Plant decoloring chromatography resin column

Abstract

The utility model discloses a plant decoloring chromatography resin column, which relates to the technical field of plant decoloring equipment and comprises a chromatography column shell, a top cover and a base, the top cover and the base are respectively connected with the top end and the bottom end of the chromatography column shell, and a top chromatography column, at least one middle chromatography column and a bottom chromatography column are sequentially arranged in the chromatography column shell from top to bottom. The top chromatographic column, the middle chromatographic column and the bottom chromatographic column are sequentially connected in an inserted mode from top to bottom, and filter screens are arranged at the bottom ends of the bottom chromatographic column, the top chromatographic column and the middle chromatographic column. The technical problems of unstable decolorizing effect of a chromatographic column on plants, incapability of maximizing decolorizing efficiency and waste of labor cost and material cost of enterprises caused by digging out all macroporous resins when low-position macroporous resins need to be replaced in the prior art are solved.

Description

Technical Field

[0001] The utility model belongs to the technical field of plant decolorization equipment, in particular to a plant decolorization chromatography resin column. Background Art

[0002] The main methods of plant decolorization include macroporous resin adsorption, water extraction and alcohol precipitation, extraction and membrane separation. Among them, macroporous resin adsorption technology has great advantages due to its large adsorption capacity, good selectivity and easy regeneration.

[0003] The adsorption capacity of a chromatography column using macroporous resin as the adsorption material is negatively correlated with the diameter-to-height ratio of the resin column, that is, when the diameter of the chromatography column remains unchanged, the higher the macroporous resin chromatography column is, the stronger the adsorption capacity of the chromatography column using the macroporous resin as the adsorption material is. Therefore, in order to improve the adsorption capacity of the chromatography column, and thus improve the ability of the chromatography column to decolorize plants, it is usually necessary to make the resin column as high as possible.

[0004] However, when the overall setting of the resin column in the chromatography column is relatively high, firstly, the macroporous resin cannot be filled evenly, resulting in unstable plant decolorization efficiency; secondly, the macroporous resin at a high position will exert tremendous pressure on the macroporous resin at a low position, causing damage or agglomeration of the macroporous resin at the low position, thereby resulting in the inability to maximize the decolorization efficiency of the chromatography column; finally, when the macroporous resin at a low position needs to be replaced, all the macroporous resins need to be dug out before the macroporous resin at the low position can be replaced, thus wasting the intact macroporous resin at a high position and causing a waste of labor and material costs for the enterprise. Utility Model Content

[0005] The purpose of the utility model is to provide a plant decolorization chromatography resin column, so as to overcome the technical problems in the prior art that the overall height of the chromatography column resin column leads to unstable decolorization effect of the chromatography column on plants, the decolorization efficiency cannot be maximized, and when the low-position macroporous resin needs to be replaced, all the macroporous resin needs to be dug out, resulting in a waste of labor costs and material costs for the enterprise. The specific technical solution is as follows:

[0006] A plant decolorization chromatography resin column, comprising a chromatography column shell, a top cover covering the top end of the chromatography column shell, and a base connected to the bottom end of the chromatography column shell;

[0007] The chromatography column housing is provided with a bottom chromatography column, a top chromatography column and at least one middle chromatography column;

[0008] The bottom chromatography column is arranged at one end of the chromatography column housing close to the base, and a first annular protrusion is arranged at one end away from the base. The top chromatography column is arranged at one end of the chromatography column housing close to the top cover, and a first annular groove is arranged at one end away from the top cover. The middle chromatography column is provided with a second annular groove matched with the first annular protrusion at one end close to the bottom chromatography column, and a second annular protrusion matched with the first annular groove is arranged at one end close to the top chromatography column, and the second annular protrusion is matched with the second annular groove.

[0009] The top chromatography column, at least one of the middle chromatography columns and the bottom chromatography column are sequentially plugged in through the first annular groove, the second annular protrusion, the second annular groove and the first annular protrusion;

[0010] The bottom chromatography column, the top chromatography column and the middle chromatography column are each provided with a filter screen at one end close to the base;

[0011] The bottom end of the top cover is located inside the chromatography column housing and abuts against the top chromatography column 5 .

