Concentrated sulfuric acid adding structure for titanium dioxide acidolysis reaction

Abstract

The utility model discloses a concentrated sulfuric acid adding structure for titanium dioxide acidolysis reaction, which relates to the technical field of titanium dioxide enzyme reaction and comprises a storage bottle, a sealing cover is screwed at the top of the storage bottle, a quantifying mechanism is mounted outside the storage bottle, a ventilation component is mounted at a position close to the edge of the top of the storage bottle, and the quantifying mechanism comprises a quantifying cylinder and an infusion tube. The liquid conveying pipe is fixedly installed on the inner wall of the storage bottle, the liquid outlet pipe is installed at the top end of the liquid conveying pipe, the quantifying cylinder is installed outside the storage bottle, the gas conveying pipe is installed between the top end of the storage bottle and the position, close to the bottom end, outside the quantifying cylinder in a connected mode, a first screw is movably installed in the quantifying cylinder in a penetrating mode, and a first rotary knob is fixedly installed at the top end of the first screw. The quantitative adding of concentrated sulfuric acid is facilitated, the use of a suction pump is reduced, the corrosion of a concentrated sulfuric acid vehicle is prevented, the air exchange of the quantitative cylinder is facilitated, the cyclic quantitative adding is performed, and the internal sealing is improved.

Description

Technical Field

[0001] The utility model relates to the technical field of titanium dioxide enzymatic reaction, in particular to an adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide. Background Technique

[0002] Titanium dioxide is a chemical pigment with excellent covering power and light stability, and is widely used in products such as paints, coatings, plastics, and papers. In the process of titanium dioxide enzymatic reaction, concentrated sulfuric acid needs to be added as an acidic medium to provide an acidic environment, dissolve titanium dioxide, and promote the reaction between titanium dioxide and acid. This solution specifically relates to an adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide;

[0003] When the existing adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide is in use, due to the strong corrosiveness of concentrated sulfuric acid, it is easy to splash during the adding process, causing corrosion through the suction pump, not facilitating quantitative addition, and being prone to volatilization when contacting the external environment, resulting in pollution and harm to the human body. Summary of the Utility Model

[0004] The main purpose of the utility model is to provide an adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide, which can effectively solve the technical problems in the background technique.

[0005] To achieve the above purpose, the technical solution adopted by the utility model is as follows:

[0006] An adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide includes a storage bottle, the top of the storage bottle is screwed with a sealing cover, a quantitative mechanism is installed outside the storage bottle, a ventilation component is installed at a position near the edge of the top of the storage bottle. The quantitative mechanism includes a quantitative cylinder and an infusion tube. The infusion tube is fixedly installed on the inner wall of the storage bottle, the top of the infusion tube is installed with a liquid outlet tube, the quantitative cylinder is installed outside the storage bottle, and an air delivery tube is connected and installed between the top end of the storage bottle and the outer bottom end of the quantitative cylinder. A first screw rod is movably installed through the inside of the quantitative cylinder, the top of the first screw rod is fixedly installed with a first knob, the bottom end of the first screw rod and inside the quantitative cylinder is movably installed with a piston, and a scale window is opened on the periphery of the quantitative cylinder.

[0007] As a further solution of the utility model, the inside of the storage bottle and the quantitative cylinder are interconnected through the air delivery tube, and the first screw rod penetrates through the inside of the quantitative cylinder and is arranged in a threaded connection.

[0008] As a further solution of the utility model, the piston is arranged to slide up and down inside the quantitative cylinder, and the bottom end of the first screw rod penetrates through the top end of the piston and is connected through a bearing.

[0009] As a further solution of the present utility model, the ventilation component includes a ventilation pipe which is installed through between the top of the storage bottle and the air delivery pipe. Two fixing plates are fixedly installed inside the ventilation pipe. A plurality of through holes are provided in the upper and lower parts penetrating through the two fixing plates. A second screw rod is movably installed at the central position inside the two fixing plates. First sealing plugs and second sealing plugs are respectively fixedly installed at the positions near the top end and the bottom end of the periphery of the second screw rod. A second knob is installed at the top end of the second screw rod.

