Freezing-out device for menthol crystallization

By designing a freeze-analysis device with a synchronous rotating storage barrel and a separation partition, the problem of uneven temperature in the freeze-analysis device is solved, and uniform cooling of the menthol solution and efficient freeze-analysis crystallization are achieved.

CN222585606UActive Publication Date: 2025-03-11ANHUI HUAXIN BIO-PHARM CO LTD
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Patent Information

Application Number
CN202420478136.2
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-03-13
Publication Date
2025-03-11
Estimated Expiration
2034-03-13

AI Technical Summary

Technical Problem

The refrigerant action position and area inside the freeze-analysis device are fixed, resulting in uneven temperatures, resulting in different cooling time and efficiency of menthol solution during freeze-analysis and crystallization, resulting in a long freeze-analysis and crystallization time and low working efficiency.

Method used

A freeze-analysis device for menthol crystallization is designed, including a protective outer shell and a cooler. The cooler is installed on the inner wall of the protective outer shell, and the inner space of the two inner grooves is connected. A telescopic machine and a separation partition plate are installed at the bottom of the storage barrel. The driving shaft drives the storage barrel to rotate simultaneously to ensure that the cooling air is uniformly received at different angles.

Benefits of technology

By controlling the separation partition plate and drive shaft, uniform cooling of the menthol solution is achieved, the cooling time difference in different areas is reduced, the freeze-excitation crystallization time is reduced, and the working efficiency is improved.

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Abstract

The utility model belongs to the technical field of freeze-out devices, in particular to a freeze-out device for menthol crystallization, which comprises a protective outer shell and a cooler, the cooler is mounted on the inner wall of the protective outer shell, two inner grooves are formed in the protective outer shell, the inner spaces of the two inner grooves are communicated, and the inner grooves are communicated with the protective outer shell. Two top feeding ports corresponding to the inner grooves are formed in the top end of the protective outer shell, the top end of the protective outer shell is connected with a blocking top cover used for blocking the two top feeding ports in a clamped mode, and the inner walls of the two inner grooves are each rotationally connected with a storage barrel used for storing menthol. The two driving shafts are controlled to drive the two storage barrels to rotate synchronously, so that the areas, at different angle positions, of the storage barrels can uniformly receive cold air output by the cooling machine, the temperature uniformity of the different positions of the storage barrels is improved, and the ear canal menthol solution in the storage barrels can be cooled more uniformly and stably.
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Description

Technical Field

[0001] The utility model belongs to the technical field of freeze-out devices, and in particular relates to a freeze-out device for menthol crystallization. Background Art

[0002] Menthol is an organic substance with the chemical properties of colorless needle-shaped crystals and a refreshing mint aroma. It is soluble in organic solvents such as ethanol, acetone, ether, chloroform and benzene, and slightly soluble in water. It is chemically stable and can evaporate with steam. Menthol is produced in the leaves and is the main component of peppermint oil. The freeze-out method is a method based on the difference in freezing points between different components in the mint flavor mixture. It solidifies and precipitates high-melting-point substances by cooling them down and separates them from other liquid components.

[0003] During freeze-out, the menthol crystallization needs to be left to stand for a period of time so that the impurities and water in the solution can be precipitated, and the upper clear liquid is taken for freeze-out, which is a relatively troublesome operation and requires a new carrying space; and the temperature inside the space is lowered by a freeze-out crystallization device so that the placed menthol solution can be cooled and freeze-out, but the refrigerant action position and action area inside the freeze-out device are fixed, so that the temperature inside the freeze-out space is prone to form a step difference, and the temperature of different areas of the static menthol solution is different, which requires different cooling time and efficiency in different areas when the menthol solution is freeze-out crystallized, and it is necessary to wait for the menthol solution in the area with slow cooling rate to freeze-out crystallize before completing this step, so that the required freeze-out crystallization time is longer, resulting in low freeze-out crystallization efficiency. Utility Model Content

[0004] The utility model provides a freeze-out device for menthol crystallization, which has the characteristics of improving the uniformity and working efficiency of freeze-out of menthol solution crystallization.

