Heating equipment for manufacturing and processing high-purity metal

Abstract

The utility model discloses heating equipment for manufacturing and processing high-purity metal, which is characterized in that the top end of a fixed operation frame is fixedly connected with a separation fixed sleeve, one end of the inner side of the separation fixed sleeve is welded with a vacuum heating barrel, the other end of the inner side of the separation fixed sleeve is clamped with a condenser, and the inner side of the condenser is sleeved with a liquid storage barrel; the side end of the separation fixing sleeve is fixedly connected with an electromagnetic fixing ring, the position, corresponding to the separation fixing sleeve, of the side end of the electromagnetic fixing ring is sleeved with a sealing isolation sleeve in a magnetic attraction mode, and a plurality of incandescent heat collecting rods are installed at the position, corresponding to the separation fixing sleeve, of one end of the sealing isolation sleeve at equal intervals. The liquid storage barrel is cooled through the condenser, so that iodine steam is liquefied into iodine liquid, flowing of internal airflow is accelerated through the flow guide fan, the air outlet speed is increased, constant internal air pressure and temperature are guaranteed, meanwhile, continuous high-temperature treatment is matched, the treatment forming speed is increased, recycling of the iodine liquid is achieved, and the product treatment speed is guaranteed.

Description

Technical Field

[0001] The utility model relates to the technical field of high-purity metal manufacturing, in particular to a manufacturing, processing and heating device for high-purity metal. Background Art

[0002] High-purity metals refer to metals with very high purity and impurities often calculated in parts per million. Because their properties are significantly different from those of general industrial pure metals, they have gained special uses. High-purity metals are also widely used in scientific research. Now, when purifying high-purity metals, iodine refining methods are used to manufacture them. Iodine refining methods can effectively remove impurities that do not react with iodine, such as oxides, carbides, nitrides, etc. in metals, impurities that react with iodine but do not generate volatile iodides, and impurities that react with iodine but do not decompose at high temperatures.

[0003] However, when using the iodine refining method to produce high-purity metals, the volatile iodide and iodine vapor are discharged slowly, causing the internal gas pressure to increase during production, affecting the actual internal processing speed, and the accumulation of iodine vapor will affect the internal temperature stability, further affecting purification and metal separation. Utility Model Content

[0004] The utility model provides a heating device for the production, processing and use of high-purity metals, which can effectively solve the problem raised in the above-mentioned background technology that when high-purity metals are currently produced by the iodine refining method, the volatile iodide and iodine vapor are discharged slowly, resulting in an increase in internal air pressure during production, affecting the actual internal processing speed, and the accumulation of iodine vapor affects the internal temperature stability, thereby further affecting the purification and metal separation.

[0005] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a heating device for manufacturing and processing high-purity metals, comprising a fixed operating frame, a heating production assembly is arranged on the top of the fixed operating frame, and the heating production assembly comprises a separation fixed sleeve, a vacuum heating barrel, a condenser, a liquid storage barrel, an electromagnetic fixed ring, a sealing isolation sleeve, a hot collecting rod, a supporting moving rod, a collecting fixed pipe, a liquid injection pipe, a booster pump, a guide fan and a vacuum device;

[0006] The top of the fixed operating frame is fixedly connected with a separation fixing sleeve, one end of the inner side of the separation fixing sleeve is welded with a vacuum heating barrel, the other end of the inner side of the separation fixing sleeve is clamped with a condenser, the inner side of the condenser is sleeved with a liquid storage barrel, the side end of the separation fixing sleeve is fixedly connected with an electromagnetic fixing ring, the side end of the electromagnetic fixing ring is magnetically sleeved with a sealing isolation sleeve at the position corresponding to the separation fixing sleeve, a plurality of hot collecting rods are equidistantly installed at one end of the sealing isolation sleeve at the position corresponding to the separation fixing sleeve, a supporting moving rod is slidably connected to the inner side of the vacuum heating barrel, one end of the separation fixing sleeve is penetrated by a collecting fixing pipe, one end of the liquid storage barrel is penetrated by a liquid injection pipe, a booster pump is installed at the position of the liquid storage barrel corresponding to the liquid injection pipe through a motor seat, a plurality of guide fans are installed on the side end of the vacuum heating barrel and the inner side of the collecting fixing pipe, and a vacuum device is installed at one end of the sealing isolation sleeve.

