A high-purity palladium chloride electrolysis device

Abstract

The utility model discloses a high-purity palladium chloride electrolysis device, which relates to the technical field of palladium chloride. The device comprises a machine body and a switch, wherein a push rod is arranged inside the machine body, and the push rod is connected with a slider, and the slider is arranged on a first slider, and the slider is connected with a support rod above, and the support rod is connected with a first clamping rod and a connecting rod through a hinge shaft. The device is provided with an electrolysis structure, and the push rod electric slider is started by the switch to move on the first slider, so that the slider drives the support rod above to drive the first clamping rod and the connecting rod through the hinge shaft, and the connecting rod drives the second clamping rod through the hinge shaft, so that the first clamping rod and the second clamping rod move toward the middle at the same time to fix a metal sheet, so that the metal sheets are fixed on both sides, and at this time, the electric clamps on both sides clamp the top of the metal sheet, and at this time, the electric clamps are powered by electric wires through the switch, and since the metal sheets on both sides correspond to the positive electrode and the negative electrode respectively, the internal palladium chloride is electrolyzed at this time.

Description

Technical Field

[0001] The utility model relates to the technical field of palladium chloride, in particular to a high-purity palladium chloride electrolysis device. Background Art

[0002] Palladium chloride, also known as palladium dichloride, palladium chloride, is deliquescent, easily soluble in dilute hydrochloric acid, stable in air, and soluble in water, ethanol, acetone and hydrobromic acid. It is used to prepare special catalysts and molecular sieves. Its dihydrate is a dark red hygroscopic crystal that can be used to prepare non-conductive material coatings; to make gas sensors, analytical reagents, etc. The existing devices still have some defects; for example;

[0003] For example, a palladium electrolysis device with a publication number of CN206768239U, when used, comprises a first tank body for accommodating electrolyte; a conductive plate, which is installed on the two side walls of the electrolytic tank; an anode plate and a cathode plate installed in the electrolytic tank and electrically connected to the conductive plate, wherein a gap is reserved between the bottom end surfaces of the anode plate and the cathode plate and the bottom of the first tank body to facilitate the flow of the electrolyte; a guide rod, which is vertically installed on the top end surface of the electrolytic tank; a substrate arranged on the guide rod through a slider, and the top end surface of the substrate A cylinder is installed, and the cylinder body of the cylinder is fixedly arranged on the frame; a linear slide is installed on the bottom end surface of the base plate; a scraper unit is installed on the linear slide; a shell sleeve is sleeved on the outer wall of the electrolytic cell; wherein, a terminal connected to an external power supply is formed on one end surface of the conductive plate, the shell sleeve is a hollow structure with a hollow cavity, and a second opening is formed on the shell sleeve for the convenience of the terminal to extend out, and the shell sleeve is also provided with an air inlet end and an air outlet end so that the hollow cavity is connected to the outside, and the air inlet end is connected to an air conditioning device through a pipeline. When adjusting the temperature, the air conditioning device is turned on so that the air conditioning device produces a gas with a constant temperature, and the gas with a constant temperature enters the hollow cavity of the shell sleeve through the air inlet end, and the hollow cavity is covered by the outer ring of the electrolytic cell, so that the constant gas in the hollow cavity can have a temperature-adjusting effect on the electrolyte in the electrolytic cell, so that the electrolyte is always kept at a suitable temperature, which is convenient for the electrolysis operation, and the air outlet end is used to discharge the gas in the hollow cavity;

[0004] The above device has some problems. The device is cumbersome to use, and cannot better mix palladium and electrolyte before electrolysis. In addition, the internal temperature is adjusted by constant temperature gas, which makes it too inefficient to use.

[0005] Therefore we have proposed a high-purity palladium chloride electrolysis device to solve the above-mentioned problems. Utility Model Content

[0006] The utility model aims to provide a high-purity palladium chloride electrolysis device to solve the problems of poor electrolysis effect and low electrolysis efficiency of the high-purity palladium chloride electrolysis device on the market mentioned in the background technology.

[0007] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a high-purity palladium chloride electrolysis device, comprising a body and a switch;

[0008] A push rod is arranged inside the machine body, and the push rod is connected to a slider, and the slider is arranged on a first slider, and the slider is connected to a support rod above the slider, and the support rod is connected to a first clamping rod and a connecting rod through a hinge shaft, and the connecting rod is connected to a second clamping rod, the first clamping rod and the second clamping rod are fixed to the metal sheet, and an electric clamp is arranged on the metal sheet, and the electric clamp is connected to the machine body through an electric wire;

[0009] A motor is arranged inside the machine body, and the motor is connected to a rotating rod, and a stirring rod is arranged on the surface of the rotating rod, a temperature controller is arranged in the stirring rod, and a temperature detector is arranged inside the machine body.