[0010] As a further solution of the present utility model, the two fixing plates are symmetrically arranged with respect to each other and are fixedly installed inside the ventilation pipe.

[0011] As a further solution of the present utility model, the second screw rod penetrates through the two fixing plates and is in threaded connection. The first sealing plug and the second sealing plug are respectively located at the positions near the top end and the bottom end inside the ventilation pipe and are matched with each other.

[0012] The beneficial effects of the present utility model are as follows:

[0013] By providing a metering mechanism, the first screw rod drives the piston to lift inside the metering cylinder, changes the air pressure inside the storage bottle through the air delivery pipe, enables concentrated sulfuric acid to enter the infusion pipe for delivery and addition, and adjusts the position of the piston through the scale window, facilitating the quantitative addition of concentrated sulfuric acid, reducing the use of a suction pump, preventing corrosion caused by concentrated sulfuric acid, and at the same time reducing the pollution to the air caused by the direct exposure of concentrated sulfuric acid.

[0014] By providing a ventilation component, the second screw rod drives the first sealing plug and the second sealing plug to slide synchronously, opens and closes the bottom of the ventilation pipe, and closes and opens the top of the ventilation pipe, facilitating the ventilation of the metering cylinder for cyclic quantitative addition. During the ventilation process, the storage bottle can be sealed to prevent the volatilization of concentrated sulfuric acid into the external environment. Description of the Drawings

[0015] Figure 1 It is a schematic diagram of the overall structure of an addition structure of concentrated sulfuric acid for the acidolysis reaction of titanium dioxide in the present utility model;

[0016] Figure 2 It is a schematic diagram of the internal structure of the metering mechanism in an addition structure of concentrated sulfuric acid for the acidolysis reaction of titanium dioxide in the present utility model;

[0017] Figure 3 It is a schematic diagram of the structure of the ventilation component in an addition structure of concentrated sulfuric acid for the acidolysis reaction of titanium dioxide in the present utility model;

[0018] Figure 4 It is a front view of the overall interior of an addition structure of concentrated sulfuric acid for the acidolysis reaction of titanium dioxide in the present utility model.

[0019] In the figure: 1, storage bottle; 2, sealing cap; 3, metering mechanism; 4, air exchange component; 5, metering cylinder; 6, infusion tube; 7, liquid outlet tube; 8, gas transmission tube; 9, first screw; 10, first knob; 11, piston; 12, scale window; 13, gas exchange tube; 14, fixed disk; 15, through hole; 16, second screw; 17, first sealing plug; 18, second sealing plug; 19, second knob. Specific implementation mode

[0020] In order to make the technical means, creative features, achieved purposes and effects realized by the present utility model easy to understand, the present utility model will be further described below in conjunction with specific implementation modes.

[0021] As Figures 1-4 shown, an addition structure of concentrated sulfuric acid for the acidolysis reaction of titanium dioxide includes a storage bottle 1, a sealing cap 2 is screwed to the top of the storage bottle 1, a metering mechanism 3 is installed outside the storage bottle 1, an air exchange component 4 is installed at a position near the edge of the top of the storage bottle 1, the metering mechanism 3 includes a metering cylinder 5 and an infusion tube 6, the infusion tube 6 is fixedly installed on the inner wall of the storage bottle 1, a liquid outlet tube 7 is installed at the top end of the infusion tube 6, the metering cylinder 5 is installed outside the storage bottle 1, and a gas transmission tube 8 is connected and installed between the top end of the storage bottle 1 and the outer bottom end of the metering cylinder 5. A first screw 9 is movably installed through the inside of the metering cylinder 5, a first knob 10 is fixedly installed at the top end of the first screw 9, a piston 11 is movably installed at the bottom end of the first screw 9 and inside the metering cylinder 5, and a scale window 12 is opened on the periphery of the metering cylinder 5.