[0005] The utility model provides the following technical scheme: it comprises a protective outer shell and a cooling machine, the cooling machine is installed on the inner wall of the protective outer shell, two inner grooves are arranged in the protective outer shell, the internal spaces of the two inner grooves are communicated, the top of the protective outer shell is arranged with two top feeding ports corresponding to the inner grooves, the top of the protective outer shell is snap-connected with a blocking top cover for blocking the two top feeding ports, the inner walls of the two inner grooves are rotatably connected with a storage barrel for storing menthol, the cooling machine is located between the two storage barrels, the inner walls of the bottom ends of the two storage barrels are both installed with telescopic machines, the output ends of the two telescopic machines are both fixedly connected with a separation partition for dividing the internal space of the storage barrel, the inner wall of the protective outer shell is rotatably connected with two driving shafts for driving the storage barrels, the two driving shafts are both fixedly connected to the corresponding bottom ends of the storage barrels, the bottom ends of the two driving shafts are both fixedly connected with transmission shafts, a synchronous rotating transmission belt is arranged between the two transmission shafts, and the two transmission shafts are rotatably connected through the synchronous rotating transmission belt.

[0006] Wherein, a sealing gasket is fixedly connected to the bottom end of the sealing top cover, and the sealing gasket is clamped between the sealing top cover and the protective outer shell.

[0007] Among them, the inner walls of the two inner grooves are fixedly connected with a plurality of airflow guide plates for guiding the output airflow of the cooler, the positions of the plurality of airflow guide plates are evenly distributed, and the plurality of airflow guide plates are used to prevent contact with the storage barrel.

[0008] Wherein, an inner cavity is opened in the separation partition, and a plurality of liquid circulation holes are opened on the separation partition, and the inner cavity is connected with the inner space of the storage barrel through the plurality of liquid circulation holes.

[0009] The inner wall of the inner cavity is rotatably connected to a rotating disk, the side wall of the rotating disk is fixedly connected to a plurality of rotating blocking plates for blocking the liquid flow holes, and the rotating blocking plates are rotatably connected to the inner wall of the inner cavity.

[0010] Among them, the bottom ends of the two storage barrels are rotatably connected with a plurality of resistance reducing balls, and the plurality of resistance reducing balls are slidably connected to the inner wall of the inner groove.

[0011] The beneficial effects of the utility model are as follows: by controlling the separation partition to open or block the upper and lower layers of liquid in the storage barrel, the clear liquid of the menthol solution is stored separately, and the clear liquid of the menthol solution can be freeze-out treated without taking out the clear liquid of the menthol solution separately, which is simple to operate and improves efficiency; by controlling the two driving shafts to drive the two storage barrels to rotate synchronously, the areas at different angles of the storage barrels can evenly receive the cold air output by the cooler, thereby increasing the temperature uniformity at different positions of the storage barrels, and thus enabling the ear canal menthol solution in the storage barrel to achieve more uniform and stable cooling treatment, reducing the difference in cooling time and efficiency of different areas when the menthol solution is freeze-out crystallized, thereby reducing the required freeze-out crystallization time and improving the work efficiency of freeze-out crystallization.

[0012] The parts not involved in the device are the same as those in the prior art or can be implemented by using the prior art. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0014] Figure 2 It is a front view cross-sectional structural schematic diagram of the utility model;

[0015] Figure 3 It is a three-dimensional cross-sectional structural schematic diagram of the utility model;

[0016] Figure 4 It is a schematic diagram of the cross-sectional structure of the utility model in a top view;

[0017] Figure 5 for Figure 2 Schematic diagram of the enlarged structure of part A in the middle.