[0010] As a preferred technical solution of the present utility model, the bottom of the body is provided with support legs, and the support legs are connected to the bottom of the body through hinge shafts, and the support legs are symmetrically arranged about the center of the bottom of the body.

[0011] As a preferred technical solution of the utility model, the first slide bar is symmetrically arranged about the center of the body, and a first clamping rod and a second clamping rod are arranged above the first slide bar, and metal sheets are fixed on the first clamping rod and the second clamping rod.

[0012] As a preferred technical solution of the utility model, the metal sheets are provided with electric clamps, and the electric clamps are connected to the positive electrode and the negative electrode inside the body through electric wires respectively.

[0013] As a preferred technical solution of the utility model, a gear is arranged inside the body, and the gear is meshed with a rack, and the rack is arranged on the second sliding rod, and a baffle is arranged at the front end of the rack.

[0014] As a preferred technical solution of the utility model, a discharge port is arranged at the lower right side of the machine body, a filter screen and a rotating shaft are arranged in the discharge port, and a rotating plate is arranged on the surface of the rotating shaft.

[0015] As a preferred technical solution of the present utility model, an observation window is arranged on the surface of the body, and the observation window is arranged at the center of the surface of the body, and the material of the observation window is transparent glass material.

[0016] Compared with the prior art, the beneficial effects of the utility model are:

[0017] 1. The device is provided with an electrolysis structure. The push rod electric slider is started by a switch to move on the first slide rod, so that the slider drives the upper support rod to drive the first clamping rod and the connecting rod through the hinge shaft, and the connecting rod drives the second clamping rod through the hinge shaft, so that the first clamping rod and the second clamping rod move toward the middle at the same time to fix the metal sheet, so that the metal sheet is fixed on both sides. At this time, the electric clamps on both sides clamp the upper part of the metal sheet. At this time, the electric clamps are powered by the switch through the wire. Since the metal sheets on both sides correspond to the positive electrode and the negative electrode respectively, the internal palladium chloride is electrolyzed at this time;

[0018] 2. The device is provided with a structure for increasing electrolysis efficiency. High-purity palladium chloride is added into the body, and then the electrolyte is added into the body again. The motor is started by the switch to drive the rotating rod to rotate, so that the multiple stirring rods on the surface of the rotating rod rotate to make the electrolyte and palladium chloride mixed better. At the same time, during the electrolysis process, the temperature controller in the stirring rod is started to heat the electrolyte mixed with palladium chloride inside, and the internal temperature is detected by the internal temperature detector, so that the electrolysis effect is better. BRIEF DESCRIPTION OF THE DRAWINGS

[0019] Figure 1 It is a schematic diagram of the main cross-sectional structure of the utility model;

[0020] Figure 2 This is a schematic diagram of the main structure of the utility model;

[0021] Figure 3 This is a schematic diagram of the baffle structure of the utility model;

[0022] Figure 4 This is a schematic diagram of the first clamping rod structure of the utility model;

[0023] Figure 5 This is a schematic diagram of the electric clamp structure of the utility model

[0024] Figure 6 It is a schematic diagram of the three-dimensional structure of the machine body of the utility model.

[0025] In the figure: 1. body; 2. switch; 3. push rod; 4. first slide bar; 5. slider; 6. support rod; 7. first clamping rod; 8. connecting rod; 9. second clamping rod; 10. metal sheet; 11. electric clamp; 12. motor; 13. rotating rod; 14. stirring rod; 15. temperature controller; 16. temperature detector; 17. gear; 18. rack; 19. second slide bar; 20. baffle; 21. filter; 22. rotating shaft; 23. rotating plate. DETAILED DESCRIPTION

[0026] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all of the embodiments.

