A chenodeoxycholic acid bile paste mother liquor extraction circulation device

Abstract

The utility model discloses a chenodeoxycholic acid bile paste mother liquor extraction circulation device, which comprises: a protective frame is fixedly connected to the upper surface of a bottom plate, a mother liquor separation box is arranged inside the protective frame, a concentration box is arranged inside the protective frame, a delivery pipeline is arranged between the mother liquor separation box and the concentration box, and delivery channels are arranged at both ends of the delivery pipeline; a fixed plate is detachably connected to the upper surface of the mother liquor separation box, a sealing cover is detachably connected inside the fixed plate, a fixed block is fixedly connected to the upper surface of the sealing cover, a connecting plate is fixedly connected to the upper surface of the fixed plate, a sealing plate is detachably connected to the upper surface of the concentration box, a fixing screw is spirally connected inside the sealing plate, and an extraction device is fixedly connected to the upper surface of the fixed plate. Through the above structure, the mother liquor is thoroughly extracted and moderately concentrated, the quality of the obtained mother liquor is guaranteed, and the device can be ensured to have high sealing performance and avoid the interference of external impurities.

Description

Technical Field

[0001] The utility model relates to the technical field of extraction devices, in particular to a chenodeoxycholic acid bile paste mother liquor extraction circulation device. Background Art

[0002] Chenodeoxycholic acid bile paste mother liquor is a mixed solution extracted from chenodeoxycholic acid during the production process. Chenodeoxycholic acid is an important bile acid with multiple medicinal and medical uses. Chenodeoxycholic acid bile paste mother liquor is an intermediate product in the extraction process. Therefore, the mother liquor needs to be extracted and concentrated to ensure the stability of the mother liquor quality. However, the stability and safety of the traditional extraction device during operation are poor, and it is easily affected by external air impurities. The sealing performance of the device during operation is poor, and it is easy to leak or intrusion of external impurities. For example, the Chinese patent discloses "A bile acid concentration device", whose application number is "CN201620269403.0", includes: a concentration tank, a condenser and a liquid collecting tank. A jacket is provided on the outer side of the concentration tank. The steam outlet of the concentration tank located on one side of the top of the concentration tank is divided into two paths through a pipeline after passing through a vacuum pump, one path is connected to the jacket medium inlet, and the other path is connected to the feed port of the condenser. The jacket medium outlet is also connected to the feed port of the condenser through a pipeline, and the discharge port of the condenser is connected to the feed port of the liquid collecting tank through a pipeline via a condensate delivery pump. Utility Model Content

[0003] The utility model aims to solve at least one of the technical problems existing in the prior art, and provides a chenodeoxycholic acid bile paste mother liquor extraction circulation device, wherein the extraction device is fixed by a sealing round cover, a sealing ring and a support rod, and the support rod is fixed by a fixing plate, and the mother liquor is processed by the extraction device, the mother liquor separation box and the concentration box, so that the mother liquor is extracted, separated and concentrated layer by layer, so as to ensure that the mother liquor can be stably obtained and the quality of the mother liquor is ensured, so that the mother liquor extraction device can stably perform the extraction work, and the extraction device has a high sealing and supporting stability function, which can effectively ensure that the extraction work is free from external influences, and the mother liquor separation box and the extraction device are safely protected by a protective frame, and the concentration box and the mother liquor separation box are respectively sealed in combination with the sealing plate and the sealing cover fixed by fixing screws, the fixing plate and the fixing block, and the extraction device, the mother liquor separation box and the concentration box are directly connected through the conveying channel and the rubber conveying pipe, so that the mother liquor extraction device is highly sealed, so that the device can effectively reduce the probability of external impurities and air invading the device, so that the external impurities and air can avoid the advantages of affecting the internal separation, recovery and concentration work.

[0004] The utility model also provides a chenodeoxycholic acid bile paste mother liquor extraction circulation device, comprising: a bottom plate, a protective frame is fixedly connected to the upper surface of the bottom plate, a mother liquor separation box is arranged inside the protective frame, a concentration box is arranged inside the protective frame, a delivery pipeline is arranged between the mother liquor separation box and the concentration box, and delivery channels are arranged at both ends of the delivery pipeline; a fixed plate is detachably connected to the upper surface of the mother liquor separation box, a sealing cover is detachably connected to the inner part of the fixed plate, a fixed block is fixedly connected to the upper surface of the sealing cover, a connecting plate is fixedly connected to the upper surface of the fixed plate, a sealing plate is detachably connected to the upper surface of the concentration box, a fixing screw is spirally connected to the inner part of the sealing plate, the fixing screw is detachably connected to the concentration box, and an extraction device is fixedly connected to the upper surface of the fixed plate. Through the above device, the mother liquor is thoroughly extracted and moderately concentrated, so that the quality of the obtained mother liquor is guaranteed, and the device can be ensured to have high sealing performance and avoid the intrusion and interference of external impurities.