[0007] Preferably, one end of the sealing isolation sleeve is embedded and installed inside the separation fixing sleeve, and the input ends of the vacuum heating barrel, condenser, electromagnetic fixing ring, hot collection rod, booster pump, guide fan and vacuum device are all electrically connected to the output end of the external power supply.

[0008] Preferably, the collecting fixed tube is installed through one end of the liquid storage barrel, and one end of the booster pump is connected to one end of the liquid injection tube through an adapter.

[0009] Preferably, a collecting assembly is provided at the top of the fixed operating frame, and the collecting assembly includes a movable electric slide rail, a movable lifting plate, a collecting limit box, a material unloading operation box, a scraping electric push rod, a scraping operation plate and a cleaning scraping hole;

[0010] A movable electric slide rail is symmetrically installed on the inner side of the fixed operating frame, a movable lifting plate is installed between the two movable electric slide rails through a slide rail seat, a collecting limit box is fixedly connected to the top of the movable lifting plate, a unloading operation box is welded at the bottom of the side end of the separation fixed sleeve corresponding to the position of the collecting limit box, a scraping electric push rod is symmetrically installed at one end of the sealing isolation sleeve, one end of the two scraping electric push rods is fixedly connected to a scraping operating plate, and a plurality of cleaning scraping holes are equidistantly opened at one end of the scraping operating plate.

[0011] Preferably, the collecting limit box is slidably fitted with the unloading operation box, and the input ends of the movable electric slide rail and the scraping electric push rod are electrically connected to the output end of the external power supply.

[0012] Preferably, the scraping operation plate is slidably mounted on the inner side of the separation fixing sleeve, and the side end of the cleaning scraping hole is sleeve-assembled with the hot collection rod.

[0013] Compared with the prior art, the utility model has the following beneficial effects: the utility model has a scientific and reasonable structure and is safe and convenient to use:

[0014] 1. A heating production component is provided, and a vacuum treatment is performed on the inside through a sealed isolation sleeve vacuum device. At the same time, the iodine liquid in the liquid storage barrel is extracted by a booster pump and a liquid injection pipe. The iodine liquid is evenly sprayed to the side end of the raw material under the action of high pressure. The volatile iodide is evenly dispersed and separated inside the fixed sleeve driven by a guide fan. Then, iodine vapor is injected into the inside of the liquid storage barrel through a collecting fixed pipe and a guide fan. The liquid storage barrel is cooled by a condenser to liquefy the iodine vapor into iodine liquid. The internal air flow is accelerated by the guide fan, the gas outlet speed is accelerated, and the internal air pressure and temperature are guaranteed to be constant. At the same time, continuous high-temperature treatment is coordinated to accelerate the processing and molding speed, and the iodine liquid is recycled and utilized, thereby ensuring the speed of product processing.

[0015] 2. A collecting component is provided, and the collecting limit box is placed on the top of the movable lifting plate. The movable lifting plate and the collecting limit box are driven up by the movable electric slide rail, and the collecting limit box is inserted into the inner side of the unloading operation box. The scraping electric push rod drives the scraping operation plate and the cleaning scraping hole to scrape and separate the high-purity metal on the surface of the hot collecting rod, thereby realizing rapid material collection and cleaning of the surface of the hot collecting rod, and avoiding the continuous stacking of high-purity metal affecting the speed of subsequent purification. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] The accompanying drawings are used to provide a further understanding of the present invention and constitute a part of the specification. They are used together with the embodiments of the present invention to explain the present invention and do not constitute a limitation to the present invention.