[0012] Preferably, two opposite sides of the chromatography column housing are provided with slide grooves, and two opposite sides of the bottom chromatography column, the top chromatography column and at least one of the middle chromatography columns are provided with sliders;

[0013] The bottom chromatography column, the top chromatography column and the middle chromatography column are all slidably sleeved inside the chromatography column housing through the sliding block and the sliding groove.

[0014] Preferably, sealing rings are provided in both the first annular groove and the second annular groove.

[0015] Preferably, the first annular protrusion, the second annular protrusion and the top of the top chromatography column are provided with lifting ears on two opposite sides, and the first annular groove and the second annular groove are provided with lifting ear grooves matched with the lifting ears on two opposite sides.

[0016] Preferably, the first end of the top cover is hinged to the first side of the top end of the chromatography column housing, and the second end of the top cover is connected to the second side of the top end of the chromatography column housing via a spring buckle assembly;

[0017] The spring buckle assembly includes a first buckling base, a second buckling base, a buckling rod and two elastic members. The first buckling base is fixedly installed on the second end of the top cover, and its bottom end is set as an arc-shaped end. The second buckling base is fixedly connected to the top of the chromatography column shell. One end of each of the two elastic members is hinged to the two sides of the second buckling base at the same horizontal height, and the other end of each is connected to the two ends of the buckling rod respectively. The second side of the top of the chromatography column shell is buckled with the second end of the top cover through the buckling rod and the first buckling base.

[0018] Preferably, the elastic member is a tension spring.

[0019] Preferably, an anti-overflow component is further provided at one end of the chromatography column housing close to the top cover, and the anti-overflow component includes a float, a connecting rod, an insulating slide, an electrode, a power supply, a warning light and a buzzer;

[0020] The float is arranged in the top chromatography column, the insulating slide is vertically arranged on the inner side of the chromatography column shell, one end of the connecting rod is connected to the float, and the other end is connected to a metal slider slidably connected to the insulating slide, the electrode is arranged at one end of the insulating slide close to the top cover, the other end of the electrode, the warning light, the buzzer and one end of the power supply are connected in series in sequence, and the other end of the power supply is connected to the metal slider.

[0021] Preferably, a splash-proof assembly is provided at the bottom end of the top cover, and the splash-proof assembly includes a perforated plate and a conical guide plate;

[0022] The perforated plate is connected to the bottom end of the top cover and is provided with a plurality of guide holes;

[0023] The conical guide plate is arranged at one end of the porous plate close to the top chromatography column, and the end with a larger diameter is connected to the porous plate.

[0024] Preferably, the filter screen is a quartz sand filter screen.

[0025] Preferably, an ultrasonic transmitter is also provided on the inner side of the chromatography column housing at one end of the top chromatography column.

[0026] Compared with the existing technology, the utility model has the following beneficial effects:

[0027] The utility model provides a plant decolorization chromatography resin column, which arranges a top cover and a base at the top and bottom of a chromatography column shell respectively, arranges a bottom chromatography column, a top chromatography column and at least one middle chromatography column in the chromatography column shell, and arranges a filter screen at one end of each of the bottom chromatography column, the top chromatography column and the middle chromatography column close to the base, so as to divide a higher chromatography column as a whole into several chromatography columns, thereby solving the technical problems in the prior art that the overall height of the resin column in the chromatography column is too high, resulting in unstable decolorization effect of the chromatography column on plants, the decolorization efficiency cannot be maximized, and when it is necessary to replace the low-position macroporous resin, all the macroporous resins need to be dug out, resulting in waste of labor costs and material costs for the enterprise. BRIEF DESCRIPTION OF THE DRAWINGS

[0028] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following briefly introduces the drawings required for describing the embodiments. In all drawings, similar elements or parts are generally identified by similar reference numerals. In the drawings, the elements or parts are not necessarily drawn according to the actual scale.

[0029] Figure 1 It is a structural schematic diagram of the utility model.

