Novel musk rectification device

Abstract

The utility model discloses a novel musk rectification device which comprises a rectification frame, a supporting plate is installed on the lower half portion of the rectification frame, a rectification tank is installed at the upper end of the supporting plate, an air guide pipe is installed at the upper end of the rectification tank, the other end of the air guide pipe is communicated with a condensation assembly, and a three-way pipe is installed at the lower end of the condensation assembly. A return pipe of the three-way pipe is communicated with the rectification tank, a liquid outlet pipe of the three-way pipe is communicated with a product tank on the rectification frame, an electromagnetic valve I is mounted on the liquid outlet pipe, and an electromagnetic valve II is mounted on the return pipe; the recycling mechanism is mounted on the supporting plate and is used for recycling rectified products in the rectifying tank; the feeding mechanism is mounted on the supporting plate and is used for adding product raw materials into the rectification tank; the rectification device disclosed by the utility model has the advantages that the structure is reasonable, a product can be rectified for multiple times according to actual requirements, the purity of the product is improved, and the use requirements can be better met.

Description

Technical Field

[0001] The utility model relates to the technical field of rectification equipment, in particular to a novel musk essence rectification device. Background Technique

[0002] As a substitute for the endangered animal medicine musk, artificial musk is used in the same formula as natural musk. It is a major scientific research achievement and a confidential variety of the country. There are nearly 400 kinds of Chinese patent medicines produced with artificial musk, covering common dosage forms of Chinese patent medicines. It is a major breakthrough in the research of substitutes for rare animal medicines, opening up an important new way for the application of other rare animal medicines, creating a model for the popularization of other scientific research achievements, and promoting the sustainable and healthy development of the Chinese medicine cause. Usually, the processing of artificial musk requires the help of rectification equipment to improve the product purity.

[0003] For example, the utility model patent with the authorization announcement number CN215741870U discloses a synthetic musk essence rectification device. Through the cooperation of a filter screen, a first spring and a top block, the occurrence of steam countercurrent can be avoided. And the design of the filter screen can filter the steam to prevent impurities from entering the inside of the collection box, improving the rectification purity. And the working steps are simple, reducing the input of labor cost. Through the cooperation of a heating plate, a temperature sensor and a controller, the heating temperature can be freely adjusted, and heating can be carried out according to different materials to ensure rectification at the most suitable temperature, expanding the application range of the equipment.

[0004] However, this device can only rectify the product once, and cannot well guarantee the purity of the rectified product, reducing the practicability of the device and not well meeting the use requirements. Content of the Utility Model

[0005] The purpose of the utility model is to provide a novel musk essence rectification device to solve the problems put forward in the above background technique.

[0006] To achieve the above purpose, the utility model provides the following technical solutions:

[0007] A novel musk essence rectification device includes: a rectification frame, a tray is installed at the lower half of the rectification frame, a rectification tank is installed at the upper end of the tray, a gas guide pipe is installed at the upper end of the rectification tank, the other end of the gas guide pipe is communicated with a condensation assembly, a three-way pipe is installed at the lower end of the condensation assembly, the reflux pipe of the three-way pipe is communicated with the rectification tank, the liquid outlet pipe of the three-way pipe is communicated with a product tank on the rectification frame, a solenoid valve one is installed on the liquid outlet pipe, and a solenoid valve two is installed on the reflux pipe; a recovery mechanism, installed on the tray, for recovering the rectified product in the rectification tank; a feeding mechanism, installed on the tray, for adding product raw materials into the rectification tank; a condensation mechanism, installed on the rectification frame, for conveying condensed water to the condensation assembly.

[0008] As a preferred solution, the condensation assembly includes a condensation tank, a condensation coil is installed in the condensation tank, an inlet end of the condensation coil is communicated with an air guide pipe, and an outlet end of the condensation coil is communicated with a tee.

[0009] As a preferred solution, the recovery mechanism includes a recovery tank installed on a pallet, the recovery tank and the rectification tank are communicated through a recovery pipe, and a recovery valve is installed on the recovery pipe.

[0010] As a preferred solution, the feeding mechanism includes a storage tank installed on a pallet, the storage tank is communicated with a preheating coil in the recovery tank through a transfer pipe, the other end of the preheating coil penetrates through the recovery tank and is fixed with a feeding pipe, the feeding pipe is communicated with the rectification tank, and a feeding pump is also installed on the transfer pipe.

[0011] As a preferred solution, the condensation mechanism includes a condensation box and a collection box installed on a rectification rack, the condensation box is communicated with the condensation tank through a liquid inlet pipe, the collection box is communicated with the condensation tank through a collection pipe, and a condensation pump is installed on the liquid inlet pipe.