[0027] See also Figure 1-6 The utility model provides a technical solution: a high-purity palladium chloride electrolysis device, including a body 1 and a switch 2, an observation window is arranged on the surface of the body 1, and the observation window is arranged at the center of the surface of the body 1, and the material of the observation window is transparent glass material, a support leg is arranged at the bottom of the body 1, and the support leg is connected to the bottom of the body 1 through a hinge shaft, and the support leg is symmetrically arranged about the center of the bottom of the body 1, a gear 17 is arranged inside the body 1, and the gear 17 is meshed with a rack 18, and the rack 18 is arranged on a second slide bar 19, and a baffle 20 is arranged at the front end of the rack 18, a discharge port is arranged at the lower right side of the body 1, and a filter screen 21 and a rotating shaft 22 are arranged in the discharge port, and a rotating plate 23 is arranged on the surface of the rotating shaft 22, and a A push rod 3, and the push rod 3 is connected to a slider 5, and the slider 5 is arranged on a first slide rod 4, the first slide rod 4 is symmetrically arranged about the center of the body 1, and a first clamping rod 7 and a second clamping rod 9 are arranged above the first slide rod 4, and a metal sheet 10 is fixed on the first clamping rod 7 and the second clamping rod 9, and an electric clamp 11 is arranged on the metal sheet 10, and the electric clamp 11 is respectively connected to the positive and negative electrodes inside the body 1 through electric wires, the slider 5 is connected to the support rod 6 above, and the support rod 6 is connected to the first clamping rod 7 and the connecting rod 8 through a hinge axis, and the connecting rod 8 is connected to the second clamping rod 9, the first clamping rod 7 and the second clamping rod 9 fix the metal sheet 10, and the metal sheet 10 is provided with an electric clamp 11, and the electric clamp 11 is connected to the body 1 through electric wires;

[0028] First, after moving the machine body 1 to the designated position, the multiple support legs at the bottom of the machine body 1 are opened through the hinge axis, and the machine body 1 is fixed through the support legs. At this time, the metal sheet 10 is taken out, and at the same time, the push rod 3 is started through the switch 2 to move the electric slider 5 on the first slide bar 4, so that the slider 5 drives the upper support rod 6 to drive the first clamping rod 7 and the connecting rod 8 through the hinge axis, and at the same time, the connecting rod 8 drives the second clamping rod 9 through the hinge axis, so that the first clamping rod 7 and the second clamping rod 9 move toward the middle at the same time to fix the metal sheet 10, so that the metal sheet 10 is fixed on both sides. At this time, the electric clamps 11 on both sides clamp the upper part of the metal sheet 10. The switch 2 supplies power to the electric clamp 11 through the wire. Since the metal sheets 10 on both sides correspond to the positive electrode and the negative electrode respectively, the palladium chloride inside is electrolyzed at this time. At this time, the gear 17 is started to rotate by the switch 2. Since the gear 17 and the rack 18 are meshed, the rack 18 moves on the second slide bar 19 and drives the baffle 20 to move upward, so that the remaining electrolyte after electrolysis enters the discharge port on the right side of the body 1. At the same time, the internal filter 21 is filtered to prevent the palladium chloride that has not been electrolyzed from flowing out. At the same time, the internal rotating shaft 22 rotates, driving the multiple rotating plates 23 on the surface to rotate, so that the discharge effect of the electrolyte is better;

[0029] A motor 12 is arranged inside the machine body 1, and the motor 12 is connected to a rotating rod 13, and a stirring rod 14 is arranged on the surface of the rotating rod 13, a temperature controller 15 is arranged in the stirring rod 14, and a temperature detector 16 is arranged inside the machine body 1;

[0030] At this time, high-purity palladium chloride is added into the body 1, and then the electrolyte is added into the body 1 again. The motor 12 is started by the switch 2 to drive the rotating rod 13 to rotate, so that the multiple stirring rods 14 on the surface of the rotating rod 13 rotate to make the electrolyte and palladium chloride mix better. At the same time, the temperature controller 15 in the stirring rod 14 is started to heat the electrolyte mixed with palladium chloride inside, and the internal temperature is detected by the internal temperature detector 16 to make the electrolysis effect better.