[0030] Figure 2 yes Figure 1 A is a partial enlarged schematic diagram of the middle part.

[0031] Figure 3 yes Figure 1 A partial enlarged schematic diagram of B in the figure.

[0032] Figure 4 It is a structural schematic diagram of the anti-sputtering component in the utility model.

[0033] Figure 5 It is a circuit structure diagram of the anti-overflow component in the utility model.

[0034] Description of main reference numerals:

[0035] 1-chromatography column housing, 2-top cover, 3-base, 4-bottom chromatography column, 5-top chromatography column, 6-middle chromatography column, 7-first annular protrusion, 8-first annular groove, 9-second annular protrusion, 10-filter screen, 11-chute, 12-slider, 13-lifting ear, 14-first buckling base, 15-second buckling base, 16-buckle rod, 17-elastic member, 18-floating ball, 19-connecting rod, 20-insulating chute, 21-electrode, 22-power supply, 23-warning light, 24-buzzer, 25-perforated plate, 26-conical guide plate, 27-guide hole, 28-ultrasonic transmitter. DETAILED DESCRIPTION

[0036] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0037] In the description of the present invention, it should be noted that the terms "center", "longitudinal", "lateral", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "top", "bottom", "top surface", "bottom surface", "inside", "outside", "inside", "outside" and the like indicate orientations or positional relationships based on the orientations or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the referred device or element must have a specific orientation, be constructed and operated in a specific orientation, and therefore cannot be understood as a limitation on the present invention.

[0038] In the description of the present utility model, "several" means one or more, "more" means more than two, "greater than", "less than", "exceed" etc. are understood to exclude the number itself, and "above", "below", "within" etc. are understood to include the number itself. If the terms "first", "second", "third" are described, they are only used for the purpose of description and distinguishing technical features, and cannot be understood as indicating or implying relative importance or implicitly indicating the number of the indicated technical features or implicitly indicating the order of the indicated technical features.

[0039] In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installed", "connected", "connected", and "set" should be understood in a broad sense. For example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal connection of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances. The following is a description of the embodiments of the present invention based on its overall structure.

[0040] Example

[0041] like Figures 1 to 5 As shown, an embodiment of the present application provides a plant decolorization chromatography resin column, comprising a chromatography column housing 1, a top cover 2 covering the top end of the chromatography column housing 1, and a base 3 connected to the bottom end of the chromatography column housing 1.

[0042] The first end of the top cover 2 is hinged to the first side of the top end of the chromatography column housing 1, and the second end of the top cover 2 is connected to the second side of the top end of the chromatography column housing 1 through a spring buckle assembly. Figure 1 As shown, the left side of the top cover 2 is the first end, and the right side is the second section, the left side of the top end of the chromatography column housing 1 is the first side, and the right side is the second side, the spring buckle assembly includes a first buckle base 14, a second buckle base 15, a buckle rod 16 and two elastic members 17, the first buckle base 14 is fixedly installed on the second end of the top cover 2, and its bottom end is set as an arc end, the second buckle base 15 is fixedly connected to the top of the chromatography column housing 1, one end of each of the two elastic members 17 is respectively hinged to the two sides of the second buckle base 15 located at the same horizontal height, and the other end of each is respectively connected to the two ends of the buckle rod 16, the second side of the top end of the chromatography column housing 1 is buckled with the second end of the top cover 2 through the buckle rod 16 and the first buckle base 14, a liquid inlet pipe is provided in the middle of the top cover 2, a liquid outlet pipe is provided in the middle of the base 1, and valves are provided on the liquid inlet pipe and the liquid outlet pipe.

[0043] Wherein, the elastic member 17 is a tension spring.

[0044] The chromatography column housing 1 is provided with a bottom chromatography column 4, a top chromatography column 5 and at least one middle chromatography column 6. The bottom chromatography column 4 is arranged at one end of the chromatography column housing 1 close to the base 3, the top chromatography column 5 is arranged at one end of the chromatography column housing 1 close to the top cover 2, and the middle chromatography column 6 is placed between the bottom chromatography column 4 and the top chromatography column 5. When the top cover 2 is covered directly above the chromatography column housing 1, the bottom end of the top cover 2 is located in the chromatography column housing 1 and abuts against the top chromatography column 5. The bottom chromatography column 4, the top chromatography column 5 and the middle chromatography column 6 are each provided with a filter screen 10 at one end close to the base 3.

