Conveying device for purifying yellow phosphorus from phosphorus sludge

Abstract

The utility model relates to the technical field of yellow phosphorus production, in particular to a conveying device for purifying yellow phosphorus from phosphorus sludge, which adopts the technical scheme that the conveying device comprises a bin body, a feeding pipe is communicated and mounted at the rear end of the bin body, an air inlet pipe is communicated and mounted at the bottom of one side of the bin body, a transmission shaft is rotatably mounted in the bin body, and a stirring frame is fixedly mounted on the transmission shaft; the device further comprises a communicating pipe; the communicating pipe is communicated with the top of the bin body; wherein a cover body is fixedly mounted at the top of the communicating pipe, a reserved hole is formed in the upper surface of the cover body, and a condensing pipe is mounted on the cover body in a communicating manner; wherein the condensation pipe is designed to be of a spiral structure, and the bottom end of the condensation pipe is communicated with the storage bin; one corner of the upper end face of the storage bin is provided with a hole and communicated with a pressure release valve, and the other corner of the upper end face of the storage bin is provided with a hole and communicated with a sealing valve. The yellow phosphorus extraction device solves the problem that potential safety hazards exist in the conveying stage after extraction due to the fact that yellow phosphorus is prone to spontaneous combustion after making contact with air.

Description

Technical Field

[0001] The utility model relates to the technical field of yellow phosphorus production, in particular to a conveying device for purifying yellow phosphorus from muddy phosphorus. Background Technique

[0002] Muddy phosphorus is usually a by-product in the process of processing phosphate rock. By extracting yellow phosphorus, the originally wasted resources can be transformed into valuable products, realizing the recycling of resources. Environmental protection benefits: Traditional methods for producing yellow phosphorus may generate a large amount of waste and pollutants, while extracting yellow phosphorus from muddy phosphorus can reduce the impact on the environment and is a more environmentally friendly production method. After a large number of searches, the publication number is CN1218869C, which discloses a production method for recovering yellow phosphorus from muddy phosphorus and a device for realizing this method. The quality of the yellow phosphorus recovered by this device can meet the national standards.

[0003] However, when the above device extracts yellow phosphorus from muddy phosphorus, it mainly separates yellow phosphorus from other impurities by precipitation. In actual use, the above device does not consider the chemical properties of yellow phosphorus. Since yellow phosphorus is highly reactive and easily reacts with oxygen in the air and catches fire spontaneously, when the above device is in the conveying stage after extraction, yellow phosphorus is likely to come into contact with air, resulting in spontaneous combustion of yellow phosphorus and posing a safety hazard. Therefore, a conveying device for purifying yellow phosphorus from muddy phosphorus is needed to solve the above problems. Summary of the Utility Model

[0004] The purpose of the utility model is to provide a conveying device for purifying yellow phosphorus from muddy phosphorus, which has the advantage of improving the safety of yellow phosphorus during the transmission process after extraction, and solves the problem of potential safety hazards in the conveying stage after extraction due to the easy spontaneous combustion of yellow phosphorus when it comes into contact with air.

[0005] To achieve the above purpose, the utility model provides the following technical solution: A conveying device for purifying yellow phosphorus from muddy phosphorus, including a bin body, a feed pipe is connected and installed at the rear end of the bin body, an air inlet pipe is connected and installed at the bottom of one side of the bin body, a transmission shaft is rotatably installed in the bin body, a stirring frame is fixedly installed on the transmission shaft, and further includes a connecting pipe;

[0006] The connecting pipe is connected and installed at the top of the bin body;

[0007] Wherein, a cover body is fixedly installed at the top of the connecting pipe, a reserved hole is opened on the upper surface of the cover body and a condensing pipe is connected and installed;

[0008] Wherein, the condensing pipe is designed with a spiral structure, and the bottom end of the condensing pipe is connected and installed with a storage bin;

[0009] Wherein, a pressure relief valve is connected and installed at one corner of the upper end surface of the storage bin, and a sealing valve is connected and installed at the other corner of the upper end surface of the storage bin.