[0017] In the attached picture:

[0018] Figure 1 It is a three-dimensional structural schematic diagram of the utility model;

[0019] Figure 2 It is a schematic diagram of the installation structure of the separation fixing sleeve of the utility model;

[0020] Figure 3 It is a structural schematic diagram of the heating production component of the utility model;

[0021] Figure 4 It is a structural schematic diagram of the collection component of the utility model;

[0022] Numbers in the figure: 1. Fixed operating frame;

[0023] 2. Heating production assembly; 201. Separation fixing sleeve; 202. Vacuum heating barrel; 203. Condenser; 204. Liquid storage barrel; 205. Electromagnetic fixing ring; 206. Sealing isolation sleeve; 207. Incandescent collecting rod; 208. Support moving rod; 209. Collecting fixing pipe; 210. Liquid injection pipe; 211. Booster pump; 212. Diversion fan; 213. Vacuum device;

[0024] 3. Collecting assembly; 301. Moving electric slide rail; 302. Moving lifting plate; 303. Collecting limit box; 304. Unloading operation box; 305. Scraping electric push rod; 306. Scraping operation board; 307. Cleaning scraping hole. DETAILED DESCRIPTION

[0025] The preferred embodiments of the present invention are described below in conjunction with the accompanying drawings. It should be understood that the preferred embodiments described herein are only used to illustrate and explain the present invention, and are not used to limit the present invention.

[0026] Example: Figure 1-4 As shown, the utility model provides a technical solution, a heating device for manufacturing and processing high-purity metals, comprising a fixed operating frame 1, a heating production assembly 2 is arranged on the top of the fixed operating frame 1, and the heating production assembly 2 comprises a separation fixed sleeve 201, a vacuum heating barrel 202, a condenser 203, a liquid storage barrel 204, an electromagnetic fixed ring 205, a sealing isolation sleeve 206, a hot collecting rod 207, a supporting moving rod 208, a collecting fixed pipe 209, a liquid injection pipe 210, a booster pump 211, a guide fan 212 and a vacuum device 213;

[0027] A separation fixing sleeve 201 is fixedly connected to the top of the fixed operation frame 1, a vacuum heating barrel 202 is welded to one end of the inner side of the separation fixing sleeve 201, a condenser 203 is clamped to the other end of the inner side of the separation fixing sleeve 201, a liquid storage barrel 204 is sleeved to the inner side of the condenser 203, an electromagnetic fixing ring 205 is fixedly connected to the side end of the separation fixing sleeve 201, a sealing isolation sleeve 206 is magnetically sleeved at the side end of the electromagnetic fixing ring 205 corresponding to the position of the separation fixing sleeve 201, one end of the sealing isolation sleeve 206 is embedded and installed in the inner side of the separation fixing sleeve 201, so that it can be operated steadily during the sleeve connection and overall sealing, and a plurality of incandescent collecting rods 206 are equidistantly installed at one end of the sealing isolation sleeve 206 corresponding to the position of the separation fixing sleeve 201 7. A supporting moving rod 208 is slidably connected to the inner side of the vacuum heating barrel 202. A collecting fixed pipe 209 is connected through one end of the separation fixed sleeve 201. The collecting fixed pipe 209 is installed through one end of the liquid storage barrel 204, so that it can be operated steadily during recovery. A liquid injection pipe 210 is connected through one end of the liquid storage barrel 204. A booster pump 211 is installed at the position of the liquid injection pipe 210 at one end of the liquid storage barrel 204 through a motor seat. One end of the booster pump 211 is connected to one end of the liquid injection pipe 210 through an adapter to ensure the continuous continuity of liquid addition. Several guide fans 212 are installed on the side end of the vacuum heating barrel 202 and the inner side of the collecting fixed pipe 209. A vacuum device 213 is installed at one end of the sealing isolation sleeve 206;

[0028] In order to ensure stable operation of the equipment, the input ends of the vacuum heating barrel 202, the condenser 203, the electromagnetic fixing ring 205, the hot collecting rod 207, the booster pump 211, the guide fan 212 and the vacuum device 213 are all electrically connected to the output end of the external power supply.

