gas outlet pipe (43), a sealing ring (421) is fixedly connected in the groove provided in the top extension of the spiral distillation tube (42), the sealing ring (421) is movably sleeved on the right outer side of the n-type gas outlet pipe (43), the bottom end of the spiral distillation tube (42) extends to the bottom of the condensation box (4), the left end of the n-type gas outlet pipe (43) is fixedly penetrated to the inner side of the reaction tank (1), and an air intake speed adjustment structure (5) is connected to the reaction tank (1), and the air intake speed adjustment structure (5) can be conveniently used to adjust the speed of steam entering the spiral distillation tube (42) according to different preparation requirements; It also includes a reciprocating up and down transmission structure (6), which is installed on the reaction tank (1) and connected to the transmission shaft. The reciprocating up and down transmission structure (6) can realize the up and down vibration of the condensation box (4), so that the liquid condensed on the inner wall of the spiral distillation tube (42) can be quickly discharged.

2. A 1-adamantanol preparation device according to claim 1, characterized in that: A discharge pipe (11) is fixed at the discharge port at the center of the bottom end of the reaction tank (1), and an electric valve is installed on the discharge pipe (11).

3. The 1-adamantanol preparation device according to claim 1, characterized in that: The air intake speed adjustment structure (5) comprises an air intake cylinder (51) fixedly connected to the outer side of the left end extension portion of the n-type air outlet pipe (43); the left end of the air intake cylinder (51) is closed; an L-shaped baffle plate (52) is movably fitted to the right end opening of the air intake cylinder (51); the L-shaped baffle plate (52) is slidably sleeved on the outer side of an L-shaped sliding rod (53); and the L-shaped sliding rod (53) is fixedly connected to the inner top wall of the reaction tank (1).

4. The 1-adamantanol preparation device according to claim 3, characterized in that: The L-shaped baffle (52) is threadedly connected with a hand screw (54), the top end of which is rotatably connected to the inner top wall of the reaction tank (1), and extends to the top of the reaction tank (1) and is fixedly connected with a handle.

5. The 1-adamantanol preparation device according to claim 1, characterized in that: The reciprocating up and down transmission structure (6) comprises a bevel gear a (61) fixedly connected to the outside of the stirring shaft (31); a bevel gear b (62) is meshedly connected to the bottom of the bevel gear a (61); the bevel gear b (62) is fixedly connected to a connecting shaft (63) and the bevel gear b is located on the outside of the left end of the connecting shaft (63); the connecting shaft (63) is rotatably connected to the reaction tank (1); the right end of the connecting shaft (63) extends to the outside of the reaction tank (1) and is fixedly connected to a cam (64); the cam (64) is movably overlapped with the bottom of the condensation box (4).

6. The 1-adamantanol preparation device according to claim 5, characterized in that: A sliding seat (65) having a convex cross-section is fixedly connected to the left side wall of the condensation box (4). The sliding seat (65) is slidably connected to a sliding groove provided on a connecting seat (66). The connecting seat (66) is fixedly connected to the outer side of the reaction tank (1). The top end of the sliding seat (65) is connected to the inner top wall of the sliding groove via a spring (67).

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