[0010] Preferably, the bottom end of the silo is recessed toward the center and connected to a slag discharge pipe, and support frames are fixedly installed at the four corners of the bottom of the silo. In the design, the bottom end of the silo is specially designed to be recessed toward the center. This structure is conducive to the concentration and discharge of non-yellow phosphorus components in mud phosphorus. The installation of the slag discharge pipe makes the slag discharge process more efficient and centralized, reduces pollution to the environment, and improves the purification efficiency. Although not mentioned, a valve is provided on the slag discharge pipe. The provision of the support frame enhances the structural stability of the silo and ensures the safety and reliability of the entire device during operation.

[0011] Preferably, an air intake valve is fixedly installed on the air intake pipe, and the air intake valve adopts an electric control valve structure design, and the end of the air intake valve away from the air intake pipe is connected and installed with the gas heat source pipeline. In the design, the air intake valve installed on the air intake pipe adopts an advanced electric control valve structure design. This intelligent control method can accurately adjust the air intake volume according to actual needs, thereby optimizing the extraction process of yellow phosphorus. At the same time, the connection installation with the gas heat source pipeline ensures a stable supply of heat source gas and provides the necessary heat energy for the vaporization of yellow phosphorus.

[0012] Preferably, the rear end of the transmission shaft passes through the bin and is driven by a drive motor, which is fixedly mounted on the outer wall of the other side of the bin. The connection between the rear end of the transmission shaft and the drive motor in the design realizes the effective transmission of power. The fixed installation of the drive motor not only saves space, but also improves the stability and efficiency of the entire transmission system. This design enables the stirring rack to operate continuously and stably, providing a guarantee for the uniform heating of the mud phosphorus and the sufficient vaporization of the yellow phosphorus.

[0013] Preferably, a hole is opened on one side of the upper surface of the cover body and a pressure gauge is embedded therein, and the pressure gauge adopts a high temperature resistant pressure gauge structure design. The high temperature resistant pressure gauge embedded in the cover body in the design can monitor the pressure changes in the bin in real time to ensure that the operation is carried out within a safe pressure range. This high temperature resistant design enables the pressure gauge to work stably in a high temperature environment, improving the accuracy of the measurement and the safety of the device.

[0014] Preferably, a discharge valve is fixedly installed on the top of the condenser tube, and the discharge valve adopts a manual angle valve structure design, and a first quick connector is fixedly installed on the bottom of the condenser tube. In the design, the discharge valve on the top of the condenser tube adopts a manual angle valve structure design, which makes the discharge operation of yellow phosphorus simpler and faster. The installation of the first quick connector provides the function of quick connection and disconnection, improves the discharge efficiency, and also facilitates the maintenance and cleaning of the equipment.

[0015] Preferably, one side of the storage bin is grooved and embedded with an observation window. The observation window is designed with tempered glass material. The upper end face of the storage bin is connected and installed with a second quick connector through a sealing valve. The second quick connector is matched with the first quick connector and can be inserted. In the design, the observation window on the storage bin is made of tempered glass material, providing an intuitive observation of the internal state of yellow phosphorus, which helps the operator to monitor the extraction process in real time and make adjustments in a timely manner. The matching design of the second quick connector and the first quick connector realizes the rapid and safe transmission of yellow phosphorus, improving the efficiency of the entire extraction and transmission process.

[0016] Compared with the prior art, the beneficial effects of the present utility model are as follows:

[0017] In the present utility model, the condensing pipe is designed with a spiral structure. This design increases the surface area of the condensing pipe, improves the cooling efficiency, enables the yellow phosphorus vapor to be cooled and condensed into solid yellow phosphorus more quickly when passing through the condensing pipe, and avoids the time and opportunity for the yellow phosphorus vapor to contact the air. The storage bin is designed as a sealed structure, and the entry and exit of yellow phosphorus are controlled through a sealing valve, effectively isolating the outside air. Moreover, by means of internal water injection, it can prevent yellow phosphorus from spontaneous combustion due to contact with air. A pressure relief valve is installed on the upper end face of the storage bin. During the yellow phosphorus extraction process, if the pressure in the storage bin is too high, it can be released through the pressure relief valve to avoid safety accidents caused by excessive pressure. The use of the sealing valve ensures the tightness of the storage bin during the non-extraction stage, preventing yellow phosphorus from contacting the air, and at the same time facilitating the control of the extraction and transmission of yellow phosphorus. At the same time, although the design of the first quick connector and the second quick connector is not mentioned, through the above design, the plugging and unplugging between the storage bin and the condensing pipe are made more rapid. The design of the entire device ensures that the entire process from the extraction to the transmission of yellow phosphorus is carried out in a sealed or controllable environment, greatly reducing the risk of yellow phosphorus contacting the air and achieving the effect of improving the safety of the extracted yellow phosphorus during the transmission process. BRIEF DESCRIPTION OF THE DRAWINGS