[0018] In the figure: 1. protective outer shell; 11. cooler; 12. inner tank; 121. top feed inlet; 13. sealing top cover; 131. sealing gasket; 14. air flow guide plate; 2. storage barrel; 21. telescopic machine; 22. separation partition; 221. inner cavity; 23. liquid flow hole; 24. rotating disk; 241. rotating sealing plate; 25. resistance reducing ball; 3. driving shaft; 31. transmission shaft; 32. synchronous rotating transmission belt. DETAILED DESCRIPTION

[0019] See also Figure 1-Figure 5The utility model provides the following technical solutions: comprising a protective outer shell 1 and a cooling machine 11, the cooling machine 11 is installed on the inner wall of the protective outer shell 1, two inner grooves 12 are provided in the protective outer shell 1, the inner spaces of the two inner grooves 12 are connected, the top of the protective outer shell 1 is provided with two top feed ports 121 corresponding to the inner grooves 12, the top of the protective outer shell 1 is snap-connected with a blocking top cover 13 for blocking the two top feed ports 121, the inner walls of the two inner grooves 12 are rotatably connected with a storage barrel 2 for storing menthol, and the cooling machine 11 is located between the two Between the storage barrels 2, telescopic machines 21 are installed on the inner walls of the bottom ends of the two storage barrels 2, and the output ends of the two telescopic machines 21 are fixedly connected to the separation partitions 22 for dividing the internal space of the storage barrel 2. The inner wall of the protective outer shell 1 is rotatably connected to two driving shafts 3 for driving the storage barrel 2. The two driving shafts 3 are fixedly connected to the bottom ends of the corresponding storage barrels 2, and the bottom ends of the two driving shafts 3 are fixedly connected to transmission shafts 31. A synchronously rotating transmission belt 32 is arranged between the two transmission shafts 31, and the two transmission shafts 31 are rotatably connected through the synchronously rotating transmission belt 32.

[0020] In this embodiment, the protective outer shell 1 supports and protects the components of the device from the outside. The protective outer shell 1 forms a connected cavity through two inner grooves 12. The blocking top cover 13 blocks the top of the internal cavity of the protective outer shell 1 to prevent the external air from exchanging with the internal air of the protective outer shell 1 when the device is in use. The size of the top feed port 121 corresponds to the inner diameter of the storage barrel 2. The storage barrel 2 carries the menthol solution. The menthol solution is put into the storage barrel 2 through the top feed port 121. The storage barrel 2 supports the telescopic machine 21, and the telescopic machine 21 separates the partition 2. 2 is supported and driven. When the separation partition 22 is opened, the menthol solution stored in the storage barrel 2 can flow in series. After the menthol solution in the storage barrel 2 is left to stand and stratify, the separation partition 22 is closed to achieve sealing of the separation partition 22 to separate the internal space of the storage barrel 2, so that the menthol solution above the separation partition 22 is the clear liquid, and the impurities and water below the separation partition 22 are, and the menthol solution can be frozen out without taking out the clear liquid separately. The inner tank 12 gives way to the storage barrel 2. The storage barrel 2 is designed to rotate inside the inner tank 12. The protective outer shell 1 is provided with For the driving element driven by one of the transmission shafts 31, when the transmission shaft 31 rotates, the other transmission shaft 31 is driven to rotate through the synchronously rotating transmission belt 32, so that the two transmission shafts 31 can realize synchronous rotation, and the two transmission shafts 31 drive the two storage barrels 2 to realize synchronous rotation. When the storage barrel 2 rotates, the menthol solution clear liquid inside is driven to rotate, and the cooling machine 11 is controlled to output cold air. The cold air output by the cooling machine 11 acts on the two storage barrels 2. The storage barrel 2 is made of a material with good thermal conductivity. The storage barrel 2 transfers the cold air temperature to the menthol solution inside, so that the menthol solution The menthol solution is driven to rotate by the two storage barrels 2 so that different angular positions of the storage barrel 2 can correspond to the cooler 11 alternately, so that the areas at different angular positions of the storage barrel 2 can evenly receive the cold air output by the cooler 11, thereby increasing the temperature uniformity at different positions of the storage barrel 2, and thus enabling the menthol solution in the ear canal of the storage barrel 2 to achieve a more uniform and stable cooling treatment, so that the difference in cooling time and efficiency in different areas when the menthol solution is freeze-thawed and crystallized is reduced, thereby reducing the required freeze-thaw crystallization time and improving the freeze-thaw crystallization work efficiency.