[0045] Specifically, slide grooves 11 are provided on two opposite sides of the chromatography column housing 1, and sliders 12 are provided on two opposite sides of the outer side of the bottom chromatography column 4, two opposite sides of the outer side of the top chromatography column 5, and two opposite sides of the outer side of all the middle chromatography columns 6. The bottom chromatography column 4, the top chromatography column 5, and the middle chromatography column 6 are all slidably mounted inside the chromatography column housing 1 through the sliders 12 and the slide grooves 11.

[0046] Among them, the bottom chromatography column 4, the top chromatography column 5 and the middle chromatography column 6 are all filled with macroporous resin, the macroporous resin in each chromatography column is located above each filter 10, and the thickness of the corresponding macroporous resin layer of the chromatography column is less than the height of the chromatography column. In order to prevent the filter 10 from being corroded by the solution during long-term use, the filter 10 is a quartz sand filter.

[0047] The bottom chromatography column 4 is provided with a first annular protrusion 7 at one end away from the base 3, the top chromatography column 5 is provided with a first annular groove 8 at one end away from the top cover 2, the middle chromatography column 6 is provided with a second annular groove matching the first annular protrusion 7 at one end close to the bottom chromatography column 4, and a second annular protrusion 9 matching the first groove is provided at one end close to the top chromatography column 5, and the second annular protrusion 9 and the second annular groove are also matched, so the top chromatography column 5, at least one of the middle chromatography columns 6 and the bottom chromatography column 4 are sequentially plugged in through the first annular groove 8, the second annular protrusion 9, the second annular groove and the first annular protrusion 7.

[0048] Specifically, in order to improve the sealing between the bottom chromatography column 4 and the middle chromatography column 6, between the connected middle chromatography columns 6, and between the middle chromatography column 6 and the top chromatography column 5, sealing rings are provided in the first annular groove 8 and the second annular groove.

[0049] In some embodiments, in order to improve the disassembly and replacement of the bottom chromatography column 4, the top chromatography column 5 and the middle chromatography column 6, lifting ears 13 are provided on the first annular protrusion 7, the second annular protrusion 9 and the top of the top chromatography column 5 on opposite sides, and the first annular groove 8 and the second annular groove are provided with lifting ear grooves matched with the lifting ears 13 on opposite sides. When the bottom chromatography column 4, the top chromatography column 5 and the middle chromatography column 6 need to be disassembled or replaced, the bottom chromatography column 4, the top chromatography column 5 and the middle chromatography column 6 can be quickly and conveniently taken out by hooking the lifting ear 13 with the help of a long hook. It should be noted that when the lifting ear grooves are provided in the first annular groove 8 and the second annular groove, the sealing rings still exist in the first annular groove 8 and the second annular groove, and at this time the sealing rings are still in contact with the first annular groove 8 and the second annular groove.

[0050] In some embodiments, because the chromatography column is usually made of stainless steel in industrial production, the liquid level inside cannot be seen. In order to prevent the sample liquid and eluent from overflowing due to excessive speed of adding, an anti-overflow component is further provided at one end of the chromatography column housing 1 close to the top cover 2. The anti-overflow component includes a float 18, a connecting rod 19, an insulating chute 20, an electrode 21, a power supply 22, a warning light 23 and a buzzer 24. The float 18 is arranged in the top chromatography column 5, and the insulating chute 20 is vertically arranged on the inner side of the chromatography column housing 1. One end of the connecting rod 19 is connected to the float 18, and the other end is connected to a metal slider slidably connected to the insulating chute 20. The electrode 21 is arranged at one end of the insulating chute 20 close to the top cover 2. The other end of the electrode 21, the warning light 23, the buzzer 24 and one end of the power supply 22 are connected in series in sequence, and the other end of the power supply 22 is connected to the metal slider.