[0022] In this embodiment, the inside of the storage bottle 1 and the metering cylinder 5 are in mutual communication through the gas transmission tube 8. The first screw 9 is threadedly connected through the inside of the metering cylinder 5 and is arranged to slide up and down through the threaded connection of the first screw 9, which is convenient for adjusting the air pressure inside the metering cylinder 5.

[0023] In this embodiment, the piston 11 is arranged to slide up and down inside the metering cylinder 5. The bottom end of the first screw 9 passes through the top end of the piston 11 and is connected by a bearing. By lifting and lowering the piston 11, the air pressure inside the metering cylinder 5 is changed, so that air is conveyed into the storage bottle 1 to adjust the amount of concentrated sulfuric acid added.

[0024] In this embodiment, the ventilation component 4 includes a ventilation pipe 13. The ventilation pipe 13 is installed through the top of the storage bottle 1 and between the air delivery pipes 8. Two fixed disks 14 are fixedly installed inside the ventilation pipe 13. A number of through holes 15 are provided in the upper and lower parts penetrating through the two fixed disks 14. A second screw rod 16 is movably installed at the central position inside the two fixed disks 14. First sealing plugs 17 and second sealing plugs 18 are respectively fixedly installed at the positions near the top and bottom of the periphery of the second screw rod 16. A second knob 19 is installed at the top of the second screw rod 16. The upper and lower parts of the ventilation pipe 13 are alternately opened and closed by the first sealing plugs 17 and the second sealing plugs 18, so that the metering cylinder 5 is ventilated and used in a circulating and metering manner.

[0025] In this embodiment, the two fixed disks 14 are symmetrically arranged with each other. The fixed disks 14 are fixedly installed inside the ventilation pipe 13. Air enters the ventilation pipe 13 through the air delivery pipe 8 and circulates through the through holes 15 in the two fixed disks 14.

[0026] In this embodiment, the second screw rod 16 penetrates through the two fixed disks 14 and is in threaded connection. The first sealing plugs 17 and the second sealing plugs 18 are respectively located at the positions near the top and bottom inside the ventilation pipe 13 and are matched with each other. The first sealing plug 17 is used to open or close the bottom of the ventilation pipe 13, and the second sealing plug 18 is used to open or close the top of the ventilation pipe 13.

[0027] It should be noted that the present utility model is an adding structure for concentrated sulfuric acid in the acidolysis reaction of titanium dioxide. When in use, first, concentrated sulfuric acid is added into the storage bottle 1 and sealed by the sealing cover 2. One end of the liquid outlet pipe 7 is connected to the titanium dioxide enzyme reaction tank. When performing quantitative addition, by rotating the first knob 10, the first screw rod 9 rotates and drives the piston 11 to slide downward under the action of the thread, compressing the air at the bottom end inside the metering cylinder 5 and delivering it to the storage bottle 1 through the air delivery pipe 8, increasing the air pressure inside the storage bottle 1, so that the concentrated sulfuric acid enters the infusion pipe 6 and is delivered to the liquid outlet pipe 7, and the concentrated sulfuric acid is added to the titanium dioxide enzyme reaction tank for reaction. The lifting of the piston 11 is adjusted through the scale window 12, and thus the amount of concentrated sulfuric acid added is adjusted. When the piston 11 descends to the bottom end of the metering cylinder 5, by rotating the second knob 19, the second screw rod 16 rotates and drives the first sealing plugs 17 and the second sealing plugs 18 to slide upward under the action of the thread. The second sealing plug 18 enters the inside of the ventilation pipe 13 for sealing. Continuing to slide upward makes the second sealing plug 18 completely enter the ventilation pipe 13, and thus the first sealing plug 17 disengages from the ventilation pipe 13, opening the top of the ventilation pipe 13. External air enters the metering cylinder 5 through the ventilation pipe 13 and the air delivery pipe 8. By rotating the first screw rod 9, the piston 11 is driven to slide upward for another quantitative addition.