[0021] A sealing gasket 131 is fixedly connected to the bottom end of the sealing top cover 13, and the sealing gasket 131 is clamped between the sealing top cover 13 and the protective outer shell 1; when the sealing top cover 13 is connected to the top end of the protective outer shell 1, the sealing top cover 13 drives the sealing gasket 131 to contact the top end of the protective outer shell 1, and the sealing gasket 131 increases the sealing between the protective outer shell 1 and the sealing top cover 13, thereby reducing the loss of cold air inside the protective outer shell 1.

[0022] A plurality of airflow guide plates 14 for guiding the airflow output by the cooler 11 are fixedly connected to the inner walls of the two inner grooves 12. The plurality of airflow guide plates 14 are evenly distributed, and the plurality of airflow guide plates 14 are used to prevent contact with the storage barrel 2. The cross-sections of the plurality of airflow guide plates 14 are all triangular. When the cold airflow output by the cooler 11 diffuses and flows into the inner groove 12, the cold airflow is affected by the airflow guide plates 14 and changes direction, thereby increasing the effect of the cold airflow on the storage barrel 2, thereby improving the efficiency of the storage barrel 2 in driving the menthol solution to cool down, and the airflow guide plates 14 will not interfere with the rotation of the storage barrel 2.

[0023] An inner cavity 221 is provided in the separation baffle 22, and a plurality of liquid flow holes 23 are provided on the separation baffle 22. The inner cavity 221 is connected with the inner space of the storage barrel 2 through the plurality of liquid flow holes 23. The storage barrel 2 realizes the ability of the upper and lower liquids of the separation baffle 22 to intersect and flow through the plurality of liquid flow holes 23. The solution passes through the liquid flow holes 23 into the inner cavity 221, and then the solution is discharged through the inner cavity 221, thereby realizing the static stratification of the solution inside the storage barrel 2.

[0024] The inner wall of the inner cavity 221 is rotatably connected to a rotating disk 24, and a plurality of rotating sealing plates 241 for sealing the liquid flow holes 23 are fixedly connected to the side walls of the rotating disk 24, and the rotating sealing plates 241 are rotatably connected to the inner wall of the inner cavity 221; the rotating sealing plates 241 are used to seal the separation baffle 22, and the rotating disk 24 supports and drives the plurality of rotating sealing plates 241. The inner wall of the telescopic machine 21 is provided with a driving element for acting on the rotating disk 24, so that the rotating disk 24 can drive the rotating sealing plates 241 to rotate. When the solution is allowed to stand and stratify, the rotating disk 24 is controlled to drive the plurality of rotating sealing plates 241 to rotate to seal the plurality of liquid flow holes 23, so that the separation baffle 22 can separate the upper and lower layers of solution inside the storage barrel 2 to prevent impurities and moisture from flowing upward.

[0025] The bottom ends of the two storage barrels 2 are rotatably connected to a plurality of resistance reducing balls 25, and the plurality of resistance reducing balls 25 are slidably connected to the inner wall of the inner groove 12; when the storage barrel 2 rotates, the plurality of resistance reducing balls 25 are driven to rotate, and the plurality of resistance reducing balls 25 reduce the sliding friction and friction damage between the storage barrel 2 and the inner wall of the inner groove 12, thereby facilitating the rotation of the storage barrel 2.