[0005] According to the utility model, a chenodeoxycholic acid bile paste mother liquor extraction circulation device is provided, a sealing ring is fixedly connected to the side surface of the extraction device, a support rod is fixedly connected to the lower surface of the sealing ring, and the support rod is detachably connected to the fixed plate. Through the above device, auxiliary sealing is achieved, and the extraction device is supported and fixed.

[0006] According to the utility model, a chenodeoxycholic acid bile paste mother liquor extraction circulation device is composed of an extraction tank, a rubber delivery tube and a sealing round cover, and the extraction tank is located between the rubber delivery tube and the sealing round cover. Through the above device, the internal components of the extraction device are clear and stable, which can effectively ensure the stability of the extraction work.

[0007] According to the chenodeoxycholic acid bile paste mother liquor extraction circulation device described in the utility model, a sealing ring is provided on the side surface of the rubber delivery tube, and a connecting block is provided on the side surface of the sealing ring. Through the above device, the effect of stably controlling the switch of the rubber delivery tube is achieved.

[0008] According to the chenodeoxycholic acid bile paste mother liquor extraction circulation device described in the utility model, a connecting column is arranged inside the connecting block, and a sealing block is arranged on the side surface of the connecting block. Through the above device, the advantage of stably controlling the tightening and loosening of the sealing ring is achieved.

[0009] According to the chenodeoxycholic acid bile paste mother liquor extraction circulation device described in the utility model, the conveying channels are respectively located inside the mother liquor separation box and the concentration box, and a suction pump is provided inside the conveying channel. Through the above device, the effect of stably conveying the mother liquor after various types of work are completed is achieved.

[0010] According to the chenodeoxycholic acid bile paste mother liquor extraction circulation device described in the utility model, a solvent recovery box is arranged inside the mother liquor separation box, and an evaporation tank is arranged inside the solvent recovery box. Through the above device, the advantage of recycling the waste liquid generated by the mother liquor separation work is achieved.

[0011] According to the utility model, a chenodeoxycholic acid bile paste mother liquor extraction circulation device is provided inside the concentration box, a concentration device is provided on both sides of the concentration device, a heating device and a cooling device are provided respectively, a battery is provided between the heating device and the cooling device, and a protective shell is provided on the outer surface of the battery. Through the above device, the concentration device can safely and stably concentrate the mother liquor, thereby improving the quality of the mother liquor.

[0012] Beneficial Effects

[0013] 1. Compared with the prior art, the chenodeoxycholic acid bile paste mother liquor extraction circulation device fixes the extraction device through a sealing round cover, a sealing ring and a support rod, and fixes the support rod through a fixing plate, and processes the mother liquor through the extraction device, the mother liquor separation box and the concentration box, thereby realizing the extraction, separation and concentration of the mother liquor in a progressive layer-by-layer manner, thereby ensuring that the mother liquor can be stably obtained and the quality of the mother liquor is guaranteed, so that the mother liquor extraction device can stably perform the extraction work, and the extraction device has a high sealing and supporting stability function, which can effectively ensure that the extraction work is protected from external influences.

[0014] 2. Compared with the prior art, the chenodeoxycholic acid bile paste mother liquor extraction circulation device provides safety protection for the mother liquor separation box and the extraction device through a protective frame, and seals the concentration box and the mother liquor separation box respectively in combination with a sealing plate and a sealing cover fixed by fixing screws in combination with a fixing plate and a fixing block, and directly connects the extraction device, the mother liquor separation box and the concentration box through a conveying channel and a rubber conveying tube, thereby achieving a high seal for the mother liquor extraction device, enabling the device to effectively reduce the probability of external impurities and air invading the device, thereby preventing external impurities and air from affecting the internal separation, recovery and concentration work. BRIEF DESCRIPTION OF THE DRAWINGS

[0015] The utility model is further described below in conjunction with the accompanying drawings and embodiments;

[0016] Figure 1 This is the overall structure diagram of the chenodeoxycholic acid bile paste mother liquor extraction circulation device of the utility model;

[0017] Figure 2 It is a side structural diagram of the chenodeoxycholic acid bile paste mother liquor extraction circulation device of the utility model;

[0018] Figure 3It is a right side cross-sectional view of the chenodeoxycholic acid bile paste mother liquor extraction circulation device of the utility model;

[0019] Figure 4 It is a left side cross-sectional view of the chenodeoxycholic acid bile paste mother liquor extraction circulation device of the utility model.