[0028] The above has shown and described the basic principles, main features and advantages of the present utility model. Those skilled in the art should understand that the present utility model is not limited by the above embodiments. What is described in the above embodiments and the specification only illustrates the principles of the present utility model. Without departing from the spirit and scope of the present utility model, the present utility model will have various changes and improvements, and these changes and improvements all fall within the scope of the present utility model claimed. The scope of protection claimed by the present utility model is defined by the appended claims and their equivalents.

Claims

1. A structure for adding concentrated sulfuric acid to the acidolysis reaction of titanium dioxide, comprising a storage bottle (1), a sealing cover (2) being screwed to the top of the storage bottle (1), a quantitative mechanism (3) being installed on the outside of the storage bottle (1), and a ventilation component (4) being installed at a position near the edge of the top of the storage bottle (1), characterized in that: The quantitative mechanism (3) comprises a quantitative cylinder (5) and a liquid infusion tube (6), wherein the liquid infusion tube (6) is fixedly mounted on the inner wall of the storage bottle (1), a liquid outlet tube (7) is mounted on the top end of the liquid infusion tube (6), the quantitative cylinder (5) is mounted on the outside of the storage bottle (1), an air delivery tube (8) is connected and mounted between the top end of the storage bottle (1) and the outside of the quantitative cylinder (5) near the bottom end, a first screw rod (9) is movably mounted inside the quantitative cylinder (5), a first knob (10) is fixedly mounted on the top end of the first screw rod (9), a piston (11) is movably mounted at the bottom end of the first screw rod (9) and located inside the quantitative cylinder (5), and a scale window (12) is opened on the periphery of the quantitative cylinder (5).

2. The structure for adding concentrated sulfuric acid in the acidolysis reaction of titanium dioxide according to claim 1, characterized in that: The interior of the storage bottle (1) is communicated with the quantitative cylinder (5) via an air delivery pipe (8), and the first screw (9) penetrates the interior of the quantitative cylinder (5) and is arranged in a threaded connection.

3. The structure for adding concentrated sulfuric acid in the acidolysis reaction of titanium dioxide according to claim 1, characterized in that: The piston (11) is located inside the metering cylinder (5) and is slidably arranged up and down. The bottom end of the first screw (9) passes through the top end of the piston (11) and is connected via a bearing.

4. The structure for adding concentrated sulfuric acid to the titanium dioxide acidolysis reaction according to claim 1, characterized in that: The ventilation assembly (4) comprises a ventilation tube (13), wherein the ventilation tube (13) is installed between the top of the storage bottle (1) and the gas delivery tube (8), two fixed plates (14) are fixedly installed inside the ventilation tube (13), a plurality of through holes (15) are provided at the upper and lower parts of the two fixed plates (14), a second screw rod (16) is movably installed at the center position inside the two fixed plates (14), a first sealing plug (17) and a second sealing plug (18) are fixedly installed at the outer periphery of the second screw rod (16) near the top and the bottom respectively, and a second knob (19) is installed at the top end of the second screw rod (16).

5. The structure for adding concentrated sulfuric acid in the acidolysis reaction of titanium dioxide according to claim 4, characterized in that: The two fixing plates (14) are symmetrically arranged with respect to each other, and the fixing plates (14) are located inside the ventilation pipe (13) and are fixedly installed.

6. The structure for adding concentrated sulfuric acid in the acidolysis reaction of titanium dioxide according to claim 4, characterized in that: The second screw rod (16) penetrates the interior of the two fixed plates (14) and is threadedly connected. The first sealing plug (17) and the second sealing plug (18) are respectively located at the top end and the bottom end of the ventilation pipe (13) and match each other.

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