[0018] Figure 1 is the front view structural schematic diagram of the present utility model;

[0019] Figure 2 is the cross-sectional structural schematic diagram of the present utility model;

[0020] Figure 3 is the structural schematic diagram of the condensing pipe of the present utility model;

[0021] Figure 4 is the structural schematic diagram of the storage bin of the present utility model.

[0022] In the figure: 1. Silo body; 2. Feed pipe; 3. Connecting pipe; 4. Condensing pipe; 5. Support frame; 6. Storage bin; 7. Intake valve; 8. Reserved hole; 9. Cover body; 10. Pressure gauge; 11. Driving motor; 12. Transmission shaft; 13. Stirring frame; 14. Slag discharge pipe; 15. Intake pipe; 16. Discharge valve; 17. First quick connector; 18. Second quick connector; 19. Sealing valve; 20. Observation window; 21. Pressure relief valve. Detailed implementation mode

[0023] Next, the technical solutions in the embodiments of the present invention will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

[0024] Embodiment 1

[0025] As Figure 1 , Figure 2 , Figure 3 and Figure 4 shown, an embodiment provided by the present invention: A conveying device for purifying yellow phosphorus from muddy phosphorus includes a silo body 1, a feed pipe 2 is connected and installed at the rear end of the silo body 1, an intake pipe 15 is connected and installed at the bottom of one side of the silo body 1, a transmission shaft 12 is rotatably installed in the silo body 1, a stirring frame 13 is fixedly installed on the transmission shaft 12, and further includes a connecting pipe 3.

[0026] Specifically, the condensing pipe 4 adopts a spiral structure design. This design increases the surface area of the condensing pipe 4, improves the cooling efficiency, enables the yellow phosphorus vapor to be cooled and condensed into solid yellow phosphorus more quickly when passing through the condensing pipe 4, and avoids the time and opportunity for the yellow phosphorus vapor to contact the air. The storage bin 6 is designed as a sealed structure, and the entry and exit of yellow phosphorus are controlled by the sealing valve 19, effectively isolating the outside air. Moreover, by the method of injecting water inside, it can prevent yellow phosphorus from spontaneous combustion when contacting the air. A pressure relief valve 21 is installed on the upper end face of the storage bin 6. During the yellow phosphorus extraction process, if the pressure in the storage bin 6 is too high, it can be released through the pressure relief valve 21 to avoid safety accidents caused by excessive pressure. The use of the sealing valve 19 ensures the tightness of the storage bin 6 during the non-extraction stage, prevents yellow phosphorus from contacting the air, and at the same time facilitates the control of the extraction and transmission of yellow phosphorus. At the same time, although the design of the first quick connector 17 and the second quick connector 18 is not mentioned, however, through the above design, the plugging and unplugging of the storage bin 6 and the condensing pipe 4 are made more rapid. The design of the whole device ensures that the entire process from the extraction to the transmission of yellow phosphorus is carried out in a sealed or controllable environment, greatly reducing the risk of yellow phosphorus contacting the air, and achieving the effect of improving the safety of the extracted yellow phosphorus during the transmission process.

[0027] Example Two

[0028] To increase the vaporization rate of yellow phosphorus, as Figure 1 and Figure 2 shown, in this embodiment, the bottom end of the bin body 1 is recessed towards the center and is connected and installed with a slag discharge pipe 14. Support frames 5 are respectively fixedly installed at the four corners of the bottom of the bin body 1. In the design, the bottom end of the bin body 1 is specially designed to be recessed towards the center. This structure is conducive to the concentration and discharge of non-yellow phosphorus components in the muddy phosphorus. The installation of the slag discharge pipe 14 makes the slag discharge process more efficient and concentrated, reduces environmental pollution, and improves the purification efficiency. Although not mentioned, a valve is provided on the slag discharge pipe 14. The setting of the support frames 5 enhances the structural stability of the bin body 1 and ensures the safety and reliability of the entire device during operation.