[0012] As a preferred solution, the collection box and the condensation box are communicated through a circulation pipe, and a circulation pump is installed on the circulation pipe.

[0013] As a preferred solution, a first concentration sensor is installed on a side wall of the rectification tank, a second concentration sensor is installed on the liquid outlet pipe, and a third concentration sensor is installed on the reflux pipe.

[0014] As a preferred solution, an exhaust gas treatment box is also installed on the rectification rack, the exhaust gas treatment box is communicated with an exhaust pipe on the rectification tank, and a pressure relief valve is also installed on the exhaust pipe;

[0015] A controller is also installed on the exhaust gas treatment box, and the first concentration sensor, the second concentration sensor, the third concentration sensor, the recovery valve, the first solenoid valve, the second solenoid valve, the feeding pump, and the condensation pump are all electrically connected to the controller.

[0016] Compared with the prior art, the beneficial effects of the utility model are as follows: Musk is added into the rectification tank 12 through the feeding mechanism. Subsequently, the musk is heated by the electric heating rod in the rectification tank. The steam generated by heating enters the condensation coil through the air duct. At the same time, condensed water is conveyed into the condensation tank through the condensation mechanism to condense the musk steam, so that the condensed musk liquid enters the three-way pipe. If multiple rectification operations are required, solenoid valve 1 is closed and solenoid valve 2 is opened, so that the condensed musk liquid re-enters the rectification tank through the return pipe, and rectification can be carried out again to improve the product purity. If solenoid valve 1 is opened and solenoid valve 2 is closed, the condensed musk liquid can be discharged into the product tank 19 for collection. The structure of the utility model is reasonable, and the product can be rectified multiple times according to actual needs to improve the product purity, and it can better meet the use requirements. Description of the Drawings

[0017] Figure 1 It is a schematic perspective view of the overall first perspective of a new type of musk rectification device;

[0018] Figure 2 It is a schematic perspective view of the overall second perspective of a new type of musk rectification device;

[0019] Figure 3 It is a schematic perspective view of the position of the feeding mechanism of a new type of musk rectification device;

[0020] Figure 4 It is a schematic sectional view of the position of the condensation component of a new type of musk rectification device.

[0021] In the figure: 1 - rectification rack, 11 - pallet, 12 - rectification tank, 121 - air duct, 13 - concentration sensor 1, 14 - exhaust pipe, 15 - pressure relief valve, 16 - waste gas treatment box, 17 - controller, 18 - three-way pipe, 181 - return pipe, 182 - liquid outlet pipe, 183 - solenoid valve 1, 184 - concentration sensor 2, 185 - solenoid valve 2, 186 - concentration sensor 3, 19 - product tank, 2 - feeding mechanism, 21 - transfer pipe, 22 - feeding pump, 23 - feeding pipe, 24 - storage tank, 25 - preheating coil, 3 - recovery mechanism, 31 - recovery pipe, 32 - recovery valve, 33 - recovery tank, 4 - condensation component, 41 - condensation tank, 42 - condensation coil, 5 - condensation mechanism, 51 - condensation box, 52 - liquid inlet pipe, 53 - condensation pump, 54 - collection box, 55 - collection pipe, 56 - circulation pipe, 57 - circulation pump. Detailed Embodiments

[0022] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

[0023] Embodiment: Please refer to Figures 1 to 4 , a new type of musk essence distillation device, including: a distillation rack 1, a support plate 11 is installed at the lower half of the distillation rack 1, a distillation tank 12 is installed at the upper end of the support plate 11, a gas guide pipe 121 is installed at the upper end of the distillation tank 12, the other end of the gas guide pipe 121 is communicated with a condensation assembly 4, a three-way pipe 18 is installed at the lower end of the condensation assembly 4, a return pipe 181 of the three-way pipe 18 is communicated with the distillation tank 12, a liquid outlet pipe 182 of the three-way pipe 18 is communicated with a product tank 19 on the distillation rack 1, a solenoid valve one 183 is installed on the liquid outlet pipe 182, and a solenoid valve two 185 is installed on the return pipe 181; a recovery mechanism 3, installed on the support plate 11, for recovering the products after distillation in the distillation tank 1; a feeding mechanism 2, installed on the support plate 11, for adding product raw materials into the distillation tank 1; a condensation mechanism 5, installed on the distillation rack 1, for conveying condensed water to the condensation assembly 4, and the condensation assembly 4 includes a condensation tank 41, a condensation coil 42 is installed in the condensation tank 41, the inlet end of the condensation coil 42 is communicated with the gas guide pipe 121, and the outlet end of the condensation coil 42 is communicated with the three-way pipe 18. In this embodiment, an electric heating rod is installed in the distillation tank 12.