[0031] Working principle: When using the high-purity palladium chloride electrolysis device, first move the body 1 to the specified position, open the multiple support legs at the bottom of the body 1 through the hinge shaft, and fix the body 1 through the support legs. At this time, add high-purity palladium chloride into the body 1. At this time, add the electrolyte into the body 1 again, start the motor 12 through the switch 2 to drive the rotating rod 13 to rotate, so that the multiple stirring rods 14 on the surface of the rotating rod 13 rotate to make the electrolyte and palladium chloride mix better. At this time, take out the metal sheet 10, and at the same time, start the push rod 3 through the switch 2 to move the electric slider 5 on the first slide bar 4, so that the slider 5 drives the upper support rod 6 to drive the first clamping rod 7 and the connecting rod 8 through the hinge shaft, and at the same time, the connecting rod 8 drives the second clamping rod 9 through the hinge shaft, so that the first clamping rod 7 and the second clamping rod 9 move to the middle at the same time to fix the metal sheet 10, so that the metal sheet 10 is fixed on both sides, and at this time, the electric clamps 11 on both sides are pressed against the top of the metal sheet 10. The metal sheets 10 on both sides correspond to the positive electrode and the negative electrode respectively, and the palladium chloride inside is electrolyzed at this time. At the same time, the temperature controller 15 in the stirring rod 14 is started to heat the electrolyte mixed with palladium chloride inside. At the same time, the internal temperature detector 16 is used to detect the internal temperature, so that the electrolysis effect is better. After the electrolysis is completed, the electrolyzed palladium chloride is adsorbed on the metal sheet 10 corresponding to the positive electrode on the left side. At this time, the gear 17 is started to rotate by the switch 2. Since the gear 17 and the rack 18 are meshed, the rack 18 moves on the second slide bar 19 and drives the baffle 20 to move upward, so that the electrolyte remaining after the electrolysis enters the discharge port on the right side of the body 1, and the internal filter screen 21 is filtered to prevent the palladium chloride that has not been electrolyzed from flowing out. At the same time, the internal rotating shaft 22 rotates, driving the multiple rotating plates 23 on the surface to rotate, so that the discharge effect of the electrolyte is better.

[0032] Thereby completing a series of tasks, the contents not described in detail in this specification belong to the prior art known to professional and technical personnel in this field.

[0033] It is obvious to those skilled in the art that the present invention is not limited to the details of the exemplary embodiments described above, and that the present invention can be implemented in other specific forms without departing from the spirit or essential features of the present invention. Therefore, the embodiments should be regarded as exemplary and non-restrictive from any point of view, and the scope of the present invention is defined by the appended claims rather than the above description, and it is intended that all changes falling within the meaning and scope of the equivalent elements of the claims be included in the present invention. Any reference numeral in a claim should not be regarded as limiting the claim to which it relates.

Claims

1. A high-purity palladium chloride electrolysis device, comprising a body (1) and a switch (2); Features: A push rod (3) is arranged inside the machine body (1), and the push rod (3) is connected to a slider (5), and the slider (5) is arranged on a first slider (4), and the slider (5) is connected to a support rod (6) above the slider (5), and the support rod (6) is connected to a first clamping rod (7) and a connecting rod (8) through a hinge axis, and the connecting rod (8) is connected to a second clamping rod (9), the first clamping rod (7) and the second clamping rod (9) fix the metal sheet (10), and an electric clamp (11) is arranged on the metal sheet (10), and the electric clamp (11) is connected to the machine body (1) through an electric wire; A motor (12) is arranged inside the machine body (1), and the motor (12) is connected to a rotating rod (13), and a stirring rod (14) is arranged on the surface of the rotating rod (13), and a temperature controller (15) is arranged in the stirring rod (14), and a temperature detector (16) is arranged inside the machine body (1).

2. The high-purity palladium chloride electrolysis device according to claim 1, wherein The bottom of the machine body (1) is provided with support legs, which are connected to the bottom of the machine body (1) via hinge shafts, and are symmetrically arranged about the center of the bottom of the machine body (1).

3. The high-purity palladium chloride electrolysis device according to claim 1, characterized in that The first slide bar (4) is symmetrically arranged with respect to the center of the machine body (1), and a first clamping bar (7) and a second clamping bar (9) are arranged above the first slide bar (4), and metal sheets (10) are fixed to the first clamping bar (7) and the second clamping bar (9).

4. The high-purity palladium chloride electrolysis device according to claim 1, characterized in that The metal sheets (10) are each provided with an electric clamp (11), and the electric clamp (11) is connected to the positive electrode and the negative electrode inside the machine body (1) through electric wires.

5. The high-purity palladium chloride electrolysis device according to claim 1, characterized in that: A gear (17) is arranged inside the machine body (1), and the gear (17) is meshed with a rack (18), and the rack (18) is arranged on a second sliding rod (19), and a baffle (20) is arranged at the front end of the rack (18).

6. The high-purity palladium chloride electrolysis device according to claim 1, characterized in that: A discharge port is arranged at the lower right side of the machine body (1), a filter screen (21) and a rotating shaft (22) are arranged in the discharge port, and a rotating plate (23) is arranged on the surface of the rotating shaft (22).

7. The high-purity palladium chloride electrolysis device according to claim 1, characterized in that: An observation window is provided on the surface of the machine body (1), and the observation window is arranged at the center of the surface of the machine body (1), and the material of the observation window is transparent glass material.

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