[0026] The working principle and use process of the utility model are as follows: when the menthol solution is subjected to freeze-out crystallization treatment, the blocking top cover 13 is controlled to slide upward and separate from the protective outer shell 1, and then the menthol solution is put into the storage barrel 2, and then the blocking top cover 13 is closed. After the stratification of the solution inside the storage barrel 2 is completed, the two rotating disks 24 are controlled to rotate, and the rotating disks 24 drive the corresponding rotating blocking plates 241 to rotate, and the rotating blocking plates 241 rotate to block the liquid flow holes 23, so that the separation partition 22 can separate the upper and lower layer solutions inside the storage barrel 2 to prevent impurities and moisture from flowing upward, and the menthol solution clear liquid can be frozen out without taking out the menthol solution separately, and then the cooling machine 11 is controlled to output cold air, and the cold air output by the cooling machine 11 acts on the two storage barrels 2, and the storage barrel 2 transmits the cold air temperature to the menthol solution inside, so that the menthol solution can be frozen out. The alcohol solution is cooled and frozen, and then the transmission shaft 31 is controlled to rotate. When the transmission shaft 31 rotates, the synchronously rotating transmission belt 32 drives another transmission shaft 31 to rotate, so that the two transmission shafts 31 can achieve synchronous rotation, and the two transmission shafts 31 drive the two storage barrels 2 to achieve synchronous rotation. When the storage barrel 2 rotates, the menthol solution clear liquid inside is driven to rotate, so that different angular positions of the storage barrel 2 can alternately correspond to the cooling machine 11, so that the areas at different angular positions of the storage barrel 2 can evenly receive the cold air output by the cooling machine 11, thereby increasing the temperature uniformity of different positions of the storage barrel 2, and thereby enabling the ear canal menthol solution in the storage barrel 2 to achieve more uniform and stable cooling treatment, so that the difference in cooling time and efficiency in different areas when the thin alcohol solution is frozen and crystallized is reduced, thereby reducing the required freezing and crystallization time and improving the working efficiency of freezing and crystallization.

Claims

1. A freeze-out device for crystallizing menthol, comprising a protective outer shell (1) and a cooler (11), characterized in that: The cooling machine (11) is installed on the inner wall of the protective outer shell (1). Two inner grooves (12) are provided in the protective outer shell (1). The internal spaces of the two inner grooves (12) are connected. The top of the protective outer shell (1) is provided with two top material inlets (121) corresponding to the inner grooves (12). The top of the protective outer shell (1) is snap-connected with a blocking top cover (13) for blocking the two top material inlets (121). The inner walls of the two inner grooves (12) are rotatably connected with a storage barrel (2) for storing menthol. The cooling machine (11) is located between the two storage barrels (2). The two storage barrels (2 ) are installed with telescopic machines (21) on the inner wall of the bottom end, and the output ends of the two telescopic machines (21) are fixedly connected to a separation partition (22) for separating the internal space of the storage barrel (2), and the inner wall of the protective outer shell (1) is rotatably connected to two driving shafts (3) for driving the storage barrel (2), and the two driving shafts (3) are fixedly connected to the bottom ends of the corresponding storage barrels (2), and the bottom ends of the two driving shafts (3) are fixedly connected to a transmission shaft (31), and a synchronously rotating transmission belt (32) is arranged between the two transmission shafts (31), and the two transmission shafts (31) are rotatably connected through the synchronously rotating transmission belt (32).

2. A freeze-out device for menthol crystallization according to claim 1, characterized in that: A sealing gasket (131) is fixedly connected to the bottom end of the blocking top cover (13), and the sealing gasket (131) is clamped between the blocking top cover (13) and the protective outer shell (1).

3. A freeze-out device for menthol crystallization according to claim 1, characterized in that: The inner walls of the two inner grooves (12) are fixedly connected with a plurality of airflow guide plates (14) for guiding the airflow output by the cooler (11); the plurality of airflow guide plates (14) are evenly distributed in position; and the plurality of airflow guide plates (14) are used to prevent contact with the storage barrel (2).

4. A freeze-out device for menthol crystallization according to claim 1, characterized in that: An inner cavity (221) is provided in the separation baffle (22), and a plurality of liquid circulation holes (23) are provided on the separation baffle (22). The inner cavity (221) is connected to the inner space of the storage barrel (2) through the plurality of liquid circulation holes (23).

5. A freeze-out device for menthol crystallization according to claim 4, characterized in that: The inner wall of the inner cavity (221) is rotatably connected to a rotating disk (24), and the side wall of the rotating disk (24) is fixedly connected to a plurality of rotating blocking plates (241) for blocking the liquid flow hole (23), and the rotating blocking plates (241) are rotatably connected to the inner wall of the inner cavity (221).

6. A freeze-out device for menthol crystallization according to claim 1, characterized in that: The bottom ends of the two storage barrels (2) are rotatably connected to a plurality of resistance-reducing balls (25), and the plurality of resistance-reducing balls (25) are slidably connected to the inner wall of the inner groove (12).