Fatty acid fractionating tower

By designing multiple condensation mechanisms and temperature control mechanisms in the fractionation column, the problem of inconsistent condensate temperature is solved, and the fractionation efficiency and discharge volume are improved.

CN222829083UActive Publication Date: 2025-05-06HONGHU KEXIN GREASE CO LTD
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Patent Information

Application Number
CN202421807040.2
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-07-29
Publication Date
2025-05-06
Estimated Expiration
2034-07-29

AI Technical Summary

Technical Problem

In the existing fractionation column, the temperature after the condensate passes through the second condensation tube may be higher than the temperature on the uppermost side of the condensation column, which affects the condensation effect of the gaseous substance and the discharge amount of the fractionation column.

Method used

A fatty acid fractionation tower is designed, including multiple condensation mechanisms and temperature control mechanisms. The condensing mechanism increases the condensation area and speed through the combination of a conical liquid separation seat and a condensation plate. The temperature control mechanism adjusts the temperature of the coolant by connecting the pipe and the thermal grating plate to ensure that the temperature of the condensation process is consistent.

Benefits of technology

By increasing the condensation speed and temperature control, the efficiency of the fractionation process is improved, ensuring effective condensation of gaseous substances and the discharge volume of the fractionation column.

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Abstract

The utility model relates to the technical field of fractionation, in particular to a fatty acid fractionating tower which comprises a fractionating mechanism, four fractionating partition plates are vertically arranged in the fractionating mechanism, the fatty acid fractionating tower further comprises a plurality of condensing mechanisms for quickly condensing raw materials during fractionating, and a temperature control mechanism for adjusting temperature is arranged between every two condensing mechanisms. Through a cage-shaped structure formed by a plurality of first branch pipes and second branch pipes between a conical liquid separation seat and a liquid outlet ring pipe, passing materials are quickly condensed, and meanwhile, the condensation plates on the first branch pipes and the second branch pipes are used for increasing the whole condensation area, so that the condensation speed in the whole fractionation process is increased; the temperature of the material cooling liquid passing through the interior of the connecting pipe is controlled by feeding new cooling liquid with the corresponding temperature or flow speed into the temperature control box between every two adjacent condensation mechanisms, and then the temperature of the next-stage material during condensation is conveniently controlled.
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Description

Technical Field

[0001] The utility model relates to the technical field of fractionation, in particular to a fatty acid fractionation tower. Background Art

[0002] Fractional distillation is the process of heating a mixture and evaporating the different components of the mixture into gaseous state according to their boiling points. Since the boiling points are different, the condensation points of the evaporated gaseous substances in the mixture are also different. Then, the gaseous substances are condensed and separated into relatively pure single substances at different temperatures.

[0003] After searching the patent document with the publication number CN 220443212 U, it is found that two spirally intertwined first condenser tubes and second condenser tubes are connected head to tail and placed at the center of a condensation tower, and then condensate is fed into the first condenser tube and discharged from the second condenser tube. During this process, the entire condensate follows the first condenser tube and flows along the upper side of the condensation tower to the lower side thereof, and then enters the second condenser tube and flows from the lower side of the condensation tower to the upper side thereof before being discharged, so that the temperatures at both ends of the first cooling tube and the second cooling tube tend to be consistent;

[0004] In the patent document, if the two condensers adopt the above structure, the temperature in the entire cooling structure will be consistent. According to the structural principle of the condensation tower, the temperature at the top of the condensation tower will be lower than the temperature on its lower side. Therefore, after the coolant passes through the second cooling tube, its temperature may be higher than the temperature on the top of the condensation tower. The higher temperature in the second cooling tube will increase the temperature of the coolant that has just entered the first cooling tube, which may affect the condensation effect of the entire gaseous substance and also affect the discharge amount of the entire distillation tower. Utility Model Content

[0005] The purpose of the utility model is to provide a fatty acid fractionation tower in order to solve the above problems.