[0051] Among them, the float 18 is arranged in the top chromatography column 5. When the liquid level in the top chromatography column 5 is too high, the float 18 drives the connecting rod 19 to rise, so that the metal slider rises and contacts the electrode 21, so that the circuit of the anti-overflow component is turned on. At this time, the power supply 22 supplies power to the warning light 23 and the buzzer 24, the warning light 23 lights up, and the buzzer 24 makes a sound. The staff can adjust or close the valve on the liquid inlet pipe according to the above prompts to prevent the sample liquid or eluent from overflowing.

[0052] Since the sample liquid and the eluent are at a certain height from the macroporous resin in the top chromatography column 5 when they flow out from the outlet of the liquid inlet pipe, the sample liquid or the eluent will impact the macroporous resin in the top chromatography column 5, causing splashing, and at the same time, the shape of the resin column in the chromatography column is also destroyed, thereby affecting the efficiency of the chromatography column in decolorizing plants. In some embodiments, the bottom end of the top cover 2 is provided with an anti-splashing component, and the anti-splashing component includes a perforated plate 25 and a conical guide plate 26;

[0053] The perforated plate 25 is connected to the bottom end of the top cover 2 and is provided with a plurality of guide holes 27;

[0054] The conical guide plate 26 is disposed at one end of the perforated plate 25 close to the top chromatography column 5 , and the end with a larger diameter is connected to the perforated plate 25 .

[0055] In summary, the embodiments of the present application respectively arrange the top cover and the base at the top and the bottom of the chromatography column housing, arrange a bottom chromatography column, a top chromatography column and at least one middle chromatography column in the chromatography column housing, and arrange a filter screen at one end of the bottom chromatography column, the top chromatography column and the middle chromatography column close to the base, so as to divide a higher chromatography column as a whole into several chromatography columns. This solves the technical problems in the prior art that the decolorization effect of the chromatography column on plants is unstable and the decolorization efficiency cannot be maximized because the resin column in the chromatography column is too high as a whole, and when the low-level macroporous resin needs to be replaced, all the macroporous resins need to be dug out, resulting in a waste of labor costs and material costs for the enterprise.

[0056] The foregoing descriptions of specific exemplary embodiments of the present invention are for the purpose of explanation and illustration. These descriptions are not intended to limit the present invention to the precise form disclosed, and it is obvious that many changes and variations can be made based on the above teachings. Although an embodiment of the present invention has been shown and described, this specific embodiment is merely an explanation of the present invention and is not a limitation of the present invention. The specific features, structures, materials or characteristics described may be combined in a suitable manner in any one or more embodiments or examples. The purpose of selecting and describing the exemplary embodiments is to explain the specific principles of the present invention and its practical application, so that those skilled in the art can make modifications, substitutions, variations and various selections and changes to the embodiments without creative contribution as needed after reading this specification without departing from the principles and purpose of the present invention, but they are protected by patent law as long as they are within the scope of the claims of the present invention.

Claims

1. A plant decolorization chromatography resin column, characterized in that: It comprises a chromatography column housing (1), a top cover (2) covering the top end of the chromatography column housing (1), and a base (3) connected to the bottom end of the chromatography column housing (1); The chromatography column housing (1) is provided with a bottom chromatography column (4), a top chromatography column (5) and at least one middle chromatography column (6); The bottom chromatography column (4) is arranged at one end of the chromatography column housing (1) close to the base (3), and a first annular protrusion (7) is arranged at one end of the top chromatography column housing (1) close to the top cover (2), and a first annular groove (8) is arranged at one end of the top chromatography column housing (1) close to the top cover (2), and a second annular groove (7) is arranged at one end of the middle chromatography column (6) close to the bottom chromatography column (4), and a second annular protrusion (9) is arranged at one end of the middle chromatography column (6) close to the top chromatography column (5), and the second annular protrusion (9) is arranged to fit the second annular groove; The top chromatography column (5), at least one of the middle chromatography columns (6) and the bottom chromatography column (4) are sequentially plugged in through the first annular groove (8), the second annular protrusion (9), the second annular groove and the first annular protrusion (7); The bottom chromatography column (4), the top chromatography column (5) and the middle chromatography column (6) are each provided with a filter screen (10) at one end close to the base (3); The bottom end of the top cover (2) is located inside the chromatography column housing (1) and abuts against the top chromatography column (5).