[0029] A collecting assembly 3 is arranged at the top of the fixed operating frame 1, and the collecting assembly 3 includes a movable electric slide rail 301, a movable lifting plate 302, a collecting limit box 303, a material unloading operation box 304, a scraping electric push rod 305, a scraping operation plate 306 and a cleaning scraping hole 307;

[0030] A movable electric slide rail 301 is symmetrically installed on the inner side of the fixed operating frame 1, and a movable lifting plate 302 is installed between the two movable electric slide rails 301 through a slide rail seat. A collection limit box 303 is fixedly connected to the top of the movable lifting plate 302, and the collection limit box 303 is slidably fitted with a material discharge operation box 304, so that the collection can be operated steadily. A material discharge operation box 304 is welded at the bottom of the side end of the separation fixed sleeve 201 corresponding to the position of the collection limit box 303, and a scraping electric push rod 305 is symmetrically installed at one end of the sealing isolation sleeve 206. One end of the two scraping electric push rods 305 is fixedly connected to a scraping operation plate 306, and one end of the scraping operation plate 306 is equidistantly provided with a plurality of cleaning scraping holes 307, and the scraping operation plate 306 is slidably installed on the inner side of the separation fixed sleeve 201, and the side end of the cleaning scraping hole 307 is sleeved and combined with the hot collection rod 207, so as to ensure the stable operation of cleaning and slag discharge;

[0031] For stable operation of the equipment, the input ends of the movable electric slide rail 301 and the scraping electric push rod 305 are electrically connected to the output end of the external power supply.

[0032] The working principle and use process of the utility model are as follows: the staff sleeves the raw material of high-purity metal onto the side end of the supporting movable rod 208, sleeves the sealing isolation sleeve 206 onto the separation fixed sleeve 201 and the side end of the vacuum heating barrel 202, and performs vacuum treatment on the inside through the vacuum device 213. At the same time, the vacuum heating barrel 202 and the incandescent collecting rod 207 are powered on for heating. After the internal vacuum is completed, the booster pump 211 and the injection pipe 210 extract the iodine liquid in the liquid storage barrel 204, and pressurize the iodine liquid into the inner side of the vacuum heating barrel 202. The iodine liquid is evenly sprayed onto the side end of the raw material under the action of high pressure, and the excess iodine liquid is evenly spread on the inner side of the vacuum heating barrel 202. At this time, under the action of heating, the iodine liquid reacts with the raw metal to produce The iodine vapor is injected into the inner side of the liquid storage barrel 204 through the collecting fixed pipe 209 and the flow guide fan 212, and the liquid storage barrel 204 is cooled by the condenser 203, and the temperature is controlled between 120°C and 160°C, so that the iodine vapor is liquefied into iodine liquid, thereby completing the recovery of iodine and completing the manufacture of high-purity metal. The flow guide fan 212 accelerates the flow of internal airflow and the gas outlet speed, and at the same time cooperates with the continuous high-temperature treatment to accelerate the processing and molding speed;

[0033] After the high-purity metal is purified to a certain amount, the collection limit box 303 is placed on the top of the movable lifting plate 302, and the movable lifting plate 302 and the collection limit box 303 are driven up by the movable electric slide rail 301, and the collection limit box 303 is inserted into the inner side of the unloading operation box 304, and the scraping electric push rod 305 drives the scraping operation plate 306 to slide along the separation fixed sleeve 201. At this time, the cleaning scraping hole 307 and the scraping operation plate 306 scrape and separate the high-purity metal on the surface of the hot collection rod 207. At this time, the high-purity metal falls to the inner side of the collection limit box 303, so that the material can be collected quickly, while avoiding the continuous stacking of high-purity metal affecting the speed of subsequent purification.

[0034] Finally, it should be noted that the above description is only a preferred example of the present utility model and is not intended to limit the present utility model. Although the present utility model is described in detail with reference to the above embodiments, those skilled in the art can still modify the technical solutions described in the above embodiments or replace some of the technical features therein by equivalents. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present utility model shall be included in the protection scope of the present utility model.