[0006] The utility model achieves the above-mentioned purpose through the following technical solutions:

[0007] A fatty acid fractionation tower comprises a fractionation mechanism, four fractionation baffles are vertically arranged inside the fractionation mechanism, and a plurality of condensation mechanisms are used to quickly condense raw materials during fractionation, and a temperature control mechanism is provided between two condensation mechanisms for adjusting the temperature;

[0008] The condensation mechanism comprises a conical liquid separation seat, a liquid inlet pipe is fixed on the upper end of the conical liquid separation seat, a liquid outlet ring pipe is arranged below the conical liquid separation seat, a liquid outlet pipe for guiding the coolant out is arranged on one side of the liquid outlet ring pipe, a plurality of first branch pipes and second branch pipes for facilitating the flow of the coolant are arranged between the conical liquid separation seat and the liquid outlet ring pipe, and condensation plates are welded on the first branch pipes and the second branch pipes;

[0009] The temperature control mechanism comprises a connecting pipe, a plurality of heat-conducting grids are welded on the outside of the connecting pipe, a temperature control box is arranged on the outside of the connecting pipe and the heat-conducting grids, and flow guide pipes are arranged at both ends of the temperature control box to facilitate the flow of coolant.

[0010] Preferably, the conical liquid separation seat is a hollow structure, and the conical liquid separation seat and the liquid outlet ring pipe are connected through the first branch pipe and the second branch pipe.

[0011] Preferably: the interior of the temperature control box is a hollow structure, and both ends of the connecting pipe are connected to the liquid outlet pipe and the liquid inlet pipe of two adjacent condensing mechanisms.

[0012] Preferably: the distillation mechanism includes a distillation tower body, a feed pipe for introducing distillation raw materials is provided on one side of the distillation tower body, an air inlet pipe for introducing steam into the distillation tower body is provided below the feed pipe, a first discharge pipe is provided on the top of the distillation tower body, and a sixth discharge pipe is provided on the lower side of the distillation tower body.

[0013] Preferably: the distillation mechanism further comprises a second discharge pipe, the second discharge pipe is located on a side of the distillation tower body away from the feed pipe, a third discharge pipe is arranged below the second discharge pipe, a fourth discharge pipe is arranged below the third discharge pipe, and a fifth discharge pipe is arranged below the fourth discharge pipe.

[0014] Preferably, the second discharge pipe, the third discharge pipe, the fourth discharge pipe and the fifth discharge pipe are all connected to the fractionation tower body, and a through hole for facilitating material fractionation is opened at the center of the fractionation partition.

[0015] The beneficial effects compared with the prior art are as follows:

[0016] 1. The cage-type structure composed of multiple first branch pipes and second branch pipes between the conical liquid separation seat and the liquid outlet ring pipe allows the passing material to be quickly condensed. At the same time, the condensation plates on the first branch pipes and the second branch pipes are used to increase the entire condensation area, thereby increasing the condensation speed during the entire fractionation;

[0017] 2. By sending new coolant of corresponding temperature or flow rate into the temperature control box between two adjacent condensing mechanisms, the temperature of the material coolant passing through the connecting pipe is controlled, which is convenient for controlling the temperature of the next stage of material condensation. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] In order to more clearly illustrate the embodiments of the utility model or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative labor.

[0019] Figure 1 It is a structural schematic diagram of a fatty acid fractionation tower described in the utility model;

[0020] Figure 2 It is a cross-sectional view of a fatty acid fractionation tower described in the utility model;

[0021] Figure 3 It is a partial cross-sectional view of a fractionation tower body of a fatty acid fractionation tower described in the utility model;

[0022] Figure 4 It is a partial cross-sectional view of a condensation mechanism of a fatty acid fractionation tower described in the utility model;

[0023] Figure 5 It is a partial parts diagram of a heat-conducting grid plate of a fatty acid fractionation tower described in the utility model;

[0024] Figure 6 It is a partial parts diagram of a condensation plate of a fatty acid fractionation tower described in the utility model;

[0025] Figure 7 This is a diagram of the coordination of a liquid outlet pipe and a connecting pipe of a fatty acid fractionation tower described in the utility model;

[0026] Figure 8 It is a partial parts diagram of a condensation mechanism of a fatty acid fractionation tower described in the utility model.