[0020] Legend:

[0021] 1. Bottom plate; 2. Protection frame; 3. Mother liquor separation box; 4. Fixed plate; 5. Sealing cover; 6. Fixed block; 7. Delivery pipeline; 8. Support rod; 9. Connecting block; 10. Connecting column; 11. Concentration box; 12. Sealing plate; 13. Fixing screws; 14. Delivery channel; 15. Sealing block; 16. Sealing ring; 17. Rubber delivery tube; 18. Extraction tank; 19. Sealing round cover; 20. Sealing ring. DETAILED DESCRIPTION

[0022] This section will describe in detail the specific embodiments of the utility model. The preferred embodiments of the utility model are shown in the accompanying drawings. The purpose of the accompanying drawings is to supplement the description of the text part of the specification with graphics, so that people can intuitively and vividly understand each technical feature and the overall technical solution of the utility model, but it cannot be understood as a limitation on the protection scope of the utility model.

[0023] Reference Figure 1-4 The utility model embodiment is a chenodeoxycholic acid bile paste mother liquor extraction circulation device, which includes: a bottom plate 1, which is used for horizontal support of the bottom of the device as a whole; a protective frame 2 is fixedly connected to the upper surface of the bottom plate 1, which has the function of protecting the internal components of the device; a mother liquor separation box 3 is arranged inside the protective frame 2, which is used for secondary separation of the extracted mother liquor; a solvent recovery box is arranged inside the mother liquor separation box 3, which is used for recovering the waste liquid of the extraction separation; an evaporation tank is arranged inside the solvent recovery box, which is used for evaporating and recovering the collected waste liquid; a concentration box 11 is arranged inside the protective frame 2, which is used for concentrating the mother liquor after separation and recovery; a concentration device is arranged inside the concentration box 11, which is used for concentrating the mother liquor, thereby improving the quality; a heating device and a cooling device are respectively arranged on both sides of the concentration device, which are used to control the temperature inside the concentration box 11.

[0024] A battery is arranged between the heating device and the cooling device to provide energy for the heating device and the cooling device. A protective shell is arranged on the outer surface of the battery to protect the battery. A conveying pipe 7 is arranged between the mother liquor separation box 3 and the concentration box 11 to convey the mother liquor. Conveying channels 14 are arranged at both ends of the conveying pipe 7 to input or output the mother liquor. The conveying channels 14 are respectively located inside the mother liquor separation box 3 and the concentration box 11. The conveying channels 14 are limited and fixed. A suction pump is arranged inside the conveying channel 14 to absorb and deliver the mother liquor.

[0025] The upper surface of the mother liquor separation box 3 is detachably connected with a fixing plate 4 for limiting and fixing the support rod 8 and the sealing cover 5. The interior of the fixing plate 4 is detachably connected with a sealing cover 5 for sealing the mother liquor separation box 3. The upper surface of the sealing cover 5 is fixedly connected with a fixing block 6 for reinforcing the sealing cover 5. The upper surface of the fixing plate 4 is fixedly connected with a connecting plate for connecting with the fixing block 6, thereby enhancing the fixation effect.

[0026] A sealing plate 12 is detachably connected to the upper surface of the concentration box 11 for sealing the concentration box 11. A fixing screw 13 is spirally connected inside the sealing plate 12 for reinforcing the sealing plate 12. The fixing screw 13 is detachably connected to the concentration box 11. An extraction device is fixedly connected to the upper surface of the fixing plate 4 for extracting the mother liquor.

[0027] A sealing ring 20 is fixedly connected to the side surface of the extraction device for auxiliary sealing of the extraction device. A support rod 8 is fixedly connected to the lower surface of the sealing ring 20 for supporting and fixing the extraction device. The support rod 8 is detachably connected to the fixing plate 4 to limit and fix the support rod 8. The extraction device consists of an extraction tank 18, a rubber delivery tube 17 and a sealing round cover 19 to limit the components of the extraction device. The extraction tank 18 is located between the rubber delivery tube 17 and the sealing round cover 19 to fix the position of the extraction tank 18.