[0029] Furthermore, an intake valve 7 is fixedly installed on the intake pipe 15. The intake valve 7 adopts an electronically controlled valve structure design. One end of the intake valve 7 facing away from the intake pipe 15 is connected and installed with a gas heat source pipeline. In the design, the intake valve 7 installed on the intake pipe 15 adopts an advanced electronically controlled valve structure design. This intelligent control method can accurately adjust the intake air volume according to actual needs, thereby optimizing the yellow phosphorus extraction process. At the same time, the connection and installation with the gas heat source pipeline ensure the stable supply of the heat source gas and provide the necessary heat energy for the vaporization of yellow phosphorus.

[0030] Furthermore, the rear end of the transmission shaft 12 passes through the bin body 1 and is drivingly installed with a driving motor 11. The driving motor 11 is fixedly installed on the outer wall on the other side of the bin body 1. In the design, the connection between the rear end of the transmission shaft 12 and the driving motor 11 realizes the effective transmission of power. The fixed installation of the driving motor 11 not only saves space but also improves the stability and efficiency of the entire transmission system. This design enables the stirring frame 13 to operate continuously and stably, providing a guarantee for the uniform heating of the muddy phosphorus and the full vaporization of yellow phosphorus.

[0031] Furthermore, a pressure gauge 10 is installed by opening a hole on one side of the upper surface of the cover body 9 and embedding it. The pressure gauge 10 adopts a high-temperature resistant pressure gauge 10 structure design. In the design, the high-temperature resistant pressure gauge 10 embedded in the cover body 9 can monitor the pressure change inside the bin body 1 in real time, ensuring that the operation is carried out within a safe pressure range. This high-temperature resistant design enables the pressure gauge 10 to work stably in a high-temperature environment, improving the measurement accuracy and the safety of the device.

[0032] Example Three

[0033] To improve the sealing performance of the container during the yellow phosphorus transportation stage and facilitate the operator to understand and control the yellow phosphorus extraction situation, as Figure 3 and Figure 4As shown, in this embodiment, a discharge valve 16 is fixedly installed at the top of the condenser tube 4. The discharge valve 16 is designed with a manual angle valve structure. A first quick connector 17 is fixedly installed at the bottom end of the condenser tube 4. In the design, the discharge valve 16 at the top of the condenser tube 4 is designed with a manual angle valve structure, making the discharge operation of yellow phosphorus more convenient and fast. The installation of the first quick connector 17 provides the functions of quick connection and disconnection, improves the discharge efficiency, and also facilitates the maintenance and cleaning of the equipment.

[0034] Furthermore, a viewing window 20 is installed by grooving and embedding on one side of the storage bin 6. The viewing window 20 is designed with tempered glass material. A second quick connector 18 is connected and installed through a sealing valve 19 on the upper end face of the storage bin 6. The second quick connector 18 is matched with the first quick connector 17 and can be plugged in. In the design, the viewing window 20 on the storage bin 6 is made of tempered glass material, providing an intuitive observation of the internal state of yellow phosphorus, which helps the operator to monitor the extraction process in real time and make adjustments in a timely manner. The matching design of the second quick connector 18 and the first quick connector 17 realizes the fast and safe transmission of yellow phosphorus, improving the efficiency of the entire extraction and transmission process.