[0027] The following are the descriptions of the reference numerals:

[0028] 1. Distillation mechanism; 2. Distillation partition; 3. Condensation mechanism; 4. Temperature control mechanism; 11. Distillation tower body; 12. Feed pipe; 13. Air inlet pipe; 14. Sixth discharge pipe; 15. First discharge pipe; 16. Second discharge pipe; 17. Third discharge pipe; 18. Fourth discharge pipe; 19. Fifth discharge pipe; 31. Liquid inlet pipe; 32. Conical liquid separation seat; 33. Liquid discharge ring pipe; 34. Liquid discharge pipe; 35. First branch pipe; 36. Second branch pipe; 37. Condensation plate; 41. Temperature control box; 42. Connecting pipe; 43. Heat transfer grid. DETAILED DESCRIPTION

[0029] In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installation", "connection" and "connection" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be an indirect connection through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood by specific circumstances.

[0030] The utility model is further described below in conjunction with the accompanying drawings:

[0031] like Figure 1-Figure 8As shown, a fatty acid fractionation tower includes a fractionation mechanism 1, in which four fractionation baffles 2 are vertically arranged, and also includes a plurality of condensation mechanisms 3 for quickly condensing raw materials during fractionation, and a temperature control mechanism 4 for adjusting the temperature is arranged between two condensation mechanisms 3.

[0032] In this embodiment, the condensation mechanism 3 includes a conical liquid separation seat 32, a liquid inlet pipe 31 is fixed to the upper end of the conical liquid separation seat 32, a liquid outlet ring pipe 33 is provided below the conical liquid separation seat 32, and a liquid outlet pipe 34 for guiding the coolant out of the liquid outlet ring pipe 33 is provided on one side thereof, and a plurality of first branch pipes 35 and second branch pipes 36 for facilitating the flow of the coolant are provided between the conical liquid separation seat 32 and the liquid outlet ring pipe 33, and a condensation plate 37 is welded on the first branch pipe 35 and the second branch pipe 36, and the conical liquid separation seat 32 is a hollow structure, and the conical liquid separation seat 32 and the liquid outlet ring pipe 33 are connected through ... The liquid inlet pipe 31 introduces the cooling liquid into the conical liquid separation seat 32, and then introduces the cooling liquid into multiple first branch pipes 35 and second branch pipes 36 through the conical liquid separation seat 32, and the passing material is fractionated and condensed through the first branch pipe 35, the second branch pipe 36 and the condensation plate 37 on the outside of the two. Then, the condensed material liquid is guided to the corresponding distillation partition plate 2 through the cage structure of the first branch pipe 35 and the second branch pipe 36, and the condensate in the first branch pipe 35 and the second branch pipe 36 is discharged through the liquid outlet ring pipe 33 and the liquid outlet pipe 34 and guided to the next stage condensation mechanism 3 through the temperature control mechanism 4.

[0033] In this embodiment: the temperature control mechanism 4 includes a connecting pipe 42, a plurality of heat-conducting grids 43 are welded on the outside of the connecting pipe 42, a temperature control box 41 is provided on the outside of the connecting pipe 42 and the heat-conducting grids 43, and flow guide pipes are provided at both ends of the temperature control box 41 to facilitate the flow of coolant. The interior of the temperature control box 41 is a hollow structure, and the two ends of the connecting pipe 42 are connected to the liquid outlet pipe 34 and the liquid inlet pipe 31 of the two adjacent condensing mechanisms 3. The connecting pipe 42 is used to connect the liquid inlet pipe 31 and the liquid outlet pipe 34 of the upper and lower adjacent levels. Then, in this process, the temperature of the coolant flowing through the connecting pipe 42 is adjusted by changing the flow rate or temperature of the new coolant entering the temperature control box 41, and then the temperature of the coolant during the entire condensation is adjusted, which is convenient for controlling the temperature of the material during condensation.