Claims

1. A heating device for manufacturing, processing and treating high-purity metals, comprising a fixed operating frame (1), characterized in that: A heating production assembly (2) is arranged at the top of the fixed operating frame (1), and the heating production assembly (2) comprises a separation fixing sleeve (201), a vacuum heating barrel (202), a condenser (203), a liquid storage barrel (204), an electromagnetic fixing ring (205), a sealing isolation sleeve (206), a hot collecting rod (207), a supporting moving rod (208), a collecting fixing pipe (209), a liquid injection pipe (210), a booster pump (211), a guide fan (212) and a vacuum device (213); The top of the fixed operating frame (1) is fixedly connected to a separation fixing sleeve (201), one end of the inner side of the separation fixing sleeve (201) is welded with a vacuum heating barrel (202), the other end of the inner side of the separation fixing sleeve (201) is clamped with a condenser (203), the inner side of the condenser (203) is sleeved with a liquid storage barrel (204), the side end of the separation fixing sleeve (201) is fixedly connected to an electromagnetic fixing ring (205), the side end of the electromagnetic fixing ring (205) is magnetically sleeved with a sealing isolation sleeve (206) at a position corresponding to the separation fixing sleeve (201), and one end of the sealing isolation sleeve (206) is sleeved at a position corresponding to the separation fixing sleeve (201). A plurality of hot collecting rods (207) are installed at a distance, a supporting moving rod (208) is slidably connected to the inner side of the vacuum heating barrel (202), a collecting fixed pipe (209) is penetrated and connected to one end of the separation fixed sleeve (201), a liquid injection pipe (210) is penetrated and connected to one end of the liquid storage barrel (204), a booster pump (211) is installed at one end of the liquid storage barrel (204) at a position corresponding to the liquid injection pipe (210) through a motor seat, a plurality of guide fans (212) are installed at the side end of the vacuum heating barrel (202) and the inner side of the collecting fixed pipe (209), and a vacuum device (213) is installed at one end of the sealing isolation sleeve (206).

2. The heating equipment for manufacturing and processing high-purity metal according to claim 1, characterized in that: One end of the sealing isolation sleeve (206) is embedded and installed inside the separation fixing sleeve (201), and the input ends of the vacuum heating barrel (202), the condenser (203), the electromagnetic fixing ring (205), the hot collecting rod (207), the booster pump (211), the guide fan (212) and the vacuum device (213) are all electrically connected to the output end of the external power supply.

3. The manufacturing, processing and heating equipment for high-purity metal according to claim 1, characterized in that: The collecting fixed pipe (209) is installed through one end of the liquid storage barrel (204), and one end of the booster pump (211) is connected to one end of the liquid injection pipe (210) via an adapter.

4. The heating equipment for manufacturing and processing high-purity metal according to claim 1, characterized in that: A collecting assembly (3) is arranged at the top of the fixed operating frame (1), and the collecting assembly (3) comprises a movable electric slide rail (301), a movable lifting plate (302), a collecting limit box (303), a material unloading operation box (304), a scraping electric push rod (305), a scraping operation plate (306) and a cleaning scraping hole (307); A movable electric slide rail (301) is symmetrically installed on the inner side of the fixed operating frame (1), a movable lifting plate (302) is installed between the two movable electric slide rails (301) through a slide rail seat, a collection limit box (303) is fixedly connected to the top of the movable lifting plate (302), a material discharge operation box (304) is welded at the bottom of the side end of the separation fixed sleeve (201) corresponding to the position of the collection limit box (303), a scraping electric push rod (305) is symmetrically installed on one end of the sealing isolation sleeve (206), one end of the two scraping electric push rods (305) is fixedly connected to a scraping operation plate (306), and a plurality of cleaning scraping holes (307) are equidistantly opened at one end of the scraping operation plate (306).

5. The manufacturing, processing and heating equipment for high-purity metal according to claim 4, characterized in that: The collecting limit box (303) is slidably fitted with the material discharging operation box (304), and the input ends of the movable electric slide rail (301) and the scraping electric push rod (305) are both electrically connected to the output end of the external power supply.

6. The manufacturing, processing and heating equipment for high-purity metal according to claim 4, characterized in that: The scraping operation plate (306) is slidably mounted on the inner side of the separation fixing sleeve (201), and the side end of the cleaning scraping hole (307) is sleeve-connected and assembled with the incandescent collection rod (207).

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