[0024] The working principle of the present invention: Specifically, when in use, first add musk into the distillation tank 12 through the feeding mechanism 2. Subsequently, heat the musk through the electric heating rod in the distillation tank 12, and the generated steam enters the condensation coil 42 through the gas guide pipe 121. At the same time, convey condensed water into the condensation tank 41 through the condensation mechanism 5 to condense the musk steam, so that the condensed musk liquid enters the three-way pipe 18. If multiple distillation operations are required, close the solenoid valve one 183 and open the solenoid valve two 185, so that the condensate can enter the distillation tank 12 again through the return pipe 181, and distillation can be carried out again to improve the product purity. If the solenoid valve one 183 is opened and the solenoid valve two 185 is closed, the condensed musk liquid can be discharged into the product tank 19 for collection, and the waste liquid after distillation in the distillation tank 12 can be recovered through the recovery mechanism 3.

[0025] As a further solution, the recovery mechanism 3 includes a recovery tank 33 installed on the pallet 11. The recovery tank 33 is communicated with the rectification tank 12 through a recovery pipe 31, and a recovery valve 32 is installed on the recovery pipe 31. In this embodiment, the recovery tank 33 is a heat-insulated tank, which can effectively reduce heat loss, so as to better preheat the musk raw material.

[0026] The working principle of the recovery mechanism 3 is as follows: When it is necessary to recover the rectification waste liquid in the rectification tank 12, open the recovery valve 32, and the rectification waste liquid can be introduced into the recovery tank 33 through the recovery pipe 31 to complete the recovery work.

[0027] As a further solution, the feeding mechanism 2 includes a storage tank 24 installed on the pallet 11. The storage tank 24 is communicated with a preheating coil 25 in the recovery tank 33 through a transfer pipe 21. The other end of the preheating coil 25 penetrates through the recovery tank 33 and is fixed with a feeding pipe 23. The feeding pipe 23 is communicated with the rectification tank 1, and a feeding pump 22 is also installed on the transfer pipe 21.

[0028] The working principle of the feeding mechanism 2 is as follows: When it is necessary to add undistilled musk into the rectification tank 12, start the feeding pump 22, transfer the undistilled musk into the preheating coil 25 through the transfer pipe 21, preheat the musk with the rectification waste liquid recovered in the recovery tank 33, and then transfer it into the rectification tank 33 through the feeding pipe 23.

[0029] As a further solution, the condensation mechanism 5 includes a condensation box 51 and a collection box 54 installed on the rectification rack 1. The condensation box 51 is communicated with the condensation tank 41 through a liquid inlet pipe 52. The collection box 54 is communicated with the condensation tank 41 through a collection pipe 55. A condensation pump 53 is installed on the liquid inlet pipe 52. The collection box 54 and the condensation box 51 are communicated through a circulation pipe 56, and a circulation pump 57 is installed on the circulation pipe 56.

[0030] The working principle of the condensation mechanism 5 is as follows: During condensation, transfer the condensed water in the condensation box 51 into the condensation tank 41 through the condensation pump 53. The condensed water that absorbs heat is transferred into the collection box 54 through the collection pipe 55. Through the cooperation of the circulation pipe 56 and the circulation pump 57, the cooled condensed water in the collection box 54 can be transferred into the condensation box 51 for convenient subsequent use.

[0031] As a further solution, a first concentration sensor 13 is installed on the side wall of the rectification tank 12, a second concentration sensor 184 is installed on the liquid outlet pipe 182, and a third concentration sensor 186 is installed on the reflux pipe 181. As a further solution, an exhaust gas treatment box 16 is also installed on the rectification rack 1. The exhaust gas treatment box 16 is communicated with the exhaust pipe 14 on the rectification tank 12, and a pressure relief valve 15 is also installed on the exhaust pipe 14; a controller 17 is also installed on the exhaust gas treatment box 16. The first concentration sensor 13, the second concentration sensor 184, the third concentration sensor 186, the recovery valve 32, the first solenoid valve 183, the second solenoid valve 185, the feed pump 22, and the condensation pump 53 are all electrically connected to the controller 17.

[0032] When the concentration of the musk stock solution in the rectification tank 12 is lower than the set threshold, the first concentration sensor 13 transmits a signal to the controller 17, and the controller 17 controls the recovery valve 32 to open, so that the rectification waste liquid in the rectification tank 12 can be transferred to the recovery tank 33.