[0034] In the present embodiment: the fractionation mechanism 1 comprises a fractionation tower body 11, a feed pipe 12 for introducing fractionation raw materials is provided on one side of the fractionation tower body 11, an air inlet pipe 13 for introducing steam into the interior of the fractionation tower body 11 is provided below the feed pipe 12, a first discharge pipe 15 is provided on the top of the fractionation tower body 11, a sixth discharge pipe 14 is provided on the lower side of the fractionation tower body 11, the fractionation mechanism 1 further comprises a second discharge pipe 16, the second discharge pipe 16 is located on the side of the fractionation tower body 11 away from the feed pipe 12, a third discharge pipe 17 is provided below the second discharge pipe 16, a fourth discharge pipe 18 is provided below the third discharge pipe 17, a fifth discharge pipe 19 is provided below the fourth discharge pipe 18, the second discharge pipe 16, the third discharge pipe 17, The fourth discharge pipe 18 and the fifth discharge pipe 19 are both connected to the distillation tower body 11, and a through hole is opened at the center position of the distillation partition 2 to facilitate the distillation of materials. The feed pipe 12 is used to introduce the material to be distilled into the distillation tower body 11, and then the steam is introduced into the distillation tower body 11 through the air inlet pipe 13, and then the material entering the distillation tower body 11 is heated at high temperature, and then evaporated according to the boiling points of different substances in the material, and then located at different positions of the distillation tower body 11, and then condensed and discharged through the first discharge pipe 15, the second discharge pipe 16, the third discharge pipe 17, the fourth discharge pipe 18 and the fifth discharge pipe 19 respectively, and the remaining substance will flow out from the sixth discharge pipe 14.

[0035] Working principle: When in use, the material to be fractionated is introduced into the distillation tower body 11 through the feed pipe 12, and then the steam is introduced into the distillation tower body 11 through the air inlet pipe 13, and then the material entering the distillation tower body 11 is heated at high temperature, and then the different substances in the material are evaporated by the boiling point, and then they are at different positions of the distillation tower body 11;

[0036] In this process, a coolant of corresponding temperature is fed into the uppermost liquid inlet pipe 31. When the coolant enters the conical liquid separator seat 32 through the liquid inlet pipe 31, the coolant is introduced into a plurality of first branch pipes 35 and second branch pipes 36 through the conical liquid separator seat 32. The passing material is fractionated and condensed through the first branch pipe 35, the second branch pipe 36 and the condensation plates 37 on the outside of the first branch pipe 35, the second branch pipe 36 and the condensation plates 37 on the outside of the first branch pipe 35, the second branch pipe 36 and the second branch pipe 36. Then, the condensed material liquid is guided to the corresponding fractionation partition plate 2 through the cage structure of the first branch pipe 35 and the second branch pipe 36. The condensate in the first branch pipe 35 and the second branch pipe 36 is discharged through the liquid outlet ring pipe 33 and the liquid outlet pipe 34, and guided to the next-level condensation mechanism 3 through the connecting pipe 42. The above process interface is repeated to separate the multiple substances fractionated.

[0037] In addition, when the coolant flows from the upper condensing mechanism 3 to the lower condensing mechanism 3, new coolant with a corresponding flow rate or temperature can be introduced into the temperature control box 41 to cool the heat conductive grid 43, and then the heat conductive grid 43 can cool the connecting pipe 42. Then, the flow rate of the new coolant in the temperature control box 41 is controlled to adjust the temperature of the coolant flowing through the inside of the connecting pipe 42, and then the temperature of the coolant during the entire condensation is adjusted, which is convenient for accurately controlling the temperature of the materials during condensation between different layers. The materials condensed at different positions of the distillation tower body 11 can be discharged after condensation through the first discharge pipe 15, the second discharge pipe 16, the third discharge pipe 17, the fourth discharge pipe 18 and the fifth discharge pipe 19, respectively, and the remaining substances will flow out from the sixth discharge pipe 14.