2. A plant decolorization chromatography resin column according to claim 1, characterized in that, The two opposite sides of the chromatography column housing (1) are provided with slide grooves (11), and the two opposite sides of the bottom chromatography column (4), the top chromatography column (5) and at least one of the middle chromatography columns (6) are provided with sliders (12); The bottom chromatography column (4), the top chromatography column (5) and the middle chromatography column (6) are all slidably mounted inside the chromatography column housing (1) via the slider (12) and the slide groove (11).

3. A plant decolorization chromatography resin column according to claim 1, characterized in that, Sealing rings are arranged in both the first annular groove (8) and the second annular groove.

4. A plant decolorization chromatography resin column according to claim 1, characterized in that, Lifting ears (13) are provided on the first annular protrusion (7), the second annular protrusion (9) and the top of the top chromatography column (5) on opposite sides, and lifting ear grooves matching the lifting ears (13) are provided on the first annular groove (8) and the second annular groove on opposite sides.

5. A plant decolorization chromatography resin column according to claim 1, characterized in that, The first end of the top cover (2) is hinged to the first side of the top end of the chromatography column housing (1), and the second end of the top cover (2) is connected to the second side of the top end of the chromatography column housing (1) via a spring buckle assembly; The spring buckle assembly comprises a first buckle base (14), a second buckle base (15), a buckle rod (16) and two elastic members (17); the first buckle base (14) is fixedly mounted on the second end of the top cover (2), and its bottom end is set as an arc-shaped end; the second buckle base (15) is fixedly connected to the top of the chromatography column housing (1); one end of each of the two elastic members (17) is hinged to two sides of the second buckle base (15) at the same horizontal height, and the other end of each is connected to two ends of the buckle rod (16); the second side of the top of the chromatography column housing (1) is buckled and connected to the second end of the top cover (2) through the buckle rod (16) and the first buckle base (14).

6. A plant decolorization chromatography resin column according to claim 5, characterized in that: The elastic member (17) is a tension spring.

7. A plant decolorization chromatography resin column according to claim 1, characterized in that, An anti-overflow component is also provided at one end of the chromatography column housing (1) close to the top cover (2), and the anti-overflow component comprises a floating ball (18), a connecting rod (19), an insulating slide groove (20), an electrode (21), a power supply (22), a warning light (23) and a buzzer (24); The float (18) is arranged in the top chromatography column (5), the insulating slide groove (20) is vertically arranged on the inner side of the chromatography column shell (1), one end of the connecting rod (19) is connected to the float (18), and the other end is connected to a metal slider slidably connected to the insulating slide groove (20), the electrode (21) is arranged at one end of the insulating slide groove (20) close to the top cover (2), the other end of the electrode (21), the warning light (23), the buzzer (24) and one end of the power supply (22) are connected in series in sequence, and the other end of the power supply (22) is connected to the metal slider.

8. A plant decolorization chromatography resin column according to claim 1, characterized in that, The bottom end of the top cover (2) is provided with an anti-splashing assembly, and the anti-splashing assembly comprises a perforated plate (25) and a conical guide plate (26); The perforated plate (25) is connected to the bottom end of the top cover (2) and is provided with a plurality of guide holes (27); The conical guide plate (26) is arranged at one end of the porous plate (25) close to the top chromatography column (5), and the end with a larger diameter is connected to the porous plate (25).

9. A plant decolorization chromatography resin column according to claim 1, characterized in that, The filter screen (10) is a quartz sand filter screen.

10. A plant decolorization chromatography resin column according to claim 1, characterized in that: An ultrasonic transmitter (28) is also provided on the inner side of the chromatography column housing (1) located at one end of the top chromatography column (5).

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