[0035] When the utility model is in use, close the valve on the slag discharge pipe 14 and open the valve on the feed pipe 2. Convey the muddy phosphorus raw material into the bin body 1 through the feed pipe 2. Convey the heated protective gas into the bin body 1 through the air inlet pipe 15. The air inlet valve 7 is designed with an electric control valve structure to ensure the precise control of the gas flow. Start the drive motor 11, drive the stirring frame 13 to rotate through the transmission shaft 12, and realize the stirring and mixing of the muddy phosphorus. At the same time, heat and flush the muddy phosphorus in the bin body 1 through the gas heat source pipeline to promote the vaporization of yellow phosphorus. Under the action of heating and stirring, yellow phosphorus gradually vaporizes to form phosphorus-containing steam. The phosphorus-containing steam rises through the connecting pipe 3 to the reserved hole 8 of the cover body 9 and enters the condenser tube 4. The condenser tube 4 is designed with a spiral structure, which is beneficial to the cooling and condensation of the steam. After the yellow phosphorus steam is cooled in the condenser tube 4, it gradually condenses into solid yellow phosphorus. The condensed yellow phosphorus flows into the storage bin 6 through the bottom end of the condenser tube 4 for storage. And an appropriate amount of clear water has been injected into the storage bin 6 in advance to isolate the contact between yellow phosphorus and air. The pressure in the bin body 1 can be monitored through the pressure gauge 10 to ensure that the operation is within a safe range. After the purification is completed, open the valve on the slag discharge pipe 14 to discharge the non-yellow phosphorus components in the muddy phosphorus from the bin body 1. If necessary, open the pressure relief valve 21 to release the pressure in the bin body 1. Separate the storage bin 6 from the condenser tube 4, so as to transport the storage bin 6. And after arriving at the placement location, the discharge valve 16 can be opened to discharge the yellow phosphorus in the storage bin 6 for subsequent collection or further processing.

[0036] For those skilled in the art, it is obvious that the present utility model is not limited to the details of the above-described exemplary embodiments, and the present utility model can be implemented in other specific forms without departing from the spirit or basic characteristics of the present utility model. Therefore, from any point of view, the embodiments should be regarded as exemplary and non-restrictive. The scope of the present utility model is defined by the appended claims rather than the above description. Therefore, all changes falling within the meaning and scope of the equivalent elements of the claims are intended to be embraced within the present utility model. Any reference signs in the claims should not be construed as limiting the claimed rights involved.

Claims

1. A conveying device for purifying yellow phosphorus from sludge phosphorus, comprising a silo (1), a feed pipe (2) is connected and installed at the rear end of the silo (1), an air intake pipe (15) is connected and installed at the bottom of one side of the silo (1), a transmission shaft (12) is rotatably installed in the silo (1), and a stirring frame (13) is fixedly installed on the transmission shaft (12), characterized in that: Also includes: A connecting pipe (3) connected and installed on the top of the bin body (1); Wherein, a cover body (9) is fixedly installed on the top of the connecting pipe (3), and a reserved hole (8) is opened on the upper surface of the cover body (9) and a condensing pipe (4) is installed in communication therewith; The condenser tube (4) is designed with a spiral structure, and the bottom end of the condenser tube (4) is connected to a storage bin (6); A hole is opened at one corner of the upper end surface of the storage bin (6) and connected to a pressure relief valve (21), and a hole is opened at another corner of the upper end surface of the storage bin (6) and connected to a sealing valve (19).

2. A conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: The bottom end of the silo (1) is concave toward the center and is connected to a slag discharge pipe (14) installed therein, and support frames (5) are fixedly installed at the four corners of the bottom of the silo (1).

3. The conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: An intake valve (7) is fixedly mounted on the intake pipe (15). The intake valve (7) is designed as an electrically controlled valve structure. One end of the intake valve (7) facing away from the intake pipe (15) is connected to the gas heat source pipeline.

4. The conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: The rear end of the transmission shaft (12) passes through the warehouse body (1) and is transmission-mounted with a driving motor (11), which is fixedly mounted on the outer wall of the other side of the warehouse body (1).

5. The conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: A hole is opened on one side of the upper surface of the cover body (9) and a pressure gauge (10) is embedded and installed therein. The pressure gauge (10) adopts a high temperature resistant pressure gauge (10) structural design.

6. The conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: A discharge valve (16) is fixedly installed on the top of the condenser tube (4), and the discharge valve (16) adopts a manual angle valve structure design. A first quick connector (17) is fixedly installed on the bottom end of the condenser tube (4).

7. The conveying device for purifying yellow phosphorus from sludge phosphorus according to claim 1, characterized in that: A groove is formed on one side of the storage bin (6) and an observation window (20) is embedded therein. The observation window (20) is made of tempered glass. The upper end surface of the storage bin (6) is connected to a second quick connector (18) through a sealing valve (19). The second quick connector (18) is matched with the first quick connector (17) and can be plugged in.

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