[0028] A sealing ring 16 is provided on the side surface of the rubber delivery tube 17 for performing switch control on the rubber delivery tube 17. A connecting block 9 is provided on the side surface of the sealing ring 16 for performing switch control on the sealing ring 16. A connecting column 10 is provided inside the connecting block 9 for controlling the movement of the connecting block 9. A sealing block 15 is provided on the side surface of the connecting block 9 for sealing the sealing ring 16, thereby ensuring that the sealing ring 16 can stably perform switch control.

[0029] Working principle: During use, the extraction device is opened through the sealing round cover 19, and the mother liquor is added into the extraction device, and the sealing round cover 19 is closed, so that the mother liquor is extracted by the extraction tank 18. After extraction, the mother liquor is sent to the mother liquor separation box 3 through the rubber delivery tube 17 for separation, and the separated waste liquid is recycled and processed, and then the mother liquor and the treated waste liquid are sent to the concentration box 11 through the delivery channel 14 and the delivery pipeline 7 for concentration, and then the concentration work is carried out through the concentration equipment inside the concentration box 11, and the temperature during concentration is controlled in combination with the heating equipment and the cooling equipment. After the concentration is completed, the mother liquor is taken away, the work is completed, the bottom plate 1 and the protective frame 2 are installed to support and protect the separation and concentration work, the fixing plate 4, the sealing cover 5, the fixing screws 13 and the sealing plate 12 are installed to seal the separation work and the concentration work, and then the support rod 8 is installed and combined with the sealing ring 20 to fix and seal the extraction device.

[0030] The embodiments of the present invention are described in detail above in conjunction with the accompanying drawings, but the present invention is not limited to the above embodiments, and various changes can be made within the knowledge scope of ordinary technicians in the relevant technical field without departing from the purpose of the present invention.

Claims

1. A chenodeoxycholic acid bile paste mother liquor extraction circulation device, characterized in that: include: A bottom plate (1), the upper surface of the bottom plate (1) being fixedly connected to a protection frame (2), a mother liquor separation box (3) being arranged inside the protection frame (2), a concentration box (11) being arranged inside the protection frame (2), a conveying pipeline (7) being arranged between the mother liquor separation box (3) and the concentration box (11), and conveying channels (14) being arranged at both ends of the conveying pipeline (7); The upper surface of the mother liquor separation box (3) is detachably connected to a fixing plate (4), the interior of the fixing plate (4) is detachably connected to a sealing cover (5), the upper surface of the sealing cover (5) is fixedly connected to a fixing block (6), the upper surface of the fixing plate (4) is fixedly connected to a connecting plate, the upper surface of the concentration box (11) is detachably connected to a sealing plate (12), the interior of the sealing plate (12) is spirally connected to a fixing screw (13), the fixing screw (13) is detachably connected to the concentration box (11), and the upper surface of the fixing plate (4) is fixedly connected to an extraction device.

2. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 1, characterized in that: A sealing ring (20) is fixedly connected to the side surface of the extraction device, a support rod (8) is fixedly connected to the lower surface of the sealing ring (20), and the support rod (8) is detachably connected to the fixing plate (4).

3. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 1, characterized in that: The extraction device is composed of an extraction tank (18), a rubber delivery tube (17) and a sealing round cover (19), wherein the extraction tank (18) is located between the rubber delivery tube (17) and the sealing round cover (19).

4. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 3, characterized in that: A sealing ring (16) is provided on the side surface of the rubber delivery tube (17), and a connecting block (9) is provided on the side surface of the sealing ring (16).

5. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 4, characterized in that: A connecting column (10) is arranged inside the connecting block (9), and a sealing block (15) is arranged on the side surface of the connecting block (9).

6. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 1, characterized in that: The delivery channel (14) is located inside the mother liquid separation box (3) and the concentration box (11) respectively, and a suction pump is arranged inside the delivery channel (14).

7. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 1, characterized in that: The mother liquid separation box (3) is provided with a solvent recovery box inside, and the solvent recovery box is provided with an evaporation tank inside.

8. The chenodeoxycholic acid bile paste mother liquor extraction circulation device according to claim 1, characterized in that: A concentration device is arranged inside the concentration box (11), a heating device and a cooling device are arranged on both sides of the concentration device, a battery is arranged between the heating device and the cooling device, and a protective shell is arranged on the outer surface of the battery.

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