[0038] The above shows and describes the basic principle, main features and advantages of the utility model. Those skilled in the art should understand that the utility model is not limited by the above embodiments, and the above embodiments and descriptions are only for explaining the principle of the utility model. Without departing from the spirit and scope of the utility model, the utility model may have various changes and improvements, and these changes and improvements fall within the scope of the utility model to be protected.

Claims

1. A fatty acid fractionation tower, comprising a fractionation mechanism (1), wherein four fractionation baffles (2) are vertically arranged inside the fractionation mechanism (1), characterized in that: It also includes a plurality of condensing mechanisms (3) for quickly condensing the raw materials during fractionation, and a temperature control mechanism (4) for adjusting the temperature is provided between two of the condensing mechanisms (3); The condensation mechanism (3) comprises a conical liquid separation seat (32), a liquid inlet pipe (31) is fixed at the upper end of the conical liquid separation seat (32), a liquid outlet ring pipe (33) is provided below the conical liquid separation seat (32), a liquid outlet pipe (34) for guiding the coolant out is provided on one side of the liquid outlet ring pipe (33), a plurality of first branch pipes (35) and second branch pipes (36) for facilitating the flow of the coolant are provided between the conical liquid separation seat (32) and the liquid outlet ring pipe (33), and a condensation plate (37) is welded on each of the first branch pipe (35) and the second branch pipe (36); The temperature control mechanism (4) comprises a connecting pipe (42), a plurality of heat-conducting grids (43) are welded on the outside of the connecting pipe (42), a temperature control box (41) is arranged on the outside of the connecting pipe (42) and the heat-conducting grids (43), and flow guide pipes for facilitating the flow of cooling liquid are arranged at both ends of the temperature control box (41).

2. A fatty acid fractionation tower according to claim 1, characterized in that: The conical liquid separation seat (32) is a hollow structure, and the conical liquid separation seat (32) and the liquid outlet ring pipe (33) are connected through the first branch pipe (35) and the second branch pipe (36).

3. A fatty acid fractionation tower according to claim 1, characterized in that: The interior of the temperature control box (41) is a hollow structure, and the two ends of the connecting pipe (42) are connected to the liquid outlet pipe (34) and the liquid inlet pipe (31) of two adjacent condensing mechanisms (3).

4. A fatty acid fractionation tower according to claim 1, characterized in that: The fractionation mechanism (1) comprises a fractionation tower body (11), a feed pipe (12) for introducing fractionation raw materials is provided on one side of the fractionation tower body (11), an air inlet pipe (13) for introducing steam into the interior of the fractionation tower body (11) is provided below the feed pipe (12), a first discharge pipe (15) is provided at the top of the fractionation tower body (11), and a sixth discharge pipe (14) is provided at the bottom of the fractionation tower body (11).

5. A fatty acid fractionation tower according to claim 4, characterized in that: The fractionation mechanism (1) further comprises a second discharge pipe (16), the second discharge pipe (16) being located on a side of the fractionation tower body (11) away from the feed pipe (12), a third discharge pipe (17) being provided below the second discharge pipe (16), a fourth discharge pipe (18) being provided below the third discharge pipe (17), and a fifth discharge pipe (19) being provided below the fourth discharge pipe (18).

6. A fatty acid fractionation tower according to claim 5, characterized in that: The second discharge pipe (16), the third discharge pipe (17), the fourth discharge pipe (18) and the fifth discharge pipe (19) are all connected to the fractionation tower body (11), and a through hole is provided at the center of the fractionation partition (2) to facilitate material fractionation.

Citation Information

Patent Citations

  • Fatty acid fractionating tower

    CN220443212U