[0033] The concentration of the rectified musk can be conveniently monitored by the second concentration sensor 184 and the third concentration sensor 186. When the monitored concentration signal is lower than the set threshold, the controller 17 controls the first solenoid valve 183 to close and the second solenoid valve 185 to open, so that the rectified musk can enter the rectification tank 12 again through the reflux pipe 181, facilitating re-rectification, effectively improving the purity of the musk, and thus better meeting the usage requirements; when the monitored concentration signal is higher than the set threshold, the controller 17 controls the first solenoid valve 183 to open and the second solenoid valve 185 to close, so that the highly purified rectified musk can be transferred to the product tank 19 through the liquid outlet pipe 182 for collection.

[0034] In the present utility model, terms such as "upper", "lower", "left", "right", "front", "rear", "vertical", "horizontal", "side", "bottom", etc. indicate the orientation or positional relationship based on the orientation or positional relationship shown in the drawings. They are only relational terms determined to facilitate the description of the structural relationship of each component or element of the present utility model, and do not specifically refer to any component or element in the present utility model, and should not be construed as a limitation to the present utility model.

Claims

1. A novel musk distillation device, characterized in that: include: A distillation rack (1), wherein a support plate (11) is installed at the lower half of the distillation rack (1), a distillation tank (12) is installed at the upper end of the support plate (11), an air guide pipe (121) is installed at the upper end of the distillation tank (12), the other end of the air guide pipe (121) is connected to a condensation component (4), a three-way pipe (18) is installed at the lower end of the condensation component (4), a return pipe (181) of the three-way pipe (18) is connected to the distillation tank (12), a liquid outlet pipe (182) of the three-way pipe (18) is connected to a product tank (19) on the distillation rack (1), a solenoid valve 1 (183) is installed on the liquid outlet pipe (182), and a solenoid valve 2 (185) is installed on the return pipe (181); A recovery mechanism (3), mounted on the support plate (11), for recovering the product after distillation in the distillation tank (12); A feeding mechanism (2) is mounted on the support plate (11) and is used to add product raw materials into the distillation tank (12); The condensation mechanism (5) is installed on the distillation rack (1) and is used to transport condensed water to the condensation component (4).

2. A novel musk distillation device according to claim 1, characterized in that: The condensation assembly (4) comprises a condensation tank (41), a condensation coil (42) is installed in the condensation tank (41), the inlet end of the condensation coil (42) is connected to the air guide pipe (121), and the outlet end of the condensation coil (42) is connected to the three-way pipe (18).

3. A novel musk distillation device according to claim 2, characterized in that: The recovery mechanism (3) comprises a recovery tank (33) mounted on a support plate (11); the recovery tank (33) and the distillation tank (12) are connected via a recovery pipe (31); and a recovery valve (32) is mounted on the recovery pipe (31).

4. A novel musk distillation device according to claim 3, characterized in that: The feeding mechanism (2) comprises a storage tank (24) mounted on a support plate (11); the storage tank (24) is connected to a preheating coil (25) in a recovery tank (33) via a transfer pipe (21); the other end of the preheating coil (25) passes through the recovery tank (33) and is fixed with a feeding pipe (23); the feeding pipe (23) is connected to a distillation tank (12); and a feeding pump (22) is also mounted on the transfer pipe (21).

5. A novel musk distillation device according to claim 4, characterized in that: The condensing mechanism (5) comprises a condensing box (51) and a collecting box (54) mounted on the distillation rack (1); the condensing box (51) is connected to the condensing tank (41) via a liquid inlet pipe (52); the collecting box (54) is connected to the condensing tank (41) via a collecting pipe (55); and a condensing pump (53) is mounted on the liquid inlet pipe (52).

6. A novel musk distillation device according to claim 5, characterized in that: The collecting box (54) and the condensing box (51) are connected via a circulation pipe (56), and a circulation pump (57) is installed on the circulation pipe (56).

7. A novel musk distillation device according to claim 6, characterized in that: A concentration sensor 1 (13) is installed on the side wall of the distillation tank (12), a concentration sensor 2 (184) is installed on the liquid outlet pipe (182), and a concentration sensor 3 (186) is installed on the reflux pipe (181).

8. A novel musk distillation device according to claim 7, characterized in that: The rectification rack (1) is also provided with an exhaust gas treatment box (16), the exhaust gas treatment box (16) is connected to an exhaust pipe (14) on the rectification tank (12), and a pressure relief valve (15) is also provided on the exhaust pipe (14); The waste gas treatment box (16) is also equipped with a controller (17), and the concentration sensor 1 (13), the concentration sensor 2 (184), the concentration sensor 3 (186), the recovery valve (32), the solenoid valve 1 (183), the solenoid valve 2 (185), the feed pump (22), and the condensate pump (53) are all electrically connected to